CN206330825U - A kind of special analytical apparatus suitable for microwave dissolver - Google Patents
A kind of special analytical apparatus suitable for microwave dissolver Download PDFInfo
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Abstract
本实用新型涉及一种适用于微波消解仪的专用分析装置,包括天平本体,天平本体上部设置有消解罐盒,消解罐盒包括盒本体,盒本体一侧铰接有观察门,观察门上设置有门把手,门把手上设置有水平泡,消解罐架中心位置设置有转轴,消解罐架上设置有若干消解罐插槽,消解罐插槽包括第一插槽和第二插槽,第一插槽内侧壁开设有支架槽,支架槽的上端通过自动回位合页铰接有支架。本实用新型通过第一插槽和第二插槽配合,可以放置不同直径的消解罐,可使不同直径的消解罐混合放置,并且通过支架很好的解决了小直径的消解罐在插入第二插槽后的支撑问题。还通过了设置在门把手上的水平泡观察了分析装置的水平度,并通过可调节支脚来调解分析装置的水平度。
The utility model relates to a special analysis device suitable for a microwave digestion instrument, comprising a balance body, a digestion tank box is arranged on the upper part of the balance body, the digestion tank box includes a box body, an observation door is hinged on one side of the box body, and a A door handle, a horizontal bubble is arranged on the door handle, a rotating shaft is arranged at the center of the digestion tank frame, and a number of digestion tank slots are arranged on the digestion tank frame, the digestion tank slots include a first slot and a second slot, the first slot The inner wall of the groove is provided with a bracket groove, and the upper end of the bracket groove is hinged with a bracket through an automatic return hinge. The utility model can place digestion tanks of different diameters through the cooperation of the first slot and the second slot, and can place digestion tanks of different diameters in a mixed manner, and solves the problem of the small-diameter digestion tank being inserted into the second slot through the bracket. Support issues behind sockets. The levelness of the analysis device is also observed through the level bubble arranged on the door handle, and the levelness of the analysis device is regulated through adjustable feet.
Description
技术领域technical field
本实用新型涉及分析装置技术领域,尤其是一种适用于微波消解仪的专用分析装置。The utility model relates to the technical field of analysis devices, in particular to a special analysis device suitable for microwave digestion instruments.
背景技术Background technique
在公知的技术领域,微波消解仪是用于化学物质检测分析一种前处理仪器,使用微波快速加热密闭反应容器中的样品和酸,使样品迅速被破坏分解,反应后形成澄清的溶液,可满足后续分析仪器(ICP、AAS、AES等)进样要求并完成检测。而在对样品进行前处理的时候,需要对样品进行称重才可以分析单位重量中的各物质含量。现有的专用分析装置中的常用消解罐来盛装样品,消解罐有不同的尺寸型号,例如直径2.6cm和直径3.5cm的消解罐。而且在对样品称重时,需要将样品先放入消解罐内再称重,而消解罐需要放置在支架内才可以竖直放置。现有的消解罐支架的尺寸固定,不能满足不同直径的消解罐的放置问题,需要进行替换,耗费操作时间,增加了分析成本。而且分析装置需要在非常水平的平面上操作,才有利于获取更精确的分析称重数据。In the known technical field, the microwave digestion instrument is a pretreatment instrument used for the detection and analysis of chemical substances. It uses microwaves to rapidly heat the sample and acid in a closed reaction vessel, so that the sample is quickly destroyed and decomposed, and a clear solution is formed after the reaction. Satisfy the sampling requirements of subsequent analytical instruments (ICP, AAS, AES, etc.) and complete the testing. When the sample is pre-treated, it is necessary to weigh the sample to analyze the content of each substance in the unit weight. The commonly used digestion tanks in the existing dedicated analysis devices are used to contain samples, and the digestion tanks have different sizes and models, for example, digestion tanks with a diameter of 2.6 cm and a diameter of 3.5 cm. Moreover, when weighing the sample, it is necessary to put the sample into the digestion tank before weighing, and the digestion tank needs to be placed in the support before it can be placed vertically. The size of the existing digestion tank bracket is fixed, which cannot meet the problem of placement of digestion tanks with different diameters, and needs to be replaced, which consumes operation time and increases the analysis cost. Moreover, the analysis device needs to be operated on a very horizontal plane, which is conducive to obtaining more accurate analysis and weighing data.
