[go: up one dir, main page]

CN206848141U - A kind of electrochemical corrosion test device - Google Patents

A kind of electrochemical corrosion test device Download PDF

Info

Publication number
CN206848141U
CN206848141U CN201720769609.4U CN201720769609U CN206848141U CN 206848141 U CN206848141 U CN 206848141U CN 201720769609 U CN201720769609 U CN 201720769609U CN 206848141 U CN206848141 U CN 206848141U
Authority
CN
China
Prior art keywords
sample
reaction chamber
reative cell
plate
electrochemical corrosion
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
CN201720769609.4U
Other languages
Chinese (zh)
Inventor
张红红
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Binzhou University
Original Assignee
Binzhou University
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Binzhou University filed Critical Binzhou University
Priority to CN201720769609.4U priority Critical patent/CN206848141U/en
Application granted granted Critical
Publication of CN206848141U publication Critical patent/CN206848141U/en
Expired - Fee Related legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Landscapes

  • Testing Resistance To Weather, Investigating Materials By Mechanical Methods (AREA)

Abstract

本实用新型公开了一种电化学腐蚀试验装置,它涉及电化学腐蚀技术领域,第一反应室、第二反应室和第三反应室前侧均设置有计时器和透明观察板,所述第一反应室、第二反应室和第三反应室之间均通过隔离板隔离,且隔离板上设置有电解液通孔,所述第一反应室、第二反应室和第三反应室底部均设置有铂电极板。该装置设置有第一反应室、第二反应室和第三反应室,且第一反应室、第二反应室和第三反应室上端均设置有相对应的试样孔和试样套筒,可以固定不同材料的圆柱形试样,而且第一反应室、第二反应室和第三反应室前侧均设置有计时器,便于同时对多组圆柱形试样进行试验,而且每组圆柱形试样反应的时间和腐蚀深度均可进行较为准确的记录。

The utility model discloses an electrochemical corrosion test device, which relates to the technical field of electrochemical corrosion. The front sides of the first reaction chamber, the second reaction chamber and the third reaction chamber are all provided with a timer and a transparent observation plate. The first reaction chamber, the second reaction chamber and the third reaction chamber are all separated by an isolation plate, and electrolyte through holes are arranged on the isolation plate, and the bottoms of the first reaction chamber, the second reaction chamber and the third reaction chamber are all Platinum electrode plates are provided. The device is provided with a first reaction chamber, a second reaction chamber and a third reaction chamber, and the upper ends of the first reaction chamber, the second reaction chamber and the third reaction chamber are provided with corresponding sample holes and sample sleeves, Cylindrical samples of different materials can be fixed, and timers are set on the front side of the first reaction chamber, the second reaction chamber and the third reaction chamber, which is convenient for testing multiple groups of cylindrical samples at the same time, and each group of cylindrical The reaction time and corrosion depth of the sample can be recorded more accurately.

Description

一种电化学腐蚀试验装置An electrochemical corrosion test device

技术领域technical field

本实用新型涉及一种电化学腐蚀试验装置,属于电化学腐蚀技术领域。The utility model relates to an electrochemical corrosion test device, which belongs to the technical field of electrochemical corrosion.

背景技术Background technique

电化学腐蚀,指金属表面与离子导电的介质发生电化学反应而产生的破坏,在反应过程中有电流产生,如金属在海水、土壤及酸、碱、盐溶液中的腐蚀均属这一类,在金属研究中需要对金属进行电化学腐蚀试验,在电化学腐蚀的试验中,包括测试金属的极化曲线测试、阻抗测试和腐蚀面观察,是检测金属及涂层耐腐蚀性能的重要指标和手段,目前传统的电化学腐蚀试验过程过于复杂,在实验进行时需要在试样表面焊接铜丝用于导电,和电化学实验三电极体系中的工作电极相连接,其次还要在试样周围涂上密封胶,而且金属试样在腐蚀液中的裸露腐蚀面的高度不好控制,增大了电化学腐蚀试验的难度。Electrochemical corrosion refers to the damage caused by the electrochemical reaction between the metal surface and the ion-conducting medium. During the reaction, a current is generated, such as the corrosion of metals in seawater, soil, and acid, alkali, and salt solutions. , In the research of metals, it is necessary to conduct electrochemical corrosion tests on metals. In the electrochemical corrosion tests, including the polarization curve test, impedance test and corrosion surface observation of the test metal, it is an important indicator for detecting the corrosion resistance of metals and coatings. and means, the current traditional electrochemical corrosion test process is too complicated, it is necessary to weld copper wire on the surface of the sample for conduction, and to connect with the working electrode in the three-electrode system of the electrochemical experiment. Coating sealant around, and the height of the exposed corrosion surface of the metal sample in the corrosive solution is not easy to control, which increases the difficulty of the electrochemical corrosion test.

