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CN203220907U - Glutaraldehyde mixing tank supplementing device - Google Patents

Glutaraldehyde mixing tank supplementing device Download PDF

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Publication number
CN203220907U
CN203220907U CN 201320187466 CN201320187466U CN203220907U CN 203220907 U CN203220907 U CN 203220907U CN 201320187466 CN201320187466 CN 201320187466 CN 201320187466 U CN201320187466 U CN 201320187466U CN 203220907 U CN203220907 U CN 203220907U
Authority
CN
China
Prior art keywords
mixing tank
flash column
coating colors
glutaraldehyde
filter
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
Application number
CN 201320187466
Other languages
Chinese (zh)
Inventor
何友军
谢辛
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Ningxia Jinhong Bio Tech Co ltd
Original Assignee
XIANGYANG CHUTIANYUAN CHEMICAL INDUSTRY Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by XIANGYANG CHUTIANYUAN CHEMICAL INDUSTRY Co Ltd filed Critical XIANGYANG CHUTIANYUAN CHEMICAL INDUSTRY Co Ltd
Priority to CN 201320187466 priority Critical patent/CN203220907U/en
Application granted granted Critical
Publication of CN203220907U publication Critical patent/CN203220907U/en
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

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Abstract

The utility model discloses a glutaraldehyde mixing tank supplementing device. The glutaraldehyde mixing tank supplementing device comprises a mixing tank, a tubular reactor, a filter and a flash column, wherein the discharge end of the mixing tank is connected with the feed end of the tubular reactor; the discharge end of the tubular reactor is connected with the feed end of the filter; the discharge end of the filter is connected with the feed end of the flash column; two feed pipes are connected to the top of the mixing tank; the lower part of the mixing tank is connected with a nitrogen delivery pipe; the upper part of the flash column is connected with a return pipe; the return pipe is connected with the nitrogen delivery pipe. According to the glutaraldehyde mixing tank supplementing device, the return pipe is introduced on the upper part of the flash column and connected with the nitrogen delivery pipe connected to the mixing tank, and unreacted acrolein and methyl ether steamed from the flash column are put into the mixing tank through the return pipe so as to maintain the pressure required by the mixing tank, so that nitrogen is saved, other components are not introduced into the material, and the use ratio of the material is improved.

Description

Glutaraldehyde mixing tank for coating colors ftercompction device
Technical field
The utility model relates to technical field of chemical, more particularly, relates in particular to a kind of glutaraldehyde mixing tank for coating colors ftercompction device.
Background technology
Glutaraldehyde belongs to high effect disinfectants, is widely used in industries such as sterilization, pharmacy.Industrial, usually prepare glutaraldehyde with methacrylaldehyde and methyl ether, because methyl ether exists with gaseous form at normal temperatures, for the mixture that makes methacrylaldehyde and methyl ether miscible mutually, pump into reactor with liquid form by measuring pump, just must pressurize to mixing tank for coating colors, and make mixing tank for coating colors keep the pressure of 0.35~0.4MPa, conventional pressure method is the inflated with nitrogen pressurize of pressurizeing in the mixing tank for coating colors, yet, adopt the nitrogen ftercompction, not only operate cumbersome, the nitrogen consumption is big, also nitrogen can be introduced in the raw material, influences the quality of finished product glutaraldehyde.
The utility model content
The purpose of this utility model is at above-mentioned the deficiencies in the prior art, and a kind of glutaraldehyde mixing tank for coating colors ftercompction device is provided, and the overbottom pressure in the flash column is introduced mixing tank for coating colors, to keep the required pressure of mixing tank for coating colors, saves nitrogen, does not introduce other composition.
For achieving the above object, glutaraldehyde mixing tank for coating colors ftercompction device provided by the utility model, comprise mixing tank for coating colors, tubular reactor, filter, reach flash column, the discharge end of described mixing tank for coating colors links to each other with the feed end of tubular reactor, the discharge end of tubular reactor links to each other with the feed end of filter, the discharge end of filter links to each other with the feed end of flash column, the top of described mixing tank for coating colors is connected with two feed pipes, the bottom is connected with a nitrogen carrier pipe, the top of described flash column is connected with a return duct, and this return duct links to each other with the nitrogen carrier pipe.
The utility model is introduced a return duct on the top of flash column, it is linked to each other with nitrogen carrier pipe on being connected mixing tank for coating colors, by return duct unreacted methacrylaldehyde and the methyl ether that steams in the flash column dropped into mixing tank for coating colors again, overbottom pressure in the flash column is introduced mixing tank for coating colors, to keep the required pressure of mixing tank for coating colors, not only save nitrogen, can not introduce other composition in the raw material, also improved utilization ratio of raw materials simultaneously.
Description of drawings
Fig. 1 is structural representation of the present utility model.
Among the figure: the 1-mixing tank for coating colors; The 11-feed pipe; 12-nitrogen carrier pipe; The 2-tubular reactor; The 3-filter; The 4-flash column; The 5-return duct.
The specific embodiment
The utility model is described in further detail below in conjunction with the embodiment in the accompanying drawing, but do not constitute any restriction of the present utility model.
Consult shown in Figure 1, a kind of glutaraldehyde mixing tank for coating colors ftercompction device provided by the utility model, comprise mixing tank for coating colors 1, tubular reactor 2, filter 3, reach flash column 4, the discharge end of described mixing tank for coating colors 1 links to each other with the feed end of tubular reactor 2, the discharge end of tubular reactor 2 links to each other with the feed end of filter 3, and the discharge end of filter 3 links to each other with the feed end of flash column 4.The top of described mixing tank for coating colors 1 is connected with two feed pipes 11, and the bottom is connected with a nitrogen carrier pipe 12, and the top of described flash column 4 is connected with an inner return duct 5 through antiseptic stainless steel, and this return duct 5 links to each other with nitrogen carrier pipe 12.
The utility model for the production of the time, methacrylaldehyde and methyl ether sent into from two feed pipes 11 at mixing tank for coating colors 1 top respectively carry out batch mixing in the mixing tank for coating colors 1, before flash column 4 does not also have discharging, nitrogen is sent into mixing tank for coating colors 1 by nitrogen carrier pipe 12, give mixing tank for coating colors 1 pressurization, make methacrylaldehyde and methyl ether miscible mutually with liquid form, entering tubular reactor 2 after raw material is miscible reacts in the effect of catalyst, enter after the material that comes out from tubular reactor 2 filters through filter 3 and carry out gas-liquid in the flash column 4 and be separated, in case the discharge end of flash column 4 bottoms has material to flow out, stop immediately to mixing tank for coating colors 1 inflated with nitrogen, directly utilize the unreacted methacrylaldehyde and the methyl ether that in flash column 4, steam to send mixing tank for coating colors 1 back to by return duct 5, keep the required pressure of mixing tank for coating colors 1.
Because the pressure of flash column 4 and mixing tank for coating colors 1 control is close, all be 0.35~0.4MPa, therefore, utilize the unreacted methacrylaldehyde and the methyl ether that steam in the flash column 4 to drop into mixing tank for coating colors 1 again by return duct 5, overbottom pressure in the flash column 4 are introduced mixing tank for coating colors 1, in order to keep the required pressure of mixing tank for coating colors 1, not only saved nitrogen, can not introduce other composition in the raw material, also improve utilization ratio of raw materials simultaneously.