实用新型内容Utility model content
针对现有技术存在的不足,本实用新型的目的在于提供一种可解决上述问题的一种适用于微波消解仪的专用分析装置。通过第一插槽和第二插槽不同的直径配合,使一个插槽孔内可以放置不同直径的消解罐。并且通过设置在第一插槽上的支架,使小直径的消解罐插入第二插槽后,也能对消解罐进行支撑,使其很好的竖直放置。Aiming at the deficiencies in the prior art, the purpose of this utility model is to provide a special analysis device suitable for microwave digestion instruments that can solve the above problems. Through the matching of different diameters of the first slot and the second slot, digestion tanks with different diameters can be placed in one slot hole. And through the bracket arranged on the first slot, after the small-diameter digestion tank is inserted into the second slot, it can also support the digestion tank so that it can be placed vertically well.
本实用新型解决其技术问题所采用的技术方案是:一种适用于微波消解仪的专用分析装置,包括天平本体,天平本体上部设置有消解罐盒,消解罐盒包括具有容置腔室且一端开口的盒本体,盒本体一侧铰接有观察门,观察门上设置有用于打开观察门的门把手,门把手上设置有用于观察水平状态的水平泡,盒本体的开口上设置有用于覆盖开口的盒盖,盒本体内部设置有用于存放消解罐的消解罐架,消解罐架中心位置设置有用于旋转消解罐架的转轴,消解罐架上设置有若干消解罐插槽,消解罐插槽包括第一插槽和位于第一插槽下部且直径小于第一插槽的第二插槽,第一插槽内侧壁开设有支架槽,支架槽的上端且位于第一插槽上端近边缘处通过自动回位合页铰接有用于支撑消解罐的支架。The technical solution adopted by the utility model to solve the technical problem is: a special analysis device suitable for microwave digestion instrument, including a balance body, a digestion tank box is arranged on the upper part of the balance body, and the digestion tank box includes a containing chamber and one end The open box body has an observation door hinged on one side of the box body. A door handle for opening the observation door is provided on the observation door. A horizontal bubble for observing the horizontal state is provided on the door handle. The box cover, the inside of the box body is provided with a digestion tank rack for storing digestion tanks, and the center of the digestion tank rack is provided with a rotating shaft for rotating the digestion tank rack. There are several digestion tank slots on the digestion tank rack. The digestion tank slots include: The first slot and the second slot located at the bottom of the first slot and having a diameter smaller than the first slot, the inner wall of the first slot is provided with a bracket slot, and the upper end of the bracket slot is positioned at the upper edge of the first slot and passes through The self-returning hinge is hinged with a bracket for supporting the digestion tank.
为了在一个插槽内可以放置2.6cm直径和3.5cm直径的消解罐,本实用新型进一步设置为:第一插槽的内壁直径为3.5cm,第二插槽的内壁直径为2.6cm。In order to place digestion tanks with a diameter of 2.6cm and a diameter of 3.5cm in a slot, the utility model is further configured as follows: the diameter of the inner wall of the first slot is 3.5cm, and the diameter of the inner wall of the second slot is 2.6cm.
为了方便提起盒盖,本实用新型进一步设置为:盒盖上设置有用于提起盒盖的盒盖把手。In order to facilitate the lifting of the lid, the utility model is further configured as follows: the lid is provided with a lid handle for lifting the lid.
为了使分析装置的称重更为精确,本实用新型进一步设置为:天平本体的最小称重值为0.01g。In order to make the weighing of the analysis device more accurate, the utility model is further set as: the minimum weighing value of the balance body is 0.01g.
为了可以使分析装置与电脑连接,使电脑直接获取称重参数,本实用新型进一步设置为:天平本体的一侧设置有与电脑连接的数据接口。In order to connect the analyzing device with the computer, so that the computer can directly obtain the weighing parameters, the utility model is further configured as follows: one side of the balance body is provided with a data interface connected with the computer.
为了可以调节天平的水平度,本实用新型进一步设置为:天平本体的下端设置有用于调节天平本体水平度的可调节支脚。In order to be able to adjust the levelness of the balance, the utility model is further configured as follows: the lower end of the balance body is provided with adjustable feet for adjusting the levelness of the balance body.
本实用新型的有益效果是:通过第一插槽和第二插槽不同的直径范围,可以放置不同直径的消解罐,减少了分析作业时间,节约了工具成本,并可使不同直径的消解罐混合放置,并且通过支架很好的解决了小直径的消解罐在插入第二插槽后的支撑问题,使小直径的消解罐也能很好的竖直放置。还通过了设置在门把手上的水平泡观察了分析装置的水平度,并通过可调节支脚来调解分析装置的水平度。The beneficial effects of the utility model are: through the different diameter ranges of the first slot and the second slot, digestion tanks with different diameters can be placed, which reduces the analysis operation time, saves tool costs, and enables digestion tanks with different diameters Mixed placement, and the support problem of the small-diameter digestion tank after being inserted into the second slot is well solved through the bracket, so that the small-diameter digestion tank can also be placed vertically well. The levelness of the analysis device is also observed through the level bubble arranged on the door handle, and the levelness of the analysis device is regulated through adjustable feet.
