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CN118812119B - Oil-containing sludge pyrolysis treatment equipment and method - Google Patents

Oil-containing sludge pyrolysis treatment equipment and method Download PDF

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Publication number
CN118812119B
CN118812119B CN202410971331.3A CN202410971331A CN118812119B CN 118812119 B CN118812119 B CN 118812119B CN 202410971331 A CN202410971331 A CN 202410971331A CN 118812119 B CN118812119 B CN 118812119B
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pyrolysis
box
heat
tube
pipe
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CN118812119A (en
Inventor
张海明
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Dongying Jujia Environmental Protection Equipment Co ltd
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Dongying Jujia Environmental Protection Equipment Co ltd
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    • CCHEMISTRY; METALLURGY
    • C02TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02FTREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F11/00Treatment of sludge; Devices therefor
    • C02F11/10Treatment of sludge; Devices therefor by pyrolysis
    • CCHEMISTRY; METALLURGY
    • C10PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10BDESTRUCTIVE DISTILLATION OF CARBONACEOUS MATERIALS FOR PRODUCTION OF GAS, COKE, TAR, OR SIMILAR MATERIALS
    • C10B47/00Destructive distillation of solid carbonaceous materials with indirect heating, e.g. by external combustion
    • C10B47/18Destructive distillation of solid carbonaceous materials with indirect heating, e.g. by external combustion with moving charge
    • CCHEMISTRY; METALLURGY
    • C10PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10BDESTRUCTIVE DISTILLATION OF CARBONACEOUS MATERIALS FOR PRODUCTION OF GAS, COKE, TAR, OR SIMILAR MATERIALS
    • C10B53/00Destructive distillation, specially adapted for particular solid raw materials or solid raw materials in special form
    • CCHEMISTRY; METALLURGY
    • C10PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10GCRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G1/00Production of liquid hydrocarbon mixtures from oil-shale, oil-sand, or non-melting solid carbonaceous or similar materials, e.g. wood, coal
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02WCLIMATE CHANGE MITIGATION TECHNOLOGIES RELATED TO WASTEWATER TREATMENT OR WASTE MANAGEMENT
    • Y02W10/00Technologies for wastewater treatment
    • Y02W10/40Valorisation of by-products of wastewater, sewage or sludge processing

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  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Organic Chemistry (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Materials Engineering (AREA)
  • Combustion & Propulsion (AREA)
  • Wood Science & Technology (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Hydrology & Water Resources (AREA)
  • Environmental & Geological Engineering (AREA)
  • Water Supply & Treatment (AREA)
  • Production Of Liquid Hydrocarbon Mixture For Refining Petroleum (AREA)

Abstract

The invention relates to the technical field of sludge treatment, in particular to an oily sludge pyrolysis treatment device and an oily sludge pyrolysis treatment method, wherein the oily sludge pyrolysis treatment device comprises a device machine table, and a pyrolysis box and a driving machine box are erected on the device machine table; the pyrolysis box comprises a pyrolysis box body, a pyrolysis closed pipe, a driving machine box, an inner box support, a plurality of heat supply pieces, a plurality of heat conduction pieces and a plurality of heat supply pieces, wherein the pyrolysis closed pipe is arranged in the pyrolysis box body, the top of the pyrolysis box body is externally connected with the feeding hopper, the bottom end of the feeding hopper is connected with the pyrolysis closed pipe, the output end of the pyrolysis closed pipe is provided with a delivery pipe, the driving machine box is provided with a driving connecting box, the inner cavity of the pyrolysis closed pipe is provided with a turning roller, the power input end of the turning roller is connected with the driving connecting box, the inner box support is further arranged in the pyrolysis box, the heat supply pieces are arranged in the inner box support, and the outer wall of the pyrolysis closed pipe is sleeved with the heat conduction pieces in a one-to-one butt joint. The invention designs that the oil-containing sludge is continuously heated in the movement process, the inside and the outside are continuously subjected to high-temperature heat treatment, and the oil-containing sludge can be effectively arranged in a treatment production line of the whole sludge, so that the working efficiency is improved.

Description

Oil-containing sludge pyrolysis treatment equipment and method
Technical Field
The invention relates to the technical field of sludge treatment, in particular to pyrolysis treatment equipment and method for oily sludge.
Background
With the continuous development of oil exploitation and industrial production, a large amount of oily sludge waste is generated. The sludge contains a large amount of grease, heavy metals and other harmful substances, and forms a serious threat to the environment and human health. Conventional treatment methods such as landfill and incineration not only occupy a lot of land resources, but also may cause secondary pollution, and oily sludge treatment equipment is used for treating oily sludge.
The pyrolysis treatment equipment for the oily sludge in the prior art generally comprises a feeding mechanism, a pyrolysis furnace, a connecting mechanism and a transmission mechanism, wherein the pyrolysis furnace comprises an inner cylinder body and an outer cylinder body, the outer cylinder body is sleeved on the inner cylinder body, and a cavity is formed between the outer cylinder body and the inner cylinder body. However, the prior art has certain defects that the pyrolysis furnace is not uniform for pyrolyzing the oil-containing sludge, so that the oil-containing sludge positioned in the inner layer area of the cylinder cannot be pyrolyzed effectively.
Disclosure of Invention
The invention aims to provide an oil-containing sludge pyrolysis treatment device and an oil-containing sludge pyrolysis treatment method, so as to solve the problems in the background art.
