CN1568688A - Production technique of high performance plant agricultural chemicals aerosol - Google Patents
Production technique of high performance plant agricultural chemicals aerosol Download PDFInfo
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- CN1568688A CN1568688A CN 200410012288 CN200410012288A CN1568688A CN 1568688 A CN1568688 A CN 1568688A CN 200410012288 CN200410012288 CN 200410012288 CN 200410012288 A CN200410012288 A CN 200410012288A CN 1568688 A CN1568688 A CN 1568688A
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- 238000004519 manufacturing process Methods 0.000 title claims abstract description 22
- 239000000443 aerosol Substances 0.000 title claims abstract description 17
- 238000000034 method Methods 0.000 title abstract description 5
- 239000003905 agrochemical Substances 0.000 title description 6
- 235000017166 Bambusa arundinacea Nutrition 0.000 claims abstract description 44
- 235000017491 Bambusa tulda Nutrition 0.000 claims abstract description 44
- 241001330002 Bambuseae Species 0.000 claims abstract description 44
- 235000015334 Phyllostachys viridis Nutrition 0.000 claims abstract description 44
- 239000011425 bamboo Substances 0.000 claims abstract description 44
- 239000000052 vinegar Substances 0.000 claims abstract description 38
- 235000021419 vinegar Nutrition 0.000 claims abstract description 38
- 239000003795 chemical substances by application Substances 0.000 claims abstract description 23
- 239000000843 powder Substances 0.000 claims abstract description 17
- 239000000575 pesticide Substances 0.000 claims abstract description 14
- 241000196324 Embryophyta Species 0.000 claims abstract description 12
- 241000411851 herbal medicine Species 0.000 claims abstract description 11
- 239000002994 raw material Substances 0.000 claims abstract description 7
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 6
- 230000018044 dehydration Effects 0.000 claims abstract description 4
- 238000006297 dehydration reaction Methods 0.000 claims abstract description 4
- 239000012752 auxiliary agent Substances 0.000 claims abstract description 3
- 238000005516 engineering process Methods 0.000 claims description 14
- 239000000203 mixture Substances 0.000 claims description 10
- 241000218378 Magnolia Species 0.000 claims description 7
- 241001145009 Sophora alopecuroides Species 0.000 claims description 7
- 238000007493 shaping process Methods 0.000 claims description 6
- 239000000779 smoke Substances 0.000 claims description 6
- 238000003756 stirring Methods 0.000 claims description 6
- 235000003092 Artemisia dracunculus Nutrition 0.000 claims description 4
- 240000001851 Artemisia dracunculus Species 0.000 claims description 4
- 241000206469 Pulsatilla Species 0.000 claims description 4
- 235000016639 Syzygium aromaticum Nutrition 0.000 claims description 4
- 244000223014 Syzygium aromaticum Species 0.000 claims description 4
- 238000002156 mixing Methods 0.000 claims description 4
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 claims description 2
- 229910052799 carbon Inorganic materials 0.000 claims description 2
- 238000002485 combustion reaction Methods 0.000 claims description 2
- 239000007800 oxidant agent Substances 0.000 claims description 2
- 230000001590 oxidative effect Effects 0.000 claims description 2
- VKJKEPKFPUWCAS-UHFFFAOYSA-M potassium chlorate Chemical compound [K+].[O-]Cl(=O)=O VKJKEPKFPUWCAS-UHFFFAOYSA-M 0.000 claims description 2
- 235000014347 soups Nutrition 0.000 claims description 2
- 239000002023 wood Substances 0.000 claims description 2
- 239000003814 drug Substances 0.000 abstract description 10
- 239000000126 substance Substances 0.000 abstract description 9
- 239000006227 byproduct Substances 0.000 abstract description 2
- 239000003610 charcoal Substances 0.000 abstract description 2
- 229940079593 drug Drugs 0.000 abstract description 2
- 239000000446 fuel Substances 0.000 abstract description 2
