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CN116407878A - A separation device for liquid containing polypropylene particles - Google Patents

A separation device for liquid containing polypropylene particles Download PDF

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Publication number
CN116407878A
CN116407878A CN202111643433.5A CN202111643433A CN116407878A CN 116407878 A CN116407878 A CN 116407878A CN 202111643433 A CN202111643433 A CN 202111643433A CN 116407878 A CN116407878 A CN 116407878A
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China
Prior art keywords
dust
liquid
water
chamber
heat exchanger
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Pending
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CN202111643433.5A
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Chinese (zh)
Inventor
高妍
宋文波
周姣龙
翟建宏
胡晓石
邹发生
赵泽昊
周春
陈志敏
令永功
赵梦垚
徐健
宁波
米超
苏洪
董清生
张帆
谢晓玲
王辛幸
赵旭
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Shanghai Institute of Organic Chemistry of CAS
Sinopec Beijing Research Institute of Chemical Industry
China Petroleum and Chemical Corp
Sinopec Yangzi Petrochemical Co Ltd
Sinopec Engineering Inc
Tianhua Institute of Chemical Machinery and Automation Co Ltd
Original Assignee
Shanghai Institute of Organic Chemistry of CAS
Sinopec Beijing Research Institute of Chemical Industry
China Petroleum and Chemical Corp
Sinopec Yangzi Petrochemical Co Ltd
Sinopec Engineering Inc
Tianhua Institute of Chemical Machinery and Automation Co Ltd
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Application filed by Shanghai Institute of Organic Chemistry of CAS, Sinopec Beijing Research Institute of Chemical Industry, China Petroleum and Chemical Corp, Sinopec Yangzi Petrochemical Co Ltd, Sinopec Engineering Inc, Tianhua Institute of Chemical Machinery and Automation Co Ltd filed Critical Shanghai Institute of Organic Chemistry of CAS
Priority to CN202111643433.5A priority Critical patent/CN116407878A/en
Publication of CN116407878A publication Critical patent/CN116407878A/en
Pending legal-status Critical Current

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    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02WCLIMATE CHANGE MITIGATION TECHNOLOGIES RELATED TO WASTEWATER TREATMENT OR WASTE MANAGEMENT
    • Y02W30/00Technologies for solid waste management
    • Y02W30/50Reuse, recycling or recovery technologies
    • Y02W30/62Plastics recycling; Rubber recycling

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  • Heat-Exchange Devices With Radiators And Conduit Assemblies (AREA)

Abstract

The invention relates to a separation device for liquid containing polypropylene particles, which comprises: the liquid storage tank is internally provided with a baffle, the height of the baffle is smaller than that of the liquid storage tank, and the liquid storage tank is separated into a water purifying chamber and a dust-containing water chamber; the dust-containing water chamber is provided with a dust-containing water outlet below, and the water purifying chamber is provided with a first purified water outlet below. The fluid filtration is realized by utilizing the characteristic that the density of impurities such as dust and the like contained in the process fluid is smaller than that of the process fluid and floats on the surface of the fluid.

Description

一种含聚丙烯颗粒液体的分离装置A separation device for liquid containing polypropylene particles

技术领域technical field

本发明涉及聚烯烃行业固液分离技术领域,具体涉及一种含聚丙烯颗粒液体的分离装置。The invention relates to the technical field of solid-liquid separation in the polyolefin industry, in particular to a separation device for a liquid containing polypropylene particles.

背景技术Background technique

聚丙烯水下切粒过程中会产生大量细粉,该细粉进入切粒水中,并随切粒水在系统内循环,为了防止细粉在系统内累计影响冷却器等下游设备的正常工作,需在进入冷却器前增加过滤装置将细分过滤去除。国内普遍采用曲张筛作为分离装置、该装置为一开一备使用,占地面积大,且筛网需要定期清洗更换。A large amount of fine powder will be produced during the underwater granulation of polypropylene. The fine powder enters the granulation water and circulates in the system with the granulation water. In order to prevent the accumulation of fine powder in the system and affect the normal operation of downstream equipment such as coolers, it is necessary Before entering the cooler, a filter device is added to remove the subdivided filter. Varicose sieves are generally used as separation devices in China. This device is used for one opening and one standby. It occupies a large area, and the screen needs to be cleaned and replaced regularly.