In order to achieve the above purpose, the present invention provides the following technical solutions:
The oil-containing sludge pyrolysis treatment equipment comprises an equipment machine table, wherein a pyrolysis box and a driving machine box are erected on the equipment machine table, a pyrolysis closed pipe is arranged in the pyrolysis box, a feeding hopper is externally connected to the top of a box body of the pyrolysis box, the bottom end of the feeding hopper is connected with the pyrolysis closed pipe, an output end of the pyrolysis closed pipe is provided with a delivery pipe, a driving connecting box is arranged on the driving machine box, a turning roller is arranged in an inner cavity of the pyrolysis closed pipe, a power input end of the turning roller is connected with the driving connecting box, the tail end of the turning roller extends into the delivery pipe, an inner box support is further arranged in the pyrolysis box, a plurality of heat supply pieces are arranged in the inner box support, a plurality of heat conduction pieces are sleeved on the outer wall of the pyrolysis closed pipe and are in one-to-one butt joint, an air exhaust pipe group is externally connected to the pyrolysis closed pipe, a condenser machine box is arranged on the outer box wall of the pyrolysis box, and the end of the air exhaust pipe group is connected with the condenser machine box.
The pyrolysis closed tube comprises a heating tank body and a guide tube body, wherein the heating tank body and the guide tube body are connected into an integrated structure through a first tube connecting sleeve, the driving connecting box comprises a driving end butt joint box and a closed frame arranged on the periphery of the driving end butt joint box, a box outer support frame is arranged on the box body of the pyrolysis box, the closed frame is arranged in the box outer support frame through an inner connecting sleeve, the other end of the guide tube body and the inner connecting sleeve are connected into an integrated structure through an inner connecting frame, and the other end of the heating tank body and the guide tube are connected into an integrated structure through a second tube connecting sleeve.
As a further scheme of the invention, the feeding hopper comprises a hopper body and a discharging valve port arranged at the hopper bottom of the hopper body, and the discharging valve port is communicated with the inner cavity of the guide pipe body.
The material turning roller comprises a roller body and a roller shaft arranged at the driving end of the roller body, wherein an auxiliary spiral auger, a scattering piece, a diffusion spiral piece and a main spiral auger are arranged on the roller body of the roller body, the auxiliary spiral auger is positioned in a pipe inner area of a guide pipe body, the main spiral auger is positioned in the pipe inner area of a heating tank body, the scattering piece is arranged behind the auxiliary spiral auger and is positioned at the bottom of a discharging valve port, the scattering piece comprises a plurality of groups of cutting claw blocks, each group of cutting claw blocks are distributed in an equidistant annular mode, the diffusion spiral piece is positioned between the scattering piece and the main spiral auger, and each row of the diffusion spiral pieces comprises a plurality of rows of hook-shaped blocks which are distributed spirally along the roller surface of the roller body.
As a further scheme of the invention, a support mounting frame is arranged in the inner box support, the heat supply part comprises a heat supply machine arranged on the heat supply machine, a heating component arranged in the heat supply machine and a heat conduction pipeline arranged at an air outlet of the heating component, and the heat supply machine is externally connected with a gas supply conduit.
The heat conduction piece comprises an annular heat conduction frame, the annular heat conduction frame is of an annular structure and is sleeved on the periphery of the guide pipe body, a heat flow guide opening is formed in the annular heat conduction frame, the heat conduction pipeline is communicated with an inner cavity of the annular heat conduction frame through the heat flow guide opening, a heat flow guide rail is arranged on the inner wall of the annular heat conduction frame, a plurality of heat flow guide grooves are formed in the inner surface of the heat flow guide rail, and a heat conduction interval is formed in the heat flow guide groove.
As a further scheme of the invention, the heat conduction piece further comprises a heat absorption piece sleeved on the outer wall of the guide pipe body, wherein the heat absorption piece is positioned in the corresponding annular heat conduction frame, and a heat conduction inner ring is arranged between the heat absorption piece and the pipe wall of the heating tank body.
As a still further scheme of the invention, the condensing box comprises a box body and a plurality of rows of condensing tube groups arranged in the box body, the box body is fixed on the outer box wall of the pyrolysis box through a fixing plate, a condensing zone is arranged in the inner cavity of the box body, a condensate inlet pipe is externally connected to the condensing zone, the condensing tube groups are arranged in the condensing zone, and each row of condensing tube groups comprises a plurality of heat exchange curved tubes.
The invention also discloses a treatment method for pyrolysis of the oily sludge, which comprises the following steps:
opening a valve at the feed hopper, conveying the oily sludge into the feed hopper by adopting a conveying belt, and falling into a pyrolysis closed tube along a hopper body of the feed hopper;
Starting a driving machine case, driving a turning roller to move by the driving machine case, setting the rotating speed of the turning roller to be 100 revolutions per minute, and slowly guiding the oily sludge to the rear of the inner cavity of the pipe body of the pyrolysis closed pipe 13;
step three, after the pyrolysis amount of the single oily sludge is completely injected, closing a valve at a feed hopper, continuously driving a turning roller, and compressing and concentrating the oily sludge in an inner pipe area of a guide pipe body;
step four, the rotating speed of the roller body of the turning roller is increased, the rotating speed of the turning roller is set to be 250 revolutions per minute of a condenser case, the heat supply part is controlled to continuously supply heat, and the heat supply temperature of the heat conduction part is increased to 500 ℃, so that heavy oil starts to thermally crack and continuously pyrolyzes for 3 hours;
stopping the movement of the turning roll, starting the air exhaust pipe group, exhausting the air flow in the pyrolysis closed pipe, leading out the gas mixture of oil, water and noncondensable gas,
And step six, after the extraction is completed, opening a valve in the delivery pipe, starting the turning roller again at the moment, and collecting the solid coke through the discharge of the delivery pipe.
