CN212293711U - Leaching and collecting device for mixture generated in reduction of titanium sponge - Google Patents
Leaching and collecting device for mixture generated in reduction of titanium sponge Download PDFInfo
- Publication number
- CN212293711U CN212293711U CN202022233034.9U CN202022233034U CN212293711U CN 212293711 U CN212293711 U CN 212293711U CN 202022233034 U CN202022233034 U CN 202022233034U CN 212293711 U CN212293711 U CN 212293711U
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- pipe
- tank body
- titanium
- valve
- leaching
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- RTAQQCXQSZGOHL-UHFFFAOYSA-N Titanium Chemical compound [Ti] RTAQQCXQSZGOHL-UHFFFAOYSA-N 0.000 title claims abstract description 31
- 239000000203 mixture Substances 0.000 title claims abstract description 21
- 230000009467 reduction Effects 0.000 title claims abstract description 12
- 238000002386 leaching Methods 0.000 title claims abstract description 8
- 239000007921 spray Substances 0.000 claims abstract description 21
- 239000010865 sewage Substances 0.000 claims abstract description 14
- 238000005507 spraying Methods 0.000 claims abstract description 5
- 238000000034 method Methods 0.000 claims description 3
- 239000010936 titanium Substances 0.000 abstract description 16
- 229910052719 titanium Inorganic materials 0.000 abstract description 16
- XJDNKRIXUMDJCW-UHFFFAOYSA-J titanium tetrachloride Chemical compound Cl[Ti](Cl)(Cl)Cl XJDNKRIXUMDJCW-UHFFFAOYSA-J 0.000 abstract description 13
- 238000004519 manufacturing process Methods 0.000 abstract description 8
- 239000000126 substance Substances 0.000 abstract description 7
- 238000003912 environmental pollution Methods 0.000 abstract description 6
- XKRFYHLGVUSROY-UHFFFAOYSA-N Argon Chemical compound [Ar] XKRFYHLGVUSROY-UHFFFAOYSA-N 0.000 description 10
- 238000006722 reduction reaction Methods 0.000 description 8
- 229910052786 argon Inorganic materials 0.000 description 5
- 239000007789 gas Substances 0.000 description 5
- FYYHWMGAXLPEAU-UHFFFAOYSA-N Magnesium Chemical compound [Mg] FYYHWMGAXLPEAU-UHFFFAOYSA-N 0.000 description 3
- 229910052749 magnesium Inorganic materials 0.000 description 3
- 239000011777 magnesium Substances 0.000 description 3
- 238000005406 washing Methods 0.000 description 3
- TWRXJAOTZQYOKJ-UHFFFAOYSA-L Magnesium chloride Chemical compound [Mg+2].[Cl-].[Cl-] TWRXJAOTZQYOKJ-UHFFFAOYSA-L 0.000 description 2
- 239000003513 alkali Substances 0.000 description 2
- 239000007788 liquid Substances 0.000 description 2
- 230000002378 acidificating effect Effects 0.000 description 1
- 238000003915 air pollution Methods 0.000 description 1
- 230000004075 alteration Effects 0.000 description 1
- 230000008901 benefit Effects 0.000 description 1
- 239000003518 caustics Substances 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- 230000005484 gravity Effects 0.000 description 1
- 238000007689 inspection Methods 0.000 description 1
- 229910001629 magnesium chloride Inorganic materials 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 239000003595 mist Substances 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000008092 positive effect Effects 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 239000000376 reactant Substances 0.000 description 1
- 238000004064 recycling Methods 0.000 description 1
- 238000006479 redox reaction Methods 0.000 description 1
- 238000011946 reduction process Methods 0.000 description 1
- 210000002345 respiratory system Anatomy 0.000 description 1
- 239000000779 smoke Substances 0.000 description 1
- 238000006467 substitution reaction Methods 0.000 description 1
- 239000002699 waste material Substances 0.000 description 1
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Abstract
A leaching and collecting device for a mixture generated in titanium sponge reduction comprises a tank body, an air outlet pipe, a spraying pipe, a mixture inlet pipe, a drain valve, a drain pipe, a passageway pipe and a fan; the top of the tank body is provided with an air outlet pipe, and the lower part of the side of the tank body is connected with a fan through a passage pipe; one end of the spray pipe with the spray head is arranged at the central part in the tank body; the mixture inlet pipe is arranged at the middle lower part of the tank body; an anti-fog net is arranged at the upper part in the tank body; the tank body below the anti-fog net is provided with an access hole corresponding to the spray head; the blow-off pipe is arranged at the lower part of the side of the tank body and is provided with a blow-off valve; a filter screen is arranged in the tank body at the corresponding position of the sewage discharge pipe; the bottom of the tank body is provided with a collecting pipe, and a valve is arranged on the collecting pipe. The utility model realizes the leaching of titanium tetrachloride in the emissions when the titanium sponge is reduced, and avoids the environmental pollution; and the granular titanium low-price substances in the discharge are leached and collected, so that the titanium low-price substances are reused, the resources are saved, and the production cost is saved.
