CN203291553U - Rotary type ultrasonic frequency biological active ingredient extracting device - Google Patents
Rotary type ultrasonic frequency biological active ingredient extracting device Download PDFInfo
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- CN203291553U CN203291553U CN2013203364886U CN201320336488U CN203291553U CN 203291553 U CN203291553 U CN 203291553U CN 2013203364886 U CN2013203364886 U CN 2013203364886U CN 201320336488 U CN201320336488 U CN 201320336488U CN 203291553 U CN203291553 U CN 203291553U
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- 239000004480 active ingredient Substances 0.000 title claims abstract description 9
- 239000007788 liquid Substances 0.000 claims abstract description 19
- 238000000605 extraction Methods 0.000 claims abstract description 18
- 238000001802 infusion Methods 0.000 claims abstract description 8
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 6
- 238000010438 heat treatment Methods 0.000 abstract description 3
- 238000000034 method Methods 0.000 description 9
- 238000005516 engineering process Methods 0.000 description 7
- 239000002994 raw material Substances 0.000 description 5
- 238000000926 separation method Methods 0.000 description 4
- 239000000126 substance Substances 0.000 description 4
- 238000003756 stirring Methods 0.000 description 3
- 230000009286 beneficial effect Effects 0.000 description 2
- 229930014626 natural product Natural products 0.000 description 2
- 239000002893 slag Substances 0.000 description 2
- 230000000975 bioactive effect Effects 0.000 description 1
- 238000003889 chemical engineering Methods 0.000 description 1
- 238000006243 chemical reaction Methods 0.000 description 1
- 238000013375 chromatographic separation Methods 0.000 description 1
- 238000002425 crystallisation Methods 0.000 description 1
- 230000008025 crystallization Effects 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- 238000001035 drying Methods 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 238000001704 evaporation Methods 0.000 description 1
- 230000008020 evaporation Effects 0.000 description 1
- 238000001914 filtration Methods 0.000 description 1
- 239000012535 impurity Substances 0.000 description 1
- 239000004615 ingredient Substances 0.000 description 1
- 239000012528 membrane Substances 0.000 description 1
- 238000000874 microwave-assisted extraction Methods 0.000 description 1
- 238000000199 molecular distillation Methods 0.000 description 1
- 230000001766 physiological effect Effects 0.000 description 1
- 238000001556 precipitation Methods 0.000 description 1
- 238000002360 preparation method Methods 0.000 description 1
- 238000000746 purification Methods 0.000 description 1
- 238000007670 refining Methods 0.000 description 1
- 239000011347 resin Substances 0.000 description 1
- 229920005989 resin Polymers 0.000 description 1
- 238000001179 sorption measurement Methods 0.000 description 1
- 238000000194 supercritical-fluid extraction Methods 0.000 description 1
- 238000002604 ultrasonography Methods 0.000 description 1
- 238000002137 ultrasound extraction Methods 0.000 description 1
- 238000005406 washing Methods 0.000 description 1
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Abstract
一种旋转式超音频生物有效成分提取装置,包括罐体(8)、超音频发生器(7)和控制器(4),罐体带有盖(1),该盖外安装有带阀门的滴液漏斗(2)、搅拌器的电机(3)、温度感应器(5)和控制器(4),搅拌器的搅杆(6)上安装有至少一个超音频发生器(7),控制器通过导线与电机、超音频发生器和温度感应器连接,罐体底部有带阀门的输液管与接液瓶(9)相连,该接液瓶底部有带阀门的出液口(10),接液瓶与滴液漏斗之间有带水泵(11)的循环输液管(12)相连。采用本装置进行提取具有操作与加热方便、提取充分等优点。
A rotary ultrasonic audio biological active ingredient extraction device, including a tank (8), an ultrasonic generator (7) and a controller (4), the tank has a cover (1), and the cover is equipped with a valve The motor (3) of the dropping funnel (2), the stirrer, the temperature sensor (5) and the controller (4), and at least one supersound generator (7) is installed on the stirrer (6) of the stirrer, and the control The device is connected with the motor, the supersound frequency generator and the temperature sensor through wires, and the infusion tube with a valve at the bottom of the tank is connected with the liquid receiving bottle (9), and the bottom of the liquid receiving bottle has a liquid outlet (10) with a valve. A circulation infusion tube (12) with a water pump (11) is arranged between the liquid receiving bottle and the dropping funnel to link to each other. Using the device for extraction has the advantages of convenient operation and heating, sufficient extraction and the like.
Description
【技术领域】【Technical field】
本实用新型涉及一种运用超音频提取生物体或生物物质中的有效成分的装置。The utility model relates to a device for extracting effective components in living organisms or biological substances by using supersonic sound.
