CN203140001U - Reactor for gas chromatographic method analysis - Google Patents
Reactor for gas chromatographic method analysis Download PDFInfo
- Publication number
- CN203140001U CN203140001U CN 201320020965 CN201320020965U CN203140001U CN 203140001 U CN203140001 U CN 203140001U CN 201320020965 CN201320020965 CN 201320020965 CN 201320020965 U CN201320020965 U CN 201320020965U CN 203140001 U CN203140001 U CN 203140001U
- Authority
- CN
- China
- Prior art keywords
- sealing
- reactor
- heater
- flange
- tube
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
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- 238000004458 analytical method Methods 0.000 title claims abstract description 18
- 238000004587 chromatography analysis Methods 0.000 title abstract 5
- 238000007789 sealing Methods 0.000 claims abstract description 24
- 238000010438 heat treatment Methods 0.000 claims abstract description 9
- 238000010276 construction Methods 0.000 claims description 16
- 239000002184 metal Substances 0.000 claims description 6
- 229910052751 metal Inorganic materials 0.000 claims description 6
- 238000006243 chemical reaction Methods 0.000 abstract description 9
- 230000000903 blocking effect Effects 0.000 abstract 1
- 229920003086 cellulose ether Polymers 0.000 description 3
- -1 hydroxy ethoxy, propoxyl Chemical group 0.000 description 3
- 239000000463 material Substances 0.000 description 3
- 238000010586 diagram Methods 0.000 description 2
- 238000006073 displacement reaction Methods 0.000 description 2
- 238000004817 gas chromatography Methods 0.000 description 2
- 239000007788 liquid Substances 0.000 description 2
- 238000000034 method Methods 0.000 description 2
- RYGMFSIKBFXOCR-UHFFFAOYSA-N Copper Chemical compound [Cu] RYGMFSIKBFXOCR-UHFFFAOYSA-N 0.000 description 1
- 241000973497 Siphonognathus argyrophanes Species 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 229910052802 copper Inorganic materials 0.000 description 1
- 239000010949 copper Substances 0.000 description 1
- 230000008878 coupling Effects 0.000 description 1
- 238000010168 coupling process Methods 0.000 description 1
- 238000005859 coupling reaction Methods 0.000 description 1
- 238000005336 cracking Methods 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 238000002474 experimental method Methods 0.000 description 1
- 239000000284 extract Substances 0.000 description 1
- 239000011521 glass Substances 0.000 description 1
- XMBWDFGMSWQBCA-UHFFFAOYSA-N hydrogen iodide Chemical compound I XMBWDFGMSWQBCA-UHFFFAOYSA-N 0.000 description 1
- 229940071870 hydroiodic acid Drugs 0.000 description 1
- 238000009434 installation Methods 0.000 description 1
- 239000003960 organic solvent Substances 0.000 description 1
- 238000012207 quantitative assay Methods 0.000 description 1
- 230000000630 rising effect Effects 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 239000013595 supernatant sample Substances 0.000 description 1
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- Sampling And Sample Adjustment (AREA)
Abstract
The utility model discloses a reactor for gas chromatographic method analysis, relates to the field of chemical reaction instrument, and provides a reactor for gas chromatographic method analysis in good sealing. The reactor for gas chromatographic method analysis comprises a container tube, a sealing structure and a heater, the container tube comprises a tube port, the sealing structure is used for sealing the tube port, the heater is used for heating the container tube, the sealing structure comprises a sealing plug, a pressing cover and a pressing seat, the sealing plug is used for blocking the tube port, the container tube at the outer side of the tube port is provided with a flange, the pressing seat is arranged below the flange, the pressing cover is arranged above the flange and connected with the pressing seat, and the pressing cover is used for pressing the sealing plug. The reactor disclosed by the utility model can be applied to the gas chromatographic method analysis.
Description
Technical field
The utility model relates to a kind of chemical reaction instrument, relates in particular to a kind of reactor for gc analysis.
