CN203751336U - Device for producing nanoscale high-purity zinc powder through distillation method - Google Patents
Device for producing nanoscale high-purity zinc powder through distillation method Download PDFInfo
- Publication number
- CN203751336U CN203751336U CN201420084516.4U CN201420084516U CN203751336U CN 203751336 U CN203751336 U CN 203751336U CN 201420084516 U CN201420084516 U CN 201420084516U CN 203751336 U CN203751336 U CN 203751336U
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- CN
- China
- Prior art keywords
- zinc powder
- crucible
- zinc
- distillation
- purity
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Withdrawn - After Issue
Links
- HCHKCACWOHOZIP-UHFFFAOYSA-N Zinc Chemical compound [Zn] HCHKCACWOHOZIP-UHFFFAOYSA-N 0.000 title claims abstract description 46
- 238000004821 distillation Methods 0.000 title claims abstract description 24
- 238000000034 method Methods 0.000 title abstract 2
- 230000006698 induction Effects 0.000 claims abstract description 14
- 238000001816 cooling Methods 0.000 claims abstract description 8
- 238000005485 electric heating Methods 0.000 claims abstract description 8
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 7
- 230000004927 fusion Effects 0.000 claims description 7
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 claims description 6
- 206010020843 Hyperthermia Diseases 0.000 claims description 6
- PNEYBMLMFCGWSK-UHFFFAOYSA-N aluminium oxide Inorganic materials [O-2].[O-2].[O-2].[Al+3].[Al+3] PNEYBMLMFCGWSK-UHFFFAOYSA-N 0.000 claims description 6
- 239000010425 asbestos Substances 0.000 claims description 6
- 230000036031 hyperthermia Effects 0.000 claims description 6
- 238000009413 insulation Methods 0.000 claims description 6
- 229910052895 riebeckite Inorganic materials 0.000 claims description 6
- 229910001220 stainless steel Inorganic materials 0.000 claims description 6
- 239000010935 stainless steel Substances 0.000 claims description 6
- 239000010439 graphite Substances 0.000 claims description 5
- 229910002804 graphite Inorganic materials 0.000 claims description 5
- 230000009970 fire resistant effect Effects 0.000 claims description 4
- 238000010992 reflux Methods 0.000 claims description 3
- 229910010271 silicon carbide Inorganic materials 0.000 claims description 3
- 239000000203 mixture Substances 0.000 claims description 2
- 229910052725 zinc Inorganic materials 0.000 abstract description 13
- 239000011701 zinc Substances 0.000 abstract description 13
- 238000005265 energy consumption Methods 0.000 abstract description 4
- 239000000463 material Substances 0.000 abstract description 3
- 229910052751 metal Inorganic materials 0.000 abstract description 3
- 239000002184 metal Substances 0.000 abstract description 3
- 238000009835 boiling Methods 0.000 abstract description 2
- 238000010438 heat treatment Methods 0.000 abstract description 2
- 239000012535 impurity Substances 0.000 abstract description 2
- 238000004519 manufacturing process Methods 0.000 abstract description 2
- 238000002844 melting Methods 0.000 abstract description 2
- 230000008018 melting Effects 0.000 abstract description 2
- 238000013021 overheating Methods 0.000 abstract 2
- 238000007782 splat cooling Methods 0.000 abstract 1
- 239000003517 fume Substances 0.000 description 4
- 239000004927 clay Substances 0.000 description 2
- 210000000481 breast Anatomy 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 238000009834 vaporization Methods 0.000 description 1
- 230000008016 vaporization Effects 0.000 description 1
Landscapes
- Heat Treatment Of Water, Waste Water Or Sewage (AREA)
- Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)
- Manufacture And Refinement Of Metals (AREA)
Abstract
A device for producing nanoscale high-purity zinc powder through a distillation method is characterized by comprising an induction type electric heating crucible distillation furnace, a backflow disc, a high-temperature overheating disc, a zinc powder condenser and a closed type water cooling tower, wherein materials can be continuously fed to the induction type electric heating crucible distillation furnace. Molten zinc obtained after metal zinc ingots are melted through a melting crucible absorbs energy in a distillation crucible to be vaporized and distillated, zinc steam enters the backflow disc, high-boiling-point impurities are removed, pure zinc steam enters the overheating disc for secondary heating, overheated zinc steam higher than the zinc boiling point directly enters the zinc powder condenser for splat cooling, little part of generated zinc powder is micron-order high-purity zinc powder, most generated zinc powder is nanoscale high-purity zinc powder, the granularity of the zinc powder can be controlled between 50 nm and 100 nm, and the purity is more than 99.999%. Materials can be evenly added, the zinc powder can be continuously produced, production pollution is avoided, energy consumption is low, and the automation degree is high.