实用新型内容Utility model content

针对上述问题,本实用新型要解决的技术问题是提供一种电化学腐蚀试验装置。In view of the above problems, the technical problem to be solved by the utility model is to provide an electrochemical corrosion test device.

本实用新型的一种电化学腐蚀试验装置,它包含装置主体、试样支撑架、试样套筒、圆柱形试样、试样孔、试样记录牌、计时器、透明观察板、第一反应室、第二反应室、第三反应室、隔离板、电解液通孔和铂电极板,所述装置主体上侧设置有试样支撑架,试样支撑架上侧壁设置有多个试样套筒,试样套筒内设置有圆柱形试样,圆柱形试样下端设置有试样孔,且圆柱形试样下端位于试样孔内,所述试样孔位于装置主体上侧壁,所述试样孔前侧设置有试样记录牌,所述装置主体前侧壁设置有多个计时器,计时器下侧设置有透明观察板,所述装置主体内部设置有第一反应室、第二反应室和第三反应室,且第一反应室、第二反应室和第三反应室前侧均设置有计时器和透明观察板,所述第一反应室、第二反应室和第三反应室之间均通过隔离板隔离,且隔离板上设置有电解液通孔,所述第一反应室、第二反应室和第三反应室底部均设置有铂电极板。The utility model relates to an electrochemical corrosion test device, which includes a device main body, a sample support frame, a sample sleeve, a cylindrical sample, a sample hole, a sample record card, a timer, a transparent observation plate, a first Reaction chamber, second reaction chamber, third reaction chamber, isolation plate, electrolyte through hole and platinum electrode plate, the upper side of the main body of the device is provided with a sample support frame, and the upper side wall of the sample support frame is provided with a plurality of test pieces. A sample sleeve, a cylindrical sample is arranged in the sample sleeve, a sample hole is arranged at the lower end of the cylindrical sample, and the lower end of the cylindrical sample is located in the sample hole, and the sample hole is located on the upper side wall of the device main body , the front side of the sample hole is provided with a sample record board, the front side wall of the main body of the device is provided with a plurality of timers, the lower side of the timer is provided with a transparent observation plate, and the first reaction chamber is arranged inside the main body of the device , the second reaction chamber and the third reaction chamber, and the front side of the first reaction chamber, the second reaction chamber and the third reaction chamber are provided with a timer and a transparent observation plate, the first reaction chamber, the second reaction chamber and the The third reaction chambers are separated by isolation plates, and the isolation plates are provided with electrolyte through holes, and the bottoms of the first reaction chamber, the second reaction chamber and the third reaction chamber are all provided with platinum electrode plates.

作为优选,所述的试样支撑架后侧设置有刻度比对板,刻度比对板的设置可以便于各个圆柱形试样之间腐蚀深度的比对,使试验结果更具说服力。As a preference, a scale comparison plate is provided on the rear side of the sample support frame, and the setting of the scale comparison plate can facilitate the comparison of the corrosion depth between the cylindrical samples, making the test results more convincing.

作为优选,所述的试样套筒是由橡胶材料制成,橡胶材料制成的试样套筒弹性较好,且内壁的摩擦力更大,便于对圆柱形试样的固定和调节。Preferably, the sample sleeve is made of rubber material. The sample sleeve made of rubber material has better elasticity and greater friction on the inner wall, which is convenient for fixing and adjusting the cylindrical sample.

