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CN1602716A - A method for directly producing refreshing tablets by using liquid pullulan - Google Patents

A method for directly producing refreshing tablets by using liquid pullulan Download PDF

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Publication number
CN1602716A
CN1602716A CN 200410065764 CN200410065764A CN1602716A CN 1602716 A CN1602716 A CN 1602716A CN 200410065764 CN200410065764 CN 200410065764 CN 200410065764 A CN200410065764 A CN 200410065764A CN 1602716 A CN1602716 A CN 1602716A
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Prior art keywords
film
prescription
propiram
starch
liquid
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Pending
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CN 200410065764
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Chinese (zh)
Inventor
童群义
余凤军
梁俊英
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Botou Qingqing Food LLC
Jiangnan University
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Botou Qingqing Food LLC
Jiangnan University
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Priority to CN 200410065764 priority Critical patent/CN1602716A/en
Publication of CN1602716A publication Critical patent/CN1602716A/en
Pending legal-status Critical Current

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Abstract

This is a way of producing pill directly using liquid pululan, belonging to the technical field of production of spare food. The invention use CGMCC No.1234, fenment, then we get the liquid, offering the material. The liquid is used to make the film. Control the film's dry degree, and then the pill is made over. The pill produced in this way compared with the foreign, has the close quality, but its cost is much lower, so it has the distinct competitive power.

Description

一种利用液体普鲁兰直接生产爽口片的方法A method for directly producing refreshing tablets by using liquid pullulan

技术领域technical field

一种利用液体普鲁兰直接生产爽口片的方法,属于休闲食品制备技术领域。The invention discloses a method for directly producing refreshing tablets by using liquid pullulan, which belongs to the technical field of snack food preparation.

背景技术Background technique

随着人们生活水平的提高,口香糖之类的休闲食品日益受到人们的喜爱,近年来这类休闲食品逐步成为具有广大消费者的热门商品。然而,由于口香糖也存在一些不足之处,例如:口香糖经过咀嚼之后需要吐弃废胶残渣而污染环境、清凉感不足等等。Along with the raising of people's living standard, the leisure food of chewing gum and so on is subject to liking of people day by day, and this type of leisure food gradually becomes the popular commodity with numerous consumers in recent years. Yet, because chewing gum also has some disadvantages, for example: after chewing, the chewing gum needs to spit out the waste rubber residue and pollute the environment, the refreshing feeling is not enough or the like.

近年来,美国生产了一种名为Listerine的产品在美国、加拿大等地很受欢迎,该产品具有强烈的薄荷风味或其它风味,入口即溶、气味芳香,具有提神醒脑、杀灭口腔细菌、清除口腔异味等功能,可代替口香糖而成为一种环保、时髦的休闲小食品,市场前景看好。该产品国内称为爽口片或爽口糖果。In recent years, the United States has produced a product called Listerine, which is very popular in the United States, Canada and other places. This product has a strong mint flavor or other flavors, melts in the mouth, and has an aromatic smell. It can refresh the mind and kill oral bacteria. , remove bad breath and other functions, can replace chewing gum and become a kind of environmental protection, fashionable leisure food, the market prospect is promising. This product is called refreshing tablet or refreshing candy in China.

爽口片是在速溶性可食性膜中添加薄荷醇、桉叶油、水杨酸甲酯等清凉香味料而制成的一种具有浓郁风味的膜状食品,其关键技术包括速溶性可食性膜的研究、清凉香料的稳定技术研究、以及连续制膜技术研究等。Refreshing tablet is a kind of film-shaped food with strong flavor made by adding menthol, eucalyptus oil, methyl salicylate and other cool flavors to the instant edible film. Its key technology includes instant edible film Research on the stabilization technology of refreshing spices, research on continuous film-making technology, etc.

但目前爽口片的主要成膜组份普鲁兰的生产技术受到国外的垄断,而爽口片又具有较大的市场需求。But at present, the production technology of pullulan, the main film-forming component of refreshing tablets, is monopolized by foreign countries, and refreshing tablets have a large market demand.

发明内容Contents of the invention

本发明的目的是提供一种利用液体普鲁兰直接生产爽口片的方法,所用液体普鲁兰原料为自行开发的产品,可以打破国外的垄断,实现工业化生产爽口片,满足市场的需求。The purpose of the present invention is to provide a method for directly producing refreshing tablets by using liquid pullulan. The raw material of liquid pullulan is a self-developed product, which can break the monopoly of foreign countries, realize industrial production of refreshing tablets, and meet the needs of the market.

