CN218443409U - Equipment for recycling low boiling water solution by acidolysis for synthesizing chloramine - Google Patents
Equipment for recycling low boiling water solution by acidolysis for synthesizing chloramine Download PDFInfo
- Publication number
- CN218443409U CN218443409U CN202221669593.7U CN202221669593U CN218443409U CN 218443409 U CN218443409 U CN 218443409U CN 202221669593 U CN202221669593 U CN 202221669593U CN 218443409 U CN218443409 U CN 218443409U
- Authority
- CN
- China
- Prior art keywords
- condensation
- low boiling
- liquid
- steam
- pipe
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Active
Links
- 238000009835 boiling Methods 0.000 title claims abstract description 33
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 title claims abstract description 29
- QDHHCQZDFGDHMP-UHFFFAOYSA-N Chloramine Chemical compound ClN QDHHCQZDFGDHMP-UHFFFAOYSA-N 0.000 title claims abstract description 18
- 230000002194 synthesizing effect Effects 0.000 title description 5
- 238000004064 recycling Methods 0.000 title description 3
- 239000007788 liquid Substances 0.000 claims abstract description 76
- 238000009833 condensation Methods 0.000 claims abstract description 62
- 230000005494 condensation Effects 0.000 claims abstract description 62
- 239000002826 coolant Substances 0.000 claims abstract description 16
- 238000011084 recovery Methods 0.000 claims abstract description 12
- 238000001816 cooling Methods 0.000 claims abstract description 9
- 239000007864 aqueous solution Substances 0.000 claims description 8
- 230000015572 biosynthetic process Effects 0.000 claims description 8
- 238000003786 synthesis reaction Methods 0.000 claims description 8
- 238000005903 acid hydrolysis reaction Methods 0.000 claims description 4
- 150000001412 amines Chemical class 0.000 claims 3
- 239000000243 solution Substances 0.000 description 23
- 239000000110 cooling liquid Substances 0.000 description 22
- 238000000034 method Methods 0.000 description 5
- 238000010992 reflux Methods 0.000 description 5
- 239000000126 substance Substances 0.000 description 4
- 239000005497 Clethodim Substances 0.000 description 2
- 241000196324 Embryophyta Species 0.000 description 2
- SILSDTWXNBZOGF-JWGBMQLESA-N clethodim Chemical compound CCSC(C)CC1CC(O)=C(C(CC)=NOC\C=C\Cl)C(=O)C1 SILSDTWXNBZOGF-JWGBMQLESA-N 0.000 description 2
- 230000002363 herbicidal effect Effects 0.000 description 2
- 239000004009 herbicide Substances 0.000 description 2
- 238000012986 modification Methods 0.000 description 2
- 230000004048 modification Effects 0.000 description 2
- 239000013589 supplement Substances 0.000 description 2
- 239000005501 Cycloxydim Substances 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- GGWHBJGBERXSLL-NBVRZTHBSA-N chembl113137 Chemical compound C1C(=O)C(C(=N/OCC)/CCC)=C(O)CC1C1CSCCC1 GGWHBJGBERXSLL-NBVRZTHBSA-N 0.000 description 1
- 230000007547 defect Effects 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 239000003112 inhibitor Substances 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 239000002245 particle Substances 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 239000002904 solvent Substances 0.000 description 1
Images
Landscapes
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
The utility model relates to a retrieve low boiling water solution technical field, specifically be an equipment that is used for acidolysis recovery low boiling water solution of synthetic chloramine, including the condensation storehouse, condensation storehouse internally mounted has the condensation subassembly, the backward flow subassembly is all installed to the condensation storehouse left and right sides, backward flow subassembly bottom is equipped with out the liquid subassembly. The utility model discloses a condensation of low boiling point solution is retrieved, injects the coolant liquid in the cooling cistern, inserts the steam pipe with the steam that low boiling point solution produced, gets into annular condenser pipe from the steam pipe, and the coolant liquid in the annular condenser pipe outside is with steam from the cooling condensation of gas into liquid, flows in the collecting vat that baffle bottom and condensation box formed at last, can derive liquid through opening the valve, and the backward flow subassembly of condensation box both sides can accelerate the coolant liquid to flow, improves condensation efficiency.
Description
Technical Field
The utility model relates to the technical field of recovering low boiling water solution, in particular to a device for recovering low boiling water solution by acidolysis for synthesizing chloramine.
