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CN1629593A - Heat pipe preparing method - Google Patents

Heat pipe preparing method Download PDF

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Publication number
CN1629593A
CN1629593A CN 200310117604 CN200310117604A CN1629593A CN 1629593 A CN1629593 A CN 1629593A CN 200310117604 CN200310117604 CN 200310117604 CN 200310117604 A CN200310117604 A CN 200310117604A CN 1629593 A CN1629593 A CN 1629593A
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China
Prior art keywords
hollow tube
control preparation
heat pipe
heat control
copper
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Granted
Application number
CN 200310117604
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Chinese (zh)
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CN1307399C (en
Inventor
黄全德
黄文正
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Hongfujin Precision Industry Shenzhen Co Ltd
Hon Hai Precision Industry Co Ltd
Original Assignee
Hongfujin Precision Industry Shenzhen Co Ltd
Hon Hai Precision Industry Co Ltd
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Application filed by Hongfujin Precision Industry Shenzhen Co Ltd, Hon Hai Precision Industry Co Ltd filed Critical Hongfujin Precision Industry Shenzhen Co Ltd
Priority to CNB2003101176046A priority Critical patent/CN1307399C/en
Publication of CN1629593A publication Critical patent/CN1629593A/en
Application granted granted Critical
Publication of CN1307399C publication Critical patent/CN1307399C/en
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Expired - Fee Related legal-status Critical Current

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Abstract

This invention relates to a heat tube process method, which comprises the following steps: providing proper nanometer copper compound fiber and organic solvent mixture; providing a hollow tube with one end sealed as heat tube shell; inserting one plastic bar with smaller inner radium than the hollow tube into the hollow tube to form a space between the plastic bar and the hollow tube inner wall; filling the above mixture into the above space to remove the organic solvent agent; drawing the hollow tube into vacuum tube; drilling proper working fluid into the hollow tube; sealing the hollow tube to seal the working fluid into the hollow tube.