【背景技术】【Background technique】
生物有效成分提取工艺是运用化学工程原理和方法对组成生物的化学物质进行提取、分离纯化的过程。生物有效成分组成复杂且不稳定,因此提取困难。生物有效成分的提取几乎都在溶液中进行,各种参数对溶液中各组分的综合影响常无法固定,为了保护所提取物质的生理活性及结构上的完全,传统的提取方法多采用温和的“多阶式”方法,目前生物有效成分传统分离纯化的提取方法有提取法、萃取法、微波提取、超声波提取、过滤、蒸发浓缩、沉淀法、结晶、干燥等,新型分离技术有树脂吸附分离技术、膜分离技术、分子蒸馏技术、超临界流体萃取技术、色谱分离技术等,这些方法成本不高,且提取物的有效成分含量较高,有利于进一步精制,所以一直被广泛使用,但这样的提取方式通常有以下几个缺点:(1)会引入其他杂质;(2)装置复杂、不够简便;(3)步骤繁琐,操作时间长;(4)整个过程需要另用水浴加热装置加热。本发明引入了超音频处理技术,装置简单,自动化程度高,效率高且提取效果好。超音频在处理过程中可自行升温加热,温度还可以通过调节功率来调温。且本装置把搅拌装置和超音频装置合二为一,简便装置。在旋动中扩大原料的接触深度和广度,反应更充分,利于提高提取率。目前,超音频装置用于生物有效成分的提取还未见报道。The extraction process of biological active components is the process of extracting, separating and purifying the chemical substances that make up organisms by using the principles and methods of chemical engineering. Bioactive ingredients are complex and unstable, so extraction is difficult. The extraction of biologically effective components is almost always carried out in the solution, and the comprehensive influence of various parameters on the components in the solution is often unable to be fixed. In order to protect the physiological activity and structural integrity of the extracted substances, traditional extraction methods mostly use mild "Multi-stage" method. At present, the extraction methods of traditional separation and purification of biological active ingredients include extraction method, extraction method, microwave extraction, ultrasonic extraction, filtration, evaporation concentration, precipitation method, crystallization, drying, etc. New separation technologies include resin adsorption separation technology, membrane separation technology, molecular distillation technology, supercritical fluid extraction technology, chromatographic separation technology, etc. These methods are not high in cost, and the content of active ingredients in the extract is high, which is conducive to further refining, so they have been widely used, but such methods The extraction method usually has the following disadvantages: (1) other impurities will be introduced; (2) the device is complicated and not simple enough; (3) the steps are cumbersome and the operation time is long; (4) the whole process needs to be heated by a water bath heating device. The invention introduces super audio frequency processing technology, has simple device, high degree of automation, high efficiency and good extraction effect. Ultrasound can heat up and heat up by itself during processing, and the temperature can also be adjusted by adjusting the power. And the device combines the stirring device and the supersonic device into one, which is easy to install. Enlarging the contact depth and breadth of the raw materials during the rotation, the reaction is more sufficient, and it is beneficial to improve the extraction rate. At present, there is no report on the use of ultrasonic devices for the extraction of biologically effective components.
【发明内容】【Content of invention】
本实用新型要解决的技术问题是提供一种超音频提取生物有效成分的装置。The technical problem to be solved by the utility model is to provide a device for extracting biologically effective components by supersonic audio.
解决上述技术问题采用如下技术方案:To solve the above technical problems, the following technical solutions are adopted:
本提取天然产物的超音频处理装置,包括罐体、超音频发生器和控制器,其特征是罐体带有盖,该盖外安装有带阀门的滴液漏斗、搅拌器的电机、温度感应器和控制器,搅拌器的搅杆上安装有至少一个超音频发生器,控制器通过导线与电机、超音频发生器和温度感应器连接,罐体底部有带阀门的输液管与接液瓶相连,该接液瓶底部有带阀门的出液口,接液瓶与滴液漏斗之间有带水泵的循环输液管相连。The supersound frequency processing device for extracting natural products includes a tank body, a supersonic frequency generator and a controller, and is characterized in that the tank body has a cover, and a dropping funnel with a valve, a motor of a stirrer, a temperature sensor, etc. are installed on the outside of the cover. At least one supersound generator is installed on the stirrer of the stirrer, the controller is connected with the motor, supersonic generator and temperature sensor through wires, and there are infusion tubes and liquid receiving bottles with valves at the bottom of the tank There is a liquid outlet with a valve at the bottom of the liquid receiving bottle, and a circulating infusion tube with a water pump is connected between the liquid receiving bottle and the dropping funnel.