附图说明Description of drawings
下面结合附图和实施例对本实用新型进一步说明。Below in conjunction with accompanying drawing and embodiment the utility model is further described.
图1是本实用新型的结构示意图;Fig. 1 is a structural representation of the utility model;
图2是本实用新型中消解罐盒的结构示意图;Fig. 2 is the structural representation of digestion tank box in the utility model;
图3是本实用新型中消解罐插槽的剖面结构示意图;Fig. 3 is the sectional structure schematic diagram of digestion tank slot in the utility model;
图中:1.天平本体,2.消解罐盒,21.盒本体,22.观察门,23.门把手,24.水平泡,25.盒盖,3.消解罐架,30.转轴,31.消解罐插槽,310.第一插槽,311.第二插槽,312.支架槽,313.自动回位合页,314.支架,4.盒盖把手,5.数据接口,6.可调节支脚。In the figure: 1. Balance body, 2. Digestion tank box, 21. Box body, 22. Observation door, 23. Door handle, 24. Horizontal bubble, 25. Box cover, 3. Digestion tank frame, 30. Shaft, 31 .Digestion tank slot, 310. First slot, 311. Second slot, 312. Bracket slot, 313. Automatic return hinge, 314. Bracket, 4. Lid handle, 5. Data interface, 6. Adjustable feet.
具体实施方式detailed description
现在结合附图对本实用新型作进一步详细的说明。这些附图均为简化的示意图,仅以示意方式说明本实用新型的基本结构,因此其仅显示与本实用新型有关的构成。Now in conjunction with accompanying drawing, the utility model is described in further detail. These drawings are all simplified schematic diagrams, and only schematically illustrate the basic structure of the utility model, so they only show the configurations related to the utility model.
如图1-3所示的本实用新型的优选实施例,一种适用于微波消解仪的专用分析装置,包括天平本体1,天平本体1上部设置有消解罐盒2,消解罐盒2包括具有容置腔室且一端开口的盒本体21,盒本体21一侧铰接有观察门22,观察门22可以直接打开,方便的观察消解罐盒2内部状况。观察门22上设置有用于打开观察门22的门把手23,门把手23上设置有用于观察水平状态的水平泡24,通过水平泡24可以方便的观察装置的水平状态,根绝观察到的水平状态调整装置的水平,使称量分析的数值更为精确。盒本体21的开口上设置有用于覆盖开口的盒盖25,盒本体21内部设置有用于存放消解罐的消解罐架3,消解罐架3中心位置设置有用于旋转消解罐架3的转轴30,转轴30可以方便操作装入消解罐。消解罐架3上设置有若干消解罐插槽31,消解罐插槽31包括第一插槽310和位于第一插槽310下部且直径小于第一插槽310的第二插槽311,第一插槽310内侧壁开设有支架槽312,支架槽312的上端且位于第一插槽310上端近边缘处通过自动回位合页313铰接有用于支撑消解罐的支架314。如果插入的是大直径的消解罐,消解罐罐体压住支架314,使支架314在压力和自动回位合页313的作用下收入支架槽312内,消解罐直接插入第一插槽310中,取出消解罐时,支架314在自动回位合页313的作用下弹开,呈打开状态。如果插入的是小直径的消解罐,消解罐直接插入第二插槽311中,而支架314在自动回位合页313的作用下呈打开状态,为小直径的消解罐提供了制成,使其不会晃动,提供称量分析精确性。可以在第一插槽310的内侧壁设置多组支架,效果将会更好。并且支架314与消解罐解除的一端,可以设置为与消解罐罐体贴合的弧形结构,更好的支撑消解罐。As shown in Figures 1-3, a preferred embodiment of the present utility model is a special analysis device suitable for microwave digestion instruments, including a balance body 1, and a digestion tank box 2 is arranged on the top of the balance body 1, and the digestion tank box 2 includes a A box body 21 with an accommodating chamber and an opening at one end. An observation door 22 is hinged on one side of the box body 21. The observation door 22 can be opened directly to observe the internal conditions of the digestion tank box 2 conveniently. The observation door 22 is provided with a door handle 23 for opening the observation door 22, and the door handle 23 is provided with a horizontal bubble 24 for observing the horizontal state. The horizontal state of the device can be easily observed by the horizontal bubble 24, and the observed horizontal state can be eliminated. Adjust the level of the device to make the weighing analysis more accurate. The opening of the box body 21 is provided with a box cover 25 for covering the opening. Inside the box body 21 is provided a digestion tank rack 3 for storing digestion tanks. The center of the digestion tank rack 3 is provided with a rotating shaft 30 for rotating the digestion tank rack 3. The rotating shaft 30 can be conveniently operated and loaded into the digestion tank. The digestion tank rack 3 is provided with several digestion tank slots 31, the digestion tank slots 31 include a first slot 310 and a second slot 311 positioned at the bottom of the first slot 310 and having a diameter smaller than the first