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CN116373063A - Low-formaldehyde ultrathin fiber board and preparation method thereof - Google Patents

Low-formaldehyde ultrathin fiber board and preparation method thereof Download PDF

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Publication number
CN116373063A
CN116373063A CN202310305352.7A CN202310305352A CN116373063A CN 116373063 A CN116373063 A CN 116373063A CN 202310305352 A CN202310305352 A CN 202310305352A CN 116373063 A CN116373063 A CN 116373063A
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hot
pressing
preparation
wood chips
pressure
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余三同
董荣丹
魏明
闵德秀
齐智超
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Shandong Xingang Group Co ltd
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Shandong Xingang Group Co ltd
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    • BPERFORMING OPERATIONS; TRANSPORTING
    • B27WORKING OR PRESERVING WOOD OR SIMILAR MATERIAL; NAILING OR STAPLING MACHINES IN GENERAL
    • B27NMANUFACTURE BY DRY PROCESSES OF ARTICLES, WITH OR WITHOUT ORGANIC BINDING AGENTS, MADE FROM PARTICLES OR FIBRES CONSISTING OF WOOD OR OTHER LIGNOCELLULOSIC OR LIKE ORGANIC MATERIAL
    • B27N3/00Manufacture of substantially flat articles, e.g. boards, from particles or fibres
    • B27N3/04Manufacture of substantially flat articles, e.g. boards, from particles or fibres from fibres
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B27WORKING OR PRESERVING WOOD OR SIMILAR MATERIAL; NAILING OR STAPLING MACHINES IN GENERAL
    • B27NMANUFACTURE BY DRY PROCESSES OF ARTICLES, WITH OR WITHOUT ORGANIC BINDING AGENTS, MADE FROM PARTICLES OR FIBRES CONSISTING OF WOOD OR OTHER LIGNOCELLULOSIC OR LIKE ORGANIC MATERIAL
    • B27N3/00Manufacture of substantially flat articles, e.g. boards, from particles or fibres
    • B27N3/08Moulding or pressing
    • DTEXTILES; PAPER
    • D21PAPER-MAKING; PRODUCTION OF CELLULOSE
    • D21BFIBROUS RAW MATERIALS OR THEIR MECHANICAL TREATMENT
    • D21B1/00Fibrous raw materials or their mechanical treatment
    • D21B1/04Fibrous raw materials or their mechanical treatment by dividing raw materials into small particles, e.g. fibres
    • D21B1/12Fibrous raw materials or their mechanical treatment by dividing raw materials into small particles, e.g. fibres by wet methods, by the use of steam
    • D21B1/14Disintegrating in mills
    • D21B1/16Disintegrating in mills in the presence of chemical agents
    • DTEXTILES; PAPER
    • D21PAPER-MAKING; PRODUCTION OF CELLULOSE
    • D21CPRODUCTION OF CELLULOSE BY REMOVING NON-CELLULOSE SUBSTANCES FROM CELLULOSE-CONTAINING MATERIALS; REGENERATION OF PULPING LIQUORS; APPARATUS THEREFOR
    • D21C3/00Pulping cellulose-containing materials
    • DTEXTILES; PAPER
    • D21PAPER-MAKING; PRODUCTION OF CELLULOSE
    • D21CPRODUCTION OF CELLULOSE BY REMOVING NON-CELLULOSE SUBSTANCES FROM CELLULOSE-CONTAINING MATERIALS; REGENERATION OF PULPING LIQUORS; APPARATUS THEREFOR
    • D21C5/00Other processes for obtaining cellulose, e.g. cooking cotton linters ; Processes characterised by the choice of cellulose-containing starting materials
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02WCLIMATE CHANGE MITIGATION TECHNOLOGIES RELATED TO WASTEWATER TREATMENT OR WASTE MANAGEMENT
    • Y02W30/00Technologies for solid waste management
    • Y02W30/50Reuse, recycling or recovery technologies
    • Y02W30/91Use of waste materials as fillers for mortars or concrete

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  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Wood Science & Technology (AREA)
  • Manufacturing & Machinery (AREA)
  • Forests & Forestry (AREA)
  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Mechanical Engineering (AREA)
  • Dry Formation Of Fiberboard And The Like (AREA)

Abstract

Provides a low-aldehyde ultrathin fiber board and a preparation method thereof, which can obtain the fiber board with good performance, the thickness is as thin as 0.8mm, and the density is as high as 0.9g/m 3 The ultrathin high-density fiberboard. The preparation method comprises the following steps: steaming the qualified wood chips, wherein the steaming pressure is 7.5 bar-8.0 bar, the steaming temperature is 160-165 ℃, and the steaming time is 3.5-4.0 min; adding melted 58# fully refined paraffin into the steamed wood chips and carrying out hot grinding to obtain 50-100 mesh wood fibers; uniformly applying urea-formaldehyde resin adhesive and an auxiliary agent on the surface of the wood fiber in a drying pipeline; drying the glued wood fiber to obtain the wood fiber with the water content of 6.0-6.5%Paving materials; paving the paving material into a continuous slab band, setting the thickness of the target plate to be 0.8mm and the density of the fiber plate to be 1050Kg/m 3 The method comprises the steps of carrying out a first treatment on the surface of the And conveying the slab band to a hot press for hot pressing, wherein the hot press is provided with four continuous pressure sections, the hot pressing temperature of the four pressure sections is gradually reduced according to the advancing direction of the slab band, and the hot pressing pressure of at least three later pressure sections is gradually increased.

