CN207675268U - One kind reacting automatic level meter for titanium sponge reduction - Google Patents
One kind reacting automatic level meter for titanium sponge reduction Download PDFInfo
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- CN207675268U CN207675268U CN201820108521.2U CN201820108521U CN207675268U CN 207675268 U CN207675268 U CN 207675268U CN 201820108521 U CN201820108521 U CN 201820108521U CN 207675268 U CN207675268 U CN 207675268U
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- liquid level
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- titanium sponge
- level meter
- sieve plate
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Abstract
The utility model discloses one kind reacting automatic level meter for titanium sponge reduction; including high temperature resistant laser liquid-level measuring device, reactor and liquid level tube; the reactor is internally provided with sieve plate; and the side at the top of sieve plate is fixedly connected with fixed ring; the internal activity of the fixed ring is connected with protection sleeve pipe; the top movable of the reactor is connected with big lid, and the top covered greatly is provided with flange, and the utility model is related to non-ferrous metallurgy technical field of production of sponge titanium.This is used for titanium sponge reduction reaction automatic level meter, the liquid level for inside reactor in reduction process may be implemented more accurately to be measured, mitigate labor intensity, improve the safety of production operation, the liquid level during reduction can be made to ensure in processing range simultaneously, reduce previous titanium tetrachloride to be added and excessive liquid fluctuating caused by when magnesium chloride discharge, improves titanium and stick together appearance, ensure the stabilization of product quality.
Description
Technical field
The utility model is related to non-ferrous metallurgy technical field of production of sponge titanium, specially a kind of to be used for titanium sponge reduction
React automatic level meter.
Background technology
Reduction process is the important stage of Kroll process production titanium sponge, and Liquid level is shadow again in reactor during reduction
The principal element for ringing entire reduction process, during reduction in reactor liquid level it is too high or too low product quality can all be caused it is serious
It influences, the ensuring method of liquid level is that theoretical calculation goes out each addition tetrachloro of reduction phase first in previous reduction process
Change titanium amount and discharge chlorination magnesium amount, the titanium tetrachloride amount being added every time carries out volume conversion meter by head tank float level meter
Amount, but titanium tetrachloride density is affected by ambient temperature, is finally made the titanium tetrachloride amount of addition not accurate enough, is discharged every time
Chlorination magnesium amount is to be measured by the iron ware with scale, but the container high temperature deformation after use for several times is serious, makes row
High-volume also not accurate enough, the addition of titanium tetrachloride and the discharge capacity of magnesium chloride all inaccuracy make in reduction process in reactor
Level fluctuation is very big, and liquid level affects extra large in reduction process often not within the scope of technological requirement in reactor in practical operation
The generating structure that continuous titanium sticks together, the titanium black powder amount in upper cap position that sticks together increase, and product recovery rate and rate of grade is made to be substantially reduced.
Reactor is sealing in process of production, and reactor temperature is at 800 DEG C or more, it is difficult to direct with conventional equipment
Liquid level in reactor is measured, sometimes in order to measure the position of liquid level in reactor in production process, through frequently with by one
Round steel makes measurement Liquid level scale, opens big upper part of the cover and reserves flange, scale is inserted into from flange, after the waiting several seconds quickly
Scale is taken out, causes scale to burn red degree difference with on-liquid space temperature difference using liquid in reactor and carries out level gauging.
Occurs abnormal detonation in measurement process, liquid magnesium splashes, scald operative employee.
Utility model content
In view of the deficiencies of the prior art, the utility model provides a kind of for titanium sponge reduction reaction solution position automatic measuring
Device, solve in nowadays reduction process can not in precision real time measuring reactor liquid level height, can not be each tetrachloro
The discharge capacity of the addition and magnesium chloride of changing titanium provides foundation, can not ensure to restore liquid level within the scope of technological requirement, to entire
The generating structure that reduction process and titanium sponge stick together causes deleterious effect, increases the stick together black powder amount at upper cap position of titanium and asks
Topic.
