CN203610112U - Control and regulating system for coupling reactions - Google Patents
Control and regulating system for coupling reactions Download PDFInfo
- Publication number
- CN203610112U CN203610112U CN201320661422.4U CN201320661422U CN203610112U CN 203610112 U CN203610112 U CN 203610112U CN 201320661422 U CN201320661422 U CN 201320661422U CN 203610112 U CN203610112 U CN 203610112U
- Authority
- CN
- China
- Prior art keywords
- reactor
- pipeline
- regulating system
- flowmeter
- tank
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
Links
- 238000005859 coupling reaction Methods 0.000 title claims abstract description 19
- 230000001105 regulatory effect Effects 0.000 title claims abstract description 17
- 238000006243 chemical reaction Methods 0.000 claims abstract description 8
- 239000012954 diazonium Substances 0.000 claims description 15
- IJGRMHOSHXDMSA-UHFFFAOYSA-O diazynium Chemical compound [NH+]#N IJGRMHOSHXDMSA-UHFFFAOYSA-O 0.000 claims description 15
- 239000000463 material Substances 0.000 claims description 15
- 230000001276 controlling effect Effects 0.000 claims description 12
- 238000011144 upstream manufacturing Methods 0.000 claims description 6
- 238000012544 monitoring process Methods 0.000 claims description 3
- 239000002994 raw material Substances 0.000 claims description 3
- 238000004519 manufacturing process Methods 0.000 abstract description 2
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 abstract 6
- 239000012768 molten material Substances 0.000 abstract 3
- 229910052757 nitrogen Inorganic materials 0.000 abstract 3
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 abstract 1
- 239000001257 hydrogen Substances 0.000 abstract 1
- 229910052739 hydrogen Inorganic materials 0.000 abstract 1
- 238000000034 method Methods 0.000 description 2
- 230000009286 beneficial effect Effects 0.000 description 1
- 238000010168 coupling process Methods 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 239000012860 organic pigment Substances 0.000 description 1
- 239000000049 pigment Substances 0.000 description 1
Images
Landscapes
- Physical Or Chemical Processes And Apparatus (AREA)
Abstract
A control and regulating system for coupling reactions comprises a reaction kettle, a molten material tank and a heavy nitrogen tank, wherein the molten material tank is connected with the reaction kettle through a pipeline I, and a flowmeter I and a regulating valve I are arranged on the pipeline I; the heavy nitrogen tank is connected with the reaction kettle through a pipeline II, and a flowmeter II and a regulating valve II are arranged on the pipeline II; a PH (power of hydrogen) instrument is arranged at the upper end of the reaction kettle and connected with a circulating pipeline, and the other end of the circulating pipeline is connected to the reaction kettle. According to the control and regulating system, PH changes in the reaction kettle can be monitored accurately and dynamically, automatic control on addition quantities of molten materials and heavy nitrogen is realized, the coupling reactions are performed smoothly, and the working and production efficiency is improved.
Description
Technical field
The utility model belongs to pigment and makes field, is specifically related to a kind of coupling reaction controlling and regulating system.
Background technology
The significant process that coupling reaction is made as organic pigment.In coupling reaction process, for the control of material and diazonium addition, affect to a certain extent carrying out smoothly of coupling reaction.Existing coupling reaction controlling and regulating system is often difficult to automatic accurate control material and the addition of diazonium.
Summary of the invention
The purpose of this utility model is to provide a kind of coupling reaction controlling and regulating system, and it is reasonable in design, has realized the addition of automatic control material and diazonium.
The technical solution of the utility model is: a kind of coupling reaction controlling and regulating system, comprises reactor, material tank, diazonium tank; Described material tank is connected by pipeline one with reactor, and described pipeline one is provided with flowmeter one, control valve one; Described diazonium tank is connected by pipeline two with reactor, and described pipeline two is provided with flowmeter two, control valve two; The upper end of described reactor is provided with PH instrument, and described PH instrument is connected with circulating line, and the other end of described circulating line is connected to reactor.
As preferably, the other end of described circulating line is connected to the bottom of reactor.
Further, described circulating line is provided with circulating pump, enters circulating line for the raw material in abstraction reaction still, and then guarantees accuracy, the real-time of PH data that instrument is surveyed, the dynamic change of pH value in monitoring reactor.
The upper end of described reactor is connected with pipeline one, and material tank is located at the top of reactor.
The upper end of described reactor is connected with pipeline two, and diazonium tank is located at the top of reactor.
Described flowmeter one is located at the upstream of control valve one; Described flowmeter two is located at the upstream of control valve two.
Beneficial effect: the pH value that the utility model can accurately, dynamically be monitored in reactor changes, and has realized the addition of automatic control material and diazonium, has guaranteed carrying out smoothly of coupling reaction, work production efficiency is improved.
Accompanying drawing explanation
Fig. 1 is the structural representation of the utility model embodiment.
In figure 1, reactor, 2, material tank, 21, pipeline one, 22, flowmeter one, 23, control valve one, 3, diazonium tank, 31, pipeline two, 32, flowmeter two, 33, control valve two, 4, PH instrument, 5, circulating line, 6, circulating pump.
The specific embodiment
Below in conjunction with drawings and Examples, the utility model is described further.
As shown in Figure 1, a kind of coupling reaction controlling and regulating system, comprises reactor 1, material tank 2, diazonium tank 3; Described material tank 2 is connected by pipeline 1 with reactor 1, and described pipeline 1 is provided with flowmeter 1, control valve 1; Described diazonium tank 3 is connected by pipeline 2 31 with reactor 1, and described pipeline 2 31 is provided with flowmeter 2 32, control valve 2 33; The upper end of described reactor 1 is provided with PH instrument 4, and described PH instrument 4 is connected with circulating line 5, and the other end of described circulating line 5 is connected to the bottom of reactor 1, and described circulating line 5 is provided with circulating pump 6.