作为优选,所述的试样孔内侧设置有弹性垫圈,弹性垫圈的设置可以提高圆柱形试样和试样孔之间的密封性能。Preferably, an elastic washer is arranged inside the sample hole, and the arrangement of the elastic washer can improve the sealing performance between the cylindrical sample and the sample hole.

作为优选,所述的铂电极板下端设置有石墨棒,石墨棒的设置可以便于铂电极板的外接。Preferably, the lower end of the platinum electrode plate is provided with a graphite rod, and the arrangement of the graphite rod can facilitate the external connection of the platinum electrode plate.

本实用新型的有益效果:该装置设置有第一反应室、第二反应室和第三反应室,且第一反应室、第二反应室和第三反应室上端均设置有相对应的试样孔和试样套筒,可以固定不同材料的圆柱形试样,而且第一反应室、第二反应室和第三反应室前侧均设置有计时器,当反应室内的圆柱形试样进行电化学腐蚀反应时可以通过计时器来记录反应的时间,便于同时对多组圆柱形试样进行试验,而且每组圆柱形试样反应的时间和腐蚀深度均可进行较为准确的记录,使得试验结果更具说服力。Beneficial effects of the utility model: the device is provided with a first reaction chamber, a second reaction chamber and a third reaction chamber, and the upper ends of the first reaction chamber, the second reaction chamber and the third reaction chamber are all provided with corresponding samples Holes and sample sleeves can fix cylindrical samples of different materials, and there are timers on the front of the first reaction chamber, the second reaction chamber and the third reaction chamber, when the cylindrical samples in the reaction chamber are electrically charged During the chemical corrosion reaction, the timer can be used to record the reaction time, which is convenient for testing multiple groups of cylindrical samples at the same time, and the reaction time and corrosion depth of each group of cylindrical samples can be recorded more accurately, so that the test results more convincing.

附图说明Description of drawings

为了易于说明,本实用新型由下述的具体实施及附图作以详细描述。For ease of illustration, the utility model is described in detail by the following specific implementation and accompanying drawings.

图1为本实用新型的结构示意图;Fig. 1 is the structural representation of the utility model;

图2为本实用新型的装置主体内部结构示意图。Fig. 2 is a schematic diagram of the internal structure of the device main body of the present invention.

1-装置主体;2-试样支撑架;3-试样套筒;4-圆柱形试样;5-试样孔;6-试样记录牌;7-计时器;8-透明观察板;9-第一反应室;10-第二反应室;11-第三反应室;12-隔离板;13-电解液通孔;14-铂电极板。1-device main body; 2-sample support frame; 3-sample sleeve; 4-cylindrical sample; 5-sample hole; 6-sample record board; 7-timer; 8-transparent observation board; 9-first reaction chamber; 10-second reaction chamber; 11-third reaction chamber; 12-separation plate; 13-electrolyte through hole; 14-platinum electrode plate.

具体实施方式detailed description

现在结合附图对本实用新型作进一步详细的说明。这些附图均为简化的示意图,仅以示意方式说明本实用新型的基本结构,因此其仅显示与本实用新型有关的构成。Now in conjunction with accompanying drawing, the utility model is described in further detail. These drawings are all simplified schematic diagrams, and only schematically illustrate the basic structure of the utility model, so they only show the configurations related to the utility model.