发明内容Contents of the invention

本发明的目的在于提供一种含聚丙烯颗粒液体的分离装置,以解决现有技术中设备占地面积大,需要定期维护且操作不方便的问题。The object of the present invention is to provide a separation device for liquid containing polypropylene particles, so as to solve the problems in the prior art that the equipment occupies a large area, requires regular maintenance and is inconvenient to operate.

为实现上述目的,本发明提供一种含聚丙烯颗粒液体的分离装置,包括:储液罐,所述储液罐内设有隔板,所述隔板的高度小于储液罐的高度,将储液罐分离为净水室和含尘水室;所述含尘水室下方设有含尘水出口,所述净水室下方设有第一净水出口。In order to achieve the above object, the present invention provides a separation device for liquid containing polypropylene particles, comprising: a liquid storage tank, a partition is arranged in the liquid storage tank, the height of the partition is smaller than the height of the liquid storage tank, and the The liquid storage tank is separated into a clean water chamber and a dusty water chamber; a dusty water outlet is provided below the dusty water chamber, and a first clean water outlet is provided below the clean water chamber.

本发明所述的含聚丙烯颗粒液体的分离装置,其中,所述净水室下方还设有换热器,所述净水室和换热器通过降液管连接。The separation device for liquid containing polypropylene particles according to the present invention, wherein a heat exchanger is further arranged under the water purification chamber, and the water purification chamber and the heat exchanger are connected through a downcomer.

本发明所述的含聚丙烯颗粒液体的分离装置,其中,所述换热器下方设有下管箱。The separation device for liquid containing polypropylene particles according to the present invention, wherein, a down tube box is arranged below the heat exchanger.

本发明所述的含聚丙烯颗粒液体的分离装置,其中,所述含尘水室上设有上、下两个液位计,含尘水出口连接有含尘水排水管线,含尘水排水管线上设有阀门。The separation device for liquid containing polypropylene particles according to the present invention, wherein the dust-containing water chamber is provided with two liquid level gauges, upper and lower, and the dust-containing water outlet is connected with a dust-containing water drainage pipeline, and the dust-containing water is drained There is a valve on the pipeline.

本发明所述的含聚丙烯颗粒液体的分离装置,其中,所述净水室上和降液管上均设有液位计。The separation device for liquid containing polypropylene particles according to the present invention, wherein liquid level gauges are arranged on the clean water chamber and the downcomer.

本发明所述的含聚丙烯颗粒液体的分离装置,其中,所述储液罐上设有上封头,所述上封头上在对应于净水室的位置设有含尘水入口。The device for separating liquid containing polypropylene particles according to the present invention, wherein the liquid storage tank is provided with an upper head, and the upper head is provided with an inlet for dusty water at a position corresponding to the water purification chamber.

本发明所述的含聚丙烯颗粒液体的分离装置,其中,所述换热器为管壳式换热器,壳侧设有换热介质入口、换热介质出口、排净口和放空口。The separation device for liquid containing polypropylene particles according to the present invention, wherein the heat exchanger is a shell-and-tube heat exchanger, and the shell side is provided with a heat exchange medium inlet, a heat exchange medium outlet, a clean outlet and a vent.

本发明的有益效果是:The beneficial effects of the present invention are:

利用工艺流体中所含粉尘等杂质密度小于工艺流体,浮于流体表面的特点实现流体过滤,在净水室下方设有换热器,还可以将过滤冷却或过滤加热在一台设备中完成。The density of dust and other impurities contained in the process fluid is lower than that of the process fluid, and the characteristics of floating on the surface of the fluid are used to realize fluid filtration. A heat exchanger is installed under the clean water chamber, and filtration cooling or filtration heating can also be completed in one device.

