CN1216232A - Extraction of aloe extract - Google Patents
Extraction of aloe extract Download PDFInfo
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- CN1216232A CN1216232A CN 97114279 CN97114279A CN1216232A CN 1216232 A CN1216232 A CN 1216232A CN 97114279 CN97114279 CN 97114279 CN 97114279 A CN97114279 A CN 97114279A CN 1216232 A CN1216232 A CN 1216232A
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- juice
- aloe
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Abstract
After fresh aloe leaf is cleaned, soaked in disinfection solution for 10-20 min, washed and drip-dried, the rind and gel are separated in special aloe peeler, treated separately and mixed to produce aloe juice, concentrated aloe juice, aloe powder and other product, which may be mixed with some additive in certain amount to produce various final products. The present invention can retain the effective components in aloe fully and control the content of anthraquinone and glycosides. Using instantaneous high-temperature degradation process to replace chemical process in treating aloe juice can reduce production cost greatly.
Description
The present invention relates to the manufacture method of the manufacture method of aloe, particularly a kind of aloe extract.
Since ancient times, aloe just by the people in a lot of areas as traditional herbal medicine, be used to cure wound, burn, gastrointestinal disease, ulcer and anaphylactia and beauty treatment etc.About the propaganda of the existing report widely of the medical value of aloe.With regard to the composition of aloe, the various countries researcher does not thoroughly understand fully as yet at present, but taking it by and large, aloe leaf is made up of crust and gel two parts.In the fluid supply of aloe crust, mainly contain aloin, aloe-emodin, anthraquinone and glucoside material.The mesophyll that aloe leaf removes behind the crust claims aloe gel, and water content in the solid content matter of dehydration back about 1%, mainly contains mucopolysaccharide, fiber, albumen, ash and a small amount of aloin up to about 99%.Certainly, also contain abundant mineral matter and 18 seed amino acids and multivitamin in the aloe leaf.According to various countries, Ri Ben report especially, crust juice that it is generally acknowledged aloe now is to gastrointestinal disease, constipation and drunk etc. curative effect preferably arranged.This is main because the effect of aloin, aloe-emodin, anthraquinones.Aloe gel is then to repair cell, and is antitumor, and raising immunologic function etc. has better action.And think that the moisture content in the gel is special moisture content, very helpful to human body.Yet with regard to cosmetics, need to contain hardly the gel of anthraquinone, otherwise can cause cosmetics to change so that be divided into.With regard to the edible Aloe product, different physique, different diseases also differs widely to the requirement of anthraquinone, archen and aloin and reaction.So just be necessary to produce the different asparagus juice of crust content to adapt to various needs.Relatively more current at present asparagus juice production technology has following method usually:
(1) will handle clean asparagus juice sheet and pulverize, grind, slowly heat to about 80 ℃ behind the adding oxidant, use decolorizing with activated carbon again, to obtain not containing substantially the asparagus juice of anthraquinone;
(2) will handle clean aloe leaf and pulverize, grind after, use the method for membrane filtration again, by dialysis, remove anthraquinones;
(3) obtain aloe gel after peelling off the aloe crust by hand, after the grinding again with organic solvent extraction some composition wherein.
Above-mentioned first kind is maximum method of using at present, and its shortcoming is when sloughing anthraquinones, and the many effective ingredients in the aloe gel can be damaged; Second method also has same shortcoming, and incompatibility large-scale production; The third method production efficiency is too low, the incompatibility suitability for industrialized production, and in the aloe effective ingredient and not exclusively clearly under the situation, extract active principle separately and do not reach desirable effect.Comprehensive, 3 kinds of methods all have a common shortcoming, can not keep the effective ingredient of aloe preferably exactly, and have ignored the effect of aloe skin juice fully.
The objective of the invention is to overcome above-mentioned deficiency, a kind of effective ingredient that can keep aloe gel to greatest extent is provided, can control the content of anthraquinone or glucoside material effectively, and the aloe extract manufacture method of suitability for industrialized production.