Background
The chloramine is 0-3-chloro-2-propenyl hydroxylamine, which is a main raw material for producing clethodim, clethodim and cycloxydim, and the herbicide is an accase inhibitor, is a post-emergence selective herbicide and has special effect on most annual and perennial gramineous weeds. A solution is a homogeneous, stable mixture of one or more substances dispersed in another substance, the dispersed substance (solute) being dispersed as molecules or smaller particles in the other substance (solvent). And low boiling point solution is the lower solution of boiling point, and in the condensation recovery process to low boiling point solution, the mode of current condensation recovery adopts the condenser to condense more, and this kind of mode is complex operation not only, has increased the consumption of the energy, still leads to still can't condensing a large amount of steam, to this we propose a low boiling point solution condensation recovery unit. In view of this, we propose a plant for the recovery of low boiling aqueous solutions by acid hydrolysis for the synthesis of chloroamines.
SUMMERY OF THE UTILITY MODEL
In order to make up for the defects, the utility model provides a device for recycling low boiling water solution by acidolysis for synthesizing chloramine.
The technical scheme of the utility model is that:
the utility model provides an equipment that is used for acidolysis of synthetic chloramine to retrieve low boiling water solution, includes the condensation storehouse, condensation storehouse internally mounted has the condensation subassembly, the backward flow subassembly is all installed to the condensation storehouse left and right sides, backward flow subassembly bottom is equipped with out the liquid subassembly.
Preferably, the condensing assembly comprises two annular condensing pipes, and two ends of each annular condensing pipe are respectively communicated with a steam pipe and a first liquid outlet pipe.
Preferably, the condensation chamber includes the condensing box, condensing box top fixed mounting has the coolant liquid entry, set up the cooling cistern that can place the coolant liquid in the condensing box, first steam groove and second steam groove have been seted up respectively to the condensing box top, first backward flow groove and second backward flow groove have all been seted up to the condensing box left and right sides side, the inside fixed mounting of condensing box has the baffle, and the baffle can divide into cooling cistern and collecting vat two parts with the condensing box, set up two recesses that supply first drain pipe to pass in the baffle, the drain tank has been seted up to the condensing box bottom.
Preferably, the backflow component comprises a backflow pipe, a liquid outlet and a water pump are respectively and fixedly mounted at two ends of the backflow pipe, the backflow pipe is connected with an outlet of the water pump, and a liquid inlet is fixedly mounted at the other side of the water pump.
Preferably, the liquid outlet assembly comprises a valve, and a second liquid outlet pipe is fixedly mounted on the lower side of the valve.
Preferably, the two steam pipes are fixedly connected with the first steam groove and the second steam groove respectively.
Preferably, the liquid outlet and the liquid inlet are fixedly installed with the first backflow groove and the second backflow groove respectively.
Preferably, the valve is fixedly installed with the liquid outlet tank.
Compared with the prior art, the beneficial effects of the utility model are that:
the utility model discloses a condensation of low boiling point solution is retrieved, injects the coolant liquid in the coolant liquid inslot, inserts the steam pipe with the steam that low boiling point solution produced, gets into annular condenser pipe from the steam pipe, and the coolant liquid in the annular condenser pipe outside is with steam from the cooling condensing into liquid in the gas, flows in the collecting vat that baffle bottom and condensation box formed at last, can derive liquid through opening the valve, and the backward flow subassembly of condensation box both sides can accelerate the coolant liquid and flow, improves condensation efficiency.
Drawings
FIG. 1 is a schematic view of the overall structure of the present invention;
FIG. 2 is a schematic view of the structure of the condensation chamber of the present invention;
FIG. 3 is a schematic structural view of the condensing assembly of the present invention;
FIG. 4 is a schematic view of the structure of the reflow module of the present invention;
fig. 5 is a schematic view of the liquid outlet assembly of the present invention.
In the figure:
1. a condensation bin; 11. a condensing tank; 12. a coolant inlet; 13. a cooling liquid tank; 14. a first steam tank; 15. a second steam tank; 16. a first backflow groove; 17. a second reflux tank; 18. a baffle plate; 19. a liquid outlet groove;
2. a condensing assembly; 21. a steam pipe; 22. an annular condenser tube; 23. a first liquid outlet pipe;
3. a reflow assembly; 31. a return pipe; 32. a liquid outlet; 33. a water pump; 34. a liquid inlet;
4. a liquid outlet assembly; 41. a valve; 42. a second liquid outlet pipe.