Description

The heat control Preparation Method
[technical field]
The present invention relates to a kind of heat control Preparation Method, particularly a kind of saving cost, can make the imbibition core be close to the heat pipe inwall, and be fit to the heat control Preparation Method of preparation flexure type heat pipe.
[background technology]
Heat pipe is the heat-conductive assembly that dependence self internal work fluid phase transformation realizes heat conduction, and it has good characteristics such as high-termal conductivity, good isothermal, and good heat conduction effect is widely used.
Electronic technology develops rapidly in recent years, the high frequency of electronic device, high speed and integrated circuit intensive and microminiaturized, make unit volume electronic device caloric value increase severely, characteristics such as hot pipe technique is efficient with it, compactness and flexibility and reliability are fit to solve the heat dissipation problem that present electronic device is derived because of performance boost.
As shown in Figure 1, typical heat pipe 10 by shell 11, imbibition core 12 (capillary structure) and be sealed in the pipe in working fluid 13 form.The making of heat pipe 10 is sealed after being full of working fluid 13 in the imbibition core 12 of being close to pipe shell 11 inwalls filling after being evacuated in the pipe with suitable working fluid 13, making earlier usually.One end of heat pipe 10 is evaporator section 10a (bringing-up section), and the other end is condensation segment 10b (cooling section), can arrange the adiabatic section between evaporator section 10a and condensation segment 10b according to application need.Working fluid 13 evaporation gasifications form steam 14 in the imbibition core 12 when heat pipe 10 evaporator section 10a are heated, steam 14 is at the dirty condensation segment 10b to heat pipe 10 of slight pressure difference effect, condense into working fluid 13 and emit heat 15, working fluid 13 flows back to evaporator section 10a by capillarity along imbibition core 12 again.So circulation, heat 15 constantly reaches condensation segment 10b by the evaporator section 10a of heat pipe 10, and the low-temperature receiver of the section of being condensed 10b one end absorbs.
Heat pipe 10 comprises following six main processes that are mutually related in realizing conduction process:
(1) heat 15 passes to working fluid 13 from thermal source by heat pipe package 11 and the imbibition core 12 that is full of working fluid 13;
(2) hydraulic fluid 13 liquid-gas in evaporator section 10a divides on the interface and evaporates;
(3) steam 14 flows to condensation segment 10b from evaporator section 10a;
(4) steam 14 solution-air in condensation segment 10b is divided on the interface and is condensed;
(5) heat 15 divides interface to pass to low-temperature receiver by imbibition core 12, hydraulic fluid 13 and shell 11 from solution-air;
(6) in imbibition core 12 since capillarity make condensation after working fluid 13 be back to evaporator section 10a.
Find out from above-mentioned six processes, imbibition core 12 plays important conductive force in process (1) and process (5), in process (6) condensed working fluid 13 rapid backflows are played a decisive role, therefore, imbibition core 12 is extremely important for normally working effectively of heat pipe 10.
Imbibition core 12 is generally silk screen type, groove-shaped or slug type in the prior art.
Silk screen type imbibition core capillary better performances wherein, make than being easier to, purchase the silk screen of typing mesh number in market, its material is generally copper, stainless steel, wire netting, can select according to the compatibility of heat pipe work fluid, get final product through rolling into needed shape insertion heat pipe after cleaning and the necessary processing after silk screen is bought, therefore in heat pipe, use more.
But, directly the imbibition core that inserts in the heat pipe package relies on its elasticity tension to be affixed on the heat pipe package inwall, when elasticity is not enough, is prone to not tight, the uneven phenomenon of imbibition core applying inner wall of tube shell, cause heat pipe for thermal conductivity efficient to reduce, even heat pipe hot-spot and damage heat pipe even electronic device.
For guaranteeing that silk screen type imbibition core fully contacts the heat pipe package inwall, the available metal silk screen fills up heat pipe, and still, this method needs more woven wire, and the heat pipe cost is improved.
In addition, for cooperating the reasonable installation of dissipation from electronic devices device, need sometimes heat control is made flexure type.But, in the flexure type heat pipe, form relatively difficulty of capillary wick, if in straight tube, form behind the capillary structure, then destroy the capillary structure of bend easily again with straight tube bending.Therefore, the flexure type heat pipe at first forms sintering or groove-shaped capillary structure at two semicanal inwalls generally by being welded in the prior art, two semicanals is fastened to weld together again.
But inside heat pipe needs to be evacuated before pouring into working fluid, and working fluid constantly evaporates in heat pipe, cools off, refluxes, evaporates, requires no gaseous impurity to disturb, if heat pipe gas leakage will be unfavorable for that properties of hot pipe improves.The heat pipe that fastening is welded, weld seam cause heat pipe gas leakage easily, are unfavorable for that properties of hot pipe improves.
Therefore, the heat control Preparation Method that provide a kind of and save cost, make capillary wick to be close to the heat pipe package inwall, to be particularly suitable for preparing the flexure type heat pipe is very necessary.