本发明的技术方案:利用液体普鲁兰生产爽口片的方法,是以普鲁兰作为主要成膜组份,其配方以干基计各组份质量%为:Technical scheme of the present invention: the method for utilizing liquid pullulan to produce refreshing tablet is to take pullulan as main film-forming component, and its formula is with each component mass % of dry basis:

普鲁兰              35-40Pullulan 35-40

醋酸酯淀粉          23-27Acetate starch 23-27

海藻酸钠            3-4Sodium alginate 3-4

薄荷醇              11-13Menthol 11-13

薄荷香精            6-7Mint flavor 6-7

桉叶油                             2-3Eucalyptus oil 2-3

水杨酸甲酯                         2-3Methyl salicylate 2-3

聚氧乙烯山梨醇酯-80(吐温-80)       0.6-0.7Polyoxyethylene sorbitol ester-80 (Tween-80) 0.6-0.7

单硬脂酸甘油酯                     0.2-0.3Glyceryl monostearate 0.2-0.3

阿拉伯胶                           2-3Gum Arabic 2-3

辛烯基琥珀酸淀粉酯                 1-2Starch octenyl succinate 1-2

甘油                               1-2Glycerin 1-2

山梨醇                             1-2Sorbitol 1-2

甜味剂                             适量Sweetener Appropriate amount

色素                              适量Pigment Appropriate amount

按上述配方配制成的浆料在工业化连续制膜设备上连续制膜,控制膜的干燥度制得爽口片产品。The slurry prepared according to the above formula is continuously film-formed on industrialized continuous film-making equipment, and the dryness of the film is controlled to obtain refreshing tablet products.

所用原料普鲁兰为自行研制的液体普鲁兰,固形物含量为60-70%。The raw material pullulan used is self-developed liquid pullulan with a solid content of 60-70%.

所用辅助成膜组份,还可用羟丙基淀粉、羧甲基淀粉、氧化淀粉、甲基纤维素或羧甲基纤维素替代醋酸酯淀粉。The auxiliary film-forming component used can also replace acetate starch with hydroxypropyl starch, carboxymethyl starch, oxidized starch, methyl cellulose or carboxymethyl cellulose.

所用辅料还可用卡拉胶、魔芋粉或明胶代替阿拉伯胶。Carrageenan, konjac flour or gelatin can also be used instead of gum arabic as the auxiliary material.

所用香精还可用草莓香精、柠檬香精、麝香草酚等代替而生产不同风味的产品。The essence used can also be replaced by strawberry essence, lemon essence, thymol, etc. to produce products with different flavors.

所用甜味剂为蔗糖、葡萄糖、糖精、阿斯巴甜等甜味剂。The sweetener used is sweeteners such as sucrose, glucose, saccharin, aspartame.

所用的色素为柠檬黄、亮兰等。The pigments used are lemon yellow, bright blue and so on.

工业化连续制膜设备为自行研制,由江南大学与河北泊头市清清食品有限责任公司共同研制成功,制膜机由两个直径600mm的铝制烘缸和一条长13米、宽400mm、厚0.7mm的紫铜或不锈钢流涎带联成一个整体,烘缸带动流涎带以一定速度前进,流涎带置于一个基本密闭的干燥室内,由蒸汽加热烘缸和干燥室,使干燥室内的温度保持在80℃左右,干燥时产生的二次蒸汽由管道排到外面。制膜时将上述按配方配制成的浆料经一个宽为0.4-0.5mm的狭缝流向流涎带上,经刮膜装置刮成均匀薄膜,厚度30-40μm,根据产品的要求,调节狭逢的厚度可以得到不同厚度的薄膜。由于流涎带在干燥室中不断的移动,薄膜中的水分不断蒸发,便得到具有一定机械强度的薄膜。烘缸中的蒸汽压力一般控制在0.15-0.25kg/cm2(表压),压力不可过高,否则会使膜产生很多气孔,压力太小则膜不干。干燥室内要根据气候条件喷入蒸汽调湿,使干燥室保持一定的湿度,过分干燥则膜发脆,湿度太大则膜不干。The industrialized continuous film-making equipment is self-developed, jointly developed by Jiangnan University and Hebei Botou Qingqing Food Co., Ltd. The film-making machine consists of two aluminum drying cylinders with a diameter of 600mm and a 13-meter-long, 400mm-wide, thick The 0.7mm red copper or stainless steel drool belt is connected as a whole, and the drool belt is driven by the drying cylinder to move forward at a certain speed. At about 80°C, the secondary steam generated during drying is discharged to the outside through the pipe. When making the film, the above-mentioned slurry formulated according to the formula flows to the drool belt through a slit with a width of 0.4-0.5mm, and is scraped into a uniform film by a scraping device with a thickness of 30-40μm. According to the requirements of the product, adjust the slit Films of different thicknesses can be obtained. Due to the continuous movement of the drool belt in the drying room, the water in the film is continuously evaporated, and a film with certain mechanical strength is obtained. The steam pressure in the drying cylinder is generally controlled at 0.15-0.25kg/cm 2 (gauge pressure). The pressure should not be too high, otherwise it will cause many pores in the film. If the pressure is too small, the film will not dry. The drying room should be sprayed with steam according to the climatic conditions to adjust the humidity, so that the drying room can maintain a certain humidity. If it is too dry, the film will become brittle, and if the humidity is too high, the film will not dry.

