CN201352200Y - Detector for adulterated peanut oil - Google Patents
Detector for adulterated peanut oil Download PDFInfo
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- CN201352200Y CN201352200Y CNU2009201058080U CN200920105808U CN201352200Y CN 201352200 Y CN201352200 Y CN 201352200Y CN U2009201058080 U CNU2009201058080 U CN U2009201058080U CN 200920105808 U CN200920105808 U CN 200920105808U CN 201352200 Y CN201352200 Y CN 201352200Y
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- Investigating Or Analysing Materials By Optical Means (AREA)
Abstract
一种掺假花生油检测仪,属于分析仪器领域。其具有机壳,机壳表面设置有液晶显示屏、返回键、确认键、上翻键、下翻键,电源控制开关、电源插座和USB接口,机壳内装设有与表面各部件电连接的微处理器和电源,所述机壳上表面还设置模块盖,机壳内模块盖下部空间安装有前处理模块和检测模块。所述前处理模块中包括加热体和比色皿孔槽,检测模块中包括轴流风机、散热片、制冷片和比色皿孔槽。本实用新型仪器可简便、灵敏地检测出花生油中是否掺假以及掺假比例,可对花生油中掺入菜籽油、葵花油、玉米油、棉籽油、棕榈油与大豆油等进行现场快速检测。
The utility model relates to an adulterated peanut oil detector, which belongs to the field of analytical instruments. It has a casing, and the surface of the casing is provided with a liquid crystal display, a return key, a confirmation key, an up key, a down key, a power control switch, a power socket and a USB interface, and the inside of the casing is provided with a circuit breaker that is electrically connected to each component on the surface. A microprocessor and a power supply, a module cover is arranged on the upper surface of the casing, and a pre-processing module and a detection module are installed in the space under the module cover in the casing. The pretreatment module includes a heating body and a cuvette hole, and the detection module includes an axial flow fan, a cooling fin, a refrigeration sheet and a cuvette hole. The instrument of the utility model can easily and sensitively detect whether peanut oil is adulterated and the proportion of adulteration, and can quickly detect the peanut oil mixed with rapeseed oil, sunflower oil, corn oil, cottonseed oil, palm oil and soybean oil, etc. .
Description
技术领域 technical field
本实用新型属于分析仪器领域,涉及一种简便、灵敏、现场检测掺假花生油的快速检测仪器,具体涉及用于现场对花生油中掺入菜籽油、葵花油、玉米油、棉籽油、棕榈油与大豆油进行快速检测的一种分析仪器。The utility model belongs to the field of analytical instruments, and relates to a simple, sensitive, on-site rapid detection instrument for adulterated peanut oil, in particular to an on-site detection of peanut oil mixed with rapeseed oil, sunflower oil, corn oil, cottonseed oil, and palm oil An analytical instrument for rapid detection of soybean oil.
背景技术 Background technique
花生油以营养丰富而著称,在市场上属于价格最高的食用油之一。在正常情况下,花生油呈淡黄色、透明,色泽清亮,气味芬芳,滋味可口,是一种比较容易消化的食用油。在花生油中含80%以上的不饱和脂肪酸(其中含油酸41.2%,亚油酸37.6%)。而且还含有软脂酸,硬脂酸和花生酸等饱和脂肪酸。另外,花生油中还含有甾醇、麦胚酚、磷脂、维生素E、胆碱等对人体有益的物质。由上述数据可知,花生油的脂肪酸构成是比较易于人体消化吸收的。据国外资料介绍,经常食用花生油,不但可以使人体内胆固醇分解为胆汁酸并排出体外,从而降低血浆中胆固醇的含量。而且还可以防止皮肤皱裂老化,保护血管壁,防止血栓形成,有助于预防动脉硬化和冠心病。花生油中的胆碱,还可改善人脑的记忆力功能,延缓脑功能衰退。由此看来,花生油是一种对人体健康非常有益的一种食用油。由于利益驱动,花生油掺假屡禁不止。Peanut oil is known for being rich in nutrients and is one of the most expensive cooking oils on the market. Under normal circumstances, peanut oil is light yellow, transparent, clear in color, fragrant in smell and delicious in taste. It is a relatively easy-to-digest edible oil. Contain more than 80% unsaturated fatty acids in peanut oil (wherein contain oleic acid 41.2%, linoleic acid 37.6%). It also contains saturated fatty acids such as palmitic acid, stearic acid and arachidic acid. In addition, in peanut oil, also contain the materials useful to human body such as sterol, wheat germ phenol, phosphatide, vitamin E, choline. It can be seen from the above data that the fatty acid composition of peanut oil is relatively easy for the human body to digest and absorb. According to foreign data introduction, often edible peanut oil, not only can make cholesterol in human body be decomposed into bile acid and excrete, thereby reduce the content of cholesterol in blood plasma. But also can prevent wrinkled skin aging, protect blood vessel wall, prevent thrombosis, help to prevent arteriosclerosis and coronary heart disease. Choline in peanut oil can also improve the memory function of human brain and delay brain function decline. From this point of view, peanut oil is a kind of edible oil that is very beneficial to human health. Due to profit-driven, adulteration of peanut oil has been repeatedly banned.