附图说明Description of drawings

图1为本发明所述含聚丙烯颗粒液体的分离装置的结构示意图;Fig. 1 is the structural representation of the separation device containing polypropylene particle liquid of the present invention;

图2为本发明所述聚丙烯颗粒过滤冷却一体化技术工艺流程图;Fig. 2 is the process flow diagram of the integrated technology of polypropylene particle filtration and cooling in the present invention;

图3为本发明所述聚丙烯颗粒过滤加热一体化技术工艺流程图。Fig. 3 is a process flow chart of the integrated technology of filtering and heating polypropylene particles according to the present invention.

其中,附图标记:Among them, reference signs:

1 储液罐;1 liquid storage tank;

2 隔板;2 partitions;

3 净水室;3 clean water room;

4 含尘水室;4 dusty water chamber;

5 含尘水出口;5 outlet of dusty water;

6 换热器;6 heat exchangers;

7 降液管;7 downcomer;

8 下管箱;8 down tube box;

9 第二净水出口;9 the second clean water outlet;

10 温度计接口;10 thermometer interface;

11-1、11-2、11-3 11-4 液位计;11-1, 11-2, 11-3 11-4 Liquid level gauge;

12 含尘水排水管线;12 Dusty water drainage pipeline;

13 上封头;13 upper head;

14 含尘水入口;14 Inlet for dusty water;

15 换热介质出入口一;15 Heat exchange medium inlet and outlet 1;

16 换热介质出入口二;16 Heat exchange medium inlet and outlet 2;

17 排净口;17 drain port;

18 放空口;18 vents;

19 输送泵;19 transfer pump;

20 支耳。20 lugs.

具体实施方式Detailed ways

下面通过实施例对本发明进行具体描述。有必要在此指出的是以下实施例只用于对本发明进行进一步说明,不能理解为对本发明保护范围的限制,该领域的技术熟练人员可以根据上述本发明内容对本发明作出一些非本质的改进和调整。The present invention is specifically described below by way of examples. It is necessary to point out that the following examples are only used to further illustrate the present invention, and cannot be interpreted as limiting the protection scope of the present invention. Those skilled in the art can make some non-essential improvements and improvements to the present invention according to the above-mentioned content of the present invention. Adjustment.

请参考图1,本发明所述的一种含聚丙烯颗粒液体的分离装置,包括:储液罐1,所述储液罐1内设有隔板2,所述隔板2将储液罐1分离为净水室3和含尘水室4;所述含尘水室4下方设有含尘水出口5,所述净水室3下方设有第一净水出口。Please refer to Fig. 1, a kind of separating device that contains polypropylene particle liquid according to the present invention, comprises: liquid storage tank 1, is provided with dividing plate 2 in described liquid storing tank 1, and described dividing plate 2 divides liquid storing tank 1 is separated into a clean water chamber 3 and a dusty water chamber 4; a dusty water outlet 5 is provided below the dusty water chamber 4, and a first clean water outlet is provided below the water purification chamber 3.

隔板2的高度小于储液罐1的高度,使相邻的净水室3和含尘水室4顶部相通,处理过程中,含尘液体首先流入净水室3,由于含聚丙烯颗粒液体中聚丙烯颗粒密度小于液体密度,聚丙烯颗粒浮于液体表面,当液面逐渐升高至隔板2高度时,上层含有聚丙烯颗粒的液体则自流入含尘水室4,从而实现聚丙烯颗粒与液体的分离,含尘水室4内的浓缩聚丙烯颗粒废液可以通过含尘水出口5排出,去除聚丙烯颗粒的液体通过第一净水出口排出。The height of the partition 2 is smaller than the height of the liquid storage tank 1, so that the adjacent clean water chamber 3 and the top of the dust-containing water chamber 4 communicate. The density of polypropylene particles in the medium is smaller than that of the liquid, and the polypropylene particles float on the surface of the liquid. When the liquid level gradually rises to the height of the partition 2, the liquid containing polypropylene particles in the upper layer will flow into the dust-containing water chamber 4, thereby realizing the separation of polypropylene particles into the dust-containing water chamber 4. For the separation of particles and liquid, the concentrated polypropylene particle waste liquid in the dusty water chamber 4 can be discharged through the dusty water outlet 5, and the liquid from which the polypropylene particles are removed is discharged through the first clean water outlet.