Description
Technical Field
The utility model relates to a titanium sponge's apparatus for producing, in particular to a drip washing collection device that is arranged in the mixture that produces in the titanium sponge reduction.
Background
At present, the sponge titanium is industrially produced at home and abroad by adopting a Claur method, the main raw materials are magnesium, titanium tetrachloride and argon, and the method for reducing the titanium tetrachloride by the magnesium is that liquid titanium tetrachloride is continuously introduced into a reactor, and the titanium tetrachloride and magnesium in a molten state undergo an oxidation-reduction reaction to mainly generate the sponge titanium and magnesium chloride. During the production process, proper argon gas is required to be filled for protection, air pollution products are prevented from entering the reactor, the pressure in the reactor is required to be kept positive, but the pressure cannot be too high, the production must be controlled within a certain range, titanium tetrachloride is gasified when meeting high temperature, and when the pressure in the reactor is too high, manual pressure discharge is also required.
The titanium sponge reduction production in each furnace has high exhaust frequency due to pressure rise, and particularly, the mixture of titanium tetrachloride gas, argon and granular titanium low-price substances is discharged very frequently at the later stage of reduction charging production.
Titanium tetrachloride gas is an acidic corrosive substance, is white smoke in the air, and can cause damage to the respiratory system after being inhaled by people carelessly.
The low-price titanium has strong pungent smell, and the direct discharge is easy to cause environmental pollution and harm to human bodies of operators.
Discharged titanium low-price substances are not recycled, so that the environmental pollution is serious, and the waste of resources is caused.
SUMMERY OF THE UTILITY MODEL
The utility model relates to a solve in the titanium sponge reduction production process, the low price thing of discharged titanium tetrachloride gas and titanium is not handled, not only serious to environmental pollution, and caused the extravagant technical problem of low price material resources of titanium.
In order to solve the technical problem, the utility model adopts the following technical scheme:
a leaching and collecting device for a mixture generated in titanium sponge reduction mainly comprises a tank body 1, an air outlet pipe 3, a spraying pipe 5, a mixture inlet pipe 6, a blow-off valve 7, a blow-off pipe 8, a passageway pipe 12 and a fan 13;
the top of the tank body 1 is provided with an air outlet pipe 3, and the lower part of the side of the tank body is connected with a fan 13 through a pipeline 12;
one end of the spray pipe 5 with a spray head is arranged at the central part in the tank body 1; the mixture inlet pipe 6 is arranged at the middle lower part of the tank body 1;
an anti-fog net 2 is arranged at the upper part in the tank body 1;
the tank body 1 below the anti-fog net 2 is provided with an access hole 4 corresponding to the spray head;
the sewage discharge pipe 8 is arranged at the lower part of the side of the tank body 1, and a sewage discharge valve 7 is arranged on the sewage discharge pipe;
a filter screen 9 is arranged in the tank body 1 corresponding to the sewage discharge pipe 8;
the bottom of the tank body 1 is provided with a collecting pipe 10, and a valve 11 is arranged on the collecting pipe.
The number of the spray pipes 5 with the spray heads is three to six.
The utility model discloses specific advantage is with positive effect:
1. the utility model discloses a when the titanium sponge is reduced, carry out the drip washing to the titanium tetrachloride in the emission, stop environmental pollution.
2. The utility model discloses a when the titanium sponge is reduced, drip washing and collection are carried out to the graininess titanium low price thing in the emission for reuse the low price thing of titanium, practiced thrift the resource, saved manufacturing cost.
Drawings
Fig. 1 is a schematic structural diagram of the present invention.
In the figure: 1-tank body, 2-antifogging net, 3-air outlet pipe, 4-inspection hole, 5-spraying pipe, 6-mixture inlet pipe, 7-blowoff valve, 8-blowoff pipe, 9-filter screen, 10-collecting pipe, 11-valve, 12-channel pipe and 13-fan.
Detailed Description
The present invention will be described in further detail with reference to the accompanying drawings, but it should not be understood that the scope of the subject matter of the present invention is limited to the following embodiments, and various modifications, substitutions and alterations according to the common technical knowledge and conventional means in the art are included in the scope of the present invention without departing from the technical spirit of the present invention.
