CN202093004U - Automatic ion chromatography sample introduction device - Google Patents
Automatic ion chromatography sample introduction device Download PDFInfo
- Publication number
- CN202093004U CN202093004U CN2011201780854U CN201120178085U CN202093004U CN 202093004 U CN202093004 U CN 202093004U CN 2011201780854 U CN2011201780854 U CN 2011201780854U CN 201120178085 U CN201120178085 U CN 201120178085U CN 202093004 U CN202093004 U CN 202093004U
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- Prior art keywords
- sample bottle
- stopple coupon
- sample
- chromatography
- sampling apparatus
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- Expired - Fee Related
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- 238000004255 ion exchange chromatography Methods 0.000 title abstract 3
- 238000005070 sampling Methods 0.000 claims abstract description 44
- 239000000523 sample Substances 0.000 claims description 102
- 238000012360 testing method Methods 0.000 claims description 21
- 150000002500 ions Chemical class 0.000 claims description 19
- 238000004587 chromatography analysis Methods 0.000 claims description 18
- 239000012488 sample solution Substances 0.000 claims description 16
- 239000007788 liquid Substances 0.000 claims description 12
- 238000009826 distribution Methods 0.000 claims description 3
- 230000016507 interphase Effects 0.000 claims description 3
- 230000002572 peristaltic effect Effects 0.000 description 7
- 238000004458 analytical method Methods 0.000 description 5
- 238000001514 detection method Methods 0.000 description 5
- 230000035611 feeding Effects 0.000 description 4
- 238000002347 injection Methods 0.000 description 4
- 239000007924 injection Substances 0.000 description 4
- 230000008676 import Effects 0.000 description 3
- 238000004140 cleaning Methods 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 238000005516 engineering process Methods 0.000 description 2
- 238000000034 method Methods 0.000 description 2
- 238000007789 sealing Methods 0.000 description 2
- 229910000838 Al alloy Inorganic materials 0.000 description 1
- 239000000956 alloy Substances 0.000 description 1
- 239000013068 control sample Substances 0.000 description 1
- 239000000428 dust Substances 0.000 description 1
- 238000011010 flushing procedure Methods 0.000 description 1
- 239000012535 impurity Substances 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 230000003647 oxidation Effects 0.000 description 1
- 238000007254 oxidation reaction Methods 0.000 description 1
- 238000007670 refining Methods 0.000 description 1
- 239000000243 solution Substances 0.000 description 1
- 239000010935 stainless steel Substances 0.000 description 1
- 229910001220 stainless steel Inorganic materials 0.000 description 1
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- Automatic Analysis And Handling Materials Therefor (AREA)
Abstract
An automatic ion chromatography sample introduction device adopts the structure that a sample bottle driving power drives at least two sample bottles to move on a horizontal plane, a sampling tube driving power drives a sampling tube to conduct vertical movement, the sampling tube is communicated with a sampling pump, and the sample bottles are parallel with the axis of the sampling tube; the projection of the sampling tube on the horizontal plane falls into the sample bottle at the operating position; and the sample bottle driving power, the sampling tube driving power and the sampling pump are connected with a control system. The automatic ion chromatography sample introduction device can achieve automatic introduction of two or more samples, has high sample introduction efficiency and performance-price ratio, is low in cost because components of the automatic sample introduction device can be produced at home, and is easy to assemble.
Description
Technical field
The utility model relates to the sampling device of solution being cut the chromatography of ions stream, is a kind of automatic sampling apparatus of chromatography of ions specifically.
Background technology
Owing to technical reason, the chromatography of ions instrument of domestic production at present generally uses the hand sampling valve of import.The restriction and the restriction of the controlled method of hand sampling valve can only be interrupted operation by single, need manually valve to be placed earlier the sample introduction control position during each sample test, inject testing sample solution to chromatography of ions, and then manually valve are placed the analysis and Control position.Hand sampling takies manually, and effect is low, is difficult to realize automatic detection.In addition, import hand sampling valve also exists price height, the long problem of delivery cycle.
The utility model content
The utility model will solve existing hand sampling valve single and be interrupted operation, takies manually-operated, and effect is low; The technical matters that import hand sampling valve price height, delivery cycle are long, provide a kind of can be automatically to two above sample feedings, sample introduction efficiency height, the automatic sampling apparatus of the homemade chromatography of ions that cost performance is high.