Description
Technical field
The utility model relates to a kind of metal melting equipment, and particularly a kind of way of distillation is produced nanoscale high-purity zinc powder device.
Background technology
At present, what the equipment of production super-fine zinc dust generally adopted is flame-insulating type reverberatory furnace, tower retort, and all, not to pure zinc fume secondary heat patching device, the zinc powder of producing can not reach nanoscale, and energy consumption is high, it is large to pollute, automaticity is low.
Summary of the invention
The purpose of this utility model is in order to overcome above-mentioned weak point, and provides a kind of product purity high, and energy consumption is low, pollution-free, and the way of distillation that automaticity is high is produced nanoscale high-purity zinc powder device.
For achieving the above object, the technical solution adopted in the utility model is: a kind of way of distillation is produced nanoscale high-purity zinc powder device, it is characterized in that by induction type electric heating crucible retort that can continuous charging, reflux and hyperthermia and superheating dish, zinc powder condenser, enclosed water-cooling tower composition, induction type electric heating crucible retort that wherein can continuous charging comprises the distillation crucible of building upper cover, distillation crucible crucible is external coatedly successively has a high-alumina refractory heat-insulation layer, asbestos layer, coreless induction furnace coil, on cover and have charge door, steam output duct, on the charge door lower end that covers connect fusion crucible upper port, discharge opening is arranged at fusion crucible bottom, at the bottom of crucible, cover along 300mm～350mm apart from distilling on crucible.Backflow and hyperthermia and superheating dish comprise by bottom being that carborundum return tray, top are the tower tray that the overheated dish of graphite is connected, return tray disk body is coated successively outward fire-resistant mud layer, a stainless steel casing, and overheated dish disk body is coated successively outward high-alumina refractory heat-insulation layer, asbestos layer, coreless induction furnace coil, a stainless steel casing.The steam output duct output that distillation covers on crucible is communicated with return tray lower end, and overheated dish upper end is communicated with the charging aperture of zinc powder condenser, the link connection corresponding with enclosed water-cooling tower respectively of the hot water of zinc powder condenser, cold water link.
The utility model is owing to adopting above design, when use, the metallic zinc liquid of metal zinc ingot after fusion crucible fusing absorbs energy vaporization distillation in distillation crucible, zinc fume enters return tray through steam output duct, remove high-boiling-point impurity, pure zinc fume enters overheated dish and carries out secondary concurrent heating, directly enter and in zinc powder condenser, carry out chilling higher than the overheated zinc fume of zinc boiling point, it is the energy that zinc powder discharges that enclosed water-cooling tower is taken away zinc vapor condensing in time, the zinc powder of output seldom part is micron order high-purity zinc powder, the overwhelming majority is nanoscale high-purity zinc powder, product granularity is controlled at 50nm～100nm, purity is up to more than 99.999%, the continuous output of can evenly feeding in raw material, produce pollution-free, energy consumption is low, automaticity is high.
Brief description of the drawings
Fig. 1 is the utility model example structure schematic diagram.
Detailed description of the invention
Now illustrated embodiment is made detailed description to the utility model by reference to the accompanying drawings.