Claims (2)

1. glutaraldehyde mixing tank for coating colors ftercompction device, comprise mixing tank for coating colors, tubular reactor, filter, reach flash column, the discharge end of described mixing tank for coating colors links to each other with the feed end of tubular reactor, the discharge end of tubular reactor links to each other with the feed end of filter, the discharge end of filter links to each other with the feed end of flash column, it is characterized in that: the top of described mixing tank for coating colors is connected with two feed pipes, the bottom is connected with a nitrogen carrier pipe, the top of described flash column is connected with a return duct, and this return duct links to each other with the nitrogen carrier pipe.
2. glutaraldehyde mixing tank for coating colors ftercompction device according to claim 1, it is characterized in that: described return duct is the return duct of stainless steel, it is inner through preservative treatment.
CN 201320187466 2013-04-15 2013-04-15 Glutaraldehyde mixing tank supplementing device Expired - Lifetime CN203220907U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN 201320187466 CN203220907U (en) 2013-04-15 2013-04-15 Glutaraldehyde mixing tank supplementing device

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN 201320187466 CN203220907U (en) 2013-04-15 2013-04-15 Glutaraldehyde mixing tank supplementing device

Publications (1)

Publication Number Publication Date
CN203220907U true CN203220907U (en) 2013-10-02

Family

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Family Applications (1)

Application Number Title Priority Date Filing Date
CN 201320187466 Expired - Lifetime CN203220907U (en) 2013-04-15 2013-04-15 Glutaraldehyde mixing tank supplementing device

Country Status (1)

Country Link
CN (1) CN203220907U (en)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN114950327A (en) * 2022-06-24 2022-08-30 江苏博汇纸业有限公司 Styrene-butadiene latex preparation reation kettle for paper

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN114950327A (en) * 2022-06-24 2022-08-30 江苏博汇纸业有限公司 Styrene-butadiene latex preparation reation kettle for paper

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Legal Events

Date Code Title Description
C14 Grant of patent or utility model
GR01 Patent grant
C56 Change in the name or address of the patentee
CP01 Change in the name or title of a patent holder

Address after: 441048, No. 32, Shun Shun Road, Yu Lake Industrial Park, Xiangcheng Economic Development Zone, Hubei, Xiangfan

Patentee after: HUBEI JINGHONG CHEMICAL Co.,Ltd.

Address before: 441048, No. 32, Shun Shun Road, Yu Lake Industrial Park, Xiangcheng Economic Development Zone, Hubei, Xiangfan

Patentee before: XIANGYANG CHUTIANYUAN CHEMICAL INDUSTRY Co.,Ltd.

TR01 Transfer of patent right
TR01 Transfer of patent right

Effective date of registration: 20221202

Address after: 753299 9 households, including plant 1, No. 98, Shizuishan economic and Technological Development Zone, Huinong District, Shizuishan City, Ningxia Hui Autonomous Region

Patentee after: NINGXIA JINHONG BIO-TECH Co.,Ltd.

Address before: No. 32, Tianshun Avenue, Yujiahu Industrial Park, Xiangcheng Economic Development Zone, Xiangfan City, Hubei Province, 441048

Patentee before: HUBEI JINGHONG CHEMICAL Co.,Ltd.

CX01 Expiry of patent term
CX01 Expiry of patent term

Granted publication date: 20131002