Compared with the prior art, the invention has the beneficial effects that:
the feeding hopper is input equipment of oil-containing sludge, the sludge is thrown into the pipe body of the pyrolysis closed pipe, the pyrolysis closed pipe is a bearing component for sludge pyrolysis treatment, the pyrolysis closed pipe is arranged in the pyrolysis box, the pyrolysis box is operation equipment for pyrolysis treatment and provides a thermal environment for pyrolysis operation, a material turning roller is further arranged in the pipe body cavity of the pyrolysis closed pipe, a driving machine box is externally connected to the pipe body cavity of the pyrolysis closed pipe and used as driving equipment of the material turning roller, a plurality of heat conduction pieces are arranged on the outer pipe wall of the pyrolysis closed pipe and used as heat supply sources, the heat conduction pieces are arranged in a heating area of a section of the outer pipe body of the pyrolysis closed pipe, a continuous heating path is formed, the continuous heating of the oil-containing sludge is guaranteed in the movement process, the material turning roller synchronously drives continuous turning of the oil-containing sludge, so that the heat conduction effect is improved, the inside and outside of the oil-containing sludge are continuously subjected to high-temperature heat treatment, when the pipe is moved to the tail end of the material turning roller, the pipe is used as air extraction treatment, vaporized water vapor, oil vapor and non-condensable gas are guided into the condensing machine box, and solid coke is collected through the drainage. The invention can be effectively arranged on the integral sludge treatment production line, improves the working efficiency, and realizes the harmless treatment and the resource recycling of wastes.
It is to be understood that both the foregoing general description and the following detailed description are exemplary and explanatory only and are not restrictive of the application as claimed.
Drawings
The accompanying drawings, which are incorporated in and constitute a part of this specification, illustrate embodiments consistent with the application and together with the description, serve to explain the principles of the application. Meanwhile, these drawings and the written description are not intended to limit the scope of the inventive concept in any way, but to illustrate the inventive concept to those skilled in the art by referring to specific embodiments.
Fig. 1 is a schematic diagram of the overall structure of an oily sludge pyrolysis treatment device according to an embodiment of the present invention.
Fig. 2 is a schematic structural view of a pyrolysis closed tube according to an embodiment of the present invention.
Fig. 3 is a schematic structural diagram of a turning roll according to an embodiment of the present invention.
Fig. 4 is a schematic structural view of the area a in fig. 2 according to the present invention.
Fig. 5 is a schematic structural diagram of a condenser case according to an embodiment of the present invention.
11, An equipment machine; 12, pyrolysis box, 13, pyrolysis closed pipe, 14, driving box, 15, feeding hopper, 16, delivery pipe, 17, driving connection box, 18, turning roll, 21, inner box bracket, 22, heat conduction piece, 23, heating piece, 24, air extraction pipe group, 25, condensation box, 31, roll shaft, 32, roll body, 33, auxiliary spiral auger, 34, main spiral auger, 35, scattering piece, 36, diffusion spiral piece, 37, cutting claw block, 38, hook-shaped block, 41, heating tank body, 42, guide pipe body, 43, driving end butt box, 44, closed frame, 45, inner frame, 46, inner connection sleeve, 47, box outer frame, 48, first pipe body connecting sleeve, 49, second pipe body connecting sleeve, 51, bucket body, 52, blanking valve port, 61, branch installation frame, 62, heat supply machine, 63, heating component, 64, heat conduction pipe, 65, air supply pipe, 71, annular heat conduction frame, 72, heat flow inlet, 73, fixing rail, 74, guide rail, 75, guide rail, 77, heat conduction pipe, 82, heat exchange section, heat absorption section, 82, condensate section, heat absorption section, 81, condensate section, and heat exchange section.
Detailed Description
The technical solutions according to the embodiments of the present invention will be clearly and completely described below with reference to the accompanying drawings, examples of which are shown in the accompanying drawings. When the following description refers to the accompanying drawings, like numerals in the various drawings refer to like or similar elements, unless otherwise specified.
It will be apparent that the described embodiments are only some, but not all, embodiments of the invention. All other embodiments, which can be made by those skilled in the art based on the embodiments of the invention without making any inventive effort, are intended to be within the scope of the invention.
Specific implementations of the invention are described in detail below in connection with specific embodiments.