Description

低醛超薄纤维板及其制备方法Low-aldehyde ultra-thin fiberboard and its preparation method

技术领域technical field

本发明涉及超薄纤维板的制造领域,尤其涉及一种低醛超薄纤维板及其制备方法。The invention relates to the field of manufacturing ultra-thin fiberboards, in particular to a low-aldehyde ultra-thin fiberboard and a preparation method thereof.

背景技术Background technique

超薄纤维板一方面可作为饰面材料代替现有的科技木及杨木装饰单板生产超平、肤感、高光等高档家具,解决家具表面装饰后碳化、不平整、易龟裂等问题;另一方面,可以作为高档实木复合地板的平衡饰面,具有高强度、抗变形、尺寸稳定性强等特点;另外,功能性超薄纤维板还可用于高档礼盒等的绿色环保包装材料,比普通纸质材料更加绿色环保。目前其他国家鲜见超薄纤维板的研究,中国在超薄纤维板生产工艺和装备领域已步入世界前列,现已具备了最低板厚1.0mm超薄纤维板制造生产能力,但低于1mm例如0.8mm超薄纤维板未有相关技术公开,0.8mm超薄纤维板在产品应用和新领域拓展方面存在极大的产业需求。On the one hand, ultra-thin fiberboard can be used as a decorative material to replace the existing high-tech wood and poplar decorative veneer to produce high-end furniture such as super-flat, skin-feeling, and high-gloss, and solve the problems of carbonization, unevenness, and cracking on the surface of furniture after decoration; On the other hand, it can be used as a balanced finish for high-end solid wood composite flooring, with the characteristics of high strength, deformation resistance, and strong dimensional stability; Paper materials are more environmentally friendly. At present, there is little research on ultra-thin fiberboard in other countries. China has entered the forefront of the world in the field of ultra-thin fiberboard production technology and equipment, and now has the production capacity of ultra-thin fiberboard with a minimum thickness of 1.0mm, but less than 1mm such as 0.8mm There is no relevant technology disclosure for ultra-thin fiberboard, and there is a huge industrial demand for 0.8mm ultra-thin fiberboard in terms of product application and new field expansion.

发明内容Contents of the invention

本发明鉴于以上技术问题研发而成,目的在于提供薄至0.8mm、密度达0.9g/m3以上的超薄高密度纤维板及其制备方法,据此获得性能良好的低醛超薄纤维板。The present invention is developed in view of the above technical problems, and its purpose is to provide an ultra-thin high-density fiberboard with a thickness of 0.8mm and a density of more than 0.9g/ m3 and its preparation method, thereby obtaining a low-aldehyde ultra-thin fiberboard with good performance.

本发明提供以下技术方案:The invention provides the following technical solutions:

1.一种低醛超薄纤维板的制备方法,其包括步骤:1. A preparation method for low-aldehyde ultra-thin fiberboard, which comprises steps:

蒸煮处理:将合格木片进行蒸煮,蒸煮压力为7.5bar~8.0bar,蒸煮温度为160℃~165℃,蒸煮时间为3.5min~4.0min;Cooking treatment: Cook the qualified wood chips, the cooking pressure is 7.5bar~8.0bar, the cooking temperature is 160℃~165℃, and the cooking time is 3.5min~4.0min;

热磨处理:对蒸煮后的木片添加融化的58#全精炼石蜡并进行热磨,得到50-100目的木纤维;Thermal grinding treatment: add melted 58# fully refined paraffin wax to the cooked wood chips and perform thermal grinding to obtain 50-100 mesh wood fibers;

施胶处理:在干燥管道内对木纤维的表面均匀施加脲醛树脂胶和助剂;Glue sizing treatment: uniformly apply urea-formaldehyde resin glue and additives to the surface of wood fiber in the drying pipeline;

干燥处理:对施胶后的木纤维进行干燥,得到含水率6.0%~6.5%的铺装料;Drying treatment: dry the wood fiber after sizing to obtain a paving material with a moisture content of 6.0% to 6.5%;

铺装处理:将铺装料铺装成连续的板坯带,设置目标板材厚度0.8mm,纤维板密度1050Kg/m3Pavement treatment: Pave the pavement material into a continuous slab strip, set the target plate thickness to 0.8mm, and the fiberboard density to 1050Kg/m 3 ;