Technical solution of the present invention is: getting the fresh aloe blade is main material, obtains the extract of aloe as follows:
(1) with cleaning blade with cleaning machine again behind the clear water immersion Chinese aloe leaf;
(2) the few part of blade two ends meat of pruning is placed on blade in the germicidal solution and soaked 10-20 minute, drains after cleaning with clear water again;
(3) separate the crust and the gel of aloe leaf neatly with the special-purpose peeling machine of aloe, and gel and crust are ground respectively;
(4) gel after will grinding is deposited after by TRANSIENT HIGH TEMPERATURE (105 ℃-125 ℃/3-5 minute) degraded and is made it the nature cooling;
(5) juice that viscosity behind the high temperature degradation is greatly reduced carries out coarse filtration, smart filter, removes fiber and sediment, promptly obtains the juice of clarifying;
(6) in the juice of clarification, add an amount of citric acid, pH value is adjusted between the 3.2-4.2, add vitamin V E (0.01%), Vc (0.02%), potassium sorbate (0.05%), sodium benzoate (0.02%), Tea Polyphenols antioxidant and bacterial inhibitors such as (0.03%) again, stir after adding certain surfactant again;
(7), by instantaneous sterilizing (120 ℃-130 ℃/3-5 minute), promptly obtain Aloe gel juice (also claiming gravy) again with gained juice high pressure homogenizer homogeneous.
The present invention has following advantage compared with the prior art:
1. guaranteed the effective ingredient of aloe gel to greatest extent.
2. the activated carbon that can add different deals on request to aloe crust juice is to control the wherein content of anthraquinone and glucoside material.
The crust and the gel that 3. can separate aloe leaf fully neatly by the aloe leaf peeling machine, so that processing respectively, but and suitability for industrialized production.
4. the extract that the present invention obtained can adapt to different purposes, and for example: asparagus juice and inspissated juice thereof and dry powder generally are used to eat.The Aloe gel juice of decolouring mixes by a certain percentage with the outer cortex of aloe, and the full juice of the aloe of acquisition is made inspissated juice and dry powder, can be used for doing cosmetics and external application raw material.
5. owing to the method that has adopted TRANSIENT HIGH TEMPERATURE that aloe juice is degraded, replaced chemical method, thereby greatly reduced manufacturing cost.
Below in conjunction with embodiment the present invention is illustrated.
Embodiment one:
Getting the fresh aloe blade is main material, obtains Aloe gel juice as follows:
(1) with behind the clear water immersion Chinese aloe leaf, cleans blade with cleaning machine again;
(2) the few part of blade two ends meat of pruning is placed on blade in the germicidal solution and soaked 10-20 minute, drains after cleaning with clear water again;
(3) separate the crust and the gel of aloe leaf neatly with the special-purpose peeling machine of aloe, and gel and crust are ground respectively;
(4) gel after will grinding is deposited after by TRANSIENT HIGH TEMPERATURE (105 ℃-125 ℃/3-5 minute) degraded and is made it the nature cooling;
(5) juice that viscosity behind the high temperature degradation is greatly reduced carries out coarse filtration, smart filter, removes fiber and sediment, promptly obtains the juice of clarifying;
(6) in the juice of clarification, add an amount of citric acid, pH value is adjusted between the 3.2-4.2, add antioxidant and bacterial inhibitors such as vitamin V E0.01%, Vc0.02%, potassium sorbate 0.05%, sodium benzoate 0.02%, Tea Polyphenols 0.03% again, stir after adding certain surfactant again;
(7), by instantaneous sterilizing (120 ℃-130 ℃/3-5 minute), promptly obtain Aloe gel juice (also claiming gravy) again with gained juice high pressure homogenizer homogeneous.
Embodiment two:
The present invention, also can obtain as follows:
(1) with in above-mentioned (4) through the gel of TRANSIENT HIGH TEMPERATURE degraded, keep drop temperature at 80 ℃-100 ℃, carry out coarse filtration immediately, temperature adds certain powder activated carbon and nontoxic oxidant (as H after the coarse filtration in the time of 70 ℃-90 ℃
2O
2), stir on one side, allow it cool off naturally on one side, its process must not be lower than 3 hours;
(2) gained juice is carried out essence filter and obtains clarified juice after, in juice, add to stir after the certain surface activating agent and tremble evenly, and use the high pressure homogenizer homogeneous, can promptly obtains stable decolored aloe gel juice after high-temperature short-time sterilization.