In one embodiment, please refer to fig. 1, an oily sludge pyrolysis treatment device is provided, which comprises a device machine 11, wherein a pyrolysis box 12 and a driving machine box 14 are erected on the device machine 11, a pyrolysis closed pipe 13 is arranged in the pyrolysis box 12, a feeding hopper 15 is externally connected to the top of the pyrolysis box 12, the bottom end of the feeding hopper 15 is connected with the pyrolysis closed pipe 13, an output end of the pyrolysis closed pipe 13 is provided with an output pipe 16, a driving connecting box 17 is arranged on the driving machine box 14, a material turning roller 18 is arranged in an inner cavity of the pyrolysis closed pipe 13, a power input end of the material turning roller 18 is connected with the driving connecting box 17, the tail end of the material turning roller 18 extends into the output pipe 16, an inner box bracket 21 is further arranged in the pyrolysis box 12, a plurality of heating elements 23 are arranged in the inner box bracket 21, a plurality of heating elements 22 are sleeved on the outer wall of the pyrolysis closed pipe 13, the heating elements 22 are in butt joint with the elements 23, a material turning roller 18 is arranged in an inner cavity of the pyrolysis closed pipe 13, a power input end of the material turning roller 18 is connected with the driving connecting box 17, the tail end of the material turning roller 18 extends into the output pipe 16, and the tail end of the pyrolysis box is connected with a condensing pipe 25 of the condensing pipe 25 arranged on the outer wall of the pyrolysis box 12.
The embodiment is used for pyrolysis treatment of oily sludge, the feed hopper 15 is input equipment of the oily sludge, the sludge is thrown into the feed hopper 15 and falls into a pipe body of the pyrolysis closing pipe 13, the pyrolysis closing pipe 13 is a bearing component for pyrolysis treatment of the sludge, the pyrolysis closing pipe 13 is arranged in the pyrolysis box 12, the pyrolysis box 12 is operation equipment for pyrolysis treatment and provides a thermal environment for pyrolysis operation, a material turning roller 18 is further arranged in a pipe body inner cavity of the pyrolysis closing pipe 13, a driving machine box 14 is externally connected to serve as driving equipment of the material turning roller 18, a plurality of heat conduction pieces 22 are arranged on an outer pipe wall of the pyrolysis closing pipe 13, the heat conduction pieces 22 serve as heat sources, meanwhile, an air exhaust pipe group 24 is externally connected to the top of the pipe body tail end of the pyrolysis closing pipe 13, and the air exhaust pipe group 24 is used for discharging water vapor and oil gas generated by pyrolysis treatment.
During operation, sludge is output from the feed hopper 15 and continuously introduced into the inner cavity of the pyrolysis closed pipe 13 through the stirring roller 18, in the sludge pyrolysis treatment process, low-boiling-point light hydrocarbon volatilizes from the oil-containing sludge along with the rising of the temperature, when the temperature exceeds 300 ℃, heavy oil starts to thermally crack, hydrocarbon generates free radicals due to thermal activation, a series of free radical reactions occur, on one hand, the reaction proceeds towards the cracking direction for generating small molecular hydrocarbon, on the other hand, the reaction proceeds towards the condensation direction of coking raw carbon, finally four products of oil, water, noncondensable gas and coke are generated, a heating area of a section is arranged on the outer pipe body of the pyrolysis closed pipe 13, a continuous heating path is formed, the continuous heating path of the oil-containing sludge is guaranteed, the stirring roller 18 synchronously drives continuous stirring of the oil-containing sludge in the process of conveying the oil-containing sludge, the heat conduction effect is improved, the inside and outside of the oil-containing sludge is guaranteed to continuously receive high temperature heat treatment, when the stirring roller 18 moves to the tail end of the stirring roller 18, the tail end of the stirring roller carries out air extraction treatment on the air extraction pipe, and leads water vapor, noncondensable gas and coke to the outside the solid coke from the feed hopper 25 to the next to the discharge bin 16, and the coke is discharged from the solid coke is discharged from the feed hopper to the next tank 15. Can continuously operate, can be effectively arranged on the whole sludge treatment production line, and improves the operation efficiency of the production line.
In one embodiment, referring to fig. 1 and 2, this embodiment is further designed as the above embodiment, and on the basis thereof, for the specific implementation structure of the pyrolysis closing tube 13, this embodiment is designed as follows:
the pyrolysis closing tube 13 includes heating jar body 41 and direction body 42, and heating jar body 41 is connected as integrated structure through first body adapter sleeve 48 with direction body 42, drive connection case 17 includes drive end butt joint case 43 and sets up in the peripheral closed frame 44 of drive end butt joint case 43, be provided with box external support frame 47 on the box of pyrolysis case 12, closed frame 44 passes through interior cover 46 and installs in box external support frame 47, the other end and the interior cover 46 of direction body 42 are connected as integrated structure through interior cover 45, the other end and the delivery tube 16 of heating jar body 41 are connected as integrated structure through second body adapter sleeve 49.
The pyrolysis closing tube 13 is integrally arranged in the pyrolysis box 12, the heating tank 41 and the guide tube 42 are combined and arranged into an integrated structure, the driving connecting box 17 is a connecting part of the driving machine box 14 and the pyrolysis box 12, the driving machine box 14 is connected into an integrated structure through the closing frame 44 and the box outer support frame 47 on the box shell of the pyrolysis box 12 by the supporting part of the driving end butt joint box 43, the inner connecting sleeve 46 and the guide tube 42 are connected into an integrated structure, so that the heat sealing effect in the whole pyrolysis box 12 operation process is kept, and the sealing closing effect of the pyrolysis closing tube 13 on sludge is also kept.
In one embodiment, referring to fig. 1, 2 and 3, this embodiment is further designed as the above embodiment, and on the basis of this embodiment, for a specific implementation structure of the oil-containing sludge introduction, this embodiment is designed as follows:
The feed hopper 15 comprises a hopper body 51 and a discharging valve port 52 arranged at the hopper bottom of the hopper body 51, and the discharging valve port 52 is communicated with the inner cavity of the guide pipe body 42.
