CN2210708Y - Super-high pressure and high-temp chamber for synthesizing super-hard material - Google Patents
Super-high pressure and high-temp chamber for synthesizing super-hard material Download PDFInfo
- Publication number
- CN2210708Y CN2210708Y CN 95204192 CN95204192U CN2210708Y CN 2210708 Y CN2210708 Y CN 2210708Y CN 95204192 CN95204192 CN 95204192 CN 95204192 U CN95204192 U CN 95204192U CN 2210708 Y CN2210708 Y CN 2210708Y
- Authority
- CN
- China
- Prior art keywords
- high temperature
- hole
- high pressure
- lining
- temperature chamber
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
Links
- 239000000463 material Substances 0.000 title claims abstract description 20
- 230000002194 synthesizing effect Effects 0.000 title claims abstract description 8
- 239000002184 metal Substances 0.000 claims abstract description 21
- 238000010438 heat treatment Methods 0.000 claims description 10
- 238000007789 sealing Methods 0.000 claims description 7
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 claims description 4
- 239000003513 alkali Substances 0.000 claims description 4
- 230000008878 coupling Effects 0.000 claims description 4
- 238000010168 coupling process Methods 0.000 claims description 4
- 238000005859 coupling reaction Methods 0.000 claims description 4
- 229910002804 graphite Inorganic materials 0.000 claims description 4
- 239000010439 graphite Substances 0.000 claims description 4
- 229910052736 halogen Inorganic materials 0.000 claims description 4
- 150000002367 halogens Chemical class 0.000 claims description 4
- 230000009466 transformation Effects 0.000 claims description 3
- 239000006004 Quartz sand Substances 0.000 claims description 2
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims description 2
- 239000012774 insulation material Substances 0.000 claims description 2
- 239000013500 performance material Substances 0.000 claims description 2
- 229910003460 diamond Inorganic materials 0.000 abstract description 11
- 239000010432 diamond Substances 0.000 abstract description 11
- 229910052582 BN Inorganic materials 0.000 abstract description 4
- PZNSFCLAULLKQX-UHFFFAOYSA-N Boron nitride Chemical compound N#B PZNSFCLAULLKQX-UHFFFAOYSA-N 0.000 abstract description 4
- 238000009826 distribution Methods 0.000 abstract description 4
- 239000000956 alloy Substances 0.000 description 5
- 229910045601 alloy Inorganic materials 0.000 description 5
- 238000012856 packing Methods 0.000 description 4
- 229910052903 pyrophyllite Inorganic materials 0.000 description 3
- 101100456212 Arabidopsis thaliana MBD8 gene Proteins 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 238000000034 method Methods 0.000 description 2
- 230000003068 static effect Effects 0.000 description 2
- 235000013619 trace mineral Nutrition 0.000 description 2
- 239000011573 trace mineral Substances 0.000 description 2
- 230000015572 biosynthetic process Effects 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- 238000005485 electric heating Methods 0.000 description 1
- 230000001771 impaired effect Effects 0.000 description 1
- 238000009776 industrial production Methods 0.000 description 1
- 238000009413 insulation Methods 0.000 description 1
- 230000001788 irregular Effects 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 239000002245 particle Substances 0.000 description 1
- 238000003786 synthesis reaction Methods 0.000 description 1
- 229910052623 talc Inorganic materials 0.000 description 1
- 239000000454 talc Substances 0.000 description 1
- 235000012222 talc Nutrition 0.000 description 1
Landscapes
- Carbon And Carbon Compounds (AREA)
Abstract
The utility model discloses a device for synthesizing artificial diamond or cubic boron nitride, particularly a superhigh pressure and high temperature chamber for superhard material. A cylinder-shaped through hole is arranged at the cube centre, and the middle part of the through hole is provided with a liner which is provided with a metal lining layer. When the utility model is used, metal sheets are installed at the two ends of the liner, and an electric conduction lid is installed outside the liner. The distribution gradient of the high temperature field in the high temperature chamber is extremely small, the metal lining layer shielding prevents the pollution to the material, so that the saw blade stage content of the product is greatly increased and the intensity is high. Meanwhile, contact area of the top hammer and the electric conduction lid is enlarged, the consumption of the top hammer is obviously reduced, and the economical benefit is obviously increased.
Description
The utility model relates to electric heater unit, particularly in order to the high pressure high temperature chamber of superhard materials such as synthesis of artificial diamond or cubic boron nitride.
