CN118141152A

CN118141152A - Manufacturing method of jasmine flower explosion beads for cigarettes

Info

Publication number: CN118141152A
Application number: CN202410256070.7A
Authority: CN
Inventors: 李国瑞; 杨洋; 冯亚婕
Original assignee: China Tobacco Zhejiang Industrial Co Ltd
Current assignee: China Tobacco Zhejiang Industrial Co Ltd
Priority date: 2024-03-06
Filing date: 2024-03-06
Publication date: 2024-06-07

Abstract

The invention relates to a method for preparing jasmine flower pop beads for cigarettes, which comprises the steps of selecting different types of jasmine flowers, mixing the different types of jasmine flowers into a jasmine flower group, selecting liquorice, dried orange peel and acacia, mixing the components according to a set proportion, grinding to obtain mixed slurry, leaching the mixed slurry in glycerin water for 72 hours, ultrasonically extracting leaching the leaching solution with ethyl acetate, taking supernatant after the extraction, performing spin steaming in a fume hood for 10 minutes, standing for 2 hours to obtain a jasmine flower extract, mixing the jasmine flower extract with jojoba oil and coconut oil to obtain a solution A and a solution B respectively, mixing the solution A and the solution B according to a proportion to obtain a jasmine flower pop bead liquid, and injecting the jasmine flower pop bead liquid into the pop beads or coating wall shells to obtain the jasmine flower pop beads for cigarettes. According to the technical scheme, jasmine extraction is used as a main technical means, and other proper proportion of spices are matched, so that the jasmine extract is injected into the explosion beads and applied to cigarettes, and the taste and quality of the cigarettes are greatly improved.

Description

Manufacturing method of jasmine flower explosion beads for cigarettes

Technical Field

The invention belongs to the technical field of tobacco essence, and particularly relates to a manufacturing method of jasmine flower explosion beads for tobacco.

Background

With the growth of new generation tobacco consumers, the demand for various special-shaped tobacco is explosively increased, and in order to meet the consumer demand, the change of tobacco taste is a research and development direction.

In the prior art, the flavor of tobacco is changed mainly by adding flavor to cut tobacco, or adding flavor lines adhered with flavor substances to a filter tip, or dispersing flavor substance particles in the filter stick. The method has obvious defects: the fragrance retention time is short, the quality guarantee period of cigarettes is short, and active ingredients are not easy to enter main stream smoke.

The above disadvantages can be overcome by the use of a bead for flavoring, which contains the desired flavor extract. Before the consumer smokes the cigarette, the explosion beads are broken, the effective components in the explosion beads are released rapidly, and when the consumer smokes, the effective components enter the mouth and nose of the consumer to finish the change of the smoking flavor. Because the effective components are not easy to volatilize in the explosion beads, the explosion beads can be stored for a long time.

In the current market, the cigarette with the explosion beads is mostly made of peppermint, dried orange peel, cogongrass rhizome and wuliangye wine, and the preparation methods are different. At present, the jasmine flower smell absorbing and bursting beads are rare in the market. Jasmine flower, a plant of the genus jasminum of the family oleaceae, standing or climbing shrubs. The stalks are higher and are cylindrical and hollow; the leaves are opposite and made of paper, are round and have longer leaf handles; the flower is umbrella-shaped, the bud is smaller, the flower bud is conical, the corolla is white, and the flower bud is oblong; the fruit is spherical, black brown, the jasmine flower period is 5-8 months, and the fruit period is 7-9 months.

The "Ben Cao gang mu Shi" records jasmine flower "light in smell and taste, which can penetrate the top of qi, go down to the lower abdomen, dispel all stale qi in the chest, and avoid foul turbidity. The Chinese medicinal composition can calm liver, resolve depression, regulate qi and relieve pain. The jasmine flower extract is added into the cigarette burst beads, so that the smoke can be obviously improved, the flower fragrance is increased, the stimulation is lightened, and the fire is reduced and the liver is cleared. There is a need to design a method for producing jasmine flower pop beads for cigarettes, so that the jasmine flower pop beads are used in tobacco production.