The material turning roll 18 comprises a roll body 32 and a roll shaft 31 arranged at the driving end of the roll body 32, an auxiliary spiral auger 33, a scattering piece 35, a diffusion spiral piece 36 and a main spiral auger 34 are arranged on the roll body 32 of the roll body 32, the auxiliary spiral auger 33 is located in a tube inner region of a guide tube body 42, the main spiral auger 34 is located in a tube inner region of a heating tank 41, the scattering piece 35 is arranged behind the auxiliary spiral auger 33 and is located at the bottom of a material discharging valve port 52, the scattering piece 35 comprises a plurality of groups of cutting claw blocks 37, each group of cutting claw blocks 37 are distributed in an equidistant annular mode, the diffusion spiral piece 36 is located between the scattering piece 35 and the main spiral auger 34, the diffusion spiral piece 36 comprises a plurality of rows of hook-shaped blocks 38, and each row of hook-shaped blocks 38 are distributed in a spiral mode along the roll surface of the roll body 32.
In operation, the oily sludge slides down from the hopper body 51 and falls into the guide pipe body 42 through the discharging valve port 52, the scattering member 35 is located right below the discharging port of the discharging valve port 52, as an example, a mechanism arrangement mode is given in the figure, in this embodiment, every four cutting claw blocks 37 form a group, are annularly arranged on the roller body 32, the scattering member 35 is composed of four groups of cutting claw blocks 37, along with rotation of the roller body 32, the claw bodies of the cutting claw blocks 37 are in contact with the fallen oily sludge to form an effect of tearing the oily sludge, so that the oily sludge is more uniform during feeding, the problem of sludge agglomeration is reduced, the auxiliary spiral auger 33 has an auxiliary guide effect, the sludge (left side in the drawing) falling into the front end of the pyrolysis closed pipe 13 is guided to the right, the diffusion spiral member 36 is composed of the spiral arranged hook blocks 38, and the torn sludge is in a diffusion type to be conveyed backwards (right side in the drawing) on the basis of tearing the sludge of the scattering member 35, so that the sludge is further uniformly distributed on the periphery of the main spiral 34, and the subsequent pyrolysis degree of the oily sludge is improved.
In one embodiment, referring to fig. 1, 2 and 4, as a further design of the above embodiment, the embodiment is designed as follows for the specific implementation structure of the heat conducting member 22 and the heat supplying member 23:
the inner box support 21 is internally provided with a support mounting frame 61, the heat supply member 23 comprises a heat supply machine 62 arranged on the heat supply machine 62, a heating component 63 arranged in the heat supply machine 62 and a heat conduction pipeline 64 arranged at an air outlet of the heating component 63, and the heat supply machine 62 is externally connected with a gas supply conduit 65.
The heat conduction member 22 comprises an annular heat conduction frame 71, the annular heat conduction frame 71 is of an annular structure and sleeved on the periphery of the guide tube body 42 and is fixed through a fixed rail 73, a heat flow guide inlet 72 is arranged at the annular heat conduction frame 71, the heat conduction pipeline 64 is communicated with the inner cavity of the annular heat conduction frame 71 through the heat flow guide inlet 72, a heat flow guide rail 74 is arranged on the inner wall of the annular heat conduction frame 71, a plurality of heat flow guide grooves 75 are formed in the inner surface of the heat flow guide rail 74, a heat conduction section 76 is formed in the heat flow guide groove 75, the heat conduction member 22 further comprises a heat absorption member 77 sleeved on the outer wall of the guide tube body 42, and the heat absorption member 77 is positioned in the corresponding annular heat conduction frame 71 and is provided with a heat conduction inner ring 78 between the heat absorption member 77 and the tube wall of the heating tank body 41.
The heat supply machine 62 is used as a heat supply structure, the air supply conduit 65 is used as an input tool of air flow, high-temperature nitrogen is used as a heat source medium, the nitrogen is heated and guided into the heat conduction pipeline 64 through the heating component 63, the high-temperature nitrogen enters the inner cavity of the annular heat conduction frame 71 through the heat flow guide opening 72, the heat flow guide rail 74 is arranged on the inner wall of the annular heat conduction frame 71, the high-temperature nitrogen moves annularly along the heat conduction region 76 and further moves directly along the surface of the heat absorbing member 77, the heat conduction inner ring 78 is made of a heat conduction material and extends to the inner pipe wall of the guide pipe body 42 so as to be in contact with the oil-containing sludge, and therefore the oil-containing sludge is continuously subjected to heating treatment of the high-temperature nitrogen in the backward spiral movement process, and a series of free radical reactions occur through pyrolysis. On one hand, the process is carried out towards the cracking direction of the small molecular hydrocarbon, and on the other hand, the process is carried out towards the condensation direction of coking raw carbon, and finally, four products of oil, water, non-condensable gas and coke are produced.
In one embodiment, referring to fig. 1 and 5, this embodiment is further designed as the above embodiment, and on the basis thereof, for the specific implementation structure of the condensation enclosure 25, this embodiment is designed as follows:
The condensing case 25 comprises a case 82 and a plurality of rows of condensing tube groups 84 arranged in the case 82, the case 82 is fixed on the outer wall of the pyrolysis case 12 through a fixing plate 81, the inner cavity of the case 82 is provided with a condensing section 83, the condensing section 83 is externally connected with a condensate inlet tube 86, the condensing tube groups 84 are arranged in the condensing section 83, and each row of condensing tube groups 84 comprises a plurality of heat exchange curved tubes 85.