Diamond is synthetic under high pressure high temperature, commercially available industrial diamond mostly adopts static pressure method to make, said static pressure method is that the hexahedron high pressure high temperature chamber that the pyrophyllite material is made is placed cubic hinge press, makes based on the material of graphite by the heating of heavy current high temperature.The outdoor shape of used hexahedron high pressure high temperature is six squares, and the center is an axis hole shape supplies room, and convex shoulder shape is formed on the supplies room bottom, as shown in Figure 2, places conductive cap 7 in the electric cap hole 15 at convex shoulder place.Add a cover the sealing ring 16 that materials such as pyrophyllite are made at an upper portion thereof, the conductive cap 14 of packing in the hole of sealing ring after inserting material in the supplies room 4 at hot room 1 center.Said conductive cap is to fill up the pyrophyllite material to make in bottle cap shape metallic sheath.This hot room is produced in diamond or the cubic boron nitride at super-pressure and is had the big problem of high-temperature field distribution gradient, the electric current that is added on the conductive cap is concentrated to the material center when annular cap body enters in the material, separately flow to the ring cap body of this conductive cap during to other end conductive cap again, cause Temperature Distribution irregular; In addition, material contacts with master side's body, and there is pollution in the contained trace element in high pressure high temperature chamber itself to the diamond growth course.Therefore, with the synthetic diamond in existing high pressure high temperature chamber, its trade mark is MBD8, SMD, granularity be 50/60 and thick saw blade level content only between the 18-23%.Because conductive cap and hard alloy top hammer contact area are little, the top hammer damages easily in addition, and the hard alloy top hammer of every myriagram particle diamond causes the product cost height between consuming 20 to 25 kilograms, and economic benefit is not good.
The purpose of this utility model is to provide a kind of novel synthesizing superhard material to use the high pressure high temperature chamber, by improving the shape and structure of high pressure high temperature chamber, to improve synthetic diamond saw blade level content by a relatively large margin, reduce hard alloy top hammer consumption, product cost is had by a relatively large margin descend, to improve the economic benefit in the industrial production.
The purpose of this utility model is achieved by the following scheme: at the cube center cylindrical hole is set, the lining of being made by high temperature insulation materials such as alkali halogen, talcum, pyrophillite, dolomites is installed in middle part at through hole, and the inwall of lining is provided with metal lining; This high pressure high temperature chamber also is provided with sheet metal and the conductive cap that is loaded on the lining two ends and mates with through hole.
Use the synthetic synthesizing superhard material high pressure high temperature chamber production exceptional hardness material (diamond or cubic boron nitride) of the utility model, (the former conductive cap of going up is loaded in the sealing ring because of the conductive cap area at two ends strengthens, this novel conductive cap is identical with former sealing ring diameter), strengthen with the hard alloy top hammer contact area, thereby alleviated top hammer impaired possibility under high pressure-temperature, reduced spoilage, the hard alloy top hammer consumption rate can be reduced to average every myriagram and be drawn below 15 kilograms, this high pressure high temperature chamber is in high pressure-temperature control, electric current is via an end conductive cap, to partly overlapping the end sheet metal.Again in lining metal lining and material (graphite), hold sheet metal to arrive in addition to hold conductive cap in addition, to form the electrical heating field, its CURRENT DISTRIBUTION is even, forms evenly electric heating field.Lining plays insulation effect again in addition, and the sealed environment that metal lining and two ends sheet metal form can avoid the trace element of hot room to pollute.Therefore, can improve the synthetic ratio of high-quality Buddha's warrior attendant, its MBD8, SMD trade mark granularity be 50/60 and thick saw blade level content can bring up to more than 35% and intensity height.Because the reduction of top hammer consumption, product cost can reduce about 15%, and remarkable in economical benefits increases.
