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CN204395871U - Base polyurethane prepolymer for use as emulsifying systems - Google Patents

Base polyurethane prepolymer for use as emulsifying systems Download PDF

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Publication number
CN204395871U
CN204395871U CN201420829144.3U CN201420829144U CN204395871U CN 204395871 U CN204395871 U CN 204395871U CN 201420829144 U CN201420829144 U CN 201420829144U CN 204395871 U CN204395871 U CN 204395871U
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CN
China
Prior art keywords
oligomer
static mixer
pump
water pump
emulsification
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Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
Application number
CN201420829144.3U
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Chinese (zh)
Inventor
金敬东
杨永然
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Shanghai Dongrui New Materials Co ltd
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SHANGHAI DONGRUI CHEMICAL CO Ltd
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Priority to CN201420829144.3U priority Critical patent/CN204395871U/en
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  • Processes Of Treating Macromolecular Substances (AREA)

Abstract

The utility model discloses a kind of base polyurethane prepolymer for use as emulsifying systems, described system comprises a technique water pump and an oligomer pump, technique water pump is all connected with the liquid feeding end of static mixer with the outlet end of oligomer pump, hybrid chamber is provided with in static mixer, the outlet end of this static mixer is connected with the liquid feeding end of emulsifying kettle, the dehvery lift of this oligomer pump is 0.2Mpa-0.4Mpa, and the dehvery lift of technique water pump is 0.2Mpa-0.4Mpa.System adopts Liquid-liquid mixing device continuous emulsification, utilizes the high efficiency dispersion function of static mixer to carry out the emulsification of oligomer.Effectively improve the stability of product quality, guarantee that follow-up emulsifying kettle equipment operates steadily, stop potential safety hazard, greatly reduce the power of emulsifying kettle motor simultaneously.

Description

聚氨酯预聚体乳化系统Polyurethane prepolymer emulsification system

技术领域 technical field

本实用新型涉及聚氨酯乳液生产系统的技术领域,具体地说是聚氨酯预聚体乳化系统,特别涉及其系统连接结构。 The utility model relates to the technical field of a polyurethane emulsion production system, in particular to a polyurethane prepolymer emulsification system, in particular to its system connection structure.

背景技术 Background technique

生产聚氨酯乳液,首先要生产聚氨酯的低聚物。然后,用10℃左右低聚物重量2-3倍的工艺水在短时间内快速将低聚物分散成为聚氨酯乳液。分散的效果影响乳液的品质及决定乳液的稳定性。 To produce polyurethane emulsion, the first step is to produce polyurethane oligomers. Then, disperse the oligomer into a polyurethane emulsion in a short time with process water that is 2-3 times the weight of the oligomer at about 10°C. The dispersion effect affects the quality of the emulsion and determines the stability of the emulsion.

之前,是将低聚物放入乳化釜中,然后快速加入10℃的工艺水。同时在240rpm的快速搅拌下成为乳液。由于低聚物粘度大(4000-6000cps)搅拌阻力大,要求搅拌电机的功率远远超出常规反应釜的搅拌功率。如单釜1.2吨的乳液需要22KW的电机,并且由于低聚物与工艺水的粘度差别大搅拌桨受到的阻力差别大、不稳定致使乳化釜震动十分严重,带来设备及安全隐患。 Before, the oligomer was put into the emulsification tank, and then the process water at 10°C was quickly added. At the same time, it becomes an emulsion under rapid stirring at 240 rpm. Due to the high viscosity of oligomers (4000-6000cps) and high stirring resistance, the power of the stirring motor is required to far exceed the stirring power of conventional reactors. For example, a single tank of 1.2 tons of emulsion requires a 22KW motor, and due to the large viscosity difference between the oligomer and the process water, the resistance of the stirring paddle is greatly different and unstable, resulting in serious vibration of the emulsification tank, which brings equipment and safety hazards.

发明内容 Contents of the invention

本实用新型的目的是提供聚氨酯预聚体乳化系统,采用液-液混合器连续乳化,利用静态混合器的高效分散功能进行低聚物的乳化,连续乳化后的低聚物粘度大大降低,且乳化液的均匀度也有效提升,要求反应釜的搅拌功率大大降低,避免了乳化釜在工作状态中震动过度。 The purpose of this utility model is to provide polyurethane prepolymer emulsification system, adopt liquid-liquid mixer to emulsify continuously, utilize the efficient dispersion function of static mixer to carry out the emulsification of oligomer, the oligomer viscosity after continuous emulsification is greatly reduced, and The uniformity of the emulsion is also effectively improved, requiring the stirring power of the reactor to be greatly reduced to avoid excessive vibration of the emulsification kettle in the working state.