The condensing box 25 is used for condensing three gas products, namely water vapor, oil vapor and non-condensable gas, which are subjected to separation treatment, the condensate inlet pipe 86 is used as a cooling source, the inner area of the condensing zone 83 forms a cooling environment, the gas products are shunted from the air exhaust pipe group 24 to each heat exchange curved pipe 85, meanwhile, each heat exchange curved pipe 85 is in a curved fold-line type arrangement, the contact between the gas products and the inner environment of the condensing zone 83 is fully maintained, the gas products continuously release heat, in the heat release process, the water vapor and the oil vapor are subjected to exothermic reaction to liquefy, the non-condensable gas is continuously kept in a gas state, the gas and the liquid are further separated, and meanwhile, the water liquid and the oil are easily layered in the movement process of the curved pipe, so that water and oil separation is also formed initially, and the separation operation of the gas, the oil and the water of the follow-up working station is facilitated.
Opening a valve at the feed hopper 15, conveying the oily sludge into the feed hopper 15 by adopting a conveying belt, and falling into the pyrolysis closed tube 13 along a hopper body 51 of the feed hopper 15;
Starting a driving machine case 14, driving the turning roller 18 to move by the driving machine case 14, setting the rotating speed of the turning roller 18 to be 100 revolutions per minute, and slowly guiding the oily sludge to the rear of the inner cavity of the pipe body of the pyrolysis closed pipe 13, and simultaneously starting a heat supply piece 23 to enable the heat supply piece 23 to supply heat to the heat conduction piece 22 so as to heat the integral pyrolysis closed pipe 13, wherein the initial heat supply temperature is set to be 350 ℃ of a scattering piece;
Step three, after the pyrolysis amount of the single oily sludge is completely injected, closing a valve at a feed hopper 15, continuously driving a turning roll 18, and compressing and concentrating the oily sludge in the pipe inner area of a guide pipe body 42;
Step four, the rotating speed of the roller body 32 of the turning roller 18 is increased, the rotating speed of the turning roller 18 is set to be 250 revolutions per minute of a condenser case, the heat supply part 23 is controlled to continuously supply heat, and the heat supply temperature of the heat conduction part 22 is increased to 500 ℃, so that heavy oil starts to thermally crack and continuously pyrolyzes for 3 hours;
stopping the movement of the turning-over roller 18, opening the air exhaust pipe group 24, exhausting the air flow in the pyrolysis closing pipe 13, leading out the gas mixture of oil, water and noncondensable gas,
And step six, after the extraction is completed, opening a valve in the delivery pipe 16, and starting the turning roll 18 again to collect solid coke through the discharge of the delivery pipe 16.
It will be evident to those skilled in the art that the invention is not limited to the details of the foregoing illustrative embodiments, and that the present invention may be embodied in other specific forms without departing from the spirit or essential characteristics thereof. The present embodiments are, therefore, to be considered in all respects as illustrative and not restrictive, the scope of the invention being indicated by the appended claims rather than by the foregoing description, and all changes which come within the meaning and range of equivalency of the claims are therefore intended to be embraced therein.
Furthermore, it should be understood that although the present disclosure describes embodiments, not every embodiment is provided with a separate embodiment, and that this description is provided for clarity only, and that the disclosure is not limited to the embodiments described in detail below, and that the embodiments described in the examples may be combined as appropriate to form other embodiments that will be apparent to those skilled in the art.

Claims (4)

