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CN205958229U - Experimental device for be used for studying micro scale effect - Google Patents

Experimental device for be used for studying micro scale effect Download PDF

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Publication number
CN205958229U
CN205958229U CN201620941960.2U CN201620941960U CN205958229U CN 205958229 U CN205958229 U CN 205958229U CN 201620941960 U CN201620941960 U CN 201620941960U CN 205958229 U CN205958229 U CN 205958229U
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pressure sensor
flow metering
metering tube
power cord
switch
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常元昊
姜汉桥
李俊键
马康
胡锦川
王依诚
高亚军
孟凡乐
施欣燕
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China University of Petroleum Beijing
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China University of Petroleum Beijing
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Abstract

本实用新型涉及一种用于研究微尺度效应的实验装置,包括注入系统、气体过滤装置、储液罐、液体过滤装置、超声波气泡检测器、导管、开关一、压力传感器一、微管一、压力传感器二、流量计量管一、电子显微镜、电脑及温控箱。其特征在于:注入系统与气体过滤装置、储液罐、液体过滤装置依次相连;液体过滤装置所接出的导管上装有超声波气泡检测器,在一侧依次连接有开关一、压力传感器一、微管一、压力传感器二以及流量计量管一;在另一侧同样依次连接有对应的同种装置;上述的超声波气泡检测器及两侧所连接的装置均置于温控箱中;所用的压力传感器均与温控箱外的电脑相连,电脑同时连有电子显微镜,以观测所用的流量计量管。

The utility model relates to an experimental device for studying microscale effects, comprising an injection system, a gas filter device, a liquid storage tank, a liquid filter device, an ultrasonic bubble detector, a conduit, a switch one, a pressure sensor one, a microtube one, Pressure sensor two, flow metering tube one, electron microscope, computer and temperature control box. It is characterized in that: the injection system is sequentially connected with the gas filter device, the liquid storage tank, and the liquid filter device; an ultrasonic bubble detector is installed on the conduit connected to the liquid filter device, and a switch 1, a pressure sensor 1, and a micro Tube 1, pressure sensor 2, and flow metering tube 1; the other side is also connected to the corresponding device in sequence; the above-mentioned ultrasonic bubble detector and the devices connected to both sides are placed in the temperature control box; the pressure used The sensors are all connected with the computer outside the temperature control box, and the computer is connected with an electron microscope at the same time to observe the flow metering tube used.

Description

一种用于研究微尺度效应的实验装置An experimental setup for studying microscale effects

技术领域technical field

本实用新型属于流体力学领域,具体涉及一种用于研究微尺度效应的实验装置。The utility model belongs to the field of fluid mechanics, in particular to an experimental device for studying microscale effects.

背景技术Background technique

随着微电子机械系统研究的深入,微流体的流动问题得到研究人员的重视。随着尺寸的微小化,流体的一些流动规律与宏观流动有所差异,即存在微尺度效应。以油气田开发工程为例,页岩有机质中存在大量纳米孔隙,气体在纳米孔隙中的流动便存在微尺度效应。当前,用于研究微尺度效应的实验装置的设计并不严谨,在实验过程中,往往忽略了装置的进出口效应以及气泡的影响,导致了实验的误差,进而影响了对微尺度效应的认识。因此,急需设计一种更加严谨的实验装置用以研究微尺度效应。With the deepening of MEMS research, the flow of microfluids has been paid more attention by researchers. With the miniaturization of the size, some flow laws of the fluid are different from the macro flow, that is, there are micro-scale effects. Taking oil and gas field development projects as an example, there are a large number of nanopores in the organic matter of shale, and the flow of gas in the nanopores has micro-scale effects. At present, the design of the experimental device used to study the micro-scale effect is not rigorous. During the experiment, the effect of the inlet and outlet of the device and the influence of air bubbles are often ignored, which leads to experimental errors and affects the understanding of the micro-scale effect. . Therefore, it is urgent to design a more rigorous experimental device to study micro-scale effects.