Be described further below in conjunction with accompanying drawing
Fig. 1 is the utility model synthesizing superhard material high pressure high temperature cell structure schematic diagram
Fig. 2 is original hot room structural representation
As shown in Figure 1, this high pressure high temperature chamber is to be provided with cylindrical hole at the center of cube 1, and the through hole middle part is provided with lining 2, and the inwall of lining is provided with metal lining 3, is supplies room 4 in the metal lining; Behind the material of packing into, two ends cover with sheet metal 8,13, and the conductive cap 7,14 of packing at the through hole two ends at last also is the inner that sheet metal is loaded on conductive cap, and the diameter of above-mentioned sheet metal and conductive cap should mate with cubical through hole; In order further to improve the temperature field in the supplies room, improve the growth of diamond effect, can be provided with by graphite and AL203, alkali halogen or quartz sand and not be phase-changed into micro-phase transformation under HTHP, having increases the heating plate 6,11 that the resistive performance material is made, and this heating plate is disc; Sealing ring 9,12 internal diameters and heating plate coupling, cylindrical and cube through hole coupling.In use, the sheet metal 5,10 of packing at lining 2 two ends earlier, this sheet metal is identical with the sheet metal external diameter of conductive cap the inner, and then puts into sealing ring and heating plate.The sheet metal of conductive cap and the inner thereof is outside heating plate.
Claims (2)
1, the synthesizing superhard material is used the high pressure high temperature chamber, it is characterized in that cylindrical hole being set at the cube center, the lining of being made by high temperature insulation materials such as alkali halogen, dolomites (2) is installed in middle part at through hole, the inwall of lining is provided with metal lining (3), and this high pressure high temperature chamber also is provided with sheet metal and the conductive cap that is loaded on the lining two ends and mates with through hole.
2, synthesizing superhard material according to claim 1 is used the high pressure high temperature chamber, it is characterized in that being provided with by graphite and AL203, not phase transformation or micro-phase transformation is arranged under HTHP such as alkali halogen or quartz sand, and having increases the heating plate (6,11) that the resistive performance material is made, and this heating plate is disc; Sealing ring (9,12) internal diameter and heating plate coupling, cylindrical and cube through hole coupling.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 95204192 CN2210708Y (en) | 1995-03-10 | 1995-03-10 | Super-high pressure and high-temp chamber for synthesizing super-hard material |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 95204192 CN2210708Y (en) | 1995-03-10 | 1995-03-10 | Super-high pressure and high-temp chamber for synthesizing super-hard material |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN2210708Y true CN2210708Y (en) | 1995-10-25 |
Family
ID=33856780
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN 95204192 Expired - Lifetime CN2210708Y (en) | 1995-03-10 | 1995-03-10 | Super-high pressure and high-temp chamber for synthesizing super-hard material |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN2210708Y (en) |
Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN100444944C (en) * | 2004-10-29 | 2008-12-24 | 郑州人造金刚石及制品工程技术研究中心 | Medium material for diamond synthesis and medium constituted therefrom |
| CN104557068A (en) * | 2013-10-23 | 2015-04-29 | 郑州博特硬质材料有限公司 | Die for synthesis of superhard materials |
| CN106582447A (en) * | 2016-12-07 | 2017-04-26 | 鸡西浩市新能源材料有限公司 | Blackbody material for synthesis of large particle diamond |
| CN108883383A (en) * | 2016-03-16 | 2018-11-23 | 第六元素（英国）有限公司 | Component for synthesizing superhard material |
| CN111359537A (en) * | 2019-08-30 | 2020-07-03 | 三河市晶日金刚石复合材料有限公司 | Composite sheet synthetic block |
| WO2023193366A1 (en) * | 2022-04-07 | 2023-10-12 | 南方科技大学 | Testing device |
-
1995
- 1995-03-10 CN CN 95204192 patent/CN2210708Y/en not_active Expired - Lifetime
Cited By (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN100444944C (en) * | 2004-10-29 | 2008-12-24 | 郑州人造金刚石及制品工程技术研究中心 | Medium material for diamond synthesis and medium constituted therefrom |
| CN104557068A (en) * | 2013-10-23 | 2015-04-29 | 郑州博特硬质材料有限公司 | Die for synthesis of superhard materials |
| CN104557068B (en) * | 2013-10-23 | 2016-08-17 | 郑州博特硬质材料有限公司 | A kind of mould of superhard material synthesis |
| CN108883383A (en) * | 2016-03-16 | 2018-11-23 | 第六元素（英国）有限公司 | Component for synthesizing superhard material |
| CN106582447A (en) * | 2016-12-07 | 2017-04-26 | 鸡西浩市新能源材料有限公司 | Blackbody material for synthesis of large particle diamond |
| CN111359537A (en) * | 2019-08-30 | 2020-07-03 | 三河市晶日金刚石复合材料有限公司 | Composite sheet synthetic block |
| WO2023193366A1 (en) * | 2022-04-07 | 2023-10-12 | 南方科技大学 | Testing device |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| C17 | Cessation of patent right | ||
| CX01 | Expiry of patent term |