- 239000003960 organic solvent Substances 0.000 abstract description 2
- 230000008569 process Effects 0.000 abstract description 2
- 239000007788 liquid Substances 0.000 abstract 5
- 208000005156 Dehydration Diseases 0.000 abstract 1
- 238000010438 heat treatment Methods 0.000 abstract 1
- 230000000694 effects Effects 0.000 description 5
- 230000001954 sterilising effect Effects 0.000 description 5
- 235000013311 vegetables Nutrition 0.000 description 5
- 230000000844 anti-bacterial effect Effects 0.000 description 3
- 239000007921 spray Substances 0.000 description 3
- 238000004659 sterilization and disinfection Methods 0.000 description 3
- 208000031888 Mycoses Diseases 0.000 description 2
- CRQQGFGUEAVUIL-UHFFFAOYSA-N chlorothalonil Chemical compound ClC1=C(Cl)C(C#N)=C(Cl)C(C#N)=C1Cl CRQQGFGUEAVUIL-UHFFFAOYSA-N 0.000 description 2
- 235000019504 cigarettes Nutrition 0.000 description 2
- 239000002131 composite material Substances 0.000 description 2
- 201000010099 disease Diseases 0.000 description 2
- 208000037265 diseases, disorders, signs and symptoms Diseases 0.000 description 2
- 230000000857 drug effect Effects 0.000 description 2
- 239000012467 final product Substances 0.000 description 2
- 239000004033 plastic Substances 0.000 description 2
- 230000004083 survival effect Effects 0.000 description 2
- 235000005254 Allium ampeloprasum Nutrition 0.000 description 1
- 240000006108 Allium ampeloprasum Species 0.000 description 1
- 241000894006 Bacteria Species 0.000 description 1
- 239000005747 Chlorothalonil Substances 0.000 description 1
- 240000008067 Cucumis sativus Species 0.000 description 1
- 235000010799 Cucumis sativus var sativus Nutrition 0.000 description 1
- 241000221785 Erysiphales Species 0.000 description 1
- 206010017533 Fungal infection Diseases 0.000 description 1
- 241000238631 Hexapoda Species 0.000 description 1
- 235000007688 Lycopersicon esculentum Nutrition 0.000 description 1
- 241000233679 Peronosporaceae Species 0.000 description 1
- 240000003768 Solanum lycopersicum Species 0.000 description 1
- 239000003899 bactericide agent Substances 0.000 description 1
- 230000004888 barrier function Effects 0.000 description 1
- 238000000151 deposition Methods 0.000 description 1
- 238000009313 farming Methods 0.000 description 1
- 239000003337 fertilizer Substances 0.000 description 1
- 238000009408 flooring Methods 0.000 description 1
- 208000024386 fungal infectious disease Diseases 0.000 description 1
- 239000002917 insecticide Substances 0.000 description 1
- 238000000465 moulding Methods 0.000 description 1
- 230000008520 organization Effects 0.000 description 1
- 230000035699 permeability Effects 0.000 description 1
- 230000000361 pesticidal effect Effects 0.000 description 1
- 239000000447 pesticide residue Substances 0.000 description 1
- 230000003405 preventing effect Effects 0.000 description 1
- 239000000047 product Substances 0.000 description 1
- 238000010298 pulverizing process Methods 0.000 description 1
- 230000000452 restraining effect Effects 0.000 description 1
- 230000000391 smoking effect Effects 0.000 description 1
- 238000001228 spectrum Methods 0.000 description 1
- 238000003860 storage Methods 0.000 description 1
- 235000013619 trace mineral Nutrition 0.000 description 1
- 239000011573 trace mineral Substances 0.000 description 1
Landscapes
- Agricultural Chemicals And Associated Chemicals (AREA)
Abstract