Embodiment three:
The present invention also can obtain as follows:
(1) crust juice described in 1 (3) is carried out coarse filtration, add certain activity carbon and nontoxic oxidant after being heated to 70 ℃-90 ℃ (as H
2O
2) back stirring on one side, Yi Bian make its automatic cooling;
(2) the crust juice that cools off after the coarse filtration is carried out the essence filter and obtain clarified juice, and add an amount of citric acid, adjust its pH value, add certain vitamin V between the 3.2-4.2
E0.01%, V
C0.02%, potassium sorbate 0.05%, antioxidants such as sodium benzoate 0.02%, Tea Polyphenols 0.03%, stir after adding certain surfactant again, use TRANSIENT HIGH TEMPERATURE sterilizer (120 ℃-130 ℃/3-5 minute) sterilization behind the homogeneous again, promptly obtain stable aloe crust juice.
Embodiment four:
The present invention also can obtain as follows:
(1) will be in the above-mentioned clarified juice adds antioxidant and bacterial inhibitors such as certain vitamin E 0.01%, Tea Polyphenols 0.03%, card pine 0.01%, stir after adding certain surfactant again;
(2) with behind the high pressure homogenizer homogeneous again with the sterilization of TRANSIENT HIGH TEMPERATURE sterilizer (120 ℃-130 ℃/3-5 minute), promptly obtain the outer cortex of stable aloe.
Embodiment five:
The Aloe gel juice that obtains is mixed by different proportion with the outer cortex of aloe, can obtain the different full juice of various aloes of composition.
Embodiment six:
Decolored aloe gel juice mixes by a certain percentage with the outer cortex of aloe, can obtain the different full juice of various aloes of composition.
Embodiment seven:
The clarified juice that obtains is concentrated into certain proportion with vacuum decker (boiling temperature is less than 65 ℃), inserts respectively between 1 (5) and 1 (6), insert in 2 (2), insert in 3 (2), insert 4 (1) before, can correspondingly obtain various concentrated asparagus juices.
Embodiment eight:
With the clarified juice vacuum decker (boiling temperature is less than 65 ℃) that obtains, make 1: 10 concentrated asparagus juice, make dry powder with spray dryer.
Embodiment nine:
The also available freeze drier of inspissated juice that obtains is made dry powder.
Embodiment ten:
The cleaning aloe leaf that obtains laterally is cut into 0.5-0.7 centimetre thin slice with slicer, be placed on the net charging tray and place drying machine, the baking temperature control is at 60 ℃-70 ℃, air-supply makes Chinese aloe tablet slowly be dried to water content and accounts for 6%, send in the infrared oven and toasted 20-30 minute, make water content reduce to 3-3.5%, the while kill bacteria, make its sum reduce to 10/below the g, after adding a certain proportion of bacterial growth inhibitor, by the sterile working requirement the dry thing of gained is crushed to below diameter 10 μ, promptly gets aloe dry powder.
Claims (10)
1, a kind of manufacture method of aloe extract, getting the fresh aloe blade is main material, it is characterized in that this manufacture method can obtain as follows:
(1) with behind the clear water immersion Chinese aloe leaf, cleans blade with cleaning machine again;
(2) the few part of blade two ends meat of pruning is placed on blade in the germicidal solution and soaked 10-20 minute, drains after cleaning with clear water again;
(3) separate the crust and the gel of aloe leaf neatly with the special-purpose peeling machine of aloe, and gel and crust are ground respectively;
(4) gel after will grinding is deposited after by TRANSIENT HIGH TEMPERATURE (105 ℃-125 ℃/3-5 minute) degraded and is made it the nature cooling;
(5) juice that viscosity behind the high temperature degradation is greatly reduced carries out coarse filtration, smart filter, removes fiber and sediment, promptly obtains the juice of clarifying;
(6) in the juice of clarification, add an amount of citric acid, pH value is adjusted between the 3.2-4.2, add antioxidant and bacterial inhibitors such as vitamin V E0.01%, Vc0.02%, potassium sorbate 0.05%, sodium benzoate 0.02%, Tea Polyphenols 0.03% again, stir after adding certain surfactant again;
(7), by instantaneous sterilizing (120 ℃-130 ℃/3-5 minute), promptly obtain Aloe gel juice (also claiming gravy) again with gained juice high pressure homogenizer homogeneous.