In order to achieve the above object, the utility model is achieved by the following technical programs：One kind being used for titanium sponge reduction
React automatic level meter, including high temperature resistant laser liquid-level measuring device, reactor and liquid level tube, the inside of the reactor
It is provided with sieve plate, and the side at the top of sieve plate is fixedly connected with fixed ring, the internal activity of the fixed ring is connected with protection
The top movable of casing, the reactor is connected with big lid, and the top covered greatly is provided with flange.
Preferably, through-hole is offered at the top of the big lid, and is provided with water earthen bowl at the top of flange.
Preferably, the liquid level tube runs through through-hole and extends to the bottom of through-hole, and the liquid level tube extends to via bottoms
One end and flange at the top of be fixedly connected.
Preferably, gas balance hole is offered at the top of the liquid level tube.
Preferably, the outer surface of the flange is connected with seal gasket, and the internal activity connection of seal gasket
There is temperature tube.
Preferably, the inside of the sieve plate offers sieve plate hole.
Advantageous effect
The utility model provides a kind of for titanium sponge reduction reaction automatic level meter.Have following beneficial to effect
Fruit：
（1）, this be used for titanium sponge reduction reaction automatic level meter, sieve plate is internally provided with by reactor,
And the side at the top of sieve plate is fixedly connected with fixed ring, and the internal activity of fixed ring is connected with protection sleeve pipe, the top of reactor
Portion is connected with big lid, and the top covered greatly is provided with flange, then is swashed by gas balance hole, seal gasket, high temperature resistant
Light fluid level measuring instrument, liquid level tube, through-hole and sieve plate hole are equipped with, and may be implemented for inside reactor liquid level more accurately
It measures, mitigates labor intensity, improve the safety of production operation, while the liquid level during reduction can be made to ensure in technique model
In enclosing, reduce previous titanium tetrachloride and be added and excessive liquid fluctuating caused by when magnesium chloride discharge, improves titanium and stick together appearance, protect
Demonstrate,prove the stabilization of product quality.
（2）, this be used for titanium sponge reduction reaction automatic level meter, be connected with greatly by the top movable of reactor
Lid, and the top covered greatly is provided with flange, and water earthen bowl is provided at the top of flange, can be in the built-in full water of water earthen bowl
It prevents seal gasket to be reduced the amount of heat damage generated in the process, extends its service life.
Description of the drawings
FIG. 1 is a schematic structural view of the utility model；
Fig. 2 is the partial enlarged view at A in the utility model Fig. 1.
In figure：It is 1 sieve plate, 2 fixed rings, 3 protection sleeve pipes, 4 gas balance holes, 5 seal gaskets, 6 flanges, 7 water earthen bowls, 8 resistance to
High-temperature laser fluid level measuring instrument, 9 liquid level tubes, 10 through-holes, 11 big lid, 12 reactors, 13 sieve plate holes.
Specific implementation mode
The following will be combined with the drawings in the embodiments of the present invention, carries out the technical scheme in the embodiment of the utility model
Clearly and completely describe, it is clear that the described embodiments are only a part of the embodiments of the utility model, rather than whole
Embodiment.Based on the embodiments of the present invention, those of ordinary skill in the art are without making creative work
The every other embodiment obtained, shall fall within the protection scope of the present invention.
- 2 are please referred to Fig.1, the utility model provides a kind of technical solution：One kind is automatic for titanium sponge reduction reaction liquid level
Measuring device, including high temperature resistant laser liquid-level measuring device 8, reactor 12 and liquid level tube 9, the top of liquid level tube 9 offer gas
Balance hole 4, gas balance hole 4 can make the liquid level in reactor 12 identical with the liquid height in liquid level tube 9, liquid level tube
9 run through through-hole 10 and extend to the bottom of through-hole 10, and liquid level tube 9 extends to one end of 10 bottom of through-hole and consolidates with the top of flange 6
Fixed connection, reactor 12 are internally provided with sieve plate 1, and the inside of sieve plate 1 offers sieve plate hole 13, and the one of 1 top of sieve plate
Side is fixedly connected with fixed ring 2, and the internal activity of fixed ring 2 is connected with protection sleeve pipe 3, and protection sleeve pipe 3 and liquid level tube 9 use titanium
Alloy material makes, and the top movable of reactor 12 is connected with big lid 11, and the top of big lid 11 offers through-hole 10, and flange
6 top is provided with water earthen bowl 7,7 built-in full water of water earthen bowl, can prevent seal gasket 5 be reduced generate in the process it is a large amount of
Heat damages, and the top of big lid 11 is provided with flange 6, and the outer surface of flange 6 is connected with seal gasket 5, and close
The inside of potting pad 5 is flexibly connected with the outer surface of liquid level tube 9.
