CN209656525U - A kind of for transformer oil oxidizer unit that quickly oxidation is tested - Google Patents
A kind of for transformer oil oxidizer unit that quickly oxidation is tested Download PDFInfo
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- CN209656525U CN209656525U CN201822189583.3U CN201822189583U CN209656525U CN 209656525 U CN209656525 U CN 209656525U CN 201822189583 U CN201822189583 U CN 201822189583U CN 209656525 U CN209656525 U CN 209656525U
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- transformer oil
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- test cup
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- 230000003647 oxidation Effects 0.000 title claims abstract description 48
- 238000007254 oxidation reaction Methods 0.000 title claims abstract description 48
- 239000007800 oxidant agent Substances 0.000 title claims abstract description 10
- 238000012360 testing method Methods 0.000 claims abstract description 47
- 238000010438 heat treatment Methods 0.000 claims abstract description 28
- 239000002912 waste gas Substances 0.000 claims abstract description 25
- 239000007788 liquid Substances 0.000 claims abstract description 10
- 238000007789 sealing Methods 0.000 claims abstract description 4
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 claims 3
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N EtOH Substances CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims 1
- 238000006243 chemical reaction Methods 0.000 abstract description 8
- 239000003921 oil Substances 0.000 description 23
- OVYTZAASVAZITK-UHFFFAOYSA-M sodium;ethanol;hydroxide Chemical compound [OH-].[Na+].CCO OVYTZAASVAZITK-UHFFFAOYSA-M 0.000 description 8
- 239000007789 gas Substances 0.000 description 7
- 239000002253 acid Substances 0.000 description 6
- 238000000034 method Methods 0.000 description 6
- 230000003064 anti-oxidating effect Effects 0.000 description 4
- 239000002199 base oil Substances 0.000 description 2
- 238000005336 cracking Methods 0.000 description 2
- RYGMFSIKBFXOCR-UHFFFAOYSA-N Copper Chemical compound [Cu] RYGMFSIKBFXOCR-UHFFFAOYSA-N 0.000 description 1
- 230000003712 anti-aging effect Effects 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 239000003054 catalyst Substances 0.000 description 1
- 229910052802 copper Inorganic materials 0.000 description 1
- 239000010949 copper Substances 0.000 description 1
- 230000007547 defect Effects 0.000 description 1
- 238000001514 detection method Methods 0.000 description 1
- 239000011810 insulating material Substances 0.000 description 1
- 238000009413 insulation Methods 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 239000013049 sediment Substances 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 238000010561 standard procedure Methods 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
Landscapes
- Housings And Mounting Of Transformers (AREA)
- Investigating Or Analyzing Non-Biological Materials By The Use Of Chemical Means (AREA)
Abstract
本实用新型提供了一种用于变压器油快速氧化测试的氧化器装置,其包括氧化试验杯、设置在所述氧化试验杯上起密封作用的氧化试验杯盖、以及废气收集池;所述氧化试验杯和所述废气收集池之间通过连接管连通;所述废气收集池内设置有废气收集液;所述氧化试验杯上设置有加热装置。本实用新型提供的一种用于变压器油快速氧化测试的氧化器装置,利用温度升高10℃,化学反应速率增加一倍的原理,大幅度提高反应温度以及速率,降低试验时间,从而快速判别变压器油抗氧化的能力。
The utility model provides an oxidizer device for rapid oxidation test of transformer oil, which comprises an oxidation test cup, an oxidation test cup cover arranged on the oxidation test cup for sealing, and a waste gas collection pool; The test cup communicates with the waste gas collection pool through a connecting pipe; the waste gas collection liquid is arranged in the waste gas collection pool; the oxidation test cup is provided with a heating device. The utility model provides an oxidizer device for the rapid oxidation test of transformer oil, which utilizes the principle that the chemical reaction rate doubles when the temperature rises by 10°C, greatly increases the reaction temperature and rate, and reduces the test time, thereby quickly distinguishing The ability of transformer oil to resist oxidation.
Description
技术领域technical field
本实用新型涉及一种检测试验装置,尤其适用于变压器油快速氧化测试。The utility model relates to a detection test device, which is especially suitable for rapid oxidation test of transformer oil.