花生油、菜籽油与棕榈油、大豆油之间的巨额差价(目前广州市场上1吨花生油价格约人民币10250元,大豆油价格5400元,菜籽油的价格为6150元,棕榈油价格为4380元)给了不法商家可乘之机,不法之徒在花生油中掺入其它植物油,甚至全部以其他植物油代替,只以微量花生油香精调香,而这些掺假的花生油用通常的鼻闻和冷藏法难以鉴别,因此,研制一种可以鉴别掺假花生油的检测仪非常必要。The huge price difference between peanut oil, rapeseed oil, palm oil and soybean oil (currently the price of 1 ton of peanut oil in Guangzhou market is about RMB 10,250, the price of soybean oil is 5,400 yuan, the price of rapeseed oil is 6,150 yuan, and the price of palm oil is 4,380 yuan. Yuan) has given unscrupulous merchants an opportunity to mix other vegetable oils in peanut oil, or even replace them all with other vegetable oils, and only use a small amount of peanut oil essence to spice up. Therefore, it is very necessary to develop a detector that can identify adulterated peanut oil.
实用新型内容 Utility model content
针对上述问题,本实用新型的主要目的是提供一种可以简便、快速、现场检测掺假花生油的快速分析仪器。In view of the above problems, the main purpose of the utility model is to provide a quick analysis instrument which can detect adulterated peanut oil easily, quickly and on-site.
为实现上述目的,本实用新型提供的掺假花生油检测仪,具有机壳,机壳表面设置有液晶显示屏、返回键、确认键、上翻键、下翻键,电源控制开关、电源插座和USB接口,机壳内装设有与表面各部件电连接的微处理器和电源,所述机壳上表面还设置模块盖,机壳内模块盖下部空间安装有前处理模块和检测模块。In order to achieve the above object, the adulterated peanut oil detector provided by the utility model has a casing, and the surface of the casing is provided with a liquid crystal display, a return key, a confirmation key, an up key, a down key, a power control switch, a power socket and A USB interface, a microprocessor and a power supply electrically connected to the components on the surface are installed in the casing, a module cover is provided on the upper surface of the casing, and a pre-processing module and a detection module are installed in the space under the module cover in the casing.
上述掺假花生油检测仪中,所述前处理模块包括一主体及附于其底部的一加热体,所述主体上开设两个向上开口的比色皿孔槽,侧面装设一温度传感器;加热体和温度传感器均与微处理器和电源电相连。In the above adulterated peanut oil detector, the pretreatment module includes a main body and a heating body attached to its bottom, two cuvette holes opening upwards are set on the main body, and a temperature sensor is installed on the side; Both the body and the temperature sensor are electrically connected to the microprocessor and the power supply.
所述检测模块由下至上包括一轴流风机、一散热片、一制冷片和一检测模块主体,检测模块主体上,另附设一温度传感器;检测模块主体中,纵向开设两个向上开口的比色皿孔槽,并水平开设两个与比色皿孔槽相交的通孔,通孔一端装设光源/单色器,通孔另一端装设光电检测器;检测模块中轴流风机、散热片、制冷片、温度传感器、光源/单色器和光电检测器均与电源和微处理器电相连。The detection module includes an axial flow fan, a heat sink, a cooling plate and a detection module body from bottom to top, and a temperature sensor is attached to the detection module body; in the detection module body, there are two ratios with upward openings longitudinally. The cuvette hole slot, and two through holes intersecting with the cuvette hole slot are horizontally opened, the light source/monochromator is installed at one end of the through hole, and the photoelectric detector is installed at the other end of the through hole; the axial flow fan and heat dissipation in the detection module Chip, cooling chip, temperature sensor, light source/monochromator and photodetector are all electrically connected with power supply and microprocessor.