实用新型内容Utility model content

本实用新型提供了一种用于研究微尺度效应的实验装置,利用装置,能够有效避免实验过程中气泡以及进出口效应所带来的影响,较为严谨地进行微尺度效应的分析研究,同时,能够进行不同温度下微尺度效应的分析研究。The utility model provides an experimental device for studying micro-scale effects. The device can effectively avoid the influence of air bubbles and import and export effects in the experimental process, and conduct analysis and research of micro-scale effects more rigorously. At the same time, It is possible to conduct analysis and research on microscale effects at different temperatures.

为了实现上述目的,本实用新型采用以下技术方案:装置包括注入系统、气体过滤装置、储液罐、液体过滤装置、超声波气泡检测器、导管、开关一、压力传感器一、微管一、压力传感器二、流量计量管一、开关二、压力传感器三、微管二、压力传感器四、流量计量管二、电源线一、电源线二、电源线三、电源线四、电源线五、电脑、电子显微镜以及温控箱。其特征在于:该装置中,注入系统与气体过滤装置、储液罐、液体过滤装置通过导管依次相连,其中,注入系统用以气体的注入并为实验提供动力支持;在液体过滤装置所接出的导管上装有超声波气泡检测器,随后在一侧依次连接有开关一、压力传感器一、微管一、压力传感器二以及流量计量管一;在另一侧同样依次连接有开关二、压力传感器三、微管二、压力传感器四以及流量计量管二;上述的超声波气泡检测器及两侧所连接的一系列装置均置于温控箱中;压力传感器一、压力传感器二、压力传感器三、压力传感器四分别通过电源线一、电源线二、电源线三、电源线四与电脑相连;电脑同时通过电源线五连接有电子显微镜,用以观测流量计量管一和流量计量管二。In order to achieve the above object, the utility model adopts the following technical solutions: the device includes an injection system, a gas filter device, a liquid storage tank, a liquid filter device, an ultrasonic bubble detector, a catheter, a switch one, a pressure sensor one, a microtube one, a pressure sensor 2. Flow metering tube 1, switch 2, pressure sensor 3, microtube 2, pressure sensor 4, flow metering tube 2, power cord 1, power cord 2, power cord 3, power cord 4, power cord 5, computer, electronics Microscope and temperature control box. It is characterized in that: in the device, the injection system is sequentially connected with the gas filter device, liquid storage tank and liquid filter device through conduits, wherein the injection system is used to inject gas and provide power support for the experiment; An ultrasonic bubble detector is installed on the conduit of the pipe, and then a switch 1, a pressure sensor 1, a microtube 1, a pressure sensor 2 and a flow metering tube 1 are connected in sequence on one side; a switch 2 and a pressure sensor 3 are also connected in sequence on the other side , microtube two, pressure sensor four and flow metering tube two; the above-mentioned ultrasonic bubble detector and a series of devices connected on both sides are placed in the temperature control box; pressure sensor one, pressure sensor two, pressure sensor three, pressure The sensor four is connected to the computer through the power line one, the power line two, the power line three, and the power line four respectively; the computer is connected with an electron microscope through the power line five at the same time to observe the flow metering tube one and the flow metering tube two.

本实用新型具有以下有益效果:(1)该实验装置能够利用等温条件下长短管相减法消去实验中进出口效应的影响;(2)该装置能够利用超声波气泡检测器检测气泡是否存在,进而排除气泡给实验结果带来的影响;(3)利用温控箱,该装置能够研究不同温度下的微尺度效应;(4)该装置能够进行单微管微尺度效应测试,也能够进行双微管微尺度效应测试。The utility model has the following beneficial effects: (1) the experimental device can use the subtraction method of long and short tubes under isothermal conditions to eliminate the influence of the import and export effect in the experiment; (2) the device can use an ultrasonic bubble detector to detect the existence of bubbles, and then eliminate The impact of air bubbles on the experimental results; (3) Using the temperature control box, the device can study the micro-scale effects at different temperatures; (4) The device can test the micro-scale effects of single microtubes, and can also test the micro-scale effects of double microtubes. Microscale effects test.

附图说明Description of drawings

图1为本实用新型的整体外观侧视图。Fig. 1 is a side view of the overall appearance of the utility model.

具体实施方式detailed description

下面结合附图,对本实用新型进行详细描述。Below in conjunction with accompanying drawing, the utility model is described in detail.