如图1和图2所示,本具体实施方式采用以下技术方案:它包含装置主体1、试样支撑架2、试样套筒3、圆柱形试样4、试样孔5、试样记录牌6、计时器7、透明观察板8、第一反应室9、第二反应室10、第三反应室11、隔离板12、电解液通孔13和铂电极板14,所述装置主体1上侧设置有试样支撑架2,试样支撑架2上侧壁设置有多个试样套筒3,试样套筒3内设置有圆柱形试样4,圆柱形试样4下端设置有试样孔5,且圆柱形试样4下端位于试样孔5内,所述试样孔5位于装置主体1上侧壁,所述试样孔5前侧设置有试样记录牌6,所述装置主体1前侧壁设置有多个计时器7,计时器7下侧设置有透明观察板8,所述装置主体1内部设置有第一反应室9、第二反应室10和第三反应室11,且第一反应室9、第二反应室10和第三反应室11前侧均设置有计时器7和透明观察板8,所述第一反应室9、第二反应室10和第三反应室11之间均通过隔离板12隔离,且隔离板12上设置有电解液通孔13,所述第一反应室9、第二反应室10和第三反应室11底部均设置有铂电极板14。As shown in Figures 1 and 2, this specific embodiment adopts the following technical scheme: it includes a device main body 1, a sample support frame 2, a sample sleeve 3, a cylindrical sample 4, a sample hole 5, and a sample record Plate 6, timer 7, transparent observation plate 8, first reaction chamber 9, second reaction chamber 10, third reaction chamber 11, isolation plate 12, electrolyte through hole 13 and platinum electrode plate 14, said device main body 1 A sample support frame 2 is arranged on the upper side, and a plurality of sample sleeves 3 are arranged on the upper side wall of the sample support frame 2. A cylindrical sample 4 is arranged in the sample sleeve 3, and a cylindrical sample 4 is arranged at the lower end of the cylindrical sample 4. Sample hole 5, and the lower end of the cylindrical sample 4 is located in the sample hole 5, the sample hole 5 is located on the upper side wall of the device main body 1, and the front side of the sample hole 5 is provided with a sample record card 6, so The front side wall of the device main body 1 is provided with a plurality of timers 7, the lower side of the timer 7 is provided with a transparent observation plate 8, and the inside of the device main body 1 is provided with a first reaction chamber 9, a second reaction chamber 10 and a third reaction chamber. chamber 11, and the front side of the first reaction chamber 9, the second reaction chamber 10 and the third reaction chamber 11 are provided with a timer 7 and a transparent observation plate 8, the first reaction chamber 9, the second reaction chamber 10 and the first reaction chamber 10 The three reaction chambers 11 are all isolated by an isolation plate 12, and the isolation plate 12 is provided with an electrolyte through hole 13, and the bottoms of the first reaction chamber 9, the second reaction chamber 10 and the third reaction chamber 11 are all provided with platinum Electrode plate 14.

其中,所述的试样支撑架2后侧设置有刻度比对板,刻度比对板的设置可以便于各个圆柱形试样4之间腐蚀深度的比对,使试验结果更具说服力;所述的试样套筒3是由橡胶材料制成,橡胶材料制成的试样套筒3弹性较好,且内壁的摩擦力更大,便于对圆柱形试样4的固定和调节;所述的试样孔5内侧设置有弹性垫圈,弹性垫圈的设置可以提高圆柱形试样4和试样孔5之间的密封性能;所述的铂电极板14下端设置有石墨棒,石墨棒的设置可以便于铂电极板14的外接。Wherein, the rear side of the sample support frame 2 is provided with a scale comparison plate, and the setting of the scale comparison plate can facilitate the comparison of the corrosion depth between each cylindrical sample 4, making the test results more convincing; The sample sleeve 3 described above is made of rubber material, and the sample sleeve 3 made of rubber material has better elasticity, and the friction force of the inner wall is larger, which is convenient for fixing and adjusting the cylindrical sample 4; The inner side of the sample hole 5 is provided with an elastic washer, and the setting of the elastic washer can improve the sealing performance between the cylindrical sample 4 and the sample hole 5; the lower end of the platinum electrode plate 14 is provided with a graphite rod, and the setting of the graphite rod The external connection of the platinum electrode plate 14 can be facilitated.