所述机壳底部设有通风孔。The bottom of the casing is provided with ventilation holes.
所述机壳内装设一打印机,打印机出纸口设于机壳上表面,打印机与电源和微处理器电相连。A printer is installed in the casing, the paper outlet of the printer is set on the upper surface of the casing, and the printer is electrically connected with the power supply and the microprocessor.
本实用新型采用上述技术方案,其显著特点是:The utility model adopts the above-mentioned technical scheme, and its salient features are:
1、采用标准曲线及标准曲线库比对方法,使操作简便,检测结果直观性好。1. The standard curve and standard curve library comparison method is adopted, which makes the operation easy and the test results are intuitive.
2、采用模块化结构,仪器性能更加稳定。2. Modular structure is adopted, and the performance of the instrument is more stable.
3、采用微处理器控制,具有测量、设置、记录、保存和数据处理功能。设有USB接口,与PC机联机通信等功能。自动化程度高。3. It adopts microprocessor control and has the functions of measurement, setting, recording, saving and data processing. Equipped with USB interface, online communication with PC and other functions. high degree of automation.
4、大屏幕液晶中文显示,人机交互式操作,体积小、重量轻、使用方便。4. Large-screen liquid crystal display in Chinese, man-machine interactive operation, small size, light weight, easy to use.
本实用新型可以对花生油产品的质量安全进行快速检测。可对花生油中掺入菜籽油、葵花油、玉米油、棉籽油、棕榈油与大豆油等进行现场快速检测。The utility model can quickly detect the quality and safety of peanut oil products. It can quickly detect the peanut oil mixed with rapeseed oil, sunflower oil, corn oil, cottonseed oil, palm oil and soybean oil.
附图说明 Description of drawings
图1为本实用新型掺假花生油检测仪主机外部结构示意图。Figure 1 is a schematic diagram of the external structure of the host of the adulterated peanut oil detector of the present invention.
图2为本实用新型中前处理模块结构示意图。Fig. 2 is a structural schematic diagram of the pre-processing module in the utility model.
图3为本实用新型中检测模块结构示意图。Fig. 3 is a schematic structural diagram of the detection module in the present invention.
图3A为图3中检测模块主体结构左视剖面结构示意图。FIG. 3A is a left-view cross-sectional structural schematic diagram of the main structure of the detection module in FIG. 3 .
图4为本实用新型中工作部件电路、光路连接关系以及工作原理示意图。Fig. 4 is a schematic diagram of the circuit of the working components, the connection relationship of the optical path and the working principle of the utility model.
图5为本实用新型微处理器中真花生油(正品)光度分析标准曲线图。Fig. 5 is a standard curve diagram of photometric analysis of real peanut oil (genuine product) in the microprocessor of the present utility model.
具体实施方式 Detailed ways
下面结合附图说明本实用新型的具体实施方式。The specific embodiment of the utility model is described below in conjunction with accompanying drawing.
本实用新型提出的掺假花生油检测仪器,是基于样品中花生油的凝固温度与其它欲掺入的食用油的凝固温度不同,导致光的透过程度不同即吸光度不同而建立的一种分析仪器。The detection instrument for adulterated peanut oil proposed by the utility model is an analytical instrument established based on the fact that the solidification temperature of the peanut oil in the sample is different from that of other edible oils to be mixed, resulting in a difference in light transmission degree, that is, a difference in absorbance.