本发明涉及一种高效植物农药烟雾剂生产工艺，其可采用竹醋粉或竹醋液和供热剂加工制成，采用竹醋粉的生产工艺为：将竹醋粉3－7份(重量份数比)和供热剂85－95份(重量份数比)混合后搅拌均匀经压制成形；采用竹醋液的生产工艺为：将浓度为15－40％的竹醋液200－500份(重量份数比)和供热剂85－95份(重量份数比)混合后搅拌均匀进行脱水处理，将含水量控制在10－60％，经压制成形；本发明采用我国南方大部分盛产竹子地区生产的竹炭副产品竹醋液或竹醋粉为主要原料，在本发明生产工艺中竹醋液既是药的主剂，又是其他中草药的萃取剂(提取剂)，可提高原药使用效率、避免了有机溶剂的大量使用。同时可作为其它化学农药专用助剂，降低原药用量和减少使用过程中的二次污染；而中草药既作为药，又是竹醋液的载体，这样减少原有烟雾剂必用的燃料。The invention relates to a production process of high-efficiency plant pesticide aerosol, which can be processed by bamboo vinegar powder or bamboo vinegar liquid and a heating agent. The production process of bamboo vinegar powder is as follows: 3-7 parts of bamboo vinegar powder (weight parts ratio) and 85-95 parts of heat-supplying agent (ratio of parts by weight) are mixed, stirred evenly and pressed into shape; the production process of using bamboo vinegar liquid is as follows: 200-500 parts of bamboo vinegar liquid with a concentration of 15-40% (ratio by weight) and 85-95 parts (ratio by weight) of the heat supply agent are mixed and then stirred evenly for dehydration treatment, the water content is controlled at 10-60%, and then pressed and formed; The bamboo charcoal by-product bamboo vinegar liquid or bamboo vinegar powder produced in the bamboo area is the main raw material, and in the production process of the present invention, the bamboo vinegar liquid is not only the main agent of the medicine, but also the extractant (extractant) of other Chinese herbal medicines, which can improve the use efficiency of the original medicine , avoiding the large use of organic solvents. At the same time, it can be used as a special auxiliary agent for other chemical pesticides, reducing the amount of the original drug and reducing the secondary pollution in the process of use; while the Chinese herbal medicine is not only used as a medicine, but also a carrier of bamboo vinegar, which reduces the necessary fuel for the original aerosol.
Description
Technical field
The present invention relates to a kind of high efficiency plant pesticide aerosol production technology.
Technical background
The sterilization fumicants is a kind of new technology smoke type agricultural chemicals that does not need medical instruments to discharge agricultural chemicals with the smog form with chemical heat energy, smog agricultural chemicals particulate is generally at several microns, easily produce multiple-surface depositing, the unit settled density is than big thousands of times of conventional spray medicine, and high permeability and diffusibility arranged, to plant utilization rate height, booth can not be omitted everywhere; And water not, compare that spray medicinal herb grower survival dose is few, drug effect is high.The control of the multiple fungal diseases such as downy mildew, powdery mildew, anthracnose, late blight, early blight and leaf mold of crops such as the cucumber of be mainly used in plastic tunnel, greenhouse by solar heat, heat greenhouse and plastic canopy etc. being planted, tomato, leek.Present China's bactericidal smoking agent, mainly based on produce the tpn aerosol (other Chinese: it is excellent to restrain labor, mould must be clear, daconil) chemical name: 2,4,5,6-tetrachloro-1,3-tricyano benzene.Molecular formula: C
8Cl
4N
2This tpn aerosol is a kind of protectiveness wide-spectrum bactericide, and the mycosis of various crop is had the good preventing effect.Dispense smoke agent control greenhouse, booth vegetable damage by disease and insect, not only easy and simple to handle, reduced labour intensity, and control efficiency do not increase the indoor humidity of canopy after application method, particularly dispenser such as obviously being better than squirting, comparatively thorough to the control of disease.But the chlorothalonil smoke primary raw material is a chemical composition, in recent years, raising along with people's life aquatic products, China's entry into the World Trade Organization, home and abroad no matter is all being strengthened year by year to the demand of pollution-free vegetable, organic vegetable, green vegetables, and particularly developed country carries out trade " green barrier " to China, make the vegetable pesticide residue problem more and more become one of focus of people's concern, the inherent limitation that chemical sterilization, insecticide exist has limited its promotion and application.