In use, the fixed ring 2 of fixed protection sleeve pipe 3 is welded on sieve plate 1 during preparing shove charge, by protective case
Pipe 3 is inserted into fixed ring 2, and such protection sleeve pipe 3 and sieve plate 1 are bonded, and liquid level tube 9 passes through the through-hole 10 on big lid 11
It is fixed with 6 phase of flange on big lid 11, liquid level tube 9 is sealed with the seal gasket 5 of flange 6, and solid raw material magnesium ingot is packed into reaction
After device 12, big lid 11 is sling with overhead traveling crane, so that liquid level tube 9 is slowly inserted into protection sleeve pipe 3, and big lid 11 is covered, each component
After installation bolt and fastening, reactor 12 is hung in electric furnace, reactor 12 is evacuated and heated, is produced in reduction process
Raw amount of heat, to prevent seal gasket 5 from being damaged by high temperature, the 7 built-in full water of water earthen bowl on 6 top of flange, in reduction process
In, the liquid in reactor 12 flows into 1 lower part of sieve plate by the sieve plate hole 13 on sieve plate 1 and enters in liquid level tube 9, due to
9 top of liquid level tube is equipped with gas balance hole 4, in the liquid level and liquid level tube 9 in reduction process entire in this way in reactor 12
Liquid height it is identical, high temperature resistant laser liquid-level measuring device 8 is connected with liquid level tube 9, and high temperature resistant laser liquid-level measuring device 8 is sent out
Measuring signal, measuring signal is back to high temperature resistant laser liquid-level measuring device 8 after being contacted with the liquid level in liquid level tube 9, and passes through number
According to display is transmitted to, this completes the courses of work for titanium sponge reduction reaction automatic level meter.
It should be noted that herein, relational terms such as first and second and the like are used merely to a reality
Body or operation are distinguished with another entity or operation, are deposited without necessarily requiring or implying between these entities or operation
In any actual relationship or order or sequence.Moreover, the terms "include", "comprise" or its any other variant are intended to
Non-exclusive inclusion, so that the process, method, article or equipment including a series of elements is not only wanted including those
Element, but also include other elements that are not explicitly listed, or further include for this process, method, article or equipment
Intrinsic element.
While there has been shown and described that the embodiments of the present invention, for the ordinary skill in the art,
It is appreciated that can these embodiments be carried out with a variety of variations in the case where not departing from the principles of the present invention and spirit, repaiied
Change, replace and modification, the scope of the utility model are defined by the appended claims and the equivalents thereof.
Claims (6)
1. one kind reacting automatic level meter, including high temperature resistant laser liquid-level measuring device for titanium sponge reduction（8）, reaction
Device（12）And liquid level tube（9）, it is characterised in that：The reactor（12）Be internally provided with sieve plate（1）, and sieve plate（1）Top
The side in portion is fixedly connected with fixed ring（2）, the fixed ring（2）Internal activity be connected with protection sleeve pipe（3）, the reaction
Device（12）Top movable be connected with big lid（11）, and cover greatly（11）Top be provided with flange（6）.
2. according to claim 1 a kind of for titanium sponge reduction reaction automatic level meter, it is characterised in that：Institute
State big lid（11）Top offer through-hole（10）, and flange（6）Top be provided with water earthen bowl（7）.