As shown in fig. 1, a leaching and collecting device for a mixture generated in titanium sponge reduction mainly comprises a tank body 1, an air outlet pipe 3, a spraying pipe 5, a mixture inlet pipe 6, a drain valve 7, a drain pipe 8, a passageway pipe 12 and a fan 13;
the top of the tank body 1 is provided with an air outlet pipe 3, and the lower part of the side of the tank body is connected with a fan 13 through a pipeline 12;
one end of the spray pipe 5 with a spray head is arranged at the central part in the tank body 1;
the mixture inlet pipe 6 is arranged at the middle lower part of the tank body 1;
an anti-fog net 2 is arranged at the upper part in the tank body 1; which functions to prevent the generated mist from being discharged through the outlet pipe 3.
The tank body 1 below the anti-fog net 2 is provided with an access hole 4 corresponding to the spray head; when the spray head fails, the spray head is convenient to replace from the access hole 4;
the sewage discharge pipe 8 is arranged at the lower part of the side of the tank body 1, and a sewage discharge valve 7 is arranged on the sewage discharge pipe;
a filter screen 9 is arranged in the tank body 1 corresponding to the sewage discharge pipe 8 and is used for preventing granular titanium low-price objects from being discharged from the sewage discharge pipe 8;
the bottom of the tank body 1 is provided with a collecting pipe 10, a valve 11 is arranged on the collecting pipe, and the collecting pipe 10 is used for collecting granular titanium low-price objects.
The number of the spray pipes 5 with the spray heads is three to six.
In the utility model, before the reduction charging production of the titanium sponge, all pipelines are connected, the fan 13 is started, alkaline liquid is introduced into the spray pipe 5, when the pressure is discharged in the reactor, the mixture of titanium tetrachloride gas, argon and granular titanium low-price substances is discharged, the mixture enters the tank body 1 through the mixture inlet pipe 6, the sprayed alkali liquor is leached, the granular titanium low-price substances are settled to the bottom of the tank body 1 under the self gravity, and when a certain amount is reached, the valve 11 is opened, so that the titanium low-price substances are collected from the collecting pipe 10 for recycling; argon is discharged from an air outlet pipe 3; the reactants of titanium tetrachloride and alkali liquor are discharged from a discharge pipe 8. Utilize the utility model discloses the device has avoided the direct emission of titanium tetrachloride among the reduction process, reduces environmental pollution to the recycle of resource has been realized.
Claims (2)
1. A leaching and collecting device for a mixture generated in titanium sponge reduction mainly comprises a tank body (1), an air outlet pipe (3), a spraying pipe (5), a mixture inlet pipe (6), a drain valve (7), a drain pipe (8), a passageway pipe (12) and a fan (13);
the top of the tank body (1) is provided with an air outlet pipe (3), and the lower side part of the tank body is connected with a fan (13) through a channel pipe (12); one end of the spray pipe (5) with a spray head is arranged at the central part in the tank body (1); the mixture inlet pipe (6) is arranged at the middle lower part of the tank body (1); the method is characterized in that:
an anti-fog net (2) is arranged at the upper part in the tank body (1);
an access hole (4) corresponding to the spray head is formed in the tank body (1) below the anti-fog net (2);
the sewage discharge pipe (8) is arranged at the lower part of the side of the tank body (1), and a sewage discharge valve (7) is arranged on the sewage discharge pipe;
a filter screen (9) is arranged in the tank body (1) at the corresponding position of the sewage discharge pipe (8);
the bottom of the tank body (1) is provided with a collecting pipe (10) on which a valve (11) is arranged.
2. The leaching collection device for the mixture produced in the reduction of titanium sponge according to claim 1, wherein: the number of the spray pipes (5) with the spray heads is three to six.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202022233034.9U CN212293711U (en) | 2020-10-10 | 2020-10-10 | Leaching and collecting device for mixture generated in reduction of titanium sponge |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202022233034.9U CN212293711U (en) | 2020-10-10 | 2020-10-10 | Leaching and collecting device for mixture generated in reduction of titanium sponge |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN212293711U true CN212293711U (en) | 2021-01-05 |
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ID=73933970
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN202022233034.9U Active CN212293711U (en) | 2020-10-10 | 2020-10-10 | Leaching and collecting device for mixture generated in reduction of titanium sponge |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN212293711U (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111996393A (en) * | 2020-10-10 | 2020-11-27 | 遵宝钛业有限公司 | Leaching and collecting device for mixture generated in reduction of titanium sponge |
-
2020
- 2020-10-10 CN CN202022233034.9U patent/CN212293711U/en active Active
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111996393A (en) * | 2020-10-10 | 2020-11-27 | 遵宝钛业有限公司 | Leaching and collecting device for mixture generated in reduction of titanium sponge |
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