CN208111390U - Ion source with novel temperature control function - Google Patents
Ion source with novel temperature control function Download PDFInfo
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- CN208111390U CN208111390U CN201721923401.XU CN201721923401U CN208111390U CN 208111390 U CN208111390 U CN 208111390U CN 201721923401 U CN201721923401 U CN 201721923401U CN 208111390 U CN208111390 U CN 208111390U
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- NJPPVKZQTLUDBO-UHFFFAOYSA-N novaluron Chemical compound C1=C(Cl)C(OC(F)(F)C(OC(F)(F)F)F)=CC=C1NC(=O)NC(=O)C1=C(F)C=CC=C1F NJPPVKZQTLUDBO-UHFFFAOYSA-N 0.000 claims 4
- 238000010438 heat treatment Methods 0.000 claims 3
- 230000008878 coupling Effects 0.000 claims 2
- 238000010168 coupling process Methods 0.000 claims 2
- 238000005859 coupling reaction Methods 0.000 claims 2
- 239000000919 ceramic Substances 0.000 claims 1
- PCHJSUWPFVWCPO-UHFFFAOYSA-N gold Chemical group [Au] PCHJSUWPFVWCPO-UHFFFAOYSA-N 0.000 claims 1
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Abstract
Description
技术领域technical field
本实用新型涉及离子源,特别涉及具有新型控温功能的离子源。The utility model relates to an ion source, in particular to an ion source with a novel temperature control function.
背景技术Background technique
在敞开式离子源工作过程中,当高温样品离子化时,要对放电气体在密封、无电子干扰的环境下进行升温,增加气体的离子速强度与离子束能量,有助于样品的离子化。当较低离子化温度样品分析时,需要离子源在密封环境下快速的降温,达到预期的温度范围。因此,快速实现离子源的升降温控制有利于试验的有序、合理化进行。During the working process of the open ion source, when the high-temperature sample is ionized, the temperature of the discharge gas should be raised in a sealed environment without electronic interference to increase the ion velocity intensity and ion beam energy of the gas, which is conducive to the ionization of the sample. . When analyzing samples with a lower ionization temperature, the ion source needs to be cooled rapidly in a sealed environment to reach the expected temperature range. Therefore, the rapid realization of the temperature control of the ion source is conducive to the orderly and rational conduct of the experiment.
目前的敞开式离子源技术主要有以下不足:离子源热传递加热技术,能够较快的实现等径空间的加热,由于采用中空过气、外部密封的方式,导致热损耗大、利用率不高,当需要快速降温时,降温时间太长,使得实验等待时间过长;离子源风扇降温技术,由于离子源的放电特性,在良好保温装置外放置风扇,对于高温短时间内有效,但是在中等温度段效果不明显,降温时间较缓慢,导致无法满足快速升降温技术要求。The current open ion source technology mainly has the following deficiencies: the ion source heat transfer heating technology can quickly realize the heating of the equal-diameter space, and due to the use of hollow air and external sealing, the heat loss is large and the utilization rate is not high. , when rapid cooling is required, the cooling time is too long, which makes the waiting time of the experiment too long; the ion source fan cooling technology, due to the discharge characteristics of the ion source, placing a fan outside the good heat preservation device is effective for high temperature in a short time, but in the medium The effect of the temperature section is not obvious, and the cooling time is slow, which makes it impossible to meet the technical requirements for rapid heating and cooling.
实用新型内容Utility model content
为解决上述现有技术方案中的不足,本实用新型提供了一种结构简单、升温快速、降温快速的具有新型控温功能的离子源。In order to solve the shortcomings in the above-mentioned existing technical solutions, the utility model provides an ion source with a new temperature control function, which has a simple structure, rapid temperature rise and rapid temperature drop.
本实用新型的目的是通过以下技术方案实现的:The purpose of this utility model is achieved by the following technical solutions:
一种具有新型控温功能的离子源,所述离子源包括高压电极;所述具有新型控温功能的离子源进一步包括:An ion source with a novel temperature control function, the ion source includes a high-voltage electrode; the ion source with a novel temperature control function further includes:
气体管道,所述气体管道具有依次排列的内径较大段、过渡段和内径较小段,所述内径较大段的一端固定在所述第一承载件上;所述高压电极设置在所述内径较小段的远离所述内径较大段的一侧;A gas pipeline, the gas pipeline has a section with a larger inner diameter, a transition section, and a section with a smaller inner diameter arranged in sequence, one end of the section with a larger inner diameter is fixed on the first carrier; the high-voltage electrode is arranged on the the side of the smaller inner diameter section away from the larger inner diameter section;
加热件,所述加热件设置在所述内径较小段内;a heating element, the heating element is arranged in the section with a smaller inner diameter;
测温部件,所述测温部件检测所述内径较小段内气体的温度;a temperature measuring component, the temperature measuring component detects the temperature of the gas in the section with a smaller inner diameter;
输送单元,所述输送单元将气体输送到所述过渡段和内径较小段的连接处的外侧。A delivery unit that delivers gas to the outside of the junction of the transition section and the smaller inner diameter section.