Disclosure of Invention

The invention aims to provide a manufacturing method of jasmine flower explosion beads for cigarettes, which adopts jasmine flower extraction as a main technical means and is matched with other proper proportion of spices, so that the jasmine flower extract is injected into the explosion beads and is applied to cigarettes, and the taste and quality of the cigarettes are greatly improved.

In order to achieve the above purpose, the application is realized by the following technical scheme:

A manufacturing method of jasmine flower explosion beads for cigarettes comprises the following steps:

s1, selecting different varieties of jasmine flowers to be mixed into a jasmine group.

S2, selecting liquorice, dried orange peel and acacia.

S3, mixing the jasmine flower group in the step S1 with the liquorice, the dried orange peel and the acacia in the step S2 according to a set proportion, chopping and grinding to obtain mixed slurry; when in mass production, the proportion of various jasmine flowers can be properly increased or decreased according to the price.

S4, leaching the mixed slurry obtained in the step S3 in glycerol water for 72 hours to obtain leaching liquor.

S5, ultrasonically extracting the leaching solution obtained in the step S4 by using ethyl acetate.

S6, performing ultrasonic extraction by using ethyl acetate, taking supernatant after extraction, performing rotary steaming in a fume hood for 10 minutes, and standing for 2 hours to obtain the jasmine flower extract.

And S7, mixing part of jasmine flower extract and jojoba oil in the step S6 according to a set weight ratio, stirring and standing to obtain a solution A.

Jojoba (also known as Jojoba) is a native mexico plant, cultivated worldwide, and the mexico junction is most suitable for its growth and has better quality. The oil in the seeds of shrubs with how high one person is has good permeability and high temperature resistance.

And S8, mixing part of jasmine flower extract obtained in the step S6 with coconut oil according to a set weight ratio, stirring and standing to obtain a solution B.

The coconut oil is fractionated coconut oil, which is refined by taking virgin coconut oil as a raw material, and the main components are caprylic acid and capric acid triglyceride. In fractionating coconut oil, most of long-chain fatty acids and medium-chain fatty acids which are easy to generate oil consumption such as myristic acid and lauric acid are removed by fractionation, and only a part of medium-chain fatty acids and short-chain fatty acids are reserved. The fractionated coconut oil will not solidify below 24 ℃, and can remain liquid even when placed in a refrigerator for refrigeration, and is convenient for use. The greatest benefit of fractionating coconut oil is very shelf stable. Because of stable property, the product is not easy to deteriorate, no special storage and treatment process is needed, and the product is placed in a cool and dry place. Fractionated coconut oil is used as a carrier oil for jasmine extract. The jasmine essential oil can be completely fused with the jasmine essential oil, has small molecules, no impurities, no color and smell, no oil stain and no interference on the properties and the fragrance of the jasmine essential oil.

S9, mixing the solution A and the solution B according to a volume ratio of 2-10: and 1, mixing, stirring and standing to obtain jasmine flower bead-blasting liquid.

S10, injecting the jasmine flower explosion bead liquid into an explosion bead shell or pumping the jasmine flower explosion bead liquid to the jasmine flower explosion bead through a coating shell.

Preferably, the jasmine flower group is composed of star jasmine, mountain element, big flower jasmine, small flower jasmine and erigeron breviscapus.

Preferably, the weight ratio of the star jasmine, the mountain element, the big flower jasmine, the small flower jasmine to the hairy jasmine is 1-5:1-5:2-10:2-10:1-5.

Preferably, the weight ratio of the jasmine flower group to the liquorice to the dried orange peel to the acacia is 30-50:2-5:2-5:1.

Preferably, the mass concentration of the glycerol water is 30% -50%.