3. according to claim 1 a kind of for titanium sponge reduction reaction automatic level meter, it is characterised in that：Institute
State liquid level tube（9）Through through-hole（10）And extend to through-hole（10）Bottom, the liquid level tube（9）Extend to through-hole（10）Bottom
One end and flange（6）Top be fixedly connected.
4. according to claim 1 a kind of for titanium sponge reduction reaction automatic level meter, it is characterised in that：Institute
State liquid level tube（9）Top offer gas balance hole（4）.
5. according to claim 1 a kind of for titanium sponge reduction reaction automatic level meter, it is characterised in that：Institute
State flange（6）Outer surface be connected with seal gasket（5）, and seal gasket（5）Inside and liquid level tube（9）Appearance
Face is flexibly connected.
6. according to claim 1 a kind of for titanium sponge reduction reaction automatic level meter, it is characterised in that：Institute
State sieve plate（1）Inside offer sieve plate hole（13）.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201820108521.2U CN207675268U (en) | 2018-01-23 | 2018-01-23 | One kind reacting automatic level meter for titanium sponge reduction |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201820108521.2U CN207675268U (en) | 2018-01-23 | 2018-01-23 | One kind reacting automatic level meter for titanium sponge reduction |
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| Publication Number | Publication Date |
|---|---|
| CN207675268U true CN207675268U (en) | 2018-07-31 |
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| Application Number | Title | Priority Date | Filing Date |
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| CN201820108521.2U Active CN207675268U (en) | 2018-01-23 | 2018-01-23 | One kind reacting automatic level meter for titanium sponge reduction |
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Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109238402A (en) * | 2018-10-22 | 2019-01-18 | 洛阳双瑞万基钛业有限公司 | A kind of device measuring titanium sponge high temperature liquid level in closed container |
| CN113175973A (en) * | 2021-03-17 | 2021-07-27 | 洛阳双瑞万基钛业有限公司 | Liquid level measuring device and liquid level fluctuation measuring method for titanium sponge production |
| CN113268093A (en) * | 2021-06-23 | 2021-08-17 | 朝阳金达钛业股份有限公司 | Automatic titanium tetrachloride supplementing device used in titanium sponge production process |
| CN114152581A (en) * | 2021-12-03 | 2022-03-08 | 攀钢集团攀枝花钛材有限公司 | Method for rapidly judging quality abnormality of low-valence titanium ore slurry |
| WO2024098702A1 (en) * | 2022-11-10 | 2024-05-16 | 攀钢集团攀枝花钢铁研究院有限公司 | Process parameter accurate control system for titanium sponge reduction process, and control method |
-
2018
- 2018-01-23 CN CN201820108521.2U patent/CN207675268U/en active Active
Cited By (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109238402A (en) * | 2018-10-22 | 2019-01-18 | 洛阳双瑞万基钛业有限公司 | A kind of device measuring titanium sponge high temperature liquid level in closed container |
| CN109238402B (en) * | 2018-10-22 | 2024-03-01 | 洛阳双瑞万基钛业有限公司 | Device for measuring titanium sponge height Wen Yemian in closed container |
| CN113175973A (en) * | 2021-03-17 | 2021-07-27 | 洛阳双瑞万基钛业有限公司 | Liquid level measuring device and liquid level fluctuation measuring method for titanium sponge production |
| CN113268093A (en) * | 2021-06-23 | 2021-08-17 | 朝阳金达钛业股份有限公司 | Automatic titanium tetrachloride supplementing device used in titanium sponge production process |
| CN114152581A (en) * | 2021-12-03 | 2022-03-08 | 攀钢集团攀枝花钛材有限公司 | Method for rapidly judging quality abnormality of low-valence titanium ore slurry |
| CN114152581B (en) * | 2021-12-03 | 2024-03-22 | 攀钢集团攀枝花钛材有限公司 | Method for rapidly judging quality abnormality of low-valence titanium ore slurry |
| WO2024098702A1 (en) * | 2022-11-10 | 2024-05-16 | 攀钢集团攀枝花钢铁研究院有限公司 | Process parameter accurate control system for titanium sponge reduction process, and control method |
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