Circulating pump is delivered to PH instrument by the raw material in reactor by circulating line, has realized dynamic pH value monitoring.
Further, the upper end of described reactor is connected with pipeline one, and material tank is located at the top of reactor; The upper end of described reactor is connected with pipeline two, and diazonium tank is located at the top of reactor.
Described flowmeter one is located at the upstream of control valve one; Described flowmeter two is located at the upstream of control valve two.
According to coupling process requirement, set the value of PH instrument; In the time that the material in reactor is excessive, the data that flowmeter one measures are excessive, control valve one flow automatic regulation; In the time that the diazonium in reactor is excessive, the data that flowmeter two measures are excessive, control valve two flow automatic regulations.
Above-described embodiment is only for clearly illustrating the utility model; and be not the restriction to the utility model embodiment; here exhaustive without also giving all embodiments, and these belong to apparent variation or the variation that connotation of the present utility model extends out and still belong to protection domain of the present utility model.
Claims (6)
1. a coupling reaction controlling and regulating system, comprises reactor, material tank, diazonium tank; It is characterized in that: described material tank is connected by pipeline one with reactor, described pipeline one is provided with flowmeter one, control valve one; Described diazonium tank is connected by pipeline two with reactor, and described pipeline two is provided with flowmeter two, control valve two; The upper end of described reactor is provided with PH instrument, and described PH instrument is connected with circulating line, and the other end of described circulating line is connected to reactor.
2. a kind of coupling reaction controlling and regulating system according to claim 1, is characterized in that: the other end of described circulating line is connected to the bottom of reactor.
3. a kind of coupling reaction controlling and regulating system according to claim 2, it is characterized in that: described circulating line is provided with circulating pump, enter circulating line for the raw material in abstraction reaction still, and then accuracy, the real-time of assurance PH data that instrument is surveyed, the dynamic change of pH value in monitoring reactor.
4. a kind of coupling reaction controlling and regulating system according to claim 1, is characterized in that: the upper end of described reactor is connected with pipeline one, and material tank is located at the top of reactor.
5. a kind of coupling reaction controlling and regulating system according to claim 1, is characterized in that: the upper end of described reactor is connected with pipeline two, and diazonium tank is located at the top of reactor.
6. a kind of coupling reaction controlling and regulating system according to claim 1, is characterized in that: described flowmeter one is located at the upstream of control valve one; Described flowmeter two is located at the upstream of control valve two.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201320661422.4U CN203610112U (en) | 2013-10-24 | 2013-10-24 | Control and regulating system for coupling reactions |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201320661422.4U CN203610112U (en) | 2013-10-24 | 2013-10-24 | Control and regulating system for coupling reactions |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN203610112U true CN203610112U (en) | 2014-05-28 |
Family
ID=50762793
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201320661422.4U Expired - Fee Related CN203610112U (en) | 2013-10-24 | 2013-10-24 | Control and regulating system for coupling reactions |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN203610112U (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105413618A (en) * | 2015-11-25 | 2016-03-23 | 郑臣钏 | Chemical reaction device capable of detecting pH value of solution in real time and containing solution conveniently |
-
2013
- 2013-10-24 CN CN201320661422.4U patent/CN203610112U/en not_active Expired - Fee Related
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105413618A (en) * | 2015-11-25 | 2016-03-23 | 郑臣钏 | Chemical reaction device capable of detecting pH value of solution in real time and containing solution conveniently |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN203610112U (en) | Control and regulating system for coupling reactions | |
| CN203474964U (en) | Automatic liquid supplement device in polycrystalline silicon wafer etching | |
| CN204498846U (en) | Nutrient solution feeding device in a kind of Asparagus incubation | |
| CN203540497U (en) | Quantitative feeding system of liquid material | |
| CN202666807U (en) | Device for adding liquid automatically under pressure | |
| CN202097843U (en) | Automatic sewage weighing device | |
| CN204881734U (en) | Rotor flow meter fixing device | |
| CN203705966U (en) | Intelligent flow measuring and controlling apparatus | |
| CN206404740U (en) | A kind of industrial chemicals continuous feed system | |
| CN202252304U (en) | Direct through valve with indicating scales | |
| CN202191900U (en) | Reaction kettle device | |
| CN203627260U (en) | Pump outlet differential pressure regulating device | |
| CN203249726U (en) | Oil pressure sensing device for diesel engine | |
| CN206679641U (en) | A kind of storage tank with metering device | |
| CN204644306U (en) | Combustion gas in Biomass Gasification & Power Generation device is for amount automatic control system | |
| CN203565017U (en) | Automatic acid preparation device during production of furfural | |
| CN203342417U (en) | Cooling control system of esterification separation column | |
| CN203710740U (en) | Oil and water separation detection system applied to fine chemical production line | |
| CN202238963U (en) | Improved water tank of wire drawing machine | |
| CN203350726U (en) | Cooling material receiving pipe control system of esterification knockout tower | |
| CN203350727U (en) | Liquid level control system of second drainage receiver | |
| CN203342753U (en) | Heating medium feeding pipeline control system of esterification device | |
| CN205995421U (en) | A device for automatically adjusting reflux of propylene | |
| CN203350728U (en) | Liquid level control system of first drainage receiver used for material receiving of first drainage receiver | |
| CN205748517U (en) | One feeds intake metering device |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20140528 Termination date: 20171024 |
|
| CF01 | Termination of patent right due to non-payment of annual fee |