本实用新型在使用时,先向装置主体1内的第一反应室9、第二反应室10和第三反应室11内加入适量的电解液,然后根据试验的需要将一组或者多组圆柱形试样4分别放入试样套筒3内固定,圆柱形试样4的下端穿过试样孔5浸入第一反应室9、第二反应室10或第三反应室11内的电解液内,可以手动调节圆柱形试样4上端的高度来控制圆柱形试样4下端的浸入深度,在圆柱形试样4浸入电解液中进行电化学腐蚀反应时可以通过计时器7来记录反应的时间,由于第一反应室9、第二反应室10和第三反应室11前侧均设置有计时器7,所以可以通过各个计时器7来分别记录不同反应室内的反应时间,每组圆柱形试样4反应的时间和腐蚀深度均可进行较为准确的记录。When the utility model is in use, an appropriate amount of electrolyte is first added to the first reaction chamber 9, the second reaction chamber 10 and the third reaction chamber 11 in the device main body 1, and then one or more groups of cylinders are placed according to the needs of the test. The cylindrical sample 4 is fixed in the sample sleeve 3 respectively, and the lower end of the cylindrical sample 4 passes through the sample hole 5 and is immersed in the electrolyte in the first reaction chamber 9, the second reaction chamber 10 or the third reaction chamber 11. Inside, the height of the upper end of the cylindrical sample 4 can be manually adjusted to control the immersion depth of the lower end of the cylindrical sample 4, and the reaction time can be recorded by the timer 7 when the cylindrical sample 4 is immersed in the electrolyte for electrochemical corrosion reaction Time, since the first reaction chamber 9, the second reaction chamber 10 and the third reaction chamber 11 front sides are all provided with a timer 7, so the reaction times in different reaction chambers can be recorded respectively by each timer 7, each group of cylindrical The reaction time and corrosion depth of sample 4 can be recorded more accurately.

以上显示和描述了本实用新型的基本原理和主要特征和本实用新型的优点。本行业的技术人员应该了解,本实用新型不受上述实施例的限制,上述实施例和说明书中描述的只是说明本实用新型的原理,在不脱离本实用新型精神和范围的前提下,本实用新型还会有各种变化和改进,这些变化和改进都落入要求保护的本实用新型范围内。本实用新型要求保护范围由所附的权利要求书及其等效物界定。The basic principles and main features of the present utility model and the advantages of the present utility model have been shown and described above. Those skilled in the art should understand that the utility model is not limited by the above-mentioned embodiments. The above-mentioned embodiments and descriptions only illustrate the principle of the utility model. Without departing from the spirit and scope of the utility model, the utility model The new model also has various changes and improvements, and these changes and improvements all fall within the scope of the claimed utility model. The scope of protection required by the utility model is defined by the appended claims and their equivalents.

Claims (5)

  1. A kind of 1. electrochemical corrosion test device, it is characterised in that:It includes apparatus main body (1), sample support frame (2), sample It is sleeve (3), cylindrical sample (4), sample aperture (5), sample registration plate (6), timer (7), transparent observing plate (8), first anti- Answer room (9), the second reative cell (10), the 3rd reative cell (11), division board (12), electrolysis fluid through-hole (13) and platinum electrode plate (14) sample support frame (2), is provided with the upside of described device main body (1), sample support frame (2) upper side wall is provided with multiple samples Sleeve (3), sample sleeve (3) is interior to be provided with cylindrical sample (4), and cylindrical sample (4) lower end is provided with sample aperture (5), and Cylindrical sample (4) lower end is located in sample aperture (5), and the sample aperture (5) is located at apparatus main body (1) upper side wall, the sample Sample registration plate (6) is provided with front side of hole (5), described device main body (1) front side wall is provided with multiple timers (7), timer (7) downside is provided with transparent observing plate (8), and described device main body (1) is internally provided with the first reative cell (9), the second reative cell (10) and the 3rd reative cell (11), and on front side of the first reative cell (9), the second reative cell (10) and the 3rd reative cell (11) it is respectively provided with Have a timer (7) and transparent observing plate (8), first reative cell (9), the second reative cell (10) and the 3rd reative cell (11) it Between by division board (12) isolate, and be provided with division board (12) electrolysis fluid through-hole (13), first reative cell (9), Second reative cell (10) and the 3rd reative cell (11) bottom are provided with platinum electrode plate (14).
  2. A kind of 2. electrochemical corrosion test device according to claim 1, it is characterised in that:Described sample support frame (2) rear side is provided with scale and compares plate.
  3. A kind of 3. electrochemical corrosion test device according to claim 1, it is characterised in that:Described sample sleeve (3) It is made up of elastomeric material.
  4. A kind of 4. electrochemical corrosion test device according to claim 1, it is characterised in that:In described sample aperture (5) Side is provided with elastic washer.
  5. A kind of 5. electrochemical corrosion test device according to claim 1, it is characterised in that:Described platinum electrode plate (14) Lower end is provided with graphite rod.
CN201720769609.4U 2017-06-28 2017-06-28 A kind of electrochemical corrosion test device Expired - Fee Related CN206848141U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201720769609.4U CN206848141U (en) 2017-06-28 2017-06-28 A kind of electrochemical corrosion test device