2, manufacture method according to claim 1 is characterized in that also can obtaining as follows:
(1) with in above-mentioned (4) through the gel of TRANSIENT HIGH TEMPERATURE degraded, keep drop temperature at 80 ℃-100 ℃, carry out coarse filtration immediately, temperature adds certain powder activated carbon and nontoxic oxidant (as H after the coarse filtration in the time of 70 ℃-90 ℃
2O
2), stir on one side, allow it cool off naturally on one side, its process must not be lower than 3 hours;
(2) gained juice is carried out essence filter and obtains clarified juice after, in juice, add to stir after the certain surface activating agent and tremble evenly, and use the high pressure homogenizer homogeneous, can promptly obtains stable decolored aloe gel juice after high-temperature short-time sterilization.
3, manufacture method according to claim 1 is characterized in that also can obtaining as follows:
(1) crust juice described in 1 (3) is carried out coarse filtration, add certain activity carbon and nontoxic oxidant after being heated to 70 ℃-90 ℃ (as H
2O
2) back stirring on one side, Yi Bian make its automatic cooling;
(2) the crust juice that cools off after the coarse filtration is carried out the essence filter and obtain clarified juice, and add an amount of citric acid, adjust its pH value, add certain vitamin V between the 3.2-4.2
E0.01%, V
C0.02%, potassium sorbate 0.05%, antioxidants such as sodium benzoate 0.02%, Tea Polyphenols 0.03%, stir after adding certain surfactant again, use TRANSIENT HIGH TEMPERATURE sterilizer (120 ℃-130 ℃/3-5 minute) sterilization behind the homogeneous again, promptly obtain stable aloe crust juice.
4, manufacture method according to claim 3 is characterized in that also can obtaining as follows:
(1) will be in the above-mentioned clarified juice add antioxidant and bacterial inhibitors such as certain vitamin E 0.01%, Tea Polyphenols 0.03%, card pine 0.01%, stir after adding certain surfactant again:
(2) with behind the high pressure homogenizer homogeneous again with the sterilization of TRANSIENT HIGH TEMPERATURE sterilizer (120 ℃-130 ℃/3-5 minute), promptly obtain the outer cortex of stable aloe.
5,, it is characterized in that the Aloe gel juice that will obtain mixes by different proportion with the outer cortex of aloe, can obtain the different full juice of various aloes of composition according to claim 1 or 4 described manufacture methods.
6, according to claim 2 or 4 described manufacture methods, it is characterized in that: said decolored aloe gel juice mixes by a certain percentage with the outer cortex of aloe, can obtain the different full juice of various aloes of composition.
7, according to claim 1 or 2 or 3 described manufacture methods, it is characterized in that: the clarified juice that obtains is concentrated into certain proportion with vacuum decker (boiling temperature is less than 65 ℃), insert respectively between 1 (5) and 1 (6), insert in 2 (2), insert in 3 (2), insert 4 (1) before, can correspondingly obtain various concentrated asparagus juices.
8, manufacture method according to claim 1 is characterized in that: with the clarified juice vacuum decker (boiling temperature is less than 65 ℃) that obtains, make 1: 10 concentrated asparagus juice, make dry powder with spray dryer.
9, manufacture method according to claim 8 is characterized in that: described inspissated juice is made dry powder with freeze drier.
10, manufacture method according to claim 1, it is characterized in that: the cleaning aloe leaf of acquisition laterally is cut into 0.5-0.7 centimetre thin slice with slicer, be placed on the net charging tray and place drying machine, the baking temperature control is at 60 ℃-70 ℃, air-supply makes Chinese aloe tablet slowly be dried to water content and accounts for 6%, send in the infrared oven and toasted 20-30 minute, make water content reduce to 3-3.5%, the while kill bacteria, make its sum reduce to 10/below the g, after adding a certain proportion of bacterial growth inhibitor, the dry thing of gained is crushed to below diameter 10 μ, promptly gets aloe dry powder by the sterile working requirement.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 97114279 CN1216232A (en) | 1997-10-31 | 1997-10-31 | Extraction of aloe extract |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 97114279 CN1216232A (en) | 1997-10-31 | 1997-10-31 | Extraction of aloe extract |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN1216232A true CN1216232A (en) | 1999-05-12 |