Detailed Description
The technical solutions in the embodiments of the present invention will be described clearly and completely with reference to the drawings in the embodiments of the present invention, and it is obvious that the described embodiments are only some embodiments of the present invention, not all embodiments. Based on the embodiments in the present invention, all other embodiments obtained by a person skilled in the art without creative efforts all belong to the protection scope of the present invention.
In the description of the present invention, it is to be understood that the terms "center", "longitudinal", "lateral", "length", "width", "thickness", "upper", "lower", "front", "rear", "left", "right", "vertical", "horizontal", "top", "bottom", "inner", "outer", "clockwise", "counterclockwise", and the like indicate orientations or positional relationships based on the orientations or positional relationships shown in the drawings, and are only for convenience of description and for simplicity of description, but do not indicate or imply that the device or element referred to must have a particular orientation, be constructed and operated in a particular orientation, and therefore, should not be construed as limiting the present invention.
Referring to fig. 1-5, the present invention provides a technical solution:
the utility model provides an equipment that is used for acidolysis of synthetic chloramine to retrieve low boiling water solution, including condensation storehouse 1, 1 internally mounted in condensation storehouse has condensation subassembly 2, backflow subassembly 3 is all installed to the 1 left and right sides in condensation storehouse, backflow subassembly 3 bottom is equipped with out liquid subassembly 4, when needing to retrieve the low boiling water solution that produces to the acidolysis in-process of synthetic chloramine, with the coolant liquid of injecting in condensation storehouse 1, be connected condensation subassembly 2 with the steam that low boiling point solution produced, this condensation subassembly 2 outer coolant liquid is with steam from cooling condensation liquid in the gas, flow into out liquid subassembly 4 through condensation subassembly 2, and it can accelerate the coolant liquid to open backflow subassembly 3 and flow, the condensation efficiency is improved.
What need to supplement is, condensation component 2 includes two annular condenser pipes 22, and annular condenser pipe 22 both ends communicate respectively has steam pipe 21 and first drain pipe 23, when the low boiling water solution that produces need to synthesize the acidolysis in-process of chloramine retrieves, be connected the steam that two steam pipes 21 and low boiling point solution produced, make steam get into annular condenser pipe 22, annular condenser pipe 22 can increase the condensation area, the outer coolant liquid of annular condenser pipe 22 is with steam from the cooling condensing into liquid in the gas, flow through first drain pipe 23, and then accomplish the condensation.
It should be noted that the condensation bin 1 includes a condensation box 11, a cooling liquid inlet 12 is fixedly installed above the condensation box 11, a cooling liquid tank 13 capable of containing cooling liquid is opened in the condensation box 11, a first steam tank 14 and a second steam tank 15 are respectively opened above the condensation box 11, a first backflow tank 16 and a second backflow tank 17 are both opened on the left and right sides of the condensation box 11, a baffle 18 is fixedly installed inside the condensation box 11, the condensation box 11 can be divided into the cooling liquid tank 13 and a collecting tank by the baffle 18, two grooves for the first liquid outlet pipe 23 to pass through are opened in the baffle 18, a liquid outlet tank 19 is opened at the bottom of the condensation box 11, when low boiling water solution generated in the acidolysis process of the chloramine is required to be recovered, the cooling liquid inlet 12 is opened, and the cooling liquid is injected into the cooling liquid tank 13 from the cooling liquid inlet 12.
It should be added that, the reflux assembly 3 includes a reflux pipe 31, a liquid outlet 32 and a water pump 33 are respectively fixedly installed at two ends of the reflux pipe 31, the reflux pipe 31 is connected with an outlet of the water pump 33, a liquid inlet 34 is fixedly installed at the other side of the water pump 33, when low boiling water solution generated in the acidolysis process of the synthesized chloramine needs to be recovered, the water pumps 33 at two sides of the condensation bin 1 are opened, the water pump 33 conveys the cooling liquid in the cooling liquid tank 13 to the liquid outlet 32 from the liquid inlet 34, the flowing of the cooling liquid can be accelerated, and the condensation efficiency is improved.
Preferably, the liquid outlet assembly 4 comprises a valve 41, and a second liquid outlet pipe 42 is fixedly installed on the lower side of the valve 41, when liquid in a collecting tank formed by the bottom of the baffle 18 and the condensing box 11 needs to be collected, the valve 41 is opened, and the liquid flows out from the second liquid outlet pipe 42 below the valve 41.