与现有技术相比,本实用新型具有的有益效果为:Compared with the prior art, the utility model has the beneficial effects of:
1.离子源加热更快,升温温控更准。1. The ion source heats up faster, and the temperature control is more accurate.
2.离子源降温更快,更直接。2. The cooling of the ion source is faster and more direct.
3.结构简单、紧凑。3. Simple and compact structure.
4.形成的离子束更稳定。。4. The formed ion beam is more stable. .
附图说明Description of drawings
参照附图,本实用新型的公开内容将变得更易理解。本领域技术人员容易理解的是:这些附图仅仅用于举例说明本实用新型的技术方案,而并非意在对本实用新型的保护范围构成限制。图中:With reference to the accompanying drawings, the disclosure of the present utility model will become easier to understand. Those skilled in the art can easily understand that: these drawings are only used to illustrate the technical solution of the utility model, and are not intended to limit the protection scope of the utility model. In the picture:
图1是根据本实用新型实施例1的具有新型控温功能的离子源的结构简图。Fig. 1 is a schematic structural diagram of an ion source with a novel temperature control function according to Embodiment 1 of the present utility model.
具体实施方式Detailed ways
图1和以下说明描述了本实用新型的可选实施方式以教导本领域技术人员如何实施和再现本实用新型。为了教导本实用新型技术方案,已简化或省略了一些常规方面。本领域技术人员应该理解源自这些实施方式的变型或替换将在本实用新型的范围内。本领域技术人员应该理解下述特征能够以各种方式组合以形成本实用新型的多个变型。由此,本实用新型并不局限于下述可选实施方式,而仅由权利要求和它们的等同物限定。Figure 1 and the following description describe an alternative embodiment of the invention to teach those skilled in the art how to implement and reproduce the invention. In order to teach the technical solution of the utility model, some conventional aspects have been simplified or omitted. Those skilled in the art should understand that modifications or replacements from these embodiments will fall within the scope of the present invention. Those skilled in the art should understand that the following features can be combined in various ways to form multiple variations of the present invention. Accordingly, the present invention is not limited to the alternative embodiments described below, but only by the claims and their equivalents.
实施例1:Example 1:
图1示意性地给出了本实用新型实施例的具有新型控温功能的离子源的结构简图,如图1所示,所述具有新型控温功能的离子源包括:Fig. 1 schematically provides a structural diagram of an ion source with a novel temperature control function according to an embodiment of the present invention. As shown in Fig. 1, the ion source with a novel temperature control function includes:
气体管道,所述气体管道具有依次排列的内径较大段21、过渡段22和内径较小段23,所述内径较大段的一端固定在所述第一承载件上;A gas pipeline, the gas pipeline has a section 21 with a larger inner diameter, a transition section 22 and a section 23 with a smaller inner diameter arranged in sequence, and one end of the section with a larger inner diameter is fixed on the first bearing member;
第一部分,所述第一部分包括所述内径较大段和过渡段;a first section, the first section including the larger inner diameter section and a transition section;
第二部分,所述第二部分包括所述内径较小段;所述第一部分的导热率大于所述第二部分,如第一部分采用金属,第二部分采用陶瓷;The second part, the second part includes the section with a smaller inner diameter; the thermal conductivity of the first part is greater than that of the second part, for example, the first part is made of metal, and the second part is made of ceramics;
连接部分24,所述连接部分连接所述第一部分和第二部分;a connecting portion 24 connecting the first and second portions;
加热件,所述加热件设置在所述内径较小段内,所述加热件包括:A heating element, the heating element is arranged in the section with a smaller inner diameter, and the heating element includes:
基座31,所述基座处于所述气体管道内,且一端固定在所述第一承载件上,另一端伸入到所述内径较小段内;A base 31, the base is located in the gas pipeline, and one end is fixed on the first carrier, and the other end extends into the section with a smaller inner diameter;
加热丝32,所述加热丝绕在处于所述内径较小段内的基座上;heating wire 32, said heating wire is wound on the base in said smaller inner diameter section;
测温部件41,如热电偶,所述测温部件检测所述内径较小段内气体的温度;A temperature measuring component 41, such as a thermocouple, which detects the temperature of the gas in the section with a smaller inner diameter;
输送单元71,如抽气泵,所述输送单元将气体输送到所述过渡段和内径较小段的连接处的外侧。The conveying unit 71, such as an air suction pump, conveys gas to the outside of the connection between the transition section and the section with a smaller inner diameter.