[summary of the invention]
The technical problem to be solved in the present invention is that silk screen type imbibition core applying heat pipe package inwall is not tight, inhomogeneous in the prior art, cost is high.
The technical problem that the present invention further will solve is that flexure type heat pipe capillary imbibition core forms difficulty in the prior art, stays weld seam in the flexure type heat pipe preparation process, causes heat pipe to leak gas easily.
The object of the present invention is to provide a kind of cost to reduce, guarantee that the imbibition core can be close to the heat control Preparation Method of heat pipe package inwall.
Further aim of the present invention is to provide a kind of heat control Preparation Method of suitable preparation flexure type heat pipe.
The technical scheme of technical solution problem of the present invention provides the heat control Preparation Method, and this method comprises the following steps: to provide the mixture of proper amount of nano level copper-containing compound fiber with an amount of organic solvent; The hollow tube that one end closure is provided is as heat pipe package; The plastic rod of one diameter less than above-mentioned hollow tube internal diameter inserted in the hollow tube, make and form a space between plastic rod and the hollow tube inwall; Said mixture is injected above-mentioned space; In reducing atmosphere, calcine, removing plastic rod and organic solvent, and make nanoscale copper-containing compound fiber reduction become the copper fleece; Hollow tube is evacuated; In hollow tube, pour into an amount of working fluid; Hollow tube is sealed, working fluid is sealed in the hollow tube.
The preparation method of flexure type heat pipe provided by the present invention is identical with said method basically, and only many steps after plastic rod being inserted in the hollow tube promptly by machining, bend to required shape with the hollow tube that inserts plastic rod.
Compared with prior art, heat control Preparation Method provided by the present invention has the following advantages: by the plastic rod of a diameter less than the heat pipe package internal diameter, between plastic rod and hollow tube inwall, form a space, capillary wick is attached to the heat pipe package inwall by this space and calcination process, and because the plastic cement cost is starkly lower than the metallic fiber cost, thereby the heat pipe manufacturing cost reduces; In addition, this method adopts organic solvent hybrid nanoscale copper-containing compound fiber to inject heat pipe package, and the flexure type heat pipe also is suitable for, and therefore, forms no longer difficulty of capillary wick in the flexure type heat pipe package, helps preparing the flexure type heat pipe.
[description of drawings]
Fig. 1 is the general heat pipe operation principle of a prior art schematic diagram.
Fig. 2 is a heat control Preparation Method flow chart of the present invention.
Fig. 3 provides the hollow tube schematic diagram of an end closure.
Fig. 4 is the schematic diagram that inserts a plastic rod in hollow tube.
Fig. 5 is a schematic diagram of filling with mixture in the space.
Fig. 6 is the prepared straight type heat pipe axial cross section schematic diagram of first embodiment of the invention.
Fig. 7 is the prepared flexure type heat pipe axial cross section schematic diagram of second embodiment of the invention.
[specific embodiment]
Below in conjunction with icon heat control Preparation Method embodiment provided by the present invention is described:
As shown in Figure 2, the straight type heat control Preparation Method that first embodiment of the invention provided comprises:
Step 1 provides the mixture of nanoscale copper-containing compound fiber and organic solvent; Proper amount of nano level copper-containing compound fiber and an amount of organic solvent promptly are provided, and both are mixed formation one mixture;
Step 2 provides the hollow tube of an end closure; This hollow tube will be as heat pipe package, this step and the no sequencing of step 1;
Step 3 is inserted the plastic rod of a diameter less than above-mentioned hollow tube internal diameter in the hollow tube, makes and forms a space between plastic rod and the hollow tube inwall;
Step 4 is injected the space with mixture;
Step 5 is calcined in reducing atmosphere, removing plastic rod and organic solvent, and makes nanoscale copper-containing compound fiber reduction become the copper fleece;
Step 6 is evacuated hollow tube;
Step 7 pours into an amount of working fluid in hollow tube;
Step 8 is sealed hollow tube, and working fluid is sealed in the hollow tube.
The nanoscale copper-containing compound fiber that step 1 provided can prepare by electrospinning weave (electrospinning): 10% poly-vinyl alcohol solution slowly splashes in the Schweinfurt green solution, obtains the copper ions gel; This gel is packed in the container, in gel, insert a copper electrode (positive pole) and an aluminium electrode (negative pole), pass to 20 kilovolts high-tension electricity, promptly generate nanoscale copper-containing compound fiber on the aluminium electrode to gel.The copper-containing compound fibre diameter of this method gained is generally less than 200 nanometers.This step also provides an amount of organic solvent, and this organic solvent comprises ethanol, isopropyl alcohol, acetone etc.The copper-containing compound fiber that generates on the aluminium electrode is taken off, mixes with above-mentioned organic solvent, for subsequent step standby.
Step 2, as shown in Figure 3, the straight type hollow tube 21 that an end closure is provided is as heat pipe package; Shell is generally copper pipe, also can adopt different materials according to different needs, as aluminium, steel, carbon steel, stainless steel, iron, nickel, titanium etc. and alloy thereof.Caliber is 2 millimeters～200 millimeters, and pipe range can be from several millimeters to tens of centimetres.