背景技术Background technique
变压器油的抗氧化和抗老化性能是变压器油非常重要的指标,是变压器油使用等级划分的重要基础,也是变压器制造商选择变压器油的主要依据。The anti-oxidation and anti-aging properties of transformer oil are very important indicators of transformer oil, an important basis for the classification of transformer oil use, and the main basis for transformer manufacturers to choose transformer oil.
变压器油是变压器中的重要绝缘材料,其质量的好坏直接关系到电网的安全运行。目前我国环烷基基础油的产量无法满足要求,因此一些变压器油厂家就采取各种方式用其它基础油进行再加工,降低了变压器油的使用寿命和绝缘性能。变压器油的使用单位只能检测耐压、介损、微水等非常简单的指标,无法检测氧化安定性等指标,也无法判断变压器油的品质。变压器在投运几年后就出现故障断电更换变压器油,给电网造成了损失。Transformer oil is an important insulating material in transformers, and its quality is directly related to the safe operation of the power grid. At present, the output of naphthenic base oil in my country cannot meet the requirements, so some transformer oil manufacturers adopt various methods to reprocess with other base oils, which reduces the service life and insulation performance of transformer oil. The user unit of transformer oil can only detect very simple indicators such as withstand voltage, dielectric loss, and micro-water, but cannot detect indicators such as oxidation stability, and cannot judge the quality of transformer oil. A few years after the transformer was put into operation, the transformer failed and the power was cut off to replace the transformer oil, which caused losses to the power grid.
准确测定变压器油氧化安定性的方法为NB/SH/T0811,其方法概要为在待测样品中放入固体铜催化剂,恒速通入空气,在120℃温度下保持500h后,通过测定氧化后油品的挥发性酸值、油溶性酸值和沉淀物含量。但是此标准方法操作时间长,且现场可操作性不强。The method for accurately measuring the oxidation stability of transformer oil is NB/SH/T0811. The method outline is to put a solid copper catalyst into the sample to be tested, pass air in at a constant speed, and keep it at 120°C for 500 hours, then measure the oxidation stability of the transformer oil. Volatile acid value, oil soluble acid value and sediment content of oil products. However, this standard method takes a long time to operate, and the field operability is not strong.
实用新型内容Utility model content
本实用新型要解决的技术问题是克服现有的缺陷,提供一种用于变压器油快速氧化测试的氧化器装置,能够快速判别变压器油抗氧化的能力。The technical problem to be solved by the utility model is to overcome the existing defects and provide an oxidizer device for rapid oxidation test of transformer oil, which can quickly judge the anti-oxidation ability of transformer oil.
为了解决上述技术问题,本实用新型提供了如下的技术方案:In order to solve the above technical problems, the utility model provides the following technical solutions:
本实用新型公开了一种用于变压器油快速氧化测试的氧化器装置,其包括氧化试验杯、设置在所述氧化试验杯上起密封作用的氧化试验杯盖、以及废气收集池;所述氧化试验杯和所述废气收集池之间通过连接管连通;所述废气收集池内设置有废气收集液;所述氧化试验杯上设置有加热装置。The utility model discloses an oxidizer device for rapid oxidation test of transformer oil, which comprises an oxidation test cup, an oxidation test cup cover arranged on the oxidation test cup for sealing, and a waste gas collection pool; The test cup communicates with the waste gas collection pool through a connecting pipe; the waste gas collection liquid is arranged in the waste gas collection pool; the oxidation test cup is provided with a heating device.
进一步地:所述氧化试验杯及所述氧化试验杯盖之间采用螺纹连接。Further: the oxidation test cup and the oxidation test cup cover are threaded.
进一步地:所述加热装置为带温控的线圈夹套加热装置;所述带温控的线圈夹套加热装置包括加热夹条、控温开关和温度显示屏。加热夹条用于加热,控温开关用于控制加热装置的电源,温度显示屏用于显示温度。加热装置采用普通电源供电。Further: the heating device is a coil jacket heating device with temperature control; the coil jacket heating device with temperature control includes a heating clip, a temperature control switch and a temperature display screen. The heating clip is used for heating, the temperature control switch is used for controlling the power supply of the heating device, and the temperature display screen is used for displaying the temperature. The heating device is powered by common power supply.