Preferably, the mass ratio of the ethyl acetate to the leaching solution is 1-2.

Preferably, the jasmine flower extract and the jojoba oil are mixed according to the mass ratio of 1: 2-10.

Preferably, the coconut oil is fractionated coconut oil.

Preferably, the jasmine flower extract and the coconut oil are mixed according to the mass ratio of 1: 2-10.

Preferably, the volume ratio of the solution A to the solution B is 2-10: 1.

The beneficial effects of the invention are as follows:

according to the technical scheme, jasmine extraction is used as a main technical means, and other proper proportion of spices are matched, so that the jasmine extract is injected into the explosion beads and applied to cigarettes, and the taste and quality of the cigarettes are greatly improved.

Detailed Description

The following examples are given by way of illustration only and are not to be construed as limiting the scope of the invention.

The jasmine flower group used in the application is star jasmine, mountain element, big flower jasmine, small flower jasmine and Mao Moli flowers, and the jasmine flower group can be purchased in the market. In the technical scheme, the weight ratio of the star jasmine, the mountain element, the big flower jasmine, the small flower jasmine and the hairy jasmine is 1-5:1-5:2-10:2-10:1-5. In actual production, the weight ratio range can be exceeded according to the factors such as the yield, price and the like of different jasmine flowers at the time, and the fragrance of the jasmine flowers can not be obviously influenced.

Example 1

S1, selecting jasmine groups to remove impurities.

S2, selecting licorice, dried orange peel and acacia and removing impurities.

S3, mixing jasmine, liquorice, dried orange peel and acacia in a weight ratio of 30:4:2:1, chopping and grinding to obtain slurry. Wherein the weight of jasmine is prepared according to the weight ratio of star jasmine, mountain element, big flower jasmine, small flower jasmine and Mao Moli flower jasmine 1:1:2:2:1.

S4, leaching the mixed slurry in glycerol water for 72 hours to obtain leaching liquor, wherein the mass concentration of the glycerol water is 30%.

S5, ultrasonically extracting the leaching solution by using ethyl acetate.

S6, performing ultrasonic extraction by using ethyl acetate, taking supernatant, performing rotary steaming in a fume hood for 10 minutes, and standing for 2 hours to obtain the jasmine flower extract.

S7, mixing part of jasmine flower extract and jojoba oil obtained in the step S6 according to the ratio of 1: mixing the materials according to the mass ratio of 5, stirring the materials for 5 minutes, and standing the materials for 10 minutes to obtain a solution A.

S8, mixing the jasmine flower extract and the fractionated coconut oil according to the mass of 7:1, mixing and stirring for 5 minutes, and standing for 10 minutes to obtain a solution B.

And S9, mixing the solution A and the solution B according to the volume of 5:1, stirring for 5 minutes, and standing for 10 minutes to obtain the jasmine flower bead-blasting liquid.

S10, injecting the jasmine flower explosion bead liquid into the explosion beads to obtain the jasmine flower explosion beads.

Example 2

A method for preparing jasmine flower explosion beads for cigarettes comprises the following steps of mixing jasmine flower, liquorice, dried orange peel and acacia in a weight ratio of 40:4:3:1, and obtaining the jasmine flower explosion beads liquid under the condition that other conditions are unchanged.

Example 3

The preparation method of the jasmine flower explosion bead for the cigarettes comprises the following steps, which are the same as in example 1, wherein the mass concentration of glycerin water is 50%, and other conditions are unchanged, so that the jasmine flower explosion bead liquid is finally obtained.

Example 4

The preparation method of the jasmine flower explosion bead for the cigarettes comprises the following steps of the preparation method as in example 1, wherein the difference is that the mass of ethyl acetate is changed to 2 times, and other conditions are unchanged, so that the jasmine flower explosion bead liquid is finally obtained.