Summary of the invention
Technical problem to be solved by this invention provides a kind of plant pesticide aerosol production technology that has the efficient sterilizing bacteriostasis and can effectively reduce the chemical pesticide secondary pollution.
The present invention adopts following technical scheme:
The present invention adopts bamboo vinegar powder or Bamboo vinegar solution and heat supply agent to be processed into, and adopts the production technology of bamboo vinegar powder to be: with the repressed shaping that stirs after bamboo vinegar powder 3-7 part (ratio of weight and number) and heat supply agent 85-95 part (ratio of weight and number) mixing; Adopt the production technology of Bamboo vinegar solution to be: with concentration is to stir after Bamboo vinegar solution 200-500 part (ratio of weight and number) of 15-40% and heat supply agent 85-95 part (ratio of weight and number) mixing to carry out dehydration processing, water content is controlled at 10-60%, repressed shaping.
Heat supply agent of the present invention is for producing the heat supply agent that aerosol generally adopts at present, and it comprises combustion grain (wood powder, bamboo powder or powdered carbon), oxidant (potassium chlorate) and auxiliary agent (smoke agent, anti-blushing agent).
The present invention can add Sophora alopecuroide in above-mentioned concentration is Bamboo vinegar solution 200-500 part of 15-40%, frutus cnidii, radix sophorae, the bark of official magnolia, rhizoma atractylodis, each composition ratio of weight and number is: Bamboo vinegar solution 10-20, Sophora alopecuroide 1-5, frutus cnidii 1-2, radix sophorae 1-3, bark of official magnolia 1-4, rhizoma atractylodis 0.5-3, its production process is as follows: at first said herbal medicine is pulverized, cross the 60-200 mesh sieve, pour into then in the container that Bamboo vinegar solution is housed,, the Chinese herbal medicine and the soup of invading after carrying mixed with the heat supply agent through 12-24 hour invade to carry and make the pH value at pH3-6, stir, under natural temperature, dewater then, when the raw material water content is controlled at 10-60%, repressed shaping.
The present invention also can add the Chinese herbal medicine composition of following ratio of weight and number: cloves 0.2-0.6, Chinese pulsatilla 0.4-0.6, tarragon 0.3-0.8.
Good effect of the present invention is as follows: bamboo charcoal by product Bamboo vinegar solution or bamboo vinegar powder that the present invention adopts China's south major part to abound with the production of bamboo area are primary raw material, Bamboo vinegar solution is the host of medicine in production technology of the present invention, be again the extractant (extractant) of other Chinese herbal medicines, can improve former medicine service efficiency, avoid a large amount of uses of organic solvent.Can be used as other chemical pesticide special assistant simultaneously, reduce the secondary pollution in former survival dose and the minimizing use; And Chinese herbal medicine is again the carrier of Bamboo vinegar solution both as medicine, reduces the fuel that original aerosol must be used like this.
Technology of the present invention be equipped with have sterilization, antibacterial Chinese herbal medicine is as Sophora alopecuroide, frutus cnidii, radix sophorae, the bark of official magnolia, rhizoma atractylodis, cloves, the Chinese pulsatilla, tarragon etc., carry through pulverizing, invading, mix, dehydration, moulding (film-making) naturally, stoving process is composite forms.
The pure plant aerosol of the present invention agricultural chemicals is easily lighted, and the flames of anger is composite easy, easy to use, and the restraining and sterilizing bacteria effect is remarkable.
Aerosol plant pesticide prescription of the present invention has the effect of control fungal diseases of plants, mixes with other chemical pesticide when using simultaneously, can reduce the usage amount of half chemical pesticide, and drug effect does not subtract.Can also play simultaneously foliage fertilizer and increase effect of trace elements.