Family
ID=5172845
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN 97114279 Pending CN1216232A (en) | 1997-10-31 | 1997-10-31 | Extraction of aloe extract |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN1216232A (en) |
Cited By (13)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1095337C (en) * | 1999-10-23 | 2002-12-04 | 林开盛 | Aloe tea and its preparing process |
| WO2003059362A1 (en) * | 2001-12-30 | 2003-07-24 | Shouqin Zhang | Process of extracting small molecular ingredients from biological materials under super high pressure |
| CN1916064B (en) * | 2006-08-07 | 2010-05-12 | 杭州保灵养泰禾生物科技有限公司 | Dry powder of gelatinous polysaccharide of aloe, producing method and preparation |
| CN101637256B (en) * | 2009-08-19 | 2012-08-29 | 台山美环健芦荟制品有限公司 | Production method of aloe juice and application thereof |
| CN103109926A (en) * | 2012-11-27 | 2013-05-22 | 丽江安盛外贸有限责任公司 | Membrane solvent and application thereof |
| CN103156252A (en) * | 2013-03-21 | 2013-06-19 | 云南摩尔农庄生物科技开发有限公司 | Health-care aloe juice with good stability and preparation method thereof |
| CN103767032A (en) * | 2014-01-26 | 2014-05-07 | 海南钟晨生物工程有限责任公司 | Processing technology of high-content polysaccharide and O-acetyl aloe juice product |
| CN106418336A (en) * | 2016-11-22 | 2017-02-22 | 山西澳意芦荟生物科技有限公司 | Preparation method of aloe tableting food |
| CN106858222A (en) * | 2017-04-06 | 2017-06-20 | 山东晨隆晟世生物科技有限公司 | A kind of black garlic aloe beverage and preparation method thereof |
| CN109622214A (en) * | 2018-12-24 | 2019-04-16 | 贺州市骏鑫矿产品有限责任公司 | A kind of albite method for concentrating |
| CN110075039A (en) * | 2019-04-23 | 2019-08-02 | 澳梦生物科技(上海)有限公司 | A kind of extraction process of nanometer of synthesis asparagus juice |
| CN111202686A (en) * | 2020-01-03 | 2020-05-29 | 漳州市康贝卫生用品有限公司 | Preparation method of disinfection wet tissue |
| CN111685248A (en) * | 2019-03-14 | 2020-09-22 | 广州荟博大健康产业有限公司 | Aloe natural juice beverage and preparation method thereof |
-
1997
- 1997-10-31 CN CN 97114279 patent/CN1216232A/en active Pending
Cited By (13)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1095337C (en) * | 1999-10-23 | 2002-12-04 | 林开盛 | Aloe tea and its preparing process |
| WO2003059362A1 (en) * | 2001-12-30 | 2003-07-24 | Shouqin Zhang | Process of extracting small molecular ingredients from biological materials under super high pressure |
| CN1916064B (en) * | 2006-08-07 | 2010-05-12 | 杭州保灵养泰禾生物科技有限公司 | Dry powder of gelatinous polysaccharide of aloe, producing method and preparation |
| CN101637256B (en) * | 2009-08-19 | 2012-08-29 | 台山美环健芦荟制品有限公司 | Production method of aloe juice and application thereof |
| CN103109926A (en) * | 2012-11-27 | 2013-05-22 | 丽江安盛外贸有限责任公司 | Membrane solvent and application thereof |
| CN103156252A (en) * | 2013-03-21 | 2013-06-19 | 云南摩尔农庄生物科技开发有限公司 | Health-care aloe juice with good stability and preparation method thereof |
| CN103767032A (en) * | 2014-01-26 | 2014-05-07 | 海南钟晨生物工程有限责任公司 | Processing technology of high-content polysaccharide and O-acetyl aloe juice product |
| CN106418336A (en) * | 2016-11-22 | 2017-02-22 | 山西澳意芦荟生物科技有限公司 | Preparation method of aloe tableting food |
| CN106858222A (en) * | 2017-04-06 | 2017-06-20 | 山东晨隆晟世生物科技有限公司 | A kind of black garlic aloe beverage and preparation method thereof |
| CN109622214A (en) * | 2018-12-24 | 2019-04-16 | 贺州市骏鑫矿产品有限责任公司 | A kind of albite method for concentrating |
| CN111685248A (en) * | 2019-03-14 | 2020-09-22 | 广州荟博大健康产业有限公司 | Aloe natural juice beverage and preparation method thereof |
| CN110075039A (en) * | 2019-04-23 | 2019-08-02 | 澳梦生物科技(上海)有限公司 | A kind of extraction process of nanometer of synthesis asparagus juice |
| CN111202686A (en) * | 2020-01-03 | 2020-05-29 | 漳州市康贝卫生用品有限公司 | Preparation method of disinfection wet tissue |
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