It is circular copper pipe that present embodiment adopts radial section, and caliber is 10 millimeters, long 150 millimeters.
Step 3 as shown in Figure 4, is inserted the plastic rod 30 of a diameter less than above-mentioned hollow tube 21 internal diameters in the hollow tube 21, forms a space 31 between plastic rod 30 and hollow tube 21 inwalls; Wherein plastic rod 30 materials comprise polyethylene, polypropylene, polyurethane etc., and the diameter of plastic rod 30 is littler more than 1 millimeter than the internal diameter of hollow tube 21.This step purpose is to fill up with plastic rod 30 space at 21 centers of shell, makes the inwall of heat pipe capillary imbibition core copper fleece applying shell 21 in the subsequent step, and does not need the copper fiber to fill up whole shell inside, thereby reduce the heat pipe preparation cost.
Step 4 as shown in Figure 5, in step 1 gained mixture 40 implantation steps 3 formed spaces 31, is filled with the space, is beneficial to subsequent step and forms heat pipe capillary imbibition core; Because the mixture of organic solvent and nanoscale copper-containing compound fiber has flowability, be fit to inject the shell of Any shape, so this method also is suitable for preparing the capillary wick of flexure type heat pipe.
Step 5, in reducing atmosphere, calcine, removing plastic rod 30 and organic solvent, and make nanoscale copper-containing compound fiber reduction become the copper fleece, this copper fleece is attached at hollow tube 21 inwalls, promptly constitutes the capillary wick 22 (as shown in Figure 7) of the heat pipe of present embodiment formation; Calcining heat is 600～900 ℃, and reducing atmosphere is hydrogen, nitrogen or inert gas argon.Because plastic rod decomposes also carbonization with organic solvent under the high temperature, carbon has reproducibility, so when only passing to protective gas such as nitrogen or argon gas in the calcination process, carbon still can be reduced into copper compound the copper metal.
Step 6 is evacuated hollow tube.
Step 7 pours into appropriate amount of fluid as working fluid in hollow tube; Working fluid comprises liquid such as pure water, ammoniacal liquor, methyl alcohol, acetone, heptane, also can add the Heat Conduction Material particulate in liquid, is filled with the nano carbon microsphere of nanoscale copper powder etc. as copper powder, nano carbon microsphere, inside, to increase the heat conductivility of working fluid.
Step 8 is sealed hollow tube, and working fluid is sealed in the hollow tube.
As shown in Figure 6, the prepared heat pipe 20 of first embodiment of the invention comprises shell 21, imbibition core 22 and is sealed in working fluid (figure indicates) in the shell 21 that wherein imbibition core 22 is the metallic copper fleece, is close to shell 21 inwalls.
The flexure type heat control Preparation Method that second embodiment of the invention provides comprises:
Step 1 provides the mixture of nanoscale copper-containing compound fiber and organic solvent; Proper amount of nano level copper-containing compound fiber and an amount of organic solvent promptly are provided, and both are mixed formation one mixture;
Step 2 provides the hollow tube of an end closure; This hollow tube will be as heat pipe package, this step and the no sequencing of step 1;
Step 3 is inserted the plastic rod of a diameter less than above-mentioned hollow tube internal diameter in the hollow tube, makes and forms a space between plastic rod and the hollow tube inwall;
Step 4, machining; Hollow tube is processed into required curved shape, as " L " type;
Step 5 is injected the space with mixture;
Step 6 is calcined in reducing atmosphere, removing plastic rod and organic solvent, and makes nanoscale copper-containing compound fiber reduction become the copper fleece;
Step 7 is evacuated hollow tube;
Step 8 pours into an amount of working fluid in hollow tube;
Step 9 is sealed hollow tube, and working fluid is sealed in the hollow tube.
The heat control Preparation Method that second embodiment is provided is compared with the heat control Preparation Method that first embodiment is provided, step 1 is identical to step 3, the step 5 with second embodiment is identical to step 9 respectively to step 8 for the step 4 of first embodiment, two complete method differences are that second embodiment further comprises step 4 after step 3, promptly hollow tube 21 is processed into required form, so that prepare the flexure type heat pipe of differently curved degree by machining; As present embodiment hollow tube 51 is processed into " L " type.
As shown in Figure 7, the prepared heat pipe 50 of second embodiment of the invention comprises shell 51, imbibition core 52 and is sealed in working fluid (figure indicates) in the shell 51 that wherein imbibition core 52 is the metallic copper fleece, is close to shell 51 inwalls.
Heat control Preparation Method provided by the present invention has the following advantages: by the plastic rod of a diameter less than the heat pipe package internal diameter, between plastic rod and hollow tube inwall, form a space, capillary wick is attached to the heat pipe package inwall by this space and calcination process, and because the plastic cement cost is starkly lower than the metallic fiber cost, thereby the heat pipe manufacturing cost reduces; In addition, this method adopts organic solvent hybrid nanoscale copper-containing compound fiber to inject heat pipe package, and the flexure type heat pipe also is suitable for, and therefore, forms no longer difficulty of capillary wick in the flexure type heat pipe package, is fit to preparation flexure type heat pipe.