为了实现上述目的,本实用新型采用以下技术方案:包括注入系统1、气体过滤装置2、储液罐3、液体过滤装置4、超声波气泡检测器5、导管6、开关一7、压力传感器一8、微管一9、压力传感器二10、流量计量管一11、开关二12、压力传感器三13、微管二14、压力传感器四15、流量计量管二16、电源线一17、电源线二18、电源线三19、电源线四20、电源线五21、电脑22、电子显微镜23以及温控箱24。其特征在于:该装置中,注入系统1与气体过滤装置2、储液罐3、液体过滤装置4依次相连,其中,注入系统1用以气体的注入并为实验提供动力支持;在液体过滤装置4所接出的导管6上装有超声波气泡检测器5,随后在一侧依次连接有开关一7、压力传感器一8、微管一9、压力传感器二10以及流量计量管一11;在另一侧同样依次连接有开关二12、压力传感器三13、微管二14、压力传感器四15以及流量计量管二16;上述的超声波气泡检测器5及两侧所连接的一系列装置均置于温控箱24中;压力传感器一8、压力传感器二10、压力传感器三13、压力传感器四15分别通过电源线一17、电源线二18、电源线三19、电源线四20与电脑22相连;电脑22同时通过电源线五21连接有电子显微镜23,用以观测流量计量管一11和流量计量管二16。In order to achieve the above purpose, the utility model adopts the following technical solutions: including injection system 1, gas filter device 2, liquid storage tank 3, liquid filter device 4, ultrasonic bubble detector 5, catheter 6, switch one 7, pressure sensor one 8 , microtube one 9, pressure sensor two 10, flow metering tube one 11, switch two 12, pressure sensor three 13, microtube two 14, pressure sensor four 15, flow metering tube two 16, power line one 17, power line two 18. Power cord three 19, power cord four 20, power cord five 21, computer 22, electron microscope 23 and temperature control box 24. It is characterized in that: in the device, the injection system 1 is sequentially connected with the gas filter device 2, the liquid storage tank 3, and the liquid filter device 4, wherein the injection system 1 is used for injecting gas and providing power support for the experiment; in the liquid filter device 4. The connected conduit 6 is equipped with an ultrasonic bubble detector 5, and then a switch 7, a pressure sensor 8, a micropipe 9, a pressure sensor 10 and a flow metering tube 11 are sequentially connected on one side; The side is also connected with switch two 12, pressure sensor three 13, micropipe two 14, pressure sensor four 15 and flow metering tube two 16 in sequence; In control box 24; Pressure sensor one 8, pressure sensor two 10, pressure sensor three 13, pressure sensor four 15 link to each other with computer 22 by power line one 17, power line two 18, power line three 19, power line four 20 respectively; The computer 22 is connected with the electron microscope 23 through the power line 5 21 at the same time, in order to observe the flow metering tube 1 11 and the flow metering tube 2 16 .

本装置中注入系统1用以气体的注入并提供动力支持,具体气体种类及所提供压力大小根据研究情况给出;气体过滤装置2主要用于过滤气体中的杂质和水分并干燥气体,液体过滤装置4则是用来过滤实验流体中的微小杂质和气泡。The injection system 1 in this device is used to inject gas and provide power support. The specific gas type and the pressure provided are given according to the research situation; the gas filter device 2 is mainly used to filter impurities and moisture in the gas and dry the gas, liquid filter Device 4 is used to filter tiny impurities and air bubbles in the experimental fluid.

本装置中的微管一9的长度是微管二14的长度的两倍,而其他参数均相同;由于微尺度实验的流量较小,故选用流量计量管一11和流量计量管二16配合电子显微镜23进行流量的测量,电子显微镜23记录流量计量管一11和流量计量管二16中的液面移动;利用电脑22能够完成对压力传感器一8、压力传感器二10、压力传感器三13以及压力传感器四15的压力数据的整理,同时能够获得电子显微镜23所记录的液面移动图像。The length of micropipe one 9 in this device is twice of the length of micropipe two 14, and other parameters are all the same; Because the flow rate of microscale experiment is less, so select flow metering pipe one 11 and flow metering pipe two 16 to cooperate Electron microscope 23 carries out the measurement of flow rate, and electron microscope 23 records the liquid level movement in flow metering tube one 11 and flow metering tube two 16; Utilize computer 22 to be able to finish to pressure sensor one 8, pressure sensor two 10, pressure sensor three 13 and The pressure data of the pressure sensor 415 can be sorted out, and the moving image of the liquid surface recorded by the electron microscope 23 can be obtained at the same time.