如图1所示,本实用新型掺假花生油检测仪具有机壳1,机壳1的上表面设置有液晶显示屏3、返回键41、确认键42、上翻键43、下翻键44。机壳上表面还设置模块盖2和打印机出纸口5,机壳1侧面设有电源控制开关6、电源插座7和USB接口8,机壳底部设有通风孔(图中未表示)。机壳1内设有空间并装设有微处理器、打印机和电源(参见图4所示);其中,模块盖2下部空间用于安装前处理模块20和检测模块30。As shown in Figure 1, the adulterated peanut oil detector of the utility model has a
参见图2所示,前处理模块20的主体21由金属铝材料制成,其底部附一PTC加热体22,其侧面装设一温度传感器23,温度传感器型号为18B20,也可以为具有同等功效的加热体或温度传感器,在此不做特别限制;加热体22和温度传感器23均与微处理器和电源电相连。在主体20上开设两个向上开口的比色皿孔槽241和242,孔槽241和242的尺寸大小及形状与检测中使用的比色皿相配合。前处理模块20工作时,通过加热体22将主体21加热,并通过温度传感器23将主体21的温度数值传递给微处理器,通过微处理器将主体21温度控制在40℃。Referring to Fig. 2, the
如图3所示,为本实用新型检测模块30,由下至上包括一轴流风机31,散热片32,制冷片34,和一金属铝制材料的检测模块主体33,在检测模块主体33上,另附设温度传感器(18B20)35;在本实用新型中,温度传感器、制冷片、散热片、轴流风机为标准通用产品,只要整体相配合且能满足使用性能,在此不做特别限制。检测模块主体33中,纵向开设两个向上开口的比色皿孔槽333、334,比色皿孔槽的尺寸大小及形状与检测中使用的比色皿相配合;结合图3A所示,在检测模块主体33中,水平开设两个与比色皿孔槽333、334相交的通孔,通孔一端装设光源/单色器332、335,通孔另一端装设光电检测器336、331。检测模块30中,轴流风机31、散热片32、制冷片34、温度传感器35、光源/单色器332、335和光电检测器336、331均与电源35和微处理器电相连。As shown in Figure 3, it is a
检测模块30工作时,制冷片34开始制冷,产生的热量传递给散热片32,由轴流风机31将热量散出;通过温度传感器35将检测模块主体33的温度数值传递给微处理器,通过微处理器将检测模块主体33控制在3-4℃。检测时,光源/单色器332、335作为分析仪器的光源,光线通过比色皿到达光电检测器336、331,由光电检测器接收光源/单色器发出的光信号并传递给微处理器。When the
参见图4,描述了本实用新型工作部件之间的电路、光路连接关系以及工作原理:仪器接通电源后,将待测样品装入比色皿,比色皿放入前处理模块的比色皿孔槽中,微处理器控制前处理模块开始加热,保持样品恒温40℃(通过加热体和温度传感器);然后将装有样品的比色皿放入检测模块的比色皿孔槽中,微处理器控制检测模块主体温度,保持检测时样品在3-4℃(通过轴流风机、散热片、制冷片和温度传感器);检测时,光源/单色器发出的单色光穿过测模块主体中比色皿的样品后照射到光电检测器,光电检测器将检测到的光信号转换为电信号后,传输到微处理器,通过微处理器进行数据分析并将结果通过显示屏显示出来或通过打印机打印出来。Referring to Fig. 4, it describes the circuit, optical path connection relationship and working principle between the working parts of the utility model: after the instrument is powered on, the sample to be tested is packed into a cuvette, and the cuvette is put into the colorimetric cuvette of the pretreatment module. In the cuvette hole, the microprocessor controls the pretreatment module to start heating to keep the sample at a constant temperature of 40°C (through the heating body and temperature sensor); then put the cuvette containing the sample into the cuvette hole of the detection module, The temperature of the main body of the detection module is controlled by the microprocessor, and the sample is kept at 3-4°C during the detection (through the axial flow fan, heat sink, cooling plate and temperature sensor); during the detection, the monochromatic light emitted by the light source/monochromator passes through the measurement The sample in the cuvette in the main body of the module is irradiated to the photoelectric detector, and the photodetector converts the detected light signal into an electrical signal and transmits it to the microprocessor, which performs data analysis and displays the result on the display screen out or print it out on a printer.
在本实用新型中,光源/单色器为一定数目的超高亮发光二极管,既做光源又做单色器,实施中采用了日本的日亚和丰田公司生产的超高亮发光二极管,亮度参数在1000mcd以上。波长分别为420nm。光源/单色器采用连续或脉冲方式供电。该电路为常规电路,在此不再详述。In the utility model, the light source/monochromator is a certain number of ultra-bright light-emitting diodes, which are used as light source and monochromator. In the implementation, the ultra-bright light-emitting diodes produced by Nichia and Toyota of Japan are adopted. The parameters are above 1000mcd. The wavelength is 420nm respectively. The light source/monochromator is powered continuously or pulsed. This circuit is a conventional circuit and will not be described in detail here.