It is necessary to supplement that the two steam pipes 21 are respectively fixedly connected with the first steam groove 14 and the second steam groove 15, so as to prevent the steam pipes 21 from deviating.
Further, the liquid outlet 32 and the liquid inlet 34 are fixedly installed with the first return tank 16 and the second return tank 17, respectively, and the water pump 33 can convey the cooling liquid in the cooling liquid tank 13 from the liquid inlet 34 to the liquid outlet 32.
It should be added that the valve 41 is fixedly installed with the liquid outlet tank 19, and the liquid flows from the liquid outlet tank 19 to the second liquid outlet pipe 42 by opening the valve 41.
When the device is used specifically, when low boiling water solution generated in the acidolysis process for synthesizing the chloramine needs to be recovered, the cooling liquid inlet 12 is opened, the cooling liquid is injected into the cooling liquid tank 13 from the cooling liquid inlet 12, the two steam pipes 21 are connected with a steam port generated by the low boiling point solution, the steam enters the annular condensation pipe 22, the condensation area of the annular condensation pipe 22 can be increased, the cooling liquid outside the annular condensation pipe 22 cools and condenses the steam from gas into liquid, the liquid flows out of the collection tank below the baffle 18 through the first liquid outlet pipe 23, condensation is completed, the water pumps 33 on the two sides of the condensation bin 1 are started, the cooling liquid in the cooling liquid tank 13 is conveyed to the liquid outlet 32 through the liquid inlet 34 by the water pumps 33, the flow of the cooling liquid can be accelerated, the condensation efficiency is improved, when the liquid in the collection tank 11 formed by the bottom of the baffle 18 is required to be collected, the valve 41 is started, and the liquid flows out of the second liquid outlet pipe 42 below the valve 41.
The foregoing shows and describes the general principles, essential features, and advantages of the invention. It should be understood by those skilled in the art that the present invention is not limited by the above embodiments, and the description in the above embodiments and the description is only preferred examples of the present invention, and is not intended to limit the present invention, and that the present invention can have various changes and modifications without departing from the spirit and scope of the present invention, and these changes and modifications all fall into the scope of the claimed invention. The scope of the invention is defined by the appended claims and equivalents thereof.
Claims (7)
1. An equipment for the acidolysis recovery of low boiling aqueous solution for the synthesis of chloramine, comprising a condensation bin (1), characterized in that: a condensation component (2) is arranged in the condensation bin (1), backflow components (3) are arranged on the left side and the right side of the condensation bin (1), and a liquid outlet component (4) is arranged at the bottom of each backflow component (3);
the condensation assembly (2) comprises two annular condensation pipes (22), and the two ends of each annular condensation pipe (22) are respectively communicated with a steam pipe (21) and a first liquid outlet pipe (23).
2. The plant for the recovery of low boiling aqueous solutions with acid hydrolysis for the synthesis of chlorinated amines, as claimed in claim 1, characterized in that: condensation chamber (1) includes condenser box (11), condenser box (11) top fixed mounting has coolant liquid entry (12), set up cooling cistern (13) that can place the coolant liquid in condenser box (11), first steam groove (14) and second steam groove (15) have been seted up respectively to condenser box (11) top, first backward flow groove (16) and second backward flow groove (17) have all been seted up to the condenser box (11) left and right sides, condenser box (11) inside fixed mounting has baffle (18), and baffle (18) can divide into cooling cistern (13) and collecting vat two parts with condenser box (11), set up two recesses that supply first drain pipe (23) to pass in baffle (18), drain groove (19) have been seted up to condenser box (11) bottom.
3. The plant for the recovery of low boiling aqueous solutions with acid hydrolysis for the synthesis of chlorinated amines, as claimed in claim 2, characterized in that: the backflow component (3) comprises a backflow pipe (31), a liquid outlet (32) and a water pump (33) are fixedly mounted at two ends of the backflow pipe (31) respectively, the backflow pipe (31) is connected with an outlet of the water pump (33), and a liquid inlet (34) is fixedly mounted at the other side of the water pump (33).
4. The plant for the recovery of low boiling aqueous solutions for the acidolysis of the synthesis of chloramine according to claim 1, characterized in that: the liquid outlet assembly (4) comprises a valve (41), and a second liquid outlet pipe (42) is fixedly mounted on the lower side of the valve (41).