为了实现上述目的,本实用新型的技术方案是:聚氨酯预聚体乳化系统,其特征在于:所述系统包括一工艺水泵和一低聚物泵,工艺水泵和低聚物泵的出液端均与静态混合器的进液端连接,静态混合器内设有混合腔,该静态混合器的出液端与乳化釜的进液端连接,该低聚物泵的输送扬程为0.2Mpa-0.4Mpa,工艺水泵的输送扬程为0.2Mpa-0.4Mpa。 In order to achieve the above object, the technical solution of the utility model is: a polyurethane prepolymer emulsification system, characterized in that: the system includes a process water pump and an oligomer pump, and the liquid outlets of the process water pump and the oligomer pump are both It is connected to the liquid inlet of the static mixer. The static mixer is equipped with a mixing chamber. The liquid outlet of the static mixer is connected to the liquid inlet of the emulsification tank. The delivery head of the oligomer pump is 0.2Mpa-0.4Mpa , The delivery head of the process water pump is 0.2Mpa-0.4Mpa.

本实用新型公开了聚氨酯预聚体乳化系统,系统采用液-液混合器连续乳化,利用静态混合器的高效分散功能进行低聚物的乳化。有效提升了产品质量的稳定性,确保后续乳化釜设备运行平稳,杜绝安全隐患,同时大大降低了乳化釜电机的功率。系统整体设计合理,构思巧妙,具有很好的实用性,易于推广应用。 The utility model discloses a polyurethane prepolymer emulsification system. The system adopts a liquid-liquid mixer for continuous emulsification, and utilizes the high-efficiency dispersion function of a static mixer to emulsify oligomers. It effectively improves the stability of product quality, ensures the smooth operation of subsequent emulsification kettle equipment, eliminates potential safety hazards, and greatly reduces the power of the emulsification kettle motor. The overall design of the system is reasonable, ingenious in conception, has good practicability, and is easy to popularize and apply.

附图说明 Description of drawings

图1为本实用新型系统原理图。 Fig. 1 is the schematic diagram of the utility model system.

其中: in:

1、工艺水泵; 1. Process water pump;

2、低聚物泵; 2. Oligomer pump;

3、静态混合器; 3. Static mixer;

4、乳化釜。 4. Emulsification kettle.

具体实施方式 Detailed ways

下面结合附图和实施例对本实用新型进一步的描述。 Below in conjunction with accompanying drawing and embodiment the utility model is further described.

本实用新型公开了聚氨酯预聚体乳化系统,其区别于现有技术在于:所述系统包括一工艺水泵1和一低聚物泵2,工艺水泵1和低聚物泵2的出液端均与静态混合器3的进液端连接,静态混合器3内设有混合腔,混合腔内横向设有至少一根螺旋状搅拌辊,该搅拌辊的表面分布有螺旋纹,便于提升混合效果,且低转速便于控制设备的稳定性,该静态混合器3的出液端与乳化釜4的进液端连接,该低聚物泵2的输送扬程为0.2Mpa-0.4Mpa,工艺水泵1的输送扬程为0.2Mpa-0.4Mpa,该输送扬程能确保低聚物和工艺水在静态混合器的混合腔内高效分散连续乳化。 The utility model discloses a polyurethane prepolymer emulsification system, which is different from the prior art in that: the system includes a process water pump 1 and an oligomer pump 2, and the liquid outlets of the process water pump 1 and the oligomer pump 2 are both It is connected to the liquid inlet end of the static mixer 3, and the static mixer 3 is provided with a mixing chamber, and at least one helical stirring roller is arranged horizontally in the mixing chamber, and the surface of the stirring roller is distributed with spiral patterns, which is convenient for improving the mixing effect. And the low speed is convenient to control the stability of the equipment. The liquid outlet of the static mixer 3 is connected to the liquid inlet of the emulsification tank 4. The conveying head of the oligomer pump 2 is 0.2Mpa-0.4Mpa, and the conveying head of the process water pump 1 The delivery head is 0.2Mpa-0.4Mpa, which can ensure efficient dispersion and continuous emulsification of oligomers and process water in the mixing chamber of the static mixer.

在具体实施时,本系统的工艺原理为:低聚物泵(0.3Mpa) + 工艺水泵(0.3Mpa)+乳化釜,其中,低聚物泵的功率为1.1KW,工艺水泵的功率2.2KW,乳化釜的搅拌功率3KW。 In the specific implementation, the process principle of this system is: oligomer pump (0.3Mpa) + process water pump (0.3Mpa) + emulsification kettle, among which, the power of the oligomer pump is 1.1KW, and the power of the process water pump is 2.2KW. The stirring power of the emulsification tank is 3KW.