Example 5

The preparation method of the jasmine flower explosion bead for the cigarettes comprises the following steps, which are the same as in example 1, wherein the mass concentration of glycerin water is 40%, and other conditions are unchanged, so that the jasmine flower explosion bead liquid is finally obtained.

Example 6

A method for preparing jasmine flower explosion beads for cigarettes comprises the following steps, which are the same as in example 1, wherein jasmine flower extracts and jojoba oil are mixed according to a mass ratio of 3:1, stirred and then kept stand, and other conditions are unchanged, so that the jasmine flower explosion bead liquid is finally obtained.

Example 7

The preparation method of the jasmine flower explosion beads for cigarettes comprises the following steps of, as in example 1, mixing jasmine flower extract and fractionated coconut oil according to a mass ratio of 9:1, mixing and stirring for 5 minutes, and standing for 10 minutes to finally obtain the jasmine flower bead-blasting liquid.

Example 8

A method for preparing jasmine flower explosion beads for cigarettes comprises the following steps, which are the same as in example 1, wherein the difference is that a solution A and a solution B are mixed according to a volume ratio of 3:1, stirred for 5 minutes and kept stand for 10 minutes to obtain the jasmine flower explosion bead liquid.

Comparative example 1

A preparation method of jasmine flower explosion beads for cigarettes is characterized in that the mass concentration of glycerin water is 100%, namely pure glycerin, is mixed according to the mass ratio of jasmine flower to liquorice to dried orange peel to acacia in a ratio of 30:4:2:1, and is cut up and ground to obtain slurry. Wherein the quality of jasmine is prepared according to the ratio of 1:1:2:2:1 of the jasmine of asterias amurensis, mountain element, big flower jasmine, small flower jasmine and Mao Moli flower. The mixed slurry was leached in glycerol (100% strength) for 72 hours, and the solution obtained after leaching was too thick to be filtered and the hydrophilic aroma was not leached, so that the next step could not be achieved.

Comparative example 2

A preparation method of jasmine flower explosion beads for cigarettes is characterized in that the mass concentration of glycerin water is 0%, namely distilled water, and the jasmine flower explosion beads, the liquorice, the dried orange peel and the acacia are mixed according to the mass ratio of 30:4:2:1, cut up and ground to obtain slurry. Wherein the quality of jasmine is prepared according to the ratio of 1:1:2:2:1 of the jasmine of asterias amurensis, mountain element, big flower jasmine, small flower jasmine and Mao Moli flower. The mixed slurry is leached in distilled water for 72 hours, and the lipophilic and fragrant substances cannot be leached during leaching, so that the fragrance is not strong, and the next step cannot be realized.

Comparative example 3

A method for preparing jasmine flower explosion beads for cigarettes comprises the following steps:

S1, selecting jasmine flowers and removing impurities;

s2, selecting chrysanthemum, liquorice and dried orange peel to remove impurities.

S3, mixing jasmine, liquorice, dried orange peel and acacia in a mass ratio of 30:4:2:1, chopping and grinding to obtain slurry. Wherein the quality of jasmine is prepared according to the ratio of 1:1:2:2:1 of the jasmine of asterias amurensis, mountain element, big flower jasmine, small flower jasmine and Mao Moli flower.

And S4, leaching the mixed slurry in glycerol water for 72 hours to obtain a solution A. The mass concentration of the glycerol water is 30%, and the solid matters are discarded.

S5, extracting the solution A by using n-butanol, oscillating for 10 minutes by using ultrasonic waves at room temperature during extraction, and standing for 30 minutes.

After extraction, the n-butanol smell masks the jasmine fragrance, and the next step cannot be performed.