作为一优选实施方案,所述净水室3下方还设有换热器6,所述净水室3和换热器6通过降液管7连接。所述降液管7应具有一定高度,从而增加细粉浮力,同时防止流体进入净水室时将细粉带入换热器。As a preferred embodiment, a heat exchanger 6 is further provided below the water purification chamber 3 , and the water purification chamber 3 and the heat exchanger 6 are connected through a downcomer 7 . The downcomer 7 should have a certain height, thereby increasing the buoyancy of the fine powder, and preventing the fine powder from being brought into the heat exchanger when the fluid enters the clean water chamber.

作为一优选实施方案,所述换热器6下方设有下管箱8,下管箱8上设有第二净水出口9和温度计接口10。温度计接口10可以设置温度检测仪表,通过控制管线上的调节阀保持净化水温度满足工艺要求As a preferred embodiment, a lower tube box 8 is provided below the heat exchanger 6 , and a second clean water outlet 9 and a thermometer interface 10 are provided on the lower tube box 8 . The thermometer interface 10 can be equipped with a temperature detection instrument, and the temperature of the purified water can be maintained to meet the process requirements through the regulating valve on the control pipeline

请同时参考图1和图2,作为一优选实施方案,所述含尘水室4上设有上、下两个液位计11-1和11-2,含尘水出口5连接有含尘水排水管线12,含尘水排水管线12上设有阀门。当含尘水室4中含尘水累计到达高液位后联锁定排含尘水排水管线12上的两位阀开,将含尘水排出设备;当水位到达低液位后联锁定排含尘水排水管线12上的两位阀关闭。Please refer to Fig. 1 and Fig. 2 at the same time. As a preferred embodiment, the dusty water chamber 4 is provided with upper and lower liquid level gauges 11-1 and 11-2, and the dusty water outlet 5 is connected with a dusty water The water drainage pipeline 12 is provided with a valve on the dusty water drainage pipeline 12. When the accumulation of dusty water in the dusty water chamber 4 reaches a high liquid level, the two-position valve on the dusty water drainage pipeline 12 of the locked drain is opened, and the dusty water is discharged from the equipment; when the water level reaches a low level, the locked drain is connected The two-position valve on the dust water drain line 12 is closed.

作为一优选实施方案,所述净水室3上和降液管7上分别设有液位计11-3和11-4。通过控制净水室3上液位计11-3控制净水排出管线上的调节阀保持储液罐1中水位处于正常液位。As a preferred embodiment, liquid level gauges 11-3 and 11-4 are respectively provided on the water purification chamber 3 and the downcomer 7. Keep the water level in the liquid storage tank 1 at a normal liquid level by controlling the liquid level gauge 11-3 on the clean water chamber 3 to control the regulating valve on the clean water discharge pipeline.

作为一优选实施方案,所述储液罐1上设有上封头13,所述上封头13上在对应于净水室3的位置设有含尘水入口14。As a preferred embodiment, the liquid storage tank 1 is provided with an upper head 13 , and the upper head 13 is provided with a dusty water inlet 14 at a position corresponding to the clean water chamber 3 .