Aerosol using method of the present invention:
1, every mu in general booth or greenhouse are each with invention fumicants 200-300 gram, and from their early stage every medication in 7-10 days once, use 4-5 full vegetative period.
When 2, using earlier airtight booth, greenhouse, again medicine box is placed on the canopy flooring equably, outwards the order regression is lighted one by one from the lining.
3, the time point of generally knocking off is between the lights seted off cigarette, and is once airtight, opens canopy chamber door and window morning next day and just can be engaged in normal farming operation.
Points for attention: 1, use the smoke type agricultural chemicals, booth or greenhouse must airtight, not leak cigarette, otherwise influence protection effect; 2, this fumicants is the safety-type fumicants, wants inflammable, protection against the tide during storage; 3, this fumicants can not use by open country, can not spray by thin up, and taboo enters the mouth and is strayed into intraocular.
Embodiment
Adopt bamboo vinegar powder can implement to get final product by the strict operation of above-mentioned production process for the raw material embodiment, its proportioning components be as shown in table 1:
Table 1
| Composition | Content (ratio of weight and number) | ||
| Bamboo vinegar powder | ????3 | ????5 | ????7 |
| The heat supply agent | ????90 | ????85 | ????95 |
Adopt Bamboo vinegar solution can implement to get final product by the strict operation of above-mentioned production process for the raw material embodiment, its proportioning components be shown in table 2, table 3, table 4:
Table 2
| Composition | Content (ratio of weight and number) | ||
| Bamboo vinegar solution | ????200 | ????350 | ????500 |
| The heat supply agent | ????90 | ????85 | ????95 |
Table 3
| Composition | Content (ratio of weight and number) | ||
| Bamboo vinegar solution | ????15 | ????10 | ????20 |
| Sophora alopecuroide | ????1 | ????3 | ????5 |
| Frutus cnidii | ????2 | ????1.5 | ????1 |
| Radix sophorae | ????3 | ????2 | ????1 |
| The bark of official magnolia | ????1 | ????4 | ????2.5 |
| Rhizoma atractylodis | ????0.5 | ????1.5 | ????3 |
Table 4
| Composition | Content (ratio of weight and number) | ||
| Bamboo vinegar solution | ????15 | ????10 | ????20 |
| Sophora alopecuroide | ????3 | ????1 | ????5 |
| Frutus cnidii | ????1 | ????1.5 | ????2 |
| Radix sophorae | ????3 | ????2 | ????1 |
| The bark of official magnolia | ????1 | ????4 | ????2.5 |
| Rhizoma atractylodis | ????0.5 | ????1.8 | ????3 |
| Cloves | ????0.6 | ????0.4 | ????0.2 |
| The Chinese pulsatilla | ????0.4 | ????0.6 | ????0.5 |
| Tarragon | ????0.3 | ????0.5 | ????0.8 |
Claims (4)
1, a kind of high efficiency plant pesticide aerosol production technology, it is characterized in that adopting bamboo vinegar powder or Bamboo vinegar solution and heat supply agent to be processed into, adopt the production technology of bamboo vinegar powder to be: with the repressed shaping that stirs after bamboo vinegar powder 3-7 part (ratio of weight and number) and heat supply agent 85-95 part (ratio of weight and number) mixing; Adopt the production technology of Bamboo vinegar solution to be: with concentration is to stir after Bamboo vinegar solution 200-500 part (ratio of weight and number) of 15-40% and heat supply agent 85-95 part (ratio of weight and number) mixing to carry out dehydration processing, water content is controlled at 10-60%, repressed shaping.
2, a kind of high efficiency plant pesticide aerosol production technology according to claim 1 is characterized in that described heat supply agent comprises combustion grain (wood powder, bamboo powder or powdered carbon), oxidant (potassium chlorate) and auxiliary agent (smoke agent, anti-blushing agent).