In order to solve the problems of the technologies described above, the technical scheme that the utility model is taked is: a kind of automatic sampling apparatus of chromatography of ions, comprise sample bottle, sample bottle drives at least two sample bottles of power drive and moves on surface level, stopple coupon drives the power drive stopple coupon and does vertical movement, stopple coupon is communicated with sampling pump, the parallel axes of sample bottle and stopple coupon; The projection of stopple coupon on surface level drops in the sample bottle on the working position; Sample bottle drives power, stopple coupon drives power and sampling pump connection control system.
Under control system control, sample bottle drives power, stopple coupon drives power and sampling pump coordination, finishes auto injection.Sample bottle drives the power drive sample bottle and is stopped at the working position successively.Drive under the power drive at stopple coupon, stopple coupon stretches in the liquid of a sample bottle that is stopped at the working position, is transported to liquid in the detection stream of chromatography of ions via stopple coupon by sampling pump; Stopple coupon drives the power drive stopple coupon and rises, and breaks away from sample bottle; Drive under the power drive at sample bottle, another sample bottle is stopped at the working position, and stopple coupon drives the power drive stopple coupon and stretches in the liquid of another sample bottle, is transported to liquid in the detection stream of chromatography of ions via stopple coupon by sampling pump, so, realize auto injection.The utility model can be automatically to two or more sample feedings, the sample introduction efficiency height, and the cost performance height, the parts of automatic sampling apparatus are domestic can be produced, low price, assembling is easily.There are many prior aries can realize that sample bottle drives the motion of power drive sample bottle, drive power motor,, order about sample bottle back and forth movement on surface level by the tooth bar engagement on the carriage of gear on its main shaft and support sample bottle such as sample bottle; And for example sample bottle drives power motor, by the gearing mesh on the carriage central shaft of gear on its main shaft and support sample bottle, orders about sample bottle and make circular motion or the like on surface level.There are many prior aries can realize that stopple coupon drives the motion of power drive stopple coupon, drive power motor, mesh with the vertical tooth rack of fixedlying connected on the stopple coupon support, order about stopple coupon in movement in vertical direction by the gear on its horizontal spindle such as stopple coupon; And for example stopple coupon drives the rotation of power motor drive sprocket, and stopple coupon is fixed on the chain with sprocket engagement, and stopple coupon drives power motor and orders about stopple coupon in movement in vertical direction or the like.
Sample bottle is placed on the carriage of being made up of upper tray and lower tray, and it is the sample bottle drive stepping motor that sample bottle drives power, and sample bottle drive stepping motor output shaft is fixedlyed connected with the carriage central shaft is concentric.The sample bottle drive stepping motor drives sample bottle and make circular motion on surface level.
The fixedly connected stopple coupon support in the rear end of stopple coupon, it is the stopple coupon drive stepping motor that stopple coupon drives power, the stopple coupon drive stepping motor is fixed on the automatic sampling apparatus base, and the output shaft of stopple coupon drive stepping motor connects screw mandrel, and screw mandrel cooperates with screw on the stopple coupon support.The stopple coupon drive stepping motor drives stopple coupon and does vertical movement.
Sample bottle has even number, and sample bottle holds testing sample solution and leacheate respectively, holds the sample bottle and the sample bottle interphase distribution that holds leacheate of testing sample solution.Stopple coupon alternately stretches into sample bottle that holds testing sample solution and the sample bottle that holds leacheate, has been infected with the stopple coupon of testing sample solution, cleans through leacheate, has avoided exerting an influence between the testing sample.
Stopple coupon is the suction spindle that is hollow needle.Liquid in the similar injection needle of suction spindle, sample bottle is sucked out from the hollow cavity of suction spindle.
After sample bottle held testing sample solution, film was sealed in its covering suitable for reading.Sealing film is used for dustproof and avoids sample oxidation by air, stopple coupon to puncture sealing film stretching in the liquid of sample bottle.
The interior liquid level of sample bottle that holds leacheate is higher than liquid level in the sample bottle that holds testing sample solution.With what guarantee that each sample bottle that holds leacheate can both be authentic and valid stopple coupon is carried out the cleaning of outside surface, take place with the situation of avoiding contaminated samples.
The utility model has the advantages that: the utility model can be automatically to two or more sample feedings, the sample introduction efficiency height, and the cost performance height, the parts of automatic sampling apparatus are domestic can be produced, low price, assembling is easily.
Description of drawings
Fig. 1 is the structural representation of an embodiment of the utility model;
Fig. 2 is the vertical view of Fig. 1.
Embodiment
Accompanying drawings.Clear for what show, among Fig. 1 slide unit shell 5 fronts are removed, place the upper tray 1 and lower tray 15 parts of sample bottle 2 carriages and take to analyse and observe.