请同时参考图1、图2和图3,作为一优选实施方案,所述换热器6为管壳式换热器,壳侧设有换热介质出入口一15、换热介质出入口二16、排净口17和放空口18。净水室3中的水自上而下流过换热器6的管程进行换热至所需温度,然后排出根据需要利用高位差自流至用水点或是通过输送泵19送至用水点。换热介质可以是冷却介质,如循环冷却水、低温水、冷冻盐水等,也可以是加热介质,如热水、蒸汽等,用于加热净化水。换热时,如果换热介质为冷却介质,则换热介质从换热介质出入口一15进入换热器6,从换热介质出入口二16流出换热器6;如果化热介质为加热介质,则换热介质从换热介质出入口二16进入换热器6,从换热介质出入口一15流出换热器6;所述输送泵19可以是离心式、容积式或其他形式的泵。Please refer to Fig. 1, Fig. 2 and Fig. 3 at the same time. As a preferred embodiment, the heat exchanger 6 is a shell-and-tube heat exchanger, and the shell side is provided with a heat exchange medium inlet and outlet 15, a heat exchange medium inlet and outlet 16, Drain port 17 and vent port 18. The water in the clean water chamber 3 flows through the tube side of the heat exchanger 6 from top to bottom to exchange heat to the required temperature, and then discharges to the water point by self-flowing with a high head difference or sent to the water point by the transfer pump 19 as required. The heat exchange medium can be a cooling medium, such as circulating cooling water, low-temperature water, frozen brine, etc., or a heating medium, such as hot water, steam, etc., for heating and purifying water. During heat exchange, if the heat exchange medium is a cooling medium, the heat exchange medium enters the heat exchanger 6 from the heat exchange medium inlet and outlet 15, and flows out of the heat exchanger 6 from the heat exchange medium inlet and outlet 16; if the heat transfer medium is a heating medium, Then the heat exchange medium enters the heat exchanger 6 from the second heat exchange medium inlet and outlet 16, and flows out of the heat exchanger 6 from the first heat exchange medium inlet and outlet 15; the delivery pump 19 can be centrifugal, positive displacement or other pumps.

作为一优选实施方案,储液罐侧壁上还可以设有支耳20,用于固定分离装置。As a preferred embodiment, lugs 20 may also be provided on the side wall of the liquid storage tank for fixing the separation device.

当然,本发明还可有其它多种实施例,在不背离本发明精神及其实质的情况下,熟悉本领域的技术人员可根据本发明作出各种相应的改变和变形,但这些相应的改变和变形都应属于本发明权利要求的保护范围。Certainly, the present invention also can have other multiple embodiments, without departing from the spirit and essence of the present invention, those skilled in the art can make various corresponding changes and deformations according to the present invention, but these corresponding changes All changes and modifications should belong to the protection scope of the claims of the present invention.

Claims (7)

1. A separator for a polypropylene-containing particulate liquid, comprising: the liquid storage tank is internally provided with a baffle, the height of the baffle is smaller than that of the liquid storage tank, and the liquid storage tank is separated into a water purifying chamber and a dust-containing water chamber; the dust-containing water chamber is provided with a dust-containing water outlet below, and the water purifying chamber is provided with a first purified water outlet below.
2. The polypropylene particle-containing liquid separation device according to claim 1, wherein a heat exchanger is further provided below the clean water chamber, and the clean water chamber and the heat exchanger are connected through a downcomer.
3. The separation device of polypropylene-containing granular liquid according to claim 2, wherein a down tube box is provided below the heat exchanger.
4. The device for separating liquid containing polypropylene particles according to claim 1, wherein the dust-containing water chamber is provided with an upper liquid level meter and a lower liquid level meter, the dust-containing water outlet is connected with a dust-containing water drain line, and the dust-containing water drain line is provided with a valve.
5. The polypropylene particle-containing liquid separation device of claim 1, wherein the water purification chamber and the downcomer are provided with liquid level gauges.
6. The separation device of polypropylene-containing granular liquid according to claim 1, wherein an upper head is provided on the liquid storage tank, and a dust-containing water inlet is provided on the upper head at a position corresponding to the clean water chamber.
7. The separator of claim 2, wherein the heat exchanger is a shell-and-tube heat exchanger, and the shell side is provided with a heat exchange medium inlet, a heat exchange medium outlet, a purge port and a vent port.
CN202111643433.5A 2021-12-29 2021-12-29 A separation device for liquid containing polypropylene particles Pending CN116407878A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN202111643433.5A CN116407878A (en) 2021-12-29 2021-12-29 A separation device for liquid containing polypropylene particles

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN202111643433.5A CN116407878A (en) 2021-12-29 2021-12-29 A separation device for liquid containing polypropylene particles

Publications (1)

Publication Number Publication Date
CN116407878A true CN116407878A (en) 2023-07-11

Family

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Family Applications (1)

Application Number Title Priority Date Filing Date
CN202111643433.5A Pending CN116407878A (en) 2021-12-29 2021-12-29 A separation device for liquid containing polypropylene particles

Country Status (1)

Country Link
CN (1) CN116407878A (en)

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