CN118236276A - 一种添加椰壳活性炭粉的洁面乳及其制备方法 - Google Patents
一种添加椰壳活性炭粉的洁面乳及其制备方法 Download PDFInfo
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- CN118236276A CN118236276A CN202410265351.9A CN202410265351A CN118236276A CN 118236276 A CN118236276 A CN 118236276A CN 202410265351 A CN202410265351 A CN 202410265351A CN 118236276 A CN118236276 A CN 118236276A
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Abstract
本发明提供一种添加椰壳活性炭粉的洁面乳及其制备方法,洁面乳由A相、B相、C相、D相和E相混合而成,含有乳化剂I、乳化剂II和乳化剂III,能够帮助去除皮肤表面的污垢和油脂,使洁面乳更容易起泡并具有更好的清洁效果;加入椰壳活性炭粉,可以利用其吸附作用去除皮肤表面的污垢、油脂和化妆品残留物,从而达到更深层次的清洁效果,洋甘菊提取物、金缕梅蒸馏液可以调节油脂分泌,平衡代谢,在清洁时具有舒缓镇静的功效,能够缓解面部肌肤的不适和敏感,本发明的洁面乳具有较好的皮肤油脂清除率和污垢清除率,油脂清除率达到96.3‑98.8%,污垢清除率达到97.5‑99.5%,水分含量增加率4.2‑5.1%,黑色素抑制率70.6‑72.3%。
Description
技术领域
本发明涉及化妆品技术领域,特别涉及一种添加椰壳活性炭粉的洁面乳及其制备方法。
背景技术
洁面乳的首要功能是清洁皮肤,去除表面的污垢、油脂、汗液和化妆品残留物。这需要借助特定的化学成分来实现,其中包括表面活性剂,它们能够降低水的表面张力,帮助分离和去除附着在皮肤上的污垢,传统的洁面产品可能只停留在表面的清洁,无法有效去除深层的污垢和油脂,随着人们对皮肤健康的关注不断提高,对洁面产品的要求也日益增加,洁面乳不仅仅局限于清洁功能,还融入了多种护肤成分,如保湿剂、抗氧化剂和抗炎成分等。这些成分可以在清洁的同时,为皮肤提供额外的护理和滋养;并且近年来,越来越多的消费者倾向于选择含有天然成分的个人护理产品,在使用天然成分温和清洁皮肤,达到温和清洁和保湿、美白的效果;而目前的功能型洁面乳中可能含有刺激性或强效的清洁成分,容易过度清洁皮肤,导致皮肤紧绷、干燥和不适。过度清洁还可能破坏皮肤的天然屏障,使皮肤容易受到外界环境的侵害,可能含有刺激性或过敏性成分,如香料、酒精、色素等。这些成分可能对敏感肌肤或特定肤质造成不适或过敏反应,导致皮肤发红、瘙痒、刺痛等症状;洁面乳的酸碱度对皮肤的健康也有一定影响。如果洁面乳的酸碱度过高或过低,可能会破坏皮肤的酸碱平衡,导致皮肤问题。
活性炭以其强大的吸附能力而著称,能够有效地吸附和清除环境中的有害物质。随着科学技术的不断发展,对活性炭的制备和应用技术也在不断进步。椰壳活性炭粉作为一种高质量的活性炭产品,其制备技术已经相当成熟,为将其应用于洁面乳中提供了有力的技术支持,但是目前的椰壳活性炭洁面乳添加量不足或颗粒过大,导致清洁效果不尽如人意,还有过于注重清洁效果,而忽视了保湿的重要性。这可能导致清洁后皮肤感觉干燥和紧绷,除了椰壳活性炭粉外,洁面乳中还可能包含其他成分,这些成分与活性炭不兼容或可能产生不良反应,影响洁面乳的整体效果。