本发明的有益效果:本发明方法所生产的爽口片与国外的固体普鲁兰所生产的爽口片进行比较,产品质量相近,但本发明产品的成本大幅度降低,经济上具有明显的竞争力。所用液体普鲁兰原料为自行开发的产品,以出芽短梗霉CGMCCNo.1234为菌种,经发酵罐培养制得的液体普鲁兰(已另行申请中国专利),可以打破国外的垄断,实现工业化生产爽口片,满足市场的需求。Beneficial effects of the present invention: the refreshing tablets produced by the method of the present invention are compared with the refreshing tablets produced by foreign solid pullulan, and the product quality is similar, but the cost of the product of the present invention is greatly reduced, and the economy has obvious competitiveness . The raw material of the liquid pullulan used is a self-developed product, with Aureobasidium pullulans CGMCCNo. The industrialized production of refreshing tablets meets the needs of the market.

具体实施方式Detailed ways

实施例1Example 1

以普鲁兰作为主要成膜组份,其配方以干基计为:With pullulan as the main film-forming component, its formula is calculated on a dry basis:

普鲁兰                          30gPullulan 30g

醋酸酯淀粉                      20gAcetate starch 20g

海藻酸钠                        3gSodium Alginate 3g

薄荷醇                          10gMenthol 10g

薄荷香精                        5gPeppermint Flavor 5g

桉叶油                          2gEucalyptus oil 2g

水杨酸甲酯                      2gMethyl salicylate 2g

聚氧乙烯山梨醇酯-80(吐温-80)    0.5gPolyoxyethylene sorbitol ester-80 (Tween-80) 0.5g

单硬脂酸甘油酯                  0.2gGlyceryl monostearate 0.2g

阿拉伯胶                        1.5gGum Arabic 1.5g

辛烯基琥珀酸淀粉酯              1gStarch octenyl succinate 1g

甘油                            1gGlycerin 1g

山梨醇                          1gSorbitol 1g

甜味剂                          适量Sweetener Appropriate amount

色素                            适量Pigment Appropriate amount

按上述配方配制成的浆料在工业化连续制膜设备上连续制膜,控制膜的干燥度和卫生指标,制得符合SB10018-2001要求的爽口片产品。The slurry prepared according to the above formula is continuously film-formed on industrial continuous film-making equipment, and the dryness and hygienic index of the film are controlled to obtain refreshing tablet products that meet the requirements of SB10018-2001.

所用原料普鲁兰为液体普鲁兰,固形物含量为60-70%。The raw material pullulan used is liquid pullulan with a solid content of 60-70%.

实施例2Example 2

配方中不用醋酸淀粉酯,改用羟丙基淀粉;不用阿拉伯胶,改用卡拉胶;不用薄荷香精,改用柠檬香精;配方中其它原料组份、用量均同实施例1。Instead of starch acetate, hydroxypropyl starch is used in the formula; instead of gum arabic, carrageenan is used instead; instead of peppermint essence, lemon essence is used instead; other raw material components and consumptions in the formula are the same as in Example 1.

实施例3Example 3

配方中不用醋酸淀粉酯,改用羧甲基淀粉;不用阿拉伯胶,改用魔芋粉;不用薄荷香精,改用草莓香精;配方中其它原料组份、用量均同实施例1。Instead of starch acetate, carboxymethyl starch is used instead of starch acetate; instead of gum arabic, konjac powder is used;

Claims (8)

1, a kind of method of utilizing the liquid Propiram to produce refreshing tablets is characterized in that in butt, each component quality % is with the refreshing tablets prescription of Propiram as main film forming component:
Propiram 35-40
Acetate starch 23-27
Sodium alginate 3-4
Menthol 11-13
Peppermint essence 6-7
Eucalyptus oil 2-3
Gaultherolin 2-3
Polyoxyethylene sorbitan ester-80 0.6-0.7
Glycerin monostearate 0.2-0.3
Arabic gum 2-3
Starch octenyl succinate anhydride 1-2
Glycerine 1-2
Sorbierite 1-2
Sweetener is an amount of
Pigment is an amount of
Make film continuously by the slurry that above-mentioned formulated becomes on the continuous membrane equipment of industrialization, the aridity of controlling diaphragm makes the refreshing tablets product.
2, method according to claim 1, wherein raw materials used Propiram is the liquid Propiram, solid content is 60-70%.
3, method according to claim 1 in the wherein said prescription, without acetate starch, changes into hydroxypropul starch, CMS, oxidized starch, methylcellulose or carboxymethyl cellulose.
4, method according to claim 1 in the wherein said prescription, without peppermint essence, changes into strawberry essence, lemon extract or thymol.
5, method according to claim 1 in the wherein said prescription, without Arabic gum, changes into carragheen, konjaku flour or gelatin.
6, method according to claim 1, in the wherein said prescription, sweetener is sucrose, glucose, asccharin or Aspartame.
7, method according to claim 1, in the wherein said prescription, pigment is lemon yellow or bright orchid.
8, method according to claim 1, continuous filming technology condition wherein is: slurry flows on red copper or the stainless steel hydrostomia band through the slit of a wide 0.4-0.5mm, spread to the film that thickness is 30-40 μ m through scraping film device, film is loaded in and moves oven dry on the hydrostomia band in hothouse, and baking temperature is controlled to be 80 ℃.
CN 200410065764 2004-11-16 2004-11-16 A method for directly producing refreshing tablets by using liquid pullulan Pending CN1602716A (en)