1.一种含油污泥热解处理设备,包括设备机台(11),所述设备机台(11)上架设有热解箱(12)和驱动机箱(14);其特征在于,1. A pyrolysis treatment device for oily sludge, comprising a device platform (11), wherein a pyrolysis box (12) and a drive box (14) are mounted on the device platform (11); characterized in that: 所述热解箱(12)箱内设置有热解闭合管(13),所述热解箱(12)的箱体顶部外接有进料斗(15),所述进料斗(15)的底端与热解闭合管(13)相连接,所述热解闭合管(13)的输出端设置有导出管(16);The pyrolysis box (12) is provided with a pyrolysis closed tube (13), the top of the box body of the pyrolysis box (12) is externally connected to a feed hopper (15), the bottom end of the feed hopper (15) is connected to the pyrolysis closed tube (13), and the output end of the pyrolysis closed tube (13) is provided with an outlet pipe (16); 所述驱动机箱(14)上设置有驱动连接箱(17),所述热解闭合管(13)的内腔设置有翻料辊(18),所述翻料辊(18)的动力输入端与驱动连接箱(17)相连接,所述翻料辊(18)的末端延伸至导出管(16)内;The driving chassis (14) is provided with a driving connection box (17), the inner cavity of the pyrolysis closed tube (13) is provided with a material turning roller (18), the power input end of the material turning roller (18) is connected to the driving connection box (17), and the end of the material turning roller (18) extends into the outlet tube (16); 所述热解箱(12)内还设置有内箱支架(21),所述内箱支架(21)内安装有若干供热件(23),所述热解闭合管(13)的外壁上套设有若干热传导件(22),所述热传导件(22)与供热件(23)呈一一对接;The pyrolysis box (12) is further provided with an inner box support (21), a plurality of heating components (23) are installed in the inner box support (21), a plurality of heat conducting components (22) are sleeved on the outer wall of the pyrolysis closed tube (13), and the heat conducting components (22) are butted against the heating components (23) in a one-to-one manner; 所述热解闭合管(13)外接有抽气管组(24),热解箱(12)的外箱壁上设置有冷凝机箱(25),所述抽气管组(24)的管端与冷凝机箱(25)相连接;The pyrolysis closed tube (13) is externally connected to an exhaust pipe group (24); a condensing box (25) is provided on the outer box wall of the pyrolysis box (12); and the pipe end of the exhaust pipe group (24) is connected to the condensing box (25); 所述翻料辊(18)包括辊体(32)以及设置于辊体(32)驱动端的辊轴(31),所述辊体(32)的辊体(32)上设置有辅螺旋绞龙(33)、打散件(35)、扩散螺旋件(36)和主螺旋绞龙(34),所述辅螺旋绞龙(33)位于导向管体(42)的管内区域,所述主螺旋绞龙(34)位于加热罐体(41)的管内区域;The turning roller (18) comprises a roller body (32) and a roller shaft (31) arranged at a driving end of the roller body (32); the roller body (32) is provided with an auxiliary spiral auger (33), a dispersing member (35), a diffusion spiral member (36) and a main spiral auger (34); the auxiliary spiral auger (33) is located in a tube area of the guide tube body (42), and the main spiral auger (34) is located in a tube area of the heating tank body (41); 所述打散件(35)设置于辅螺旋绞龙(33)的后方并且位于下料阀口(52)的底部,所述打散件(35)包括若干组切割爪块(37),每组切割爪块(37)呈等距环形排布;The dispersing member (35) is arranged behind the auxiliary spiral auger (33) and is located at the bottom of the discharge valve port (52), and the dispersing member (35) comprises a plurality of groups of cutting claw blocks (37), and each group of cutting claw blocks (37) is arranged in an equidistant annular pattern; 所述扩散螺旋件(36)位于打散件(35)和主螺旋绞龙(34)之间,所述扩散螺旋件(36)包括若干排勾型块(38),每排勾型块(38)沿着辊体(32)的辊面呈螺旋排布;The diffusion spiral member (36) is located between the dispersing member (35) and the main spiral auger (34), and the diffusion spiral member (36) comprises a plurality of rows of hook-shaped blocks (38), and each row of hook-shaped blocks (38) is arranged in a spiral along the roller surface of the roller body (32); 所述内箱支架(21)内设置有支件安装架(61),所述供热件(23)包括设置于供热机(62)上的供热机(62)、设置于供热机(62)内的加热组件(63)以及安装于加热组件(63)出风口处的导热管道(64),所述供热机(62)外接有供气导管(65);A support mounting frame (61) is disposed inside the inner box bracket (21); the heating element (23) comprises a heating machine (62) disposed on the heating machine (62), a heating component (63) disposed inside the heating machine (62), and a heat-conducting pipe (64) installed at an air outlet of the heating component (63); the heating machine (62) is externally connected to an air supply duct (65); 所述热传导件(22)包括环形导热框(71),环形导热框(71)为环形结构并且套设于导向管体(42)的外围,所述环形导热框(71)处设置有热流导入口(72),所述导热管道(64)通过热流导入口(72)与环形导热框(71)内腔相连通,所述环形导热框(71)的内壁上设置有热流导向栏(74),热流导向栏(74)的内表面开设有若干热流引导槽(75),热流引导槽(75)内形成有导热区间(76);The heat conducting member (22) comprises an annular heat conducting frame (71), which is an annular structure and is sleeved on the periphery of the guide pipe body (42); a heat flow inlet (72) is provided on the annular heat conducting frame (71); the heat conducting pipe (64) is connected to the inner cavity of the annular heat conducting frame (71) through the heat flow inlet (72); a heat flow guide bar (74) is provided on the inner wall of the annular heat conducting frame (71); a plurality of heat flow guide grooves (75) are provided on the inner surface of the heat flow guide bar (74); and a heat conduction zone (76) is formed in the heat flow guide grooves (75); 所述热传导件(22)还包括套设于导向管体(42)的外壁上的吸热件(77),吸热件(77)位于相应的环形导热框(71)内并且与加热罐体(41)的管壁之间设置有热传导内圈(78);The heat conducting member (22) further comprises a heat absorbing member (77) sleeved on the outer wall of the guide tube body (42); the heat absorbing member (77) is located in the corresponding annular heat conducting frame (71) and a heat conducting inner ring (78) is provided between the heat absorbing member (77) and the tube wall of the heating tank body (41); 所述冷凝机箱(25)包括箱体(82)以及设置于箱体(82)内的若干排冷凝管组(84),所述箱体(82)通过固定板(81)固定于热解箱(12)的外箱壁上,所述箱体(82)的内腔设置有冷凝区间(83),冷凝区间(83)外接有冷凝液导入管(86),所述冷凝管组(84)设置于冷凝区间(83)内,每排冷凝管组(84)包括若干热交换曲管(85)。