Background technology
The gas chromatography principle of measuring ethyoxyl, hydroxy ethoxy, propoxyl, methoxyl group, propoxyl group equal size in the cellulose ether is the Cai Saier reaction method, also namely utilize hydroiodic acid at high temperature the above-mentioned substituted radical in the cracking cellulose ether generate corresponding idoalkane, utilize organic solvent that idoalkane is extracted then, drawing the supernatant sample introduction separates in gas chromatograph, idoalkane is carried out quantitative assay, thereby converse the amount of above-mentioned substituted radical in the cellulose ether.
This reaction needed is carried out in test tube, need be to test tube mouth sealing and heating test tube during reaction, and domesticly still do not have reaction tube and a heater that is exclusively used in this gas chromatography.Common test tube and heater have following shortcoming: thereby first, generate a large amount of gas in the course of reaction and cause the rapid rising of pressure to cause reaction tube to break easily or seal failure is leaked; The second, course of reaction needs to carry out under hot conditions, and the temperature uniformity between the control accuracy of heating-up temperature and the different test tube is difficult to guarantee.
The utility model content
The technical problems to be solved in the utility model is: the reactor that is used for gc analysis that a kind of good seal is provided.
For the technical scheme that addresses the above problem employing is: the reactor that is used for gc analysis comprises container tube, hermetically-sealed construction and heater, container tube comprises the mouth of pipe, the hermetically-sealed construction sealing orifice, heater heating container pipe, hermetically-sealed construction comprises sealing-plug, friction top and pressed seat, sealing-plug stops up the mouth of pipe, the container tube in the mouth of pipe outside is provided with flange, pressed seat is positioned at the flange below, and friction top is positioned at the flange top and is connected with pressed seat, and friction top compresses sealing-plug.
Further be: hermetically-sealed construction comprises sealing gasket, and sealing gasket is between rubber stopper and friction top.
Further be: hermetically-sealed construction comprises cushion, and cushion is between flange and pressed seat.
Further be: friction top and pressed seat are threaded.
Further be: heater is that thermostat metal is bathed heater, is provided with the test tube hole in the heater, and container tube is positioned at the test tube hole.
The beneficial effects of the utility model are: above-mentioned sealing device seals the container mouth of pipe, flange has effectively limited the displacement that pressed seat makes progress, and friction top is connected with pressed seat, thereby makes the friction top can be to top offset, guarantee that friction top effectively compresses sealing-plug, avoid gas leakage in the container tube.
Select for use thermostat metal to bathe the heater heating, effectively guarantee each container tube heating-up temperature homogeneous.
Description of drawings:
Fig. 1 is the structure of reactor schematic diagram for gc analysis;
Fig. 2 is container tube and hermetically-sealed construction installation diagram;
Be labeled as among the figure: friction top 1, sealing gasket 2, sealing-plug 3, the mouth of pipe 4, flange 5, container tube 6, cushion 7, pressed seat 8, heater 9.
The specific embodiment
Below in conjunction with the drawings and specific embodiments the utility model is further specified.For a kind of reactor that is used for gc analysis of good seal is provided, the reactor that is used for gc analysis comprises container tube 6, hermetically-sealed construction and heater 9, container tube 6 comprises the mouth of pipe 4, hermetically-sealed construction sealing orifice 4, heater 9 heating container pipes 6, hermetically-sealed construction comprises sealing-plug 3, friction top 1 and pressed seat 8, sealing-plug 3 stops up the mouth of pipe 4, the container tube 6 in the mouth of pipe 4 outsides is provided with flange 5, pressed seat 8 is positioned at flange 5 belows, friction top 1 is positioned at flange 5 tops and is connected with pressed seat 8, and friction top 1 compresses sealing-plug 3.Above-mentioned sealing device line up 4 seals, flange 5 has effectively limited the displacement that pressed seat 8 makes progress, and friction top 1 is connected with pressed seat 8, thereby makes the friction top 1 can be to top offset, guarantee that friction top 1 effectively compresses sealing-plug 3, avoid gas leakage in the container tube 6.The concrete set-up mode of each parts is recommended as follows: container tube 6 is made test tube shaped, and material adopts the high strength glass of thickness 4 ~ 5mm, to improve crushing resistance, avoids container tube 6 to break because internal pressure is too high; Flange 5 has been made one with container tube 6; Sealing-plug 3 is selected rubber stopper for use; Friction top 1 and pressed seat 8 are all selected copper material for use.