40 tops of present embodiment are cylindrical, the bottom is that the sample bottle 2 of taper evenly is placed in 40 through holes at circular upper tray 1 outer rim place, the upper tray 1 of refining aluminum alloy material is identical with lower tray 15 diameters, with on the lower tray 15 of the upper tray 1 through hole center of circle relative position bellmouth is arranged, be used for taper location to the sample bottle lower end.Gib screw 3 is fastenedly connected the placement carriage of forming sample bottle 2 at interval and with one heart with upper tray 1 and lower tray 15.It is each pulse step angle 0.9 degree that sample bottle drives power, the three-phase four of DC+24V/2A is clapped system sample bottle drive stepping motor 14, sample bottle drive stepping motor output shaft and carriage central shaft 16 concentric fixedlying connected, sample bottle drive stepping motor 14 drives sample bottle 2 and make circular motion on surface level.The stopple coupon of present embodiment is the suction spindle that is hollow needle 7 of stainless steel, the fixedly connected stopple coupon support in the rear end of suction spindle 7, it is each pulse step angle 0.9 degree that stopple coupon drives power, the three-phase four of DC+24V/2A is clapped system stopple coupon drive stepping motor 10, stopple coupon drive stepping motor 10 is fixed on the slide unit shell 5, its vertical output axle connects high precision screw mandrel 8, screw mandrel 8 cooperates with screw on the stopple coupon support, stopple coupon drive stepping motor 10 drives suction spindle 7 and moves up and down along suction spindle movement locus 9, does not show screw among the figure.Dust and other impurity that the slide unit shell 5 of plastic material blocks chromatography of ions automatic sampling apparatus space outerpace enter slide unit inside.Sample bottle 2 holds testing sample solution and leacheate respectively, for the sample of avoiding high concentration is finished after the detection, pollute the testing sample of low concentration, hold the sample bottle 2 and sample bottle 2 interphase distributions that hold leacheate of testing sample solution, the interior liquid level of sample bottle that holds leacheate is higher than liquid level in the sample bottle that holds testing sample solution.After sample bottle 2 held testing sample solution, its suitable for reading being covered with was sealed film.Sample bottle drive stepping motor 14 drives sample bottle 2 around central shaft 16 each rotation 9 degree, and 40 sample bottles 2 are stopped at the working position successively, and suction spindle 7 is communicated with sampling pump, and the sampling pump of present embodiment is a peristaltic pump 13, and pipeline 11 connects peristaltic pump 13 and suction spindle 7.The parallel axes of sample bottle 2 and suction spindle 7; The projection of suction spindle 7 on surface level drops in the sample bottle 2 of working position.Sample bottle drive stepping motor 14, peristaltic pump 13, slide unit shell 5 are fixedly mounted on the automatic sampling apparatus base 12.Sample bottle drives power, stopple coupon drives power and sampling pump connection control system, and under control system control, sample bottle drives power, stopple coupon drives power and sampling pump coordination, finishes auto injection.
The present embodiment workflow is as follows: after the energized, suction spindle 7 rises to the middle and upper part of screw mandrel 8 under the drive of stopple coupon drive stepping motor 10; Sample bottle drive stepping motor 14 drives sample bottle 2 and gets back to original position with placing carriage under the control of control panel; Afterwards, stopple coupon drive stepping motor 10 control suction spindles 7 drop in first sample bottle 2, open peristaltic pump 13 and draw testing sample solution, after sample introduction finishes, close peristaltic pump 13; Control stopple coupon drive stepping motor 10 rises the middle and upper part that suction spindle 7 is got back to screw mandrel 8.Thereupon, ion chromatograph begins testing sample is carried out check and analysis.After the check and analysis of testing sample are finished, 14 rotations of control sample bottle drive stepping motor, next sample bottle 2 drops on suction spindle 7 in the sample bottle 2 to the trajectory of suction spindle movement locus 9, open peristaltic pump 7 and draw leacheates, the outside surface and the whole sample introduction pipeline of suction spindle 7 washed.After flushing finishes, close peristaltic pump 7, control stopple coupon drive stepping motor 10 is raised up to suction spindle 7 middle and upper part of screw mandrel 8 once more.Carry out so repeatedly, until whole detections of all samples and analysis are finished, the chromatography of ions automatic sampling apparatus is back to the start position place again.So far, all sample feeding and pipeline cleaning processes are all over.