The condensing box (25) comprises a box body (82) and a plurality of rows of condensing tube groups (84) arranged in the box body (82); the box body (82) is fixed to the outer box wall of the pyrolysis box (12) by a fixing plate (81); the inner cavity of the box body (82) is provided with a condensing zone (83); the condensing zone (83) is externally connected to a condensate inlet pipe (86); the condensing tube group (84) is arranged in the condensing zone (83); and each row of the condensing tube group (84) comprises a plurality of heat exchange curved tubes (85). 2.根据权利要求1所述的含油污泥热解处理设备,其特征在于,所述热解闭合管(13)包括加热罐体(41)和导向管体(42),加热罐体(41)与导向管体(42)通过第一管体连接套(48)连接为一体化结构,所述驱动连接箱(17)包括驱动端对接箱(43)以及设置于驱动端对接箱(43)外围的闭合框(44),所述热解箱(12)的箱体上设置有箱体外支框(47),所述闭合框(44)通过内连接套(46)安装于箱体外支框(47)内,所述导向管体(42)的另一端与内连接套(46)通过内接框(45)连接为一体化结构,所述加热罐体(41)的另一端与导出管(16)通过第二管体连接套(49)连接为一体化结构。2. The pyrolysis treatment equipment for oily sludge according to claim 1 is characterized in that the pyrolysis closed tube (13) comprises a heating tank body (41) and a guide tube body (42), the heating tank body (41) and the guide tube body (42) are connected to form an integrated structure through a first tube body connecting sleeve (48), the driving connection box (17) comprises a driving end docking box (43) and a closed frame (44) arranged on the periphery of the driving end docking box (43), the box body of the pyrolysis box (12) is provided with a box outer support frame (47), the closed frame (44) is installed in the box outer support frame (47) through an inner connecting sleeve (46), the other end of the guide tube body (42) is connected to the inner connecting sleeve (46) through an inner connecting frame (45) to form an integrated structure, and the other end of the heating tank body (41) is connected to the outlet pipe (16) through a second tube body connecting sleeve (49) to form an integrated structure. 3.根据权利要求2所述的含油污泥热解处理设备,其特征在于,所述进料斗(15)包括斗体(51)以及设置于斗体(51)斗底位置的下料阀口(52),所述下料阀口(52)与导向管体(42)内腔相连通。3. The oily sludge pyrolysis treatment equipment according to claim 2 is characterized in that the feed hopper (15) comprises a hopper body (51) and a discharge valve port (52) arranged at the bottom of the hopper body (51), and the discharge valve port (52) is connected to the inner cavity of the guide pipe body (42). 4.根据权利要求1-3任一项所述的含油污泥热解处理设备的实施方法,其特征在于,包括以下步骤;4. The implementation method of the oily sludge pyrolysis treatment equipment according to any one of claims 1 to 3, characterized in that it comprises the following steps; 步骤一:打开进料斗(15)处的阀门,采用输送带将含油污泥输送到进料斗(15)中,并且沿着进料斗(15)下落至热解闭合管(13)中;Step 1: Open the valve at the feed hopper (15), use a conveyor belt to convey the oily sludge into the feed hopper (15), and let it fall along the feed hopper (15) into the pyrolysis closed tube (13); 步骤二:启动驱动机箱(14),驱动机箱(14)驱动翻料辊(18)运动,翻料辊(18)的转速设置为100转/min,将含油污泥缓慢导向至热解闭合管(13)的管体内腔后方;同时启动供热件(23),使得供热件(23)对热传导件(22)供热,从而加热整体热解闭合管(13),供热初始温度设置为350℃;Step 2: Start the driving chassis (14), and the driving chassis (14) drives the material turning roller (18) to move, and the rotation speed of the material turning roller (18) is set to 100 revolutions per minute, so as to slowly guide the oily sludge to the rear of the inner cavity of the pyrolysis closed tube (13); at the same time, start the heating element (23), so that the heating element (23) supplies heat to the heat conduction element (22), thereby heating the entire pyrolysis closed tube (13), and the initial heating temperature is set to 350° C.; 步骤三:单次含油污泥的热解量全部注入后,闭合进料斗(15)处的阀门,持续驱动翻料辊(18),将含油污泥压缩集中于热解闭合管(13)的加热区域;Step 3: After all the pyrolysis amount of the oily sludge is injected, the valve at the feed hopper (15) is closed, and the turning roller (18) is continuously driven to compress the oily sludge and concentrate it in the heating area of the pyrolysis closed tube (13); 步骤四:提高翻料辊(18)的辊体(32)转速,将翻料辊(18)的转速设置为250转/min,控制供热件(23)持续供热,并且将热传导件(22)的供热温度提升至500℃,使得重质油开始热裂解,并且持续热解3h;Step 4: increasing the rotation speed of the roller body (32) of the turning roller (18), setting the rotation speed of the turning roller (18) to 250 revolutions per minute, controlling the heating element (23) to continuously supply heat, and raising the heating temperature of the heat transfer element (22) to 500° C., so that the heavy oil begins to be thermally cracked, and the thermal decomposition continues for 3 hours; 步骤五:终止翻料辊(18)的运动,开启抽气管组(24),抽离热解闭合管(13)内的气流,引出油、水和不凝气的气体混合物,Step 5: Stop the movement of the turning roller (18), open the exhaust pipe group (24), extract the air flow in the pyrolysis closed tube (13), and draw out the gas mixture of oil, water and non-condensable gas. 步骤六:抽离完成后,开启导出管(16)内的阀门,此时再启动翻料辊(18),将固态的焦炭则通过导出管(16)外排收集。Step 6: After the extraction is completed, the valve in the outlet pipe (16) is opened, and the turning roller (18) is started to discharge the solid coke through the outlet pipe (16) for collection.
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