本装置中的温控箱24能够控制温控箱24内部环境的温度,并保证微管一9与微管二14的实验温度相同,由于微尺度实验的特殊性,要求温控箱24的精度尽可能高。The temperature control box 24 in this device can control the temperature of the internal environment of the temperature control box 24, and guarantee that the experimental temperature of micropipe one 9 and micropipe two 14 is the same, due to the particularity of the microscale experiment, the precision of the temperature control box 24 is required as high as possible.

实现该装置功能的方法是:实验开始前,保持开关一7与开关二12的关闭,通过注入系统1注入一定压力的某种气体,经过气体过滤装置2以及液体过滤装置4进行杂质的过滤,利用超声波气泡检测器5检测过滤后的流体,若仍然有气泡则重新进行实验,若无气泡则打开开关一7和开关二12,通过压力传感器一8与压力传感器二10计量微管一9的进出口压力,通过压力传感器三13与压力传感器四15计量微管二14的进出口压力,由于微管一9与微管二14实验条件相同,故进出口效应产生附加压差相同,即微管一9两端压降与微管二14两端压降的差值即为排除了进出口效应后所得到的微管二14的等效压降,同时,电子显微镜23将流量计量管二16的液面移动图像时时传送到电脑22中,记录移动一定距离所需的时间,即可得到微管二14的流量大小,综合流量和压力等数据,结合N-S方程,可进行微尺度效应的验证与分析。此外,根据研究需要,若可忽略进出口效应的影响,可选择只打开开关一7或开关二12,进行单微管的直接测量研究;若需要研究不同温度下的微尺度效应,可通过温控箱24进行温度的改变与控制,再进行实验操作。The method to realize the function of the device is: before the experiment starts, keep the switch one 7 and the switch two 12 closed, inject a certain gas with a certain pressure through the injection system 1, filter impurities through the gas filter device 2 and the liquid filter device 4, Utilize the ultrasonic bubble detector 5 to detect the filtered fluid, if there are still bubbles, then perform the experiment again, if there are no bubbles, then turn on the switch one 7 and the switch two 12, and measure the volume of the microtube one 9 by the pressure sensor one 8 and the pressure sensor two 10 The inlet and outlet pressures are measured by the pressure sensor 3 13 and the pressure sensor 4 15 to measure the inlet and outlet pressure of the microtube 2 14. Since the microtube 9 and the microtube 2 14 have the same experimental conditions, the additional pressure difference generated by the effect of the inlet and outlet is the same, that is, the microtube 2 The difference between the pressure drop at both ends of tube 19 and the pressure drop at both ends of microtube 2 14 is the equivalent pressure drop of microtube 2 14 obtained after the import and export effects are excluded. The moving image of the liquid surface of 16 is sent to the computer 22 from time to time, and the time required to move a certain distance can be recorded to obtain the flow rate of the microtube 14, combined with the N-S equation, the micro-scale effect can be obtained Verification and analysis. In addition, according to research needs, if the influence of import and export effects can be ignored, you can choose to turn on switch one 7 or switch two 12 to conduct direct measurement research on a single microtube; if you need to study microscale effects at different temperatures, you can use temperature The control box 24 is used to change and control the temperature, and then perform the experimental operation.

本实用新型装置能够排除微尺度实验中所出现的气泡及进出口效应的影响,较为严谨地进行微尺度的实验研究,最终能够辅助进行有关微流体流动规律的研究,具有极大的益处。The device of the utility model can eliminate the influence of air bubbles and import and export effects in micro-scale experiments, conduct micro-scale experimental research more rigorously, and finally can assist research on microfluid flow laws, which has great benefits.