As shown in Figure 1, a kind of way of distillation is produced nanoscale high-purity zinc powder device, by induction type electric heating crucible retort that can continuous charging, reflux and hyperthermia and superheating dish, zinc powder condenser 1, enclosed water-cooling tower 2 forms, induction type electric heating crucible retort that wherein can continuous charging comprises that the clay graphite distillation crucible 4 of the upper cover 3 being built up by fire-resistant pouring material is arranged at top, distillation crucible 4 crucibles are external coatedly successively has a high-alumina refractory heat-insulation layer 5, asbestos flaggy 6, coreless induction furnace coil 7, on upper cover 3, have charge door 8, steam output duct 9, breast hole 10, charge door 8 lower ends on upper cover 3 connect clay graphite fusion crucible 11 upper port, discharge opening 12 is arranged at fusion crucible 11 bottoms, at the bottom of crucible apart from distillation crucible 4 upper covers 3 along 300mm.Backflow and hyperthermia and superheating dish comprise by bottom being that carborundum return tray 13, top are the tower tray that the overheated dish 14 of graphite is connected, return tray 13 disk bodies are coated successively outward fire-resistant mud layer 15, a stainless steel casing 16, and overheated dish 14 disk bodies are coated successively outward high-alumina refractory heat-insulation layer 17, asbestos layer 18, coreless induction furnace coil 19, a stainless steel casing 16.Steam output duct 9 outputs on distillation crucible 4 upper covers 3 are communicated with return tray 13 lower ends, and overheated dish 14 upper ends are communicated with the charging aperture of zinc powder condenser 1, the link connection corresponding with enclosed water-cooling tower 2 respectively of the hot water of zinc powder condenser 1, cold water link.
Claims (1)
1. a way of distillation is produced nanoscale high-purity zinc powder device, it is characterized in that by induction type electric heating crucible retort that can continuous charging, reflux and hyperthermia and superheating dish, zinc powder condenser (1), enclosed water-cooling tower (2) composition, induction type electric heating crucible retort that wherein can continuous charging comprises the distillation crucible (4) of building upper cover (3), distillation crucible (4) crucible is external coatedly successively has a high-alumina refractory heat-insulation layer (5), asbestos layer (6), coreless induction furnace coil (7), on upper cover (3), have charge door (8), steam output duct (9), charge door (8) lower end on upper cover (3) connects fusion crucible (11) upper port, discharge opening (12) is arranged at fusion crucible (11) bottom, upper along 300mm～350mm apart from distillation crucible (4) upper cover (3) at the bottom of crucible, backflow and hyperthermia and superheating dish comprise that by bottom be carborundum return tray (13), top is the tower tray that the overheated dish of graphite (14) is connected, return tray (13) disk body is coated successively outward a fire-resistant mud layer (15), stainless steel casing (16), overheated dish (14) disk body is coated successively outward a high-alumina refractory heat-insulation layer (17), asbestos layer (18), coreless induction furnace coil (19), stainless steel casing (16), steam output duct (9) output on distillation crucible (4) upper cover (3) is communicated with return tray (13) lower end, overheated dish (14) upper end is communicated with the charging aperture of zinc powder condenser (1), the hot water of zinc powder condenser (1), the cold water link respectively link corresponding with enclosed water-cooling tower (2) connects.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201420084516.4U CN203751336U (en) | 2014-02-27 | 2014-02-27 | Device for producing nanoscale high-purity zinc powder through distillation method |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201420084516.4U CN203751336U (en) | 2014-02-27 | 2014-02-27 | Device for producing nanoscale high-purity zinc powder through distillation method |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN203751336U true CN203751336U (en) | 2014-08-06 |
Family
ID=51246647
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201420084516.4U Withdrawn - After Issue CN203751336U (en) | 2014-02-27 | 2014-02-27 | Device for producing nanoscale high-purity zinc powder through distillation method |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN203751336U (en) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103862057A (en) * | 2014-02-27 | 2014-06-18 | 赵志强 | Device for producing nano-scale high-purity zinc powder by distillation method |
| CN106756094A (en) * | 2016-12-27 | 2017-05-31 | 湖南金马冶金技术开发有限公司 | Zinc distillation furnace |
-
2014
- 2014-02-27 CN CN201420084516.4U patent/CN203751336U/en not_active Withdrawn - After Issue
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103862057A (en) * | 2014-02-27 | 2014-06-18 | 赵志强 | Device for producing nano-scale high-purity zinc powder by distillation method |
| CN103862057B (en) * | 2014-02-27 | 2015-12-30 | 赵志强 | The way of distillation produces nanoscale high-purity zinc powder device |
| CN106756094A (en) * | 2016-12-27 | 2017-05-31 | 湖南金马冶金技术开发有限公司 | Zinc distillation furnace |
| CN106756094B (en) * | 2016-12-27 | 2018-10-23 | 湖南金马冶金技术开发有限公司 | Zinc distillation furnace |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| AV01 | Patent right actively abandoned |
Granted publication date: 20140806 Effective date of abandoning: 20151230 |
|
| C25 | Abandonment of patent right or utility model to avoid double patenting |