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Cited By (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN100360048C (en) * 2006-05-25 2008-01-09 四川大学 A kind of preparation method of instant refreshing film food
CN101862024A (en) * 2010-06-07 2010-10-20 中国烟草总公司郑州烟草研究院 Refreshing tablets containing tobacco components
CN103897407A (en) * 2012-12-27 2014-07-02 辽宁阿里郎生物工程股份有限公司 Anti-doze sea cucumber polypeptide edible film and preparation method thereof
CN104256258A (en) * 2014-10-16 2015-01-07 北京中科邦尼国际科技有限责任公司 Composition for compound functional sugar, tasty tablets and preparation method of tasty tablets
CN104745648A (en) * 2015-02-06 2015-07-01 南京以标能源有限责任公司 Application of salicylic acid and analogs of salicylic acid to improving quality of microalgae biodiesel
CN104798975A (en) * 2015-04-21 2015-07-29 山东福瑞达生物科技有限公司 Solution to problem of plate sticking during production process of Pulullan refreshing and tasting chips
CN104824508A (en) * 2015-04-21 2015-08-12 山东福瑞达生物科技有限公司 Nisin oral refreshing and tasting chips and preparation method therefor
US10568839B2 (en) 2011-01-11 2020-02-25 Capsugel Belgium Nv Hard capsules
US11319566B2 (en) 2017-04-14 2022-05-03 Capsugel Belgium Nv Process for making pullulan
US11576870B2 (en) 2017-04-14 2023-02-14 Capsugel Belgium Nv Pullulan capsules

Cited By (15)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN100360048C (en) * 2006-05-25 2008-01-09 四川大学 A kind of preparation method of instant refreshing film food
CN101862024A (en) * 2010-06-07 2010-10-20 中国烟草总公司郑州烟草研究院 Refreshing tablets containing tobacco components
CN101862024B (en) * 2010-06-07 2013-04-17 中国烟草总公司郑州烟草研究院 Refreshing tablets containing tobacco components
US10568839B2 (en) 2011-01-11 2020-02-25 Capsugel Belgium Nv Hard capsules
CN103897407A (en) * 2012-12-27 2014-07-02 辽宁阿里郎生物工程股份有限公司 Anti-doze sea cucumber polypeptide edible film and preparation method thereof
CN103897407B (en) * 2012-12-27 2016-01-20 辽宁阿里郎生物工程股份有限公司 A kind of anti-drowsy sea cucumber polypeptide edible film and preparation method thereof
CN104256258A (en) * 2014-10-16 2015-01-07 北京中科邦尼国际科技有限责任公司 Composition for compound functional sugar, tasty tablets and preparation method of tasty tablets
CN104745648B (en) * 2015-02-06 2018-02-27 南京以标能源有限责任公司 The application of a kind of salicylic acid and salicylic acid and its analogs in microalgae biodiesel quality is improved
CN104745648A (en) * 2015-02-06 2015-07-01 南京以标能源有限责任公司 Application of salicylic acid and analogs of salicylic acid to improving quality of microalgae biodiesel
CN104798975A (en) * 2015-04-21 2015-07-29 山东福瑞达生物科技有限公司 Solution to problem of plate sticking during production process of Pulullan refreshing and tasting chips
CN104798975B (en) * 2015-04-21 2017-11-10 山东福瑞达生物科技有限公司 A kind of solution method of pulullan polysaccharide refreshing tablets production process haftplatte
CN104824508A (en) * 2015-04-21 2015-08-12 山东福瑞达生物科技有限公司 Nisin oral refreshing and tasting chips and preparation method therefor
US11319566B2 (en) 2017-04-14 2022-05-03 Capsugel Belgium Nv Process for making pullulan
US11576870B2 (en) 2017-04-14 2023-02-14 Capsugel Belgium Nv Pullulan capsules
US11878079B2 (en) 2017-04-14 2024-01-23 Capsugel Belgium Nv Pullulan capsules

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