3, a kind of high efficiency plant pesticide aerosol production technology according to claim 1 and 2, it is characterized in that and in above-mentioned concentration is Bamboo vinegar solution 200-500 part of 15-40%, to add Sophora alopecuroide, frutus cnidii, radix sophorae, the bark of official magnolia, rhizoma atractylodis, ratio of weight and number between each composition is: Bamboo vinegar solution 10-20, Sophora alopecuroide 1-5, frutus cnidii 1-2, radix sophorae 1-3, bark of official magnolia 1-4, rhizoma atractylodis 0.5-3, its production process is as follows: at first said herbal medicine is pulverized, crossed the 60-200 mesh sieve, pour into then in the container that Bamboo vinegar solution is housed, through 12-24 hour invade to carry and make the pH value at pH3-6,, the Chinese herbal medicine and the soup of invading after carrying mixed with above-mentioned heat supply agent, stir, under natural temperature, dewater then, when the raw material water content is controlled at 10-60%, repressed shaping.
4, a kind of high efficiency plant pesticide aerosol production technology according to claim 3 is characterized in that also can adding the Chinese herbal medicine composition of following ratio of weight and number: cloves 0.2-0.6, Chinese pulsatilla 0.4-0.6, tarragon 0.3-0.8.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 200410012288 CN1568688A (en) | 2004-05-13 | 2004-05-13 | Production technique of high performance plant agricultural chemicals aerosol |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 200410012288 CN1568688A (en) | 2004-05-13 | 2004-05-13 | Production technique of high performance plant agricultural chemicals aerosol |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN1568688A true CN1568688A (en) | 2005-01-26 |
Family
ID=34477998
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN 200410012288 Pending CN1568688A (en) | 2004-05-13 | 2004-05-13 | Production technique of high performance plant agricultural chemicals aerosol |
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| Country | Link |
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Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101999419A (en) * | 2010-10-28 | 2011-04-06 | 药圣堂（湖南）制药有限公司 | Natural bactericidal composition, method and device for sterilizing Chinese medicinal tablets |
| CN103404544A (en) * | 2013-09-02 | 2013-11-27 | 甘肃中医学院 | Sterilization and insecticide compound, smoke agent of compound and preparation method of smoke agent |
| CN104798832A (en) * | 2015-04-06 | 2015-07-29 | 韩城市秦龙花椒科技有限责任公司 | Method for processing fumigating-killing type non-polluted pesticide smoke agent through compounding of Chinese herbal medicine plants |
| CN105875597A (en) * | 2014-11-11 | 2016-08-24 | 郭秦 | Agricultural smoke agent and preparation method thereof |
-
2004
- 2004-05-13 CN CN 200410012288 patent/CN1568688A/en active Pending
Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101999419A (en) * | 2010-10-28 | 2011-04-06 | 药圣堂（湖南）制药有限公司 | Natural bactericidal composition, method and device for sterilizing Chinese medicinal tablets |
| CN101999419B (en) * | 2010-10-28 | 2013-07-03 | 药圣堂（湖南）制药有限公司 | Natural bactericidal composition, method and device for sterilizing Chinese medicinal tablets |
| CN103404544A (en) * | 2013-09-02 | 2013-11-27 | 甘肃中医学院 | Sterilization and insecticide compound, smoke agent of compound and preparation method of smoke agent |
| CN103404544B (en) * | 2013-09-02 | 2014-10-22 | 甘肃中医学院 | Sterilization and insecticide compound, smoke agent of compound and preparation method of smoke agent |
| CN105875597A (en) * | 2014-11-11 | 2016-08-24 | 郭秦 | Agricultural smoke agent and preparation method thereof |
| CN104798832A (en) * | 2015-04-06 | 2015-07-29 | 韩城市秦龙花椒科技有限责任公司 | Method for processing fumigating-killing type non-polluted pesticide smoke agent through compounding of Chinese herbal medicine plants |
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