发明内容
鉴于此,本发明提出一种添加椰壳活性炭粉的洁面乳及其制备方法,解决上述问题。
本发明的技术方案是这样实现的:一种添加椰壳活性炭粉的洁面乳:按照重量百分比计,其原料由A相、B相、C相、D相和E相混合而成:
A相:乳化剂I10-20%、乳化剂II 5-12%、乳化剂III 5-9%、丙二醇1-3%、皮肤调理剂I1-2%、甘油硬脂酸酯0.8-1.2%;
B相:水30-40%、氢氧化钾3-8%、保湿剂10-18%;
C相:表面活性剂3-8%、皮肤调理剂II 2.5-5.5%;
D相:炭粉0.8-2.0%、
E相:洋甘菊提取物0.05-0.12%、复合氨基酸0.05-0.12%、金缕梅蒸馏液0.05-0.2%、皮肤调理剂III 0.05-0.12%、防腐剂0.05-0.12%、香精0.1-0.2%。
进一步的,一种添加椰壳活性炭粉的洁面乳,按照重量百分比计,其原料由A相、B相、C相、D相和E相混合而成:
A相:乳化剂I15%、乳化剂II8%、乳化剂III7.5%、丙二醇2%、皮肤调理剂I1.5%、甘油硬脂酸酯1%;
B相:水35.6%、氢氧化钾5.7%、保湿剂14%;
C相:表面活性剂4%、皮肤调理剂II3.5%;
D相:椰壳活性炭粉1.5%、
E相:洋甘菊提取物0.1%、复合氨基酸0.1%、金缕梅蒸馏液0.15%、皮肤调理剂III0.1%、防腐剂0.1%、香精0.15%。
进一步的,所述乳化剂I包括以下重量百分比原料:月桂酸0.3%、肉豆蔻酸99.3%、棕榈酸0.4%;所述乳化剂II包括以下重量百分比原料:肉豆蔻酸0.3%、棕榈酸99.1%、硬脂酸0.6%;所述乳化剂III包括以下重量百分比原料:月桂酸0.24%、肉豆蔻酸1.25%、棕榈酸58.16%、硬脂酸39.84%、花生酸0.32%、油酸0.19%。
进一步的,所述皮肤调理剂I包括以下重量百分比原料:PEG-150二硬脂酸酯97%、水3%;所述皮肤调理剂II包括以下重量百分比原料:棕榈仁油酰胺DEA90%、甘油10%;所述皮肤调理剂III包括以下重量百分比原料:水0.05%、苯氧乙醇99.39%、乙酰基六肽-80.5%、乙基己基甘油0.06%。
进一步的,所述表面活性剂包括以下重量百分比原料:甲基椰油酰基牛磺酸钠40%、水60%。
进一步的,所述洋甘菊提取物包括以下重量百分比原料:母菊花提取物5%、水70%、丁二醇25%。
进一步的,所述复合氨基酸包括以下重量百分比原料:水15.38%、丁二醇24.45%、甘油17.35%、丝氨酸5.7%、精氨酸5.35%、谷氨酸4.45%、异亮氨酸4.37%、脯氨酸4.25%、甘氨酸3.95%、亮氨酸3.35%、丙氨酸3.35%、天冬氨酸3.21%、缬氨酸2.8%、乳酸钠1.02%、乳酸1.02%。
进一步的,所述金缕梅蒸馏液包括以下重量百分比原料:北美金缕梅水99%、苯氧乙醇1%。
进一步的,所述防腐剂包括以下重量百分比原料:甲基异噻唑啉酮0.18%、甲基氯异噻唑啉酮0.54%、氯化镁0.2%、硝酸镁1%、苯甲醇20%、三甘醇25%、丙二醇15%、水38.08%。
进一步的,一种添加椰壳活性炭粉的洁面乳的制备方法,包括以下步骤:
S1、将A相投入主锅中,搅拌加热至80-90℃,恒温搅拌至完全溶解;