5. The plant for the recovery of low boiling aqueous solutions for the acidolysis of the synthesis of chloramine according to claim 2, characterized in that: the two steam pipes (21) are respectively and fixedly connected with the first steam groove (14) and the second steam groove (15).
6. The plant for the recovery of low boiling aqueous solutions for the acidolysis of the synthesis of chloramine according to claim 3, characterized in that: the liquid outlet (32) and the liquid inlet (34) are respectively fixedly arranged with the first backflow groove (16) and the second backflow groove (17).
7. The plant for the recovery of low boiling aqueous solutions with acid hydrolysis for the synthesis of chlorinated amines, as claimed in claim 4, characterized in that: the valve (41) and the liquid outlet groove (19) are fixedly arranged.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202221669593.7U CN218443409U (en) | 2022-06-30 | 2022-06-30 | Equipment for recycling low boiling water solution by acidolysis for synthesizing chloramine |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202221669593.7U CN218443409U (en) | 2022-06-30 | 2022-06-30 | Equipment for recycling low boiling water solution by acidolysis for synthesizing chloramine |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN218443409U true CN218443409U (en) | 2023-02-03 |
Family
ID=85089631
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN202221669593.7U Active CN218443409U (en) | 2022-06-30 | 2022-06-30 | Equipment for recycling low boiling water solution by acidolysis for synthesizing chloramine |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN218443409U (en) |
-
2022
- 2022-06-30 CN CN202221669593.7U patent/CN218443409U/en active Active
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN101985369B (en) | Plate type sea water desalinating device | |
| CN108585093A (en) | The processing recycling ammonium hydrogen carbonate system and its processing recovery process of landfill leachate | |
| CN101773784A (en) | Vacuum membrane distillation device and method thereof | |
| CN212894306U (en) | Circuit board etching waste liquid recovery processing device | |
| CN218443409U (en) | Equipment for recycling low boiling water solution by acidolysis for synthesizing chloramine | |
| CN208345794U (en) | Ammonium hydrogen carbonate system is recycled in the processing of landfill leachate | |
| CN205549656U (en) | Gaseous state solvent condensation recovery device | |
| CN211570356U (en) | Material washing water recycling and circulating system | |
| CN204182144U (en) | A kind of efficient chemical industry evaporimeter | |
| CN209338574U (en) | Sugar juice vapour condensing unit | |
| CN209076080U (en) | A kind of production tail gas condensing recover of pyraclostrobin | |
| CN206896891U (en) | A kind of heavy concentration systems of water and traditional Chinese medicine extraction system | |
| CN113800704B (en) | Ion exchange resin regeneration activation wastewater distillation concentration treatment method | |
| CN213698853U (en) | Ball-type concentrator is used to traditional chinese medicine extract for animal | |
| JP3358057B2 (en) | Solar thermal and photovoltaic hybrid desalination equipment | |
| CN212983026U (en) | Desorption column and gold-loaded carbon electrolysis device | |
| CN205367778U (en) | Membrane distillation plant | |
| CN108129291A (en) | A kind of processing system for polymethoxy dimethyl ether brine waste | |
| CN210302497U (en) | Hot reflux extraction and concentration equipment | |
| CN210663441U (en) | Lithium bromide absorption heat pump unit | |
| CN219517813U (en) | Orthoformate polymer separation system | |
| CN214064857U (en) | Environment-friendly furfural production wastewater circulating evaporator | |
| CN206927646U (en) | One kind processing ammonia still of ammonia waste water containing metal complex | |
| CN111762944A (en) | Water tank for oxyhydrogen machine | |
| CN218686363U (en) | Recovery device adopting heat pump vacuum low-temperature evaporation concentration |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| GR01 | Patent grant | ||
| GR01 | Patent grant | ||
| CP01 | Change in the name or title of a patent holder | ||
| CP01 | Change in the name or title of a patent holder |
Address after: 256,800 North of Fuyuan 5th Road, Zhanhua Economic Development Zone, Binzhou, Shandong Patentee after: Shandong Jiayu Chemical Technology Co.,Ltd. Address before: 256,800 North of Fuyuan 5th Road, Zhanhua Economic Development Zone, Binzhou, Shandong Patentee before: Zhanhua Jiayu chemical industry and Trade Co.,Ltd. |