Claims (1)

1.一种用于研究微尺度效应的实验装置,包括注入系统(1)、气体过滤装置(2)、储液罐(3)、液体过滤装置(4)、超声波气泡检测器(5)、导管(6)、开关一(7)、压力传感器一(8)、微管一(9)、压力传感器二(10)、流量计量管一(11)、开关二(12)、压力传感器三(13)、微管二(14)、压力传感器四(15)、流量计量管二(16)、电源线一(17)、电源线二(18)、电源线三(19)、电源线四(20)、电源线五(21)、电脑(22)、电子显微镜(23)以及温控箱(24),其特征在于:注入系统(1)与气体过滤装置(2)、储液罐(3)、液体过滤装置(4)依次相连,其中,注入系统(1)用以气体的注入并为实验提供动力支持;在液体过滤装置(4)所接出的导管(6)上装有超声波气泡检测器(5),随后在一侧依次连接有开关一(7)、压力传感器一(8)、微管一(9)、压力传感器二(10)以及流量计量管一(11);在另一侧同样依次连接有开关二(12)、压力传感器三(13)、微管二(14)、压力传感器四(15)以及流量计量管二(16);上述的超声波气泡检测器(5)及两侧所连接的一系列装置均置于温控箱(24)中;压力传感器一(8)、压力传感器二(10)、压力传感器三(13)、压力传感器四(15)分别通过电源线一(17)、电源线二(18)、电源线三(19)、电源线四(20)与电脑(22)相连;电脑(22)同时通过电源线五(21)连接有电子显微镜(23),用以观测流量计量管一(11)和流量计量管二(16)。1. An experimental device for studying microscale effects, comprising an injection system (1), a gas filter (2), a liquid storage tank (3), a liquid filter (4), an ultrasonic bubble detector (5), Conduit (6), switch one (7), pressure sensor one (8), microtube one (9), pressure sensor two (10), flow metering tube one (11), switch two (12), pressure sensor three ( 13), microtube two (14), pressure sensor four (15), flow metering tube two (16), power cord one (17), power cord two (18), power cord three (19), power cord four ( 20), power cord five (21), computer (22), electron microscope (23) and temperature control box (24), it is characterized in that: injection system (1) and gas filtering device (2), liquid storage tank (3 ), the liquid filtering device (4) is connected in sequence, wherein, the injection system (1) is used to inject gas and provide power support for the experiment; the catheter (6) connected to the liquid filtering device (4) is equipped with ultrasonic bubble detection device (5), followed by switch one (7), pressure sensor one (8), micropipe one (9), pressure sensor two (10) and flow metering tube one (11) on one side; The side is also connected with switch two (12), pressure sensor three (13), micropipe two (14), pressure sensor four (15) and flow metering tube two (16) in sequence; the above-mentioned ultrasonic bubble detector (5) and A series of devices connected on both sides are all placed in the temperature control box (24); pressure sensor one (8), pressure sensor two (10), pressure sensor three (13), pressure sensor four (15) respectively through the power line One (17), power cord two (18), power cord three (19), power cord four (20) link to each other with computer (22); Computer (22) is connected with electron microscope (23) by power cord five (21) simultaneously ), used to observe flow metering tube one (11) and flow metering tube two (16).
CN201620941960.2U 2016-08-26 2016-08-26 Experimental device for be used for studying micro scale effect Expired - Fee Related CN205958229U (en)

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CN107389299A (en) * 2017-07-20 2017-11-24 中国人民解放军装备学院 Assess the device and method of flow transition point in miniature scale pipeline
CN108709584A (en) * 2018-01-23 2018-10-26 四川大学 It is a kind of to measure thickness of liquid film and the device and method of hydrodynamics behavior in falling liquid film microchannel using stereomicroscope
CN111412958A (en) * 2019-01-08 2020-07-14 中国石油天然气股份有限公司 Flow measurement system and method

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107389299A (en) * 2017-07-20 2017-11-24 中国人民解放军装备学院 Assess the device and method of flow transition point in miniature scale pipeline
CN108709584A (en) * 2018-01-23 2018-10-26 四川大学 It is a kind of to measure thickness of liquid film and the device and method of hydrodynamics behavior in falling liquid film microchannel using stereomicroscope
CN111412958A (en) * 2019-01-08 2020-07-14 中国石油天然气股份有限公司 Flow measurement system and method

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