Claims (7)
1. the automatic sampling apparatus of a chromatography of ions, comprise sample bottle (2), it is characterized in that sample bottle drives at least two sample bottles of power drive (2) and moves on surface level, stopple coupon drives the power drive stopple coupon and does vertical movement, stopple coupon is communicated with sampling pump, the parallel axes of sample bottle (2) and stopple coupon; The projection of stopple coupon on surface level drops in the sample bottle on the working position; Sample bottle drives power, stopple coupon drives power and sampling pump connection control system.
2. the automatic sampling apparatus of chromatography of ions according to claim 1, it is characterized in that sample bottle (2) is placed on the carriage of being made up of upper tray (1) and lower tray (15), it is sample bottle drive stepping motor (14) that sample bottle drives power, sample bottle drive stepping motor output shaft and concentric the fixedlying connected of carriage central shaft (16).
3. the automatic sampling apparatus of chromatography of ions according to claim 1, the fixedly connected stopple coupon support in rear end that it is characterized in that stopple coupon, it is stopple coupon drive stepping motor (10) that stopple coupon drives power, stopple coupon drive stepping motor (10) is fixed on the automatic sampling apparatus base (12), the output shaft of stopple coupon drive stepping motor (10) connects screw mandrel (8), and screw mandrel (8) cooperates with screw on the stopple coupon support.
4. the automatic sampling apparatus of chromatography of ions according to claim 1, it is characterized in that sample bottle (2) has even number, sample bottle (2) holds testing sample solution and leacheate respectively, holds the sample bottle (2) of testing sample solution and holds sample bottle (2) interphase distribution of leacheate.
5. the automatic sampling apparatus of chromatography of ions according to claim 1 is characterized in that stopple coupon is the suction spindle (7) that is hollow needle.
6. according to the automatic sampling apparatus of claim 1 or 2 or 4 described chromatography of ions, it is characterized in that sample bottle (2) holds testing sample solution after, film is sealed in its covering suitable for reading.
7. the automatic sampling apparatus of chromatography of ions according to claim 4 is characterized in that the interior liquid level of sample bottle that holds leacheate is higher than liquid level in the sample bottle that holds testing sample solution.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2011201780854U CN202093004U (en) | 2011-05-18 | 2011-05-18 | Automatic ion chromatography sample introduction device |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2011201780854U CN202093004U (en) | 2011-05-18 | 2011-05-18 | Automatic ion chromatography sample introduction device |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN202093004U true CN202093004U (en) | 2011-12-28 |
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN2011201780854U Expired - Fee Related CN202093004U (en) | 2011-05-18 | 2011-05-18 | Automatic ion chromatography sample introduction device |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN202093004U (en) |
Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103616358A (en) * | 2013-11-30 | 2014-03-05 | 广州蓝勃生物科技有限公司 | Environment-friendly multi-project full-automatic solid phase fluorescence detection system |
| CN110749685A (en) * | 2019-09-11 | 2020-02-04 | 青岛盛瀚色谱技术有限公司 | Automatic sample injector and needle washing method |
| CN114207434A (en) * | 2019-07-29 | 2022-03-18 | 沃特世科技公司 | Method of loading a sample into a sample manager of a chromatography system |
| CN114236161A (en) * | 2021-12-31 | 2022-03-25 | 南京国科医工科技发展有限公司 | Liquid suction structure and liquid supply device for immunoassay |
| CN114324925A (en) * | 2021-12-16 | 2022-04-12 | 浙江西热利华智能传感技术有限公司 | Automatic sampling and sample introduction instrument for water sample detection and sampling and sample introduction method |
-
2011
- 2011-05-18 CN CN2011201780854U patent/CN202093004U/en not_active Expired - Fee Related
Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103616358A (en) * | 2013-11-30 | 2014-03-05 | 广州蓝勃生物科技有限公司 | Environment-friendly multi-project full-automatic solid phase fluorescence detection system |
| CN114207434A (en) * | 2019-07-29 | 2022-03-18 | 沃特世科技公司 | Method of loading a sample into a sample manager of a chromatography system |
| CN110749685A (en) * | 2019-09-11 | 2020-02-04 | 青岛盛瀚色谱技术有限公司 | Automatic sample injector and needle washing method |
| CN114324925A (en) * | 2021-12-16 | 2022-04-12 | 浙江西热利华智能传感技术有限公司 | Automatic sampling and sample introduction instrument for water sample detection and sampling and sample introduction method |
| CN114236161A (en) * | 2021-12-31 | 2022-03-25 | 南京国科医工科技发展有限公司 | Liquid suction structure and liquid supply device for immunoassay |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| CF01 | Termination of patent right due to non-payment of annual fee | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20111228 Termination date: 20200518 |