进一步地:所述废气收集池内设置的废气收集液为0.5mol/L的氢氧化钠-乙醇溶液。Further: the waste gas collection liquid provided in the waste gas collection pool is 0.5 mol/L sodium hydroxide-ethanol solution.
工作时:所述加热装置,对加入到氧化试验杯中的变压器油升温,并将温度控制在150℃。通过所述连接管收集氧化测试过程中裂解反应产生的废气。所述的废气收集池采用的收集液为0.5mol/L的氢氧化钠-乙醇溶液。所述氢氧化钠-乙醇溶液不但可以收集中和酸性气体,而且可以通过计算所述氢氧化钠-乙醇溶液消耗量计算氧化过程中产生的酸性气体含量。When working: the heating device heats up the transformer oil added to the oxidation test cup, and controls the temperature at 150°C. The exhaust gas produced by the cracking reaction during the oxidation test is collected through the connecting pipe. The collection liquid used in the waste gas collection pool is 0.5 mol/L sodium hydroxide-ethanol solution. The sodium hydroxide-ethanol solution can not only collect and neutralize the acid gas, but also can calculate the acid gas content generated in the oxidation process by calculating the consumption of the sodium hydroxide-ethanol solution.
有益效果:本实用新型提供的装置,利用温度升高10℃,化学反应速率增加一倍的原理,大幅度提高反应温度以及速率,降低试验时间,从而能够快速判别变压器油抗氧化的能力。Beneficial effects: the device provided by the utility model utilizes the principle that the chemical reaction rate doubles when the temperature rises by 10°C, greatly increases the reaction temperature and rate, and reduces the test time, so that the anti-oxidation ability of the transformer oil can be quickly judged.
附图说明Description of drawings
附图用来提供对本实用新型的进一步理解,并且构成说明书的一部分,与本实用新型的实施例一起用于解释本实用新型,并不构成对本实用新型的限制。在附图中:The accompanying drawings are used to provide a further understanding of the utility model, and constitute a part of the description, and are used to explain the utility model together with the embodiments of the utility model, and do not constitute a limitation to the utility model. In the attached picture:
图1是本实用新型的结构示意图;Fig. 1 is a structural representation of the utility model;
图2是本实用新型氧化试验杯的结构示意图。Fig. 2 is a schematic structural view of the oxidation test cup of the present invention.
图中:1、带温控的线圈夹套加热装置;2、氧化试验杯;3、氧化试验杯盖;4、连接管;5、废气收集池;6、废气收集液;7、加热夹条;8、控温开关;9、温度显示屏。In the figure: 1. Coil jacket heating device with temperature control; 2. Oxidation test cup; 3. Oxidation test cup cover; 4. Connecting pipe; 5. Waste gas collection tank; 6. Waste gas collection liquid; 7. Heating clip ; 8. Temperature control switch; 9. Temperature display.
具体实施方式Detailed ways
以下结合附图对本实用新型的优选实施例进行说明,应当理解,此处所描述的优选实施例仅用于说明和解释本实用新型,并不用于限定本实用新型。The preferred embodiments of the present utility model are described below in conjunction with the accompanying drawings. It should be understood that the preferred embodiments described here are only used to illustrate and explain the present utility model, and are not intended to limit the present utility model.
如图1~2所示,一种用于变压器油快速氧化测试的氧化器装置,其包括氧化试验杯2、设置在所述氧化试验杯2上起密封作用的氧化试验杯盖3、以及废气收集池5;所述氧化试验杯2和所述废气收集池5之间通过连接管4连通;所述废气收集池5内设置有废气收集液6;所述氧化试验杯2上设置有加热装置。所述氧化试验杯2及所述氧化试验杯盖3之间采用螺纹连接。所述加热装置为带温控的线圈夹套加热装置1;所述带温控的线圈夹套加热装置1包括加热夹条7、控温开关8和温度显示屏9。加热夹条7用于加热,控温开关8用于控制加热装置的电源,温度显示屏用9于显示温度。加热装置采用普通电源供电。所述废气收集池5内设置的废气收集液6为0.5mol/L的氢氧化钠-乙醇溶液。As shown in Figures 1 to 2, an oxidizer device for rapid oxidation testing of transformer oil includes an oxidation test cup 2, an oxidation test cup cover 3 arranged on the oxidation test cup 2 for sealing, and exhaust gas A collection pool 5; the oxidation test cup 2 and the waste gas collection pool 5 are communicated through a connecting pipe 4; the waste gas collection pool 5 is provided with a waste gas collection liquid 6; the oxidation test cup 2 is provided with a heating device . The oxidation test cup 2 and the oxidation test cup cover 3 are connected by threads. The heating device is a coil jacket heating device 1 with temperature control; the coil jacket heating device 1 with temperature control includes a heating clip 7 , a temperature control switch 8 and a temperature display screen 9 . The heating clip 7 is used for heating, the temperature control switch 8 is used for controlling the power supply of the heating device, and the temperature display screen is used for displaying the temperature. The heating device is powered by common power supply. The waste gas collection liquid 6 provided in the waste gas collection tank 5 is a 0.5 mol/L sodium hydroxide-ethanol solution.