Claims (10)

1. a heat control Preparation Method is characterized in that comprising the following steps:
The mixture of proper amount of nano level copper-containing compound fiber with an amount of organic solvent is provided;
Provide one to comprise the two ends and the hollow tube of an end closure wherein;
The plastic rod of one diameter less than above-mentioned hollow tube internal diameter inserted in the hollow tube, make and form a space between plastic rod and the hollow tube inwall;
Said mixture is injected above-mentioned space;
In reducing atmosphere, calcine, removing plastic rod and organic solvent, and make nanoscale copper-containing compound fiber reduction become the copper fleece;
Hollow tube is evacuated;
In hollow tube, pour into an amount of working fluid;
The hollow tube other end is sealed.
2. heat control Preparation Method as claimed in claim 1 further comprises after it is characterized in that inserting plastic rod in the hollow tube and machining hollow tube is processed into required flexure type.
3. heat control Preparation Method as claimed in claim 1 is characterized in that nanoscale copper-containing compound fiber (electrospinning) method of can knitting by electrospinning prepares.
4. heat control Preparation Method as claimed in claim 1 is characterized in that organic solvent comprises ethanol, isopropyl alcohol or acetone.
5. heat control Preparation Method as claimed in claim 1 is characterized in that hollow tube is type pipe always, and its material comprises copper, aluminium, steel, carbon steel, stainless steel, iron, nickel, titanium or its alloy.
6. heat control Preparation Method as claimed in claim 1 is characterized in that the plastic rod material comprises polyethylene, polypropylene or polyurethane.
7. heat control Preparation Method as claimed in claim 1 is characterized in that calcining heat is 600～900 ℃.
8. heat control Preparation Method as claimed in claim 1 is characterized in that calcining reduction atmosphere comprises hydrogen, nitrogen or inert gas argon.
9. heat control Preparation Method as claimed in claim 1 is characterized in that being added with in the working fluid Heat Conduction Material particulate.
10. heat control Preparation Method as claimed in claim 9 is characterized in that the Heat Conduction Material particulate comprises copper powder, nano carbon microsphere or the inner nano carbon microsphere that is filled with the nanoscale copper powder.
CNB2003101176046A 2003-12-20 2003-12-20 Heat pipe preparing method Expired - Fee Related CN1307399C (en)

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Application Number Priority Date Filing Date Title
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Application Number Priority Date Filing Date Title
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CN1629593A true CN1629593A (en) 2005-06-22
CN1307399C CN1307399C (en) 2007-03-28

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Cited By (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101261096B (en) * 2007-03-08 2010-04-14 纬创资通股份有限公司 Heat pipe and method for manufacturing capillary structure on inner wall thereof
CN103921088A (en) * 2014-03-17 2014-07-16 威海洋刻新能源有限责任公司 System by utilizing nano particles to produce porous-core-panel type nano heat pipe
CN105091647A (en) * 2015-08-27 2015-11-25 朱惠冲 Plane superconduction heat pipe with graphite liquid absorption cores and preparation method of plane superconduction heat pipe
CN105841529A (en) * 2016-03-31 2016-08-10 苏州德川环保科技有限公司 Manufacturing method for nano heat pipe
CN105873411A (en) * 2015-01-19 2016-08-17 深圳兴奇宏科技有限公司 Water-cooling plate structure and manufacturing method thereof
CN109546260A (en) * 2018-11-16 2019-03-29 中山大学 A kind of novel thermal transfer devices using heat pipe-PCM coupling thermal management technology
CN111426226A (en) * 2020-04-21 2020-07-17 福建永安市永清石墨烯研究院有限公司 Graphene heat pipe and preparation method thereof

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US9763359B2 (en) 2015-05-29 2017-09-12 Oracle International Corporation Heat pipe with near-azeotropic binary fluid

Family Cites Families (4)

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CN2354102Y (en) * 1998-12-29 1999-12-15 中国科学院低温技术实验中心 Filled type integral heat conduction heat exchanger
JP2003155503A (en) * 2001-11-15 2003-05-30 Mitsubishi Materials Corp Method for manufacturing porous metal
KR100439258B1 (en) * 2001-12-27 2004-07-07 김영하 A Heat Pipe Manufacturing Method
KR20030065686A (en) * 2002-01-30 2003-08-09 삼성전기주식회사 Heat pipe and method thereof

Cited By (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101261096B (en) * 2007-03-08 2010-04-14 纬创资通股份有限公司 Heat pipe and method for manufacturing capillary structure on inner wall thereof
CN103921088A (en) * 2014-03-17 2014-07-16 威海洋刻新能源有限责任公司 System by utilizing nano particles to produce porous-core-panel type nano heat pipe
CN105873411A (en) * 2015-01-19 2016-08-17 深圳兴奇宏科技有限公司 Water-cooling plate structure and manufacturing method thereof
CN105091647A (en) * 2015-08-27 2015-11-25 朱惠冲 Plane superconduction heat pipe with graphite liquid absorption cores and preparation method of plane superconduction heat pipe
CN105841529A (en) * 2016-03-31 2016-08-10 苏州德川环保科技有限公司 Manufacturing method for nano heat pipe
CN109546260A (en) * 2018-11-16 2019-03-29 中山大学 A kind of novel thermal transfer devices using heat pipe-PCM coupling thermal management technology
CN111426226A (en) * 2020-04-21 2020-07-17 福建永安市永清石墨烯研究院有限公司 Graphene heat pipe and preparation method thereof

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Granted publication date: 20070328

Termination date: 20171220