光电检测器采用了美国TI公司生产集成光电传感器,型号为TSL230系列。当然,本实用新型也可以采用其它具有同等功效的集成光电传感器。The photoelectric detector adopts the integrated photoelectric sensor produced by American TI Company, the model is TSL230 series. Of course, the utility model can also adopt other integrated photoelectric sensors with equivalent efficacy.
微处理器为飞利浦公司生产的ARM系列,其主要参数为32位单片机,内部存储器40K,载有常用分光光度分析软件。微处理器主要接收光电检测器的输出信号并进行数据处理。以光源/单色器、光电检测器和微处理器为核心元件的分光光度分析仪的电路连接以及工作过程可参考申请人之前ZL200620004295.0的介绍,在此不再赘述。The microprocessor is the ARM series produced by Philips. Its main parameters are 32-bit single-chip microcomputer, internal memory 40K, and commonly used spectrophotometric analysis software. The microprocessor mainly receives the output signal of the photodetector and performs data processing. For the circuit connection and working process of the spectrophotometric analyzer with light source/monochromator, photodetector and microprocessor as the core components, please refer to the applicant's previous introduction of ZL200620004295.0, and will not repeat them here.
以下结合具体操作进一步说明利用本实用新型掺假花生油检测仪进行的掺假花生油检测的方法。The method for detecting adulterated peanut oil by using the adulterated peanut oil detector of the utility model is further described below in conjunction with specific operations.
首先将装有待检样品的比色皿放入前处理模块中40℃恒温加热10分钟,目的是为了实现样品检测的一致性。然后取出装有待检样品的比色皿放入恒温3-4℃检测模块中进行检测。检测时间25分钟。检测期间,随着温度变化,样品凝结程度会发生变化,吸光值会随之改变;光电检测器将检测信号不间断传递给微处理器而生成一条检测曲线(吸光度-时间曲线),此曲线与标准曲线库中正品标准曲线(参见图5)及各种不同掺假比例花生油曲线比对,即可判断此样品花生油的真假和掺假花生油的比例,并通过显示屏、打印机或USB接口输出。数据采集及处理过程由微处理器自动完成。First, put the cuvette containing the sample to be tested into the pretreatment module and heat it at a constant temperature of 40°C for 10 minutes, in order to achieve the consistency of sample detection. Then take out the cuvette containing the sample to be tested and put it into a constant temperature 3-4°C detection module for detection. The detection time is 25 minutes. During the detection period, as the temperature changes, the coagulation degree of the sample will change, and the absorbance value will change accordingly; the photodetector will continuously transmit the detection signal to the microprocessor to generate a detection curve (absorbance-time curve), which is consistent with Comparing the authentic standard curve (see Figure 5) and various adulterated peanut oil curves in the standard curve library, you can judge the authenticity of the sample peanut oil and the ratio of adulterated peanut oil, and output it through the display screen, printer or USB interface . Data acquisition and processing are automatically completed by the microprocessor.
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WO2010094167A1 (en) * | 2009-02-18 | 2010-08-26 | 长春吉大·小天鹅仪器有限公司 | Detector and method for adulterate peanut oil |
CN103115883A (en) * | 2013-01-24 | 2013-05-22 | 重庆大学 | Sample detecting system of micro biochemical detection instrument |
CN110257244A (en) * | 2019-04-23 | 2019-09-20 | 武汉观锐生物科技有限公司 | A kind of couveuse |
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WO2010094167A1 (en) * | 2009-02-18 | 2010-08-26 | 长春吉大·小天鹅仪器有限公司 | Detector and method for adulterate peanut oil |
CN101482494B (en) * | 2009-02-18 | 2011-05-25 | 长春吉大·小天鹅仪器有限公司 | Adulterated peanut oil detector and a method for detecting adulterated peanut oil |
CN103115883A (en) * | 2013-01-24 | 2013-05-22 | 重庆大学 | Sample detecting system of micro biochemical detection instrument |
CN103115883B (en) * | 2013-01-24 | 2016-03-02 | 重庆大学 | Miniature bio-chemical detector specimen inspection system |
CN110257244A (en) * | 2019-04-23 | 2019-09-20 | 武汉观锐生物科技有限公司 | A kind of couveuse |
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