第一承载件11,所述第一承载件的且内径较大段在所述第一承载件上的投影区域内具有第一通孔,以便气体穿过第一承载体进入气体管道内;The first carrier 11, the section of the first carrier with a larger inner diameter has a first through hole in the projection area on the first carrier, so that the gas passes through the first carrier and enters the gas pipeline;
第二承载件12,所述内径较小段的远离所述内径较大段的一端固定在所述第二承载件上,所述第二承载件的且内径较小段在所述第二承载件上的投影区域内具有第二通孔13;在气体流动方向(气体从所述第一通孔进入气体管道内,并从第二通孔排出)上,所述第二通孔的孔径逐渐变小;The second carrier 12, one end of the smaller section of the inner diameter away from the larger section of the inner diameter is fixed on the second carrier, and the smaller section of the second carrier is on the second carrier There is a second through hole 13 in the projection area on the part; in the gas flow direction (gas enters the gas pipeline from the first through hole and is discharged from the second through hole), the aperture of the second through hole gradually become smaller;
底座81,所述第一承载件和第二承载件固定在所述底座上;A base 81, on which the first carrier and the second carrier are fixed;
介质管61,所述介质管固定在所述第二承载件上,从第二通孔排出的气体进入所述介质管内;a medium pipe 61, the medium pipe is fixed on the second carrier, and the gas discharged from the second through hole enters the medium pipe;
高压电极51,所述高压电极设置在所述介质管的外侧。A high-voltage electrode 51, the high-voltage electrode is arranged on the outside of the medium pipe.
本实用新型实施例的根据上述具有新型控温功能的离子源的工作过程:According to the working process of the above-mentioned ion source with novel temperature control function according to the embodiment of the utility model:
关闭输送单元,气体穿过所述第一通孔进入到气体管道的内径较大段内;Closing the delivery unit, the gas enters the larger inner diameter section of the gas pipeline through the first through hole;
气体进入过渡段内,气体的流速和密度得到提高;When the gas enters the transition section, the flow rate and density of the gas are increased;
气体进入内径较小段内,并被加热;The gas enters the section with smaller inner diameter and is heated;
根据测温部件输出的温度、温度设定值去调整加热功率;Adjust the heating power according to the temperature output by the temperature measuring component and the temperature setting value;
高压电极放电,使得流出内径较小段的气体被电离,形成离子束;The high-voltage electrode is discharged, so that the gas flowing out of the smaller inner diameter section is ionized to form an ion beam;
关闭加热件,并打开输送单元,外界空气吹扫所述连接处,并带走热量;内径较小段的热量向所述过渡段传导;Turn off the heating element and turn on the conveying unit, the outside air blows the connection and takes away the heat; the heat from the section with a smaller inner diameter is conducted to the transition section;
冷却气体进入到内径较大段内;The cooling gas enters into the larger inner diameter section;
冷却气体进入过渡段内,气体的流速和密度得到提高;The cooling gas enters the transition section, and the flow rate and density of the gas are increased;
冷却气体流出内径较小段,并带走热量。Cooling gas exits the smaller ID section and carries away heat.
实施例2:Example 2:
本实用新型实施例1所述的具有新型控温功能的离子源的应用例。An application example of the ion source with the novel temperature control function described in Embodiment 1 of the present utility model.
在该应用例中,第一部分采用不锈钢或可伐合金;所述过渡段形成的锥体角度为30-60°;第二通孔形成的锥体的角度为30-60°;测温部件采用热电偶、热敏电阻或铂电阻(RTD);冷却气体使用氮气或氩气或空气或氦气;输送单元采用抽气泵,把气体输送到所述过渡段和内径较小段的连接处的外侧,从而带走热量;同时内径较小段的热量向所述过渡段传导。In this application example, the first part is made of stainless steel or Kovar alloy; the angle of the cone formed by the transition section is 30-60°; the angle of the cone formed by the second through hole is 30-60°; the temperature measuring part adopts Thermocouple, thermistor or platinum resistance (RTD); the cooling gas uses nitrogen or argon or air or helium; the delivery unit uses an air pump to deliver the gas to the outside of the connection between the transition section and the inner diameter section , so as to take away heat; at the same time, the heat of the smaller inner diameter section is conducted to the transition section.
Claims (8)
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Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
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CN108428607A (en) * | 2017-12-31 | 2018-08-21 | 宁波大学 | Ion source with temperature controlling function and its working method |
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Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
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CN108428607A (en) * | 2017-12-31 | 2018-08-21 | 宁波大学 | Ion source with temperature controlling function and its working method |
CN108428607B (en) * | 2017-12-31 | 2025-02-25 | 宁波大学 | Ion source with temperature control function and working method thereof |
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