Need take out the liquid in the container tube 6 during analysis, take out for convenience, method commonly used is that syringe needle stretches in the container tube 6 and extracts with syringe puncture through seal plug 3.This mode can be destroyed sealing-plug 3, makes sealing-plug 3 be difficult to reuse.In order to save cost, hermetically-sealed construction comprises sealing gasket 2, and sealing gasket 2 is between sealing-plug 3 and friction top 1.During liquid in the evacuation container pipe 6, take off behind the sealing gasket 2 puncture through seal plug 3 again.Sealing gasket 2 only is to cover on the sealing-plug 3, takes off to be easy to.After sealing-plug 3 pierces through, because sealing gasket 2 covers on the sealing-plug, this reactor good seal still when use next time, all parts can both be reused.
In order to guarantee each container tube heating-up temperature homogeneous, heater 9 is bathed heater for thermostat metal, is provided with the test tube hole in the heater 9, and container tube 6 is positioned at the test tube hole.It is prior art that thermostat metal is bathed heater, and sale is arranged on the market, is mainly used in chemical experiment heating test tube, and the advantage of homogeneous heating is arranged.Container tube 6 external diameters make with the test tube hole in can be easily bathe the heater heating with thermostat metal through coupling.
Claims (5)
1. the reactor that is used for gc analysis, comprise container tube (6), hermetically-sealed construction and heater (9), container tube (6) comprises the mouth of pipe (4), hermetically-sealed construction sealing orifice (4), heater (9) heating container pipe (6), it is characterized in that: described hermetically-sealed construction comprises sealing-plug (3), friction top (1) and pressed seat (8), sealing-plug (3) stops up the mouth of pipe (4), the container tube (6) in the mouth of pipe (4) outside is provided with flange (5), pressed seat (8) is positioned at flange (5) below, friction top (1) is positioned at flange (5) top and is connected with pressed seat (8), and friction top (1) compresses sealing-plug (3).
2. the reactor for gc analysis according to claim 1, it is characterized in that: described hermetically-sealed construction comprises sealing gasket (2), sealing gasket (2) is positioned between rubber stopper (3) and the friction top (1).
3. the reactor for gc analysis according to claim 2, it is characterized in that: described hermetically-sealed construction comprises cushion (7), cushion (7) is positioned between flange (5) and the pressed seat (8).
4. the reactor for gc analysis according to claim 3, it is characterized in that: described friction top (1) and pressed seat (8) are threaded.
5. according to the described reactor for gc analysis of 1 to 4 each claim, it is characterized in that: described heater (9) is bathed heater for thermostat metal, and heater is provided with the test tube hole in (9), and container tube (6) is positioned at the test tube hole.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 201320020965 CN203140001U (en) | 2013-01-15 | 2013-01-15 | Reactor for gas chromatographic method analysis |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 201320020965 CN203140001U (en) | 2013-01-15 | 2013-01-15 | Reactor for gas chromatographic method analysis |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN203140001U true CN203140001U (en) | 2013-08-21 |
Family
ID=48967558
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN 201320020965 Expired - Lifetime CN203140001U (en) | 2013-01-15 | 2013-01-15 | Reactor for gas chromatographic method analysis |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN203140001U (en) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104034633A (en) * | 2014-06-10 | 2014-09-10 | 苏州大学张家港工业技术研究院 | Model for determining diffusivity of dye in color paste |
| CN114003074A (en) * | 2021-12-03 | 2022-02-01 | 新疆维吾尔自治区计量测试研究院 | Temperature field calibration device of dry-type constant temperature test equipment |
-
2013
- 2013-01-15 CN CN 201320020965 patent/CN203140001U/en not_active Expired - Lifetime
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104034633A (en) * | 2014-06-10 | 2014-09-10 | 苏州大学张家港工业技术研究院 | Model for determining diffusivity of dye in color paste |
| CN114003074A (en) * | 2021-12-03 | 2022-02-01 | 新疆维吾尔自治区计量测试研究院 | Temperature field calibration device of dry-type constant temperature test equipment |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| CX01 | Expiry of patent term | ||
| CX01 | Expiry of patent term |
Granted publication date: 20130821 |