以上所述仅是本实用新型的较佳实施例而已,并非对本实用新型做任何形式上的限制,虽然本实用新型已以较佳实施例揭露如上,然而并非用以限定本新型,任何所属技术领域中具有通常知识者,在不脱离本实用新型技术方案的范围内,当可利用上述揭示的技术内容作出些许更动或修饰为等同变化的等效实施例,但凡是未脱离本实用新型技术方案的内容,依据本实用新型的技术实质对以上实施例所作的任何简单修改、等同变化与修饰,均仍属于本实用新型技术方案的范围内。 The above descriptions are only preferred embodiments of the present utility model, and are not intended to limit the utility model in any form. Although the utility model has been disclosed as above with preferred embodiments, it is not intended to limit the utility model, and any associated technology Those who have ordinary knowledge in the field, without departing from the scope of the technical solution of the present utility model, can use the technical content disclosed above to make some changes or modify equivalent embodiments with equivalent changes, but all without departing from the technical solutions of the present utility model The content of the scheme, any simple modification, equivalent change and modification made to the above embodiments according to the technical essence of the utility model still belong to the scope of the technical solution of the utility model.

Claims (1)

1. base polyurethane prepolymer for use as emulsifying systems, it is characterized in that: described system comprises a technique water pump (1) and an oligomer pump (2), technique water pump (1) is all connected with the liquid feeding end of static mixer (3) with the outlet end of oligomer pump (2), static mixer is provided with hybrid chamber in (3), the outlet end of this static mixer (3) is connected with the liquid feeding end of emulsifying kettle (4), the dehvery lift of this oligomer pump (2) is 0.2MPa-0.4MPa, and the dehvery lift of technique water pump (1) is 0.2MPa-0.4MPa.
CN201420829144.3U 2014-12-24 2014-12-24 Base polyurethane prepolymer for use as emulsifying systems Expired - Lifetime CN204395871U (en)

Priority Applications (1)

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Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2017009161A1 (en) * 2015-07-10 2017-01-19 Covestro Deutschland Ag Process and apparatus for continuous production of aqueous polyurethane dispersions
CN106362634A (en) * 2016-11-01 2017-02-01 重庆瑞恩涂料有限公司 Paint production equipment based on multi-stirring cooperative production
CN106422938A (en) * 2016-11-01 2017-02-22 重庆瑞恩涂料有限公司 Multi-stirring-mode paint production system powered by adjustable stabilized voltage source
CN110818881A (en) * 2019-11-22 2020-02-21 万华化学(北京)有限公司 Preparation method of polyurethane ink resin, polyurethane ink resin prepared by preparation method and ink

Cited By (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2017009161A1 (en) * 2015-07-10 2017-01-19 Covestro Deutschland Ag Process and apparatus for continuous production of aqueous polyurethane dispersions
CN107849208A (en) * 2015-07-10 2018-03-27 科思创德国股份有限公司 Method and apparatus for continuous production aqueous polyurethane dispersion
US10752727B1 (en) 2015-07-10 2020-08-25 Covestro Deutschland Ag Process and apparatus for continuous production of aqueous polyurethane dispersions
CN107849208B (en) * 2015-07-10 2021-02-09 科思创德国股份有限公司 Method and device for the continuous production of aqueous polyurethane dispersions
CN106362634A (en) * 2016-11-01 2017-02-01 重庆瑞恩涂料有限公司 Paint production equipment based on multi-stirring cooperative production
CN106422938A (en) * 2016-11-01 2017-02-22 重庆瑞恩涂料有限公司 Multi-stirring-mode paint production system powered by adjustable stabilized voltage source
CN110818881A (en) * 2019-11-22 2020-02-21 万华化学(北京)有限公司 Preparation method of polyurethane ink resin, polyurethane ink resin prepared by preparation method and ink
CN110818881B (en) * 2019-11-22 2021-10-22 万华化学(北京)有限公司 Preparation method of polyurethane ink resin, polyurethane ink resin prepared by preparation method and ink

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Legal Events

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C14 Grant of patent or utility model
GR01 Patent grant
CP03 Change of name, title or address
CP03 Change of name, title or address

Address after: 639 Xiasheng Road, Jinshan District, Shanghai, May 12, 2015

Patentee after: Shanghai Dongrui New Materials Co.,Ltd.

Country or region after: China

Address before: Room 1104, Building 1, No. 1089 Laoweiqing Road, Jinshanwei Town, Jinshan District, Shanghai, December 2010

Patentee before: SHANGHAI DONGRUI CHEMICAL Co.,Ltd.

Country or region before: China

CX01 Expiry of patent term
CX01 Expiry of patent term

Granted publication date: 20150617