S2、将B相投入到水锅中,搅拌加热到65-75℃,搅拌至完全溶解,边搅拌边快速抽入到主锅,4-6分钟抽完后放掉真空,控制搅拌25-40rpm,恒温搅拌40-50分钟,再加入C相搅拌均匀,
S3、当上述混料搅拌降温到45℃以下,加入预先分散均匀的D相搅匀,再加入E相,搅拌均匀,搅拌降温到35℃以下后报检,QC检验合格过滤出料静置,灌装、包装、入库,得到一种添加椰壳活性炭粉的洁面乳。
与现有技术相比,本发明的有益效果是:
本发明的洁面乳添加椰壳活性炭,具有强大的吸附能力,能够有效地吸附和清除皮肤表面的污垢、油脂和化妆品残留物,从而实现深层清洁效果;且作为椰壳活性炭粉作为一种天然成分,相对于一些化学合成的清洁剂,更加温和,对皮肤的刺激较小,适合敏感肌肤使用;多种乳化剂按比例复配,能够帮助去除皮肤表面的污垢和油脂,使洁面乳更容易起泡并具有更好的清洁效果。通过乳化作用,洁面乳能够更有效地清除皮肤表面的杂质,保持皮肤的清洁和健康;还能抑制人体细胞中的黑色素因子,改善皮肤色素沉着;有效地解决洁面乳在高温下的稳定性问题,并防止产品体系在恢复常温后出现泛粗现象。这种作用确保了洁面乳的质量和稳定性;加入洋甘菊提取物、金缕梅蒸馏液可以调节油脂分泌,平衡代谢,在清洁时具有舒缓镇静的功效,能够缓解面部肌肤的不适和敏感;同时,以复合氨基酸为原料,是皮肤的天然保湿因子,它们能够锁住皮肤水分,防止水分流失,使皮肤保持湿润和柔软,能够滋养皮肤,改善肌肤状态,使皮肤更加健康、光滑和富有弹性。
具体实施方式
为了更好理解本发明技术内容,下面提供具体实施例,对本发明做进一步的说明。
本发明实施例所用的实验方法如无特殊说明,均为常规方法。
本发明实施例所用的材料、试剂等,如无特殊说明,均可从商业途径得到。
实施例1
一种添加椰壳活性炭粉的洁面乳,按照重量百分比计,其原料由A相、B相、C相、D相和E相混合而成:
实施例2
一种添加椰壳活性炭粉的洁面乳,按照重量百分比计,其原料由A相、B相、C相、D相和E相混合而成:
实施例3
一种添加椰壳活性炭粉的洁面乳,按照重量百分比计,其原料由A相、B相、C相、D相和E相混合而成:
上述实施例1-3的洁面乳按照以下制备方法制得:
S1、将A相投入主锅中,搅拌加热至85℃,恒温搅拌至完全溶解;
S2、将B相投入到水锅中,搅拌加热到60℃,搅拌至完全溶解,边搅拌边快速抽入到主锅,5分钟抽完后放掉真空,控制搅拌30rpm,恒温搅拌45分钟,再加入C相搅拌均匀,
S3、当上述混料搅拌降温到45℃以下,加入预先分散均匀的D相搅匀,再加入E相,搅拌均匀,搅拌降温到35℃以下后报检,QC检验合格过滤出料静置,灌装、包装、入库,得到一种添加椰壳活性炭粉的洁面乳。
对比例1
本对比例与实施例3的区别在于,所述洁面乳未加入椰壳活性炭粉,替换为竹炭粉,具体为:
对比例2
本对比例与实施例3的区别在于,所述洁面乳A相原料中未加入乳化剂III。
对比例3
本对比例与实施例3的区别在于,所述洁面乳E相原料中不含有洋甘菊提取物。
对比例4
本对比例与实施例3的区别在于,所述洁面乳E相原料中不含有金缕梅蒸馏液。
一、清洁效率
选择80名志愿者,年龄20-30岁的女性,其中48名为油性肤质,32名为干性肤质,随机分为8组,每组10人,在妆后使用本发明实施例1-3和对比例1-4的洁面乳及市售洁面乳进行清洗,以每名受试者的额头和两侧鼻翼作为测试区域,早晚使用一次,连续使用20天,使用SM815皮肤油脂测量仪及皮肤污垢测量仪测定其皮肤油脂含量和皮肤污垢含量,计算其清洁效率;