slot 310, the first The inner side wall of the slot 310 is provided with a support slot 312 , and the upper end of the support slot 312 is located near the upper edge of the first slot 310 and is hinged with a support 314 for supporting the digestion tank through an automatic return hinge 313 . If a large-diameter digestion tank is inserted, the tank body of the digestion tank presses the bracket 314, so that the bracket 314 is put into the bracket groove 312 under the action of pressure and the automatic return hinge 313, and the digestion tank is directly inserted into the first slot 310 , when the digestion tank is taken out, the bracket 314 bounces off under the action of the automatic return hinge 313, and is in an open state. If a small-diameter digestion tank is inserted, the digestion tank is directly inserted into the second slot 311, and the bracket 314 is opened under the action of the automatic return hinge 313, which provides a small-diameter digestion tank, so that It does not shake, providing precision in weighing analysis. Multiple groups of brackets can be arranged on the inner wall of the first slot 310, and the effect will be better. Moreover, the end of the bracket 314 that is disconnected from the digestion tank can be set as an arc-shaped structure that fits the body of the digestion tank, so as to better support the digestion tank.
第一插槽310的内壁直径为3.5cm,第二插槽311的内壁直径为2.6cm,常规的消解罐多见此两种直径的型号,可以满足大多数状态的需求。The diameter of the inner wall of the first slot 310 is 3.5 cm, and the diameter of the inner wall of the second slot 311 is 2.6 cm. These two types of diameters are common in conventional digestion tanks, which can meet the needs of most situations.
如图1所示,为了方便打开盒盖25,盒盖25上设置有用于提起盒盖25的盒盖把手4。As shown in FIG. 1 , in order to open the lid 25 conveniently, the lid handle 4 for lifting the lid 25 is provided on the lid 25 .
天平本体1的最小称重值为0.01g,这样使天平本体1的称量精度达到了0.01g,使分析数据更为精确。The minimum weighing value of the balance body 1 is 0.01g, so that the weighing accuracy of the balance body 1 reaches 0.01g, making the analysis data more accurate.
如图1所示,天平本体1的一侧设置有与电脑连接的数据接口5。As shown in FIG. 1 , one side of the balance body 1 is provided with a data interface 5 connected to a computer.
如图1所示,为了可以根据水平泡24的水平指示调整天平本体1的水平度,天平本体1的下端设置有用于调节天平本体1水平度的可调节支脚6,通过正反方向旋转不同的可调节支脚6,即可完成装置水平度的调节。As shown in Figure 1, in order to adjust the levelness of the balance body 1 according to the level indication of the level bubble 24, the lower end of the balance body 1 is provided with an adjustable leg 6 for adjusting the levelness of the balance body 1. Adjustable leg 6 can complete the adjustment of the levelness of the device.
以上述依据本实用新型的理想实施例为启示,通过上述的说明内容,相关工作人员完全可以在不偏离本项实用新型技术思想的范围内,进行多样的变更以及修改。本项实用新型的技术性范围并不局限于说明书上的内容,必须要根据权利要求范围来确定其技术性范围。Inspired by the above-mentioned ideal embodiment according to the utility model, and through the above-mentioned description content, relevant staff can completely make various changes and modifications within the scope of not deviating from the technical idea of the utility model. The technical scope of this utility model is not limited to the content in the description, but must be determined according to the scope of the claims.
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CN108152270A (en) * | 2017-11-23 | 2018-06-12 | 中国航发北京航空材料研究院 | A kind of method of ruthenium element content in Digestion high temperature alloy |
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CN108152270A (en) * | 2017-11-23 | 2018-06-12 | 中国航发北京航空材料研究院 | A kind of method of ruthenium element content in Digestion high temperature alloy |
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