本实用新型的有益效果是:装置结构简单,操作与加热方便,提取充分,提取物浓度高。The beneficial effects of the utility model are: the device has simple structure, convenient operation and heating, sufficient extraction and high extract concentration.
【附图说明】【Description of drawings】
附图为本实用新型的配套装置结构示意图。Accompanying drawing is the structural schematic diagram of supporting device of the present utility model.
【具体实施方式】【Detailed ways】
本实用新型下面结合实例并参照附图予以详述:The utility model is described in detail below in conjunction with examples and with reference to the accompanying drawings:
包括罐体8、超音频发生器7和控制器4,其特征是罐体带有盖1,该盖外安装有带阀门的滴液漏斗2、搅拌器的电机3、温度感应器5和控制器4,搅拌器的搅杆6上安装有至少一个超音频发生器7,控制器通过导线与电机、超音频发生器和温度感应器连接,罐体底部有带阀门的输液管与接液瓶9相连,该接液瓶底部有带阀门的出液口10,接液瓶与滴液漏斗之间有带水泵11的循环输液管12相连。It includes a tank body 8, an ultrasonic audio generator 7 and a controller 4, and is characterized in that the tank body has a cover 1, and the cover is equipped with a dropping funnel 2 with a valve, a motor 3 of the stirrer, a temperature sensor 5 and a control panel. At least one supersound generator 7 is installed on the stirrer 6 of the stirrer, the controller is connected with the motor, the supersonic generator and the temperature sensor through wires, and there is an infusion tube with a valve and a liquid receiving bottle at the bottom of the tank 9 connected to each other, the bottom of the liquid receiving bottle has a liquid outlet 10 with a valve, and a circulating infusion tube 12 with a water pump 11 is connected between the liquid receiving bottle and the dropping funnel.
采用本旋转式超音频生物有效成分提取装置进行提取的方法按如下步骤进行:The method for extracting by using this rotary supersound frequency biological active ingredient extraction device is carried out as follows:
(1)前期准备:生物体或生物物质的收集、清洗、沥干后的切细或粉碎,按生物原料与提取液的重量比为1∶1准备好提取液;(1) Preliminary preparation: collecting, washing, draining, shredding or crushing of organisms or biological substances, and preparing the extract according to the weight ratio of the biological raw material to the extract as 1:1;
(2)原料的投入开机:将生物原料与提取液投入罐体后即开机;(2) Raw material input and start-up: put the biological raw material and extract into the tank and then start the machine;
(3)有效成分的提取:搅拌采用慢速或中慢速,温度控制60-120℃,常压下搅拌20-90min后,虹吸出液至接液瓶内;一次提取有效成分较彻底的掀盖取出罐体内的渣,为处理下一批做准备;不彻底的则保留渣,再从滴液漏斗上方进液口加入新的提取液,重复本步骤的工作,或启动水泵将接液瓶中的有效成分提取液泵入罐体内,重复本步骤的工作;(3) Extraction of active ingredients: Stir at a slow or medium-slow speed, control the temperature at 60-120°C, and stir for 20-90 minutes under normal pressure, then siphon the liquid into the liquid-receiving bottle; once the active ingredients are extracted thoroughly Take out the slag in the tank with the cover to prepare for the next batch; keep the slag if it is not thorough, and then add new extract from the liquid inlet above the dropping funnel, repeat this step, or start the water pump to remove the liquid from the bottle The active ingredient extract in the pump is pumped into the tank, and the work of this step is repeated;
(4)提取天然产物的深度处理:原料量少或提取物浓度要求低用单罐外加循环装置处理;否则用多罐串联处理。(4) Advanced treatment for extracting natural products: If the amount of raw materials is small or the concentration of the extract is low, use a single tank plus a circulation device for processing; otherwise, use multiple tanks for series processing.
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Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN104833188A (en) * | 2015-04-08 | 2015-08-12 | 湖北民族学院 | Extracting and drying device for effective constituents in nature product |
CN107213668A (en) * | 2017-08-07 | 2017-09-29 | 山东大学 | With reference to the ultrasonic wave and microwave cooperating extraction element and method of turbulence effect |
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Cited By (3)
Publication number | Priority date | Publication date | Assignee | Title |
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CN104833188A (en) * | 2015-04-08 | 2015-08-12 | 湖北民族学院 | Extracting and drying device for effective constituents in nature product |
CN104833188B (en) * | 2015-04-08 | 2017-06-30 | 湖北民族学院 | The extraction drying device of active ingredient in a kind of natural goods |
CN107213668A (en) * | 2017-08-07 | 2017-09-29 | 山东大学 | With reference to the ultrasonic wave and microwave cooperating extraction element and method of turbulence effect |
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Granted publication date: 20131120 Termination date: 20140608 |