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201720769609.4U CN206848141U (en) 2017-06-28 2017-06-28 A kind of electrochemical corrosion test device

Publications (1)

Publication Number Publication Date
CN206848141U true CN206848141U (en) 2018-01-05

Family

ID=60803004

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201720769609.4U Expired - Fee Related CN206848141U (en) 2017-06-28 2017-06-28 A kind of electrochemical corrosion test device

Country Status (1)

Country Link
CN (1) CN206848141U (en)

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110018209A (en) * 2018-01-09 2019-07-16 中国石油化工股份有限公司 The method of the lower metal surface pH value measurement of dirt
CN117147427A (en) * 2023-10-26 2023-12-01 鲁东大学 A sample suitable for electrochemical testing in deep-sea experiments and its packaging method

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110018209A (en) * 2018-01-09 2019-07-16 中国石油化工股份有限公司 The method of the lower metal surface pH value measurement of dirt
CN117147427A (en) * 2023-10-26 2023-12-01 鲁东大学 A sample suitable for electrochemical testing in deep-sea experiments and its packaging method

Similar Documents

Publication Publication Date Title
CN101498649B (en) Portable metallic material tensile stress etching apparatus and method
CN103792182B (en) A kind of double-electrolyzer and application of simulating underdeposit corrosion
CN101995430B (en) Detecting device and detection method of ion transmembrane migration number tracking
CN105954186B (en) The measurement device and assay method of metal welding joints position galvanic corrosion
CN206848141U (en) A kind of electrochemical corrosion test device
CN203396742U (en) Electrolytic cell device with three-electrode system for electrochemical testing
CN102288654B (en) Device and method for research on hydrogen permeation of metal in acidic atmospheric medium
CN105116229A (en) Fuel cell resistance measuring device
CN110658030A (en) A rapid sampling detection method of lake water quality
CN206648932U (en) A kind of coating electrochemical testing device
CN204514780U (en) A kind of the cannot-harm-detection device detecting metal welding joints bimetallic corrosion susceptibility
RU2532592C1 (en) Method for determining integrity of polymer coating, and device for its implementation
CN111141953A (en) Alternating current impedance testing device and method for insulating hollow fiber membrane
CN105203449B (en) The corrosion pond that steel bar corrosion is tested in a kind of reinforcing steel
CN203923432U (en) Microelectrode array electroplanting device based on testing impedance
CN205593902U (en) Metal welded joint position galvanic corrosion's survey device
CN105651847A (en) Electrophoresis coating material throwing power testing method and electrophoresis coating material throwing power detection apparatus
CN103981554A (en) Impedance test-based microelectrode array electroplating apparatus and electroplating effect assessment method
CN110501281A (en) An electrolytic cell for local electrochemical research of L-shaped samples and its application
CN105353173A (en) Electrolytic tank based on local electrochemical scanning probe research, and application of electrolytic tank
CN205374365U (en) Electrolytic tank device
CN204758455U (en) Cell electricity survey device
CN210720109U (en) Electrolytic cell for local electrochemical research of L-shaped sample
CN103558146A (en) Multifunctional same-material three-electrode probe
CN115116311B (en) An experimental device for measuring the migration number of Cu2+ ions based on Hittorf method

Legal Events

Date Code Title Description
GR01 Patent grant
GR01 Patent grant
CF01 Termination of patent right due to non-payment of annual fee
CF01 Termination of patent right due to non-payment of annual fee

Granted publication date: 20180105