工作时:所述加热装置,对加入到氧化试验杯中的变压器油升温,并将温度控制在150℃。通过所述连接管收集氧化测试过程中裂解反应产生的废气。所述的废气收集池采用的收集液为0.5mol/L的氢氧化钠-乙醇溶液。所述氢氧化钠-乙醇溶液不但可以收集中和酸性气体,而且可以通过计算所述氢氧化钠-乙醇溶液消耗量计算氧化过程中产生的酸性气体含量。When working: the heating device heats up the transformer oil added to the oxidation test cup, and controls the temperature at 150°C. The exhaust gas produced by the cracking reaction during the oxidation test is collected through the connecting pipe. The collection liquid used in the waste gas collection pool is 0.5 mol/L sodium hydroxide-ethanol solution. The sodium hydroxide-ethanol solution can not only collect and neutralize the acid gas, but also can calculate the acid gas content generated in the oxidation process by calculating the consumption of the sodium hydroxide-ethanol solution.
本实用新型提供的装置,利用温度升高10℃,化学反应速率增加一倍的原理,大幅度提高反应温度以及速率,降低试验时间,从而能够快速判别变压器油抗氧化的能力。The device provided by the utility model uses the principle that the chemical reaction rate doubles when the temperature rises by 10°C, greatly increases the reaction temperature and rate, and reduces the test time, so that the anti-oxidation ability of the transformer oil can be quickly judged.
最后应说明的是:以上所述仅为本实用新型的优选实施例而已,并不用于限制本实用新型,尽管参照前述实施例对本实用新型进行了详细的说明,对于本领域的技术人员来说,其依然可以对前述各实施例所记载的技术方案进行修改,或者对其中部分技术特征进行等同替换。凡在本实用新型的精神和原则之内,所作的任何修改、等同替换、改进等,均应包含在本实用新型的保护范围之内。Finally, it should be noted that: the above is only a preferred embodiment of the utility model, and is not intended to limit the utility model, although the utility model has been described in detail with reference to the foregoing embodiments, for those skilled in the art , it is still possible to modify the technical solutions described in the foregoing embodiments, or perform equivalent replacements for some of the technical features. Any modification, equivalent replacement, improvement, etc. made within the spirit and principles of the present utility model shall be included in the protection scope of the present utility model.
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Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN111610316A (en) * | 2020-04-16 | 2020-09-01 | 浙江中博润滑油有限公司 | High-concentration transformer oil purity detection method |
CN112649593A (en) * | 2020-11-23 | 2021-04-13 | 西安热工研究院有限公司 | Method for detecting oxidation stability of phosphate fire-resistant oil |
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2018
- 2018-12-25 CN CN201822189583.3U patent/CN209656525U/en not_active Expired - Fee Related
Cited By (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN111610316A (en) * | 2020-04-16 | 2020-09-01 | 浙江中博润滑油有限公司 | High-concentration transformer oil purity detection method |
CN112649593A (en) * | 2020-11-23 | 2021-04-13 | 西安热工研究院有限公司 | Method for detecting oxidation stability of phosphate fire-resistant oil |
WO2022105353A1 (en) * | 2020-11-23 | 2022-05-27 | 西安热工研究院有限公司 | Method for determing oxidation stability of phosphate fire-resistant oil |
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