The sensory quality of the cigarette product is according to the national standard GB5606.4-2005, and the technical requirements of the sensory quality of the cigarette product are shown in the following table 1:

TABLE 1

Preparing a cigarette sample M, preparing the preparation obtained in the examples 1-8 into explosive beads, respectively placing the explosive beads into a filter rod of the cigarette sample M, and enabling explosive bead liquid to enter the filter rod after the explosive beads are extruded. Scoring and evaluation were performed by 9 professional tobacco evaluators, and the evaluation tables of the professional tobacco evaluators are shown in the average value in Table 2:

through the smoking evaluation, all professional smoking evaluation staff consider that the cigarette sample added with the jasmine flower explosion beads in the embodiment 1 has natural and comfortable fragrance, strong jasmine flower fragrance, fine smoke smell and multiplied fragrance during smoking. Meanwhile, the tobacco flavor is matched and coordinated with the original tobacco flavor, and no obvious uncomfortable feeling is caused.

The previous description of the disclosed embodiments is provided to enable any person skilled in the art to make or use the present invention. Various modifications to these embodiments will be readily apparent to those skilled in the art, and the generic principles defined herein may be applied to other embodiments without departing from the spirit or scope of the invention. Thus, the present invention is not intended to be limited to the embodiments shown herein but is to be accorded the widest scope consistent with the principles and novel features disclosed herein.

Claims

1. The manufacturing method of the jasmine flower pop beads for the cigarettes is characterized by comprising the following steps of:

S1, selecting different varieties of jasmine flowers to be mixed into a jasmine group;

S2, selecting liquorice, dried orange peel and acacia;

S3, mixing the jasmine flower group in the step S1 with the liquorice, the dried orange peel and the acacia in the step S2 according to a set proportion, chopping and grinding to obtain mixed slurry;

s4, leaching the mixed slurry obtained in the step S3 in glycerol water for 72 hours to obtain leaching liquor;

S5, ultrasonically extracting the leaching solution obtained in the step S4 by using ethyl acetate;

S6, performing ultrasonic extraction by using ethyl acetate, taking supernatant after extraction, performing rotary steaming in a fume hood for 10 minutes, and standing for 2 hours to obtain a jasmine flower extract;

s7, mixing part of jasmine flower extract and jojoba oil in the step S6 according to a set weight ratio, stirring and standing to obtain a solution A;

s8, mixing part of jasmine flower extract and coconut oil in the step S6 according to a set weight ratio, stirring and standing to obtain a solution B;

S9, mixing the solution A and the solution B according to a volume ratio of 2-10:1, mixing, stirring and standing to obtain jasmine flower bead-blasting liquid;

2. The method for producing jasmine flower pop beads for cigarettes according to claim 1, wherein the jasmine flower group consists of star jasmine, mountain quartz, big flower jasmine, small flower jasmine and erigeron breviscapus.

3. The method for producing the jasmine flower pop beads for cigarettes according to claim 2, wherein the weight ratio of the star jasmine, the mountain element, the big flower jasmine, the small flower jasmine and the mirabilite is 1-5:1-5:2-10:2-10:1-5.

4. The method for preparing jasmine flower pop beads for cigarettes according to claim 1, wherein the weight ratio of jasmine flower groups to liquorice to dried orange peel to acacia is 30-50:2-5:2-5:1.

5. The method for producing jasmine flower pop beads for cigarettes according to claim 1, wherein the mass concentration of the glycerin water is 30% -50%.

6. The method for producing jasmine flower pop beads for cigarettes according to claim 1, wherein the mass ratio of the ethyl acetate to the leaching solution is 1-2.

7. The method for preparing the jasmine flower pop beads for cigarettes according to claim 1, wherein the mass ratio of the jasmine flower extract to the jojoba oil is 1: 2-10.

8. The method of claim 1, wherein the coconut oil is fractionated coconut oil.

9. The method for preparing the jasmine flower pop beads for cigarettes according to claim 1, wherein the mass ratio of the jasmine flower extract to the coconut oil is 1: 2-10.

10. The method for manufacturing jasmine flower pop beads for cigarettes according to claim 1, wherein the volume ratio of the solution A to the solution B is 2-10: 1.