油脂清除率=(清洁前皮肤油脂含量-清洁后皮肤油脂含量)/清洁前皮肤油脂含量×100%;
污垢清除率=(清洁前皮肤污垢含量-清洁后皮肤污垢含量)/清洁前皮肤污垢含量×100%;
在清洁的同时,测定皮肤保湿效果和美白效果,
采用皮肤水分含量测试仪测定皮肤使用前后的含水量,计算皮肤水分含量增减率;
采用MEXAMETER MX16皮肤色素分析仪,测试受试者脸部皮肤的黑色素含量;
黑色素抑制率=(使用前1天黑色素含量-使用30天后黑色素含量)/使用前1天黑色素含量×100%;
测定结果如下:
从上述表格结果可知,本发明的洁面乳具有较好的皮肤油脂清除率和污垢清除率,油脂清除率达到96.3-98.8%,污垢清除率达到97.5-99.5%,水分含量增加率4.2-5.1%,黑色素抑制率70.6-72.3%;从实施例组与对比例1比较,添加椰壳活性炭粉,其吸附作用可以去除多余的油脂,使皮肤保持清爽。这有助于减少油脂分泌过多导致的皮肤问题,能够吸附皮肤表面的污垢、油脂和化妆品残留物,从而实现深层清洁效果。这种吸附作用可以帮助清除毛孔内的堵塞物,预防和改善黑头、粉刺等皮肤问题,去除皮肤表面的老化角质细胞和死皮细胞,从而改善肤色暗沉。椰壳活性炭粉还可以吸附皮肤表面的自由基和有害物质,减少氧化应激对皮肤的损害,使肌肤更加明亮有光泽。
与对比例2比较,乳化剂III通过肉豆蔻酸、花生酸、油酸等按特定比例制得,具有清洁皮肤、去除皮肤表面油脂和污垢的作用及杀菌效果,月桂酸、肉豆蔻酸能够温和清除皮肤毛孔油脂,具有很好的杀菌效果,能够预防皮肤发炎,棕榈酸能抑制人体细胞中的黑色素因子,改善皮肤色素沉着;花生酸能够深层清洁皮肤,去除皮肤表面的污垢和多余油脂,油酸可以减少皮肤中的自由基,有助于减少紫外线对皮肤的伤害,从而起到美容养颜的作用。
与对比例3比较,加入洋甘菊提取物能够可以调节油脂分泌,平衡代谢,防止出现黑色素沉淀和过多的粉刺,具有舒缓镇静的功效,能够缓解面部肌肤的不适和敏感,减少面部炎症和红肿,同时补充肌肤所需的水分和养分,使肌肤更加柔软、光滑和富有弹性。
与对比例4比较,金缕梅所含的原花青素对皮肤有消炎作用,修复受损皮肤,减少皮肤水分损失,具有舒缓、收敛的效果,可以调节皮脂分泌,松弛毛孔,净化毛孔,软化脸部毛孔,使皮肤更加光滑。
以上所述仅为本发明的较佳实施例而已,并不用以限制本发明,凡在本发明的精神和原则之内,所作的任何修改、等同替换、改进等,均应包含在本发明的保护范围之内。
Claims (10)
1.一种添加椰壳活性炭粉的洁面乳,其特征在于:按照重量百分比计,其原料由A相、B相、C相、D相和E相混合而成:
A相:乳化剂I10-20%、乳化剂II 5-12%、乳化剂III 5-9%、丙二醇1-3%、皮肤调理剂I1-2%、甘油硬脂酸酯0.8-1.2%;
B相:水30-40%、氢氧化钾3-8%、保湿剂10-18%;
C相:表面活性剂3-8%、皮肤调理剂II 2.5-5.5%;
D相:椰壳活性炭粉0.8-2.0%、
E相:洋甘菊提取物0.05-0.12%、复合氨基酸0.05-0.12%、金缕梅蒸馏液0.05-0.2%、皮肤调理剂III 0.05-0.12%、防腐剂0.05-0.12%、香精0.1-0.2%。
2.如权利要求1所述的一种添加椰壳活性炭粉的洁面乳,其特征在于:按照重量百分比计,其原料由A相、B相、C相、D相和E相混合而成:
A相:乳化剂I15%、乳化剂II8%、乳化剂III7.5%、丙二醇2%、皮肤调理剂I1.5%、甘油硬脂酸酯1%;
B相:水35.6%、氢氧化钾5.7%、保湿剂14%,所述保湿剂包括以下重量百分比原料:甘油99.7%、水0.3%;
C相:表面活性剂4%、皮肤调理剂II3.5%;
D相:椰壳活性炭粉1.5%、
E相:洋甘菊提取物0.1%、复合氨基酸0.1%、金缕梅蒸馏液0.15%、皮肤调理剂III0.1%、防腐剂0.1%、香精0.15%。
3.如权利要求1所述的一种添加椰壳活性炭粉的洁面乳,其特征在于:所述乳化剂I包括以下重量百分比原料:月桂酸0.3%、肉豆蔻酸99.3%、棕榈酸0.4%;所述乳化剂II包括以下重量百分比原料:肉豆蔻酸0.3%、棕榈酸99.1%、硬脂酸0.6%;所述乳化剂III包括以下重量百分比原料:月桂酸0.24%、肉豆蔻酸1.25%、棕榈酸58.16%、硬脂酸39.84%、花生酸0.32%、油酸0.19%。
4.如权利要求1所述的一种添加椰壳活性炭粉的洁面乳,其特征在于:所述皮肤调理剂I包括以下重量百分比原料:PEG-150二硬脂酸酯97%、水3%;所述皮肤调理剂II包括以下重量百分比原料:棕榈仁油酰胺DEA90%、甘油10%;所述皮肤调理剂III包括以下重量百分比原料:水0.05%、苯氧乙醇99.39%、乙酰基六肽-80.5%、乙基己基甘油0.06%。
5.如权利要求1所述的一种添加椰壳活性炭粉的洁面乳,其特征在于:所述表面活性剂包括以下重量百分比原料:甲基椰油酰基牛磺酸钠40%、水60%。
6.如权利要求1所述的一种添加椰壳活性炭粉的洁面乳,其特征在于:所述洋甘菊提取物包括以下重量百分比原料:母菊花提取物5%、水70%、丁二醇25%。
7.如权利要求1所述的一种添加椰壳活性炭粉的洁面乳,其特征在于:所述复合氨基酸包括以下重量百分比原料:水15.38%、丁二醇24.45%、甘油17.35%、丝氨酸5.7%、精氨酸5.35%、谷氨酸4.45%、异亮氨酸4.37%、脯氨酸4.25%、甘氨酸3.95%、亮氨酸3.35%、丙氨酸3.35%、天冬氨酸3.21%、缬氨酸2.8%、乳酸钠1.02%、乳酸1.02%。
8.如权利要求1所述的一种添加椰壳活性炭粉的洁面乳,其特征在于:所述金缕梅蒸馏液包括以下重量百分比原料:北美金缕梅水99%、苯氧乙醇1%。
9.如权利要求1所述的一种添加椰壳活性炭粉的洁面乳,其特征在于:所述防腐剂包括以下重量百分比原料:甲基异噻唑啉酮0.18%、甲基氯异噻唑啉酮0.54%、氯化镁0.2%、硝酸镁1%、苯甲醇20%、三甘醇25%、丙二醇15%、水38.08%。
10.如权利要求1所述的一种添加椰壳活性炭粉的洁面乳的制备方法,其特征在于:包括以下步骤:
S1、将A相投入主锅中,搅拌加热至80-90℃,恒温搅拌至完全溶解;
S2、将B相投入到水锅中,搅拌加热到65-75℃,搅拌至完全溶解,边搅拌边快速抽入到主锅,4-6分钟抽完后放掉真空,控制搅拌25-40rpm,恒温搅拌40-50分钟,再加入C相搅拌均匀,
S3、当上述混料搅拌降温到45℃以下,加入预先分散均匀的D相搅匀,再加入E相,搅拌均匀,搅拌降温到35℃以下后报检,QC检验合格过滤出料静置,灌装、包装、入库,得到一种添加椰壳活性炭粉的洁面乳。
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