热压处理:将板坯带送至热压机进行热压,热压机布置四个连续的压力区间,按板坯带前进方向,设置四个压力区间的热压温度逐渐降低,并且至少后三个压力区间的热压压力逐渐增大,Hot-pressing treatment: Send the slab belt to a hot-pressing machine for hot-pressing. The hot-pressing machine arranges four continuous pressure zones. According to the advancing direction of the slab belt, the hot-pressing temperature in the four pressure zones is set to gradually decrease, and at least The hot pressing pressure in the three pressure ranges increases gradually,

其中,板坯入口处设置为6.8mm,并且按板坯带前进方向设置:第一区间的热压温度为175℃、第二区间的热压温度为165℃、第三区间的热压温度为140℃、第四区间的热压温度为130℃;第一区间的热压压力为35bar~50bar、第二区间的热压压力为25bar~55bar、第三区间的热压压力为55bar~80bar、第四区间的热压压力为120bar~150bar;热压速度均为105m/min。Among them, the slab entrance is set to 6.8mm, and is set according to the advancing direction of the slab belt: the hot-pressing temperature in the first section is 175°C, the hot-pressing temperature in the second section is 165°C, and the hot-pressing temperature in the third section is 140°C, the hot-pressing temperature in the fourth section is 130°C; the hot-pressing pressure in the first section is 35bar-50bar, the hot-pressing pressure in the second section is 25bar-55bar, the hot-pressing pressure in the third section is 55bar-80bar, The hot pressing pressure in the fourth section is 120bar-150bar; the hot pressing speed is 105m/min.

其中,所述合格木片为长度5cm~8cm、宽度5cm~8cm、厚度1cm~2cm,且含水率55%~65%的木片。Wherein, the qualified wood chips are wood chips with a length of 5 cm to 8 cm, a width of 5 cm to 8 cm, a thickness of 1 cm to 2 cm, and a moisture content of 55% to 65%.

其中,所述合格木片的制备包括水洗处理:将长度5cm~8cm、宽度5cm~8cm、厚度1cm~2cm的刨片进行水洗和脱水,并控制木片含水率为55%~65%;Wherein, the preparation of the qualified wood chips includes washing treatment: washing and dehydrating planed chips with a length of 5 cm to 8 cm, a width of 5 cm to 8 cm, and a thickness of 1 cm to 2 cm, and controlling the moisture content of the wood chips to 55% to 65%;

其中,所述合格木片的制备还包括预热处理:将水洗后的木片进行预热,控制预热温度在90℃~98℃。Wherein, the preparation of the qualified wood chips further includes preheating: preheating the washed wood chips, and controlling the preheating temperature at 90°C to 98°C.

其中,所述合格木片的制备还包括压形处理:将预热后的木片由变径螺旋挤压形成木塞。Wherein, the preparation of the qualified wood chips also includes pressing treatment: the preheated wood chips are extruded by a variable-diameter screw to form a cork.

其中,58#全精炼石蜡相对成品纤维板体积其添加量为8kg/m3~10kg/m3Among them, the amount of 58# fully refined paraffin relative to the volume of the finished fiberboard is 8kg/m 3 -10kg/m 3 .

其中,脲醛树脂胶的固含量为49%~53%,相对绝干纤维重量其施加量为11%~13%。Among them, the solid content of the urea-formaldehyde resin glue is 49%-53%, and its application amount is 11%-13% relative to the dry fiber weight.

其中,所述助剂包括固化剂和石蜡,固化剂为氯化铵,相对绝干纤维重量其添加量为0.40%~0.50%;石蜡的固含量为100%,相对绝干纤维重量其添加量为0.7%~0.9%。Wherein, the auxiliary agent includes a curing agent and paraffin, the curing agent is ammonium chloride, and its addition amount is 0.40% to 0.50% relative to the weight of the dry fiber; the solid content of the paraffin is 100%, and its addition amount is 0.7% to 0.9%.

其中,所述热压处理前还包括预压处理:将铺装好的板坯带进行预压,预压压力为95bar~130bar。Wherein, the pre-pressing treatment is also included before the hot-pressing treatment: pre-pressing the paved slab belt, and the pre-pressing pressure is 95bar-130bar.

2.一种由上述制备方法制备的低醛超薄纤维板。2. A low-aldehyde ultra-thin fiberboard prepared by the above-mentioned preparation method.

影响0.8mm超薄纤维板制备的因素主要为纤维热磨质量、干燥含水率及热压参数。热磨纤维尺寸粗细及热压参数影响超薄纤维板强度,干燥含水率影响超薄纤维板是否发生爆板现象,含水率过高超薄纤维板表面容易鼓泡,含水率过低超薄纤维板上下表面容易分层。通过本工艺制备的0.8mm超薄纤维板的性能测试均满足中国林产工业协会T/CNFPIA3007-2019《超薄高密度纤维板》。The main factors affecting the preparation of 0.8mm ultra-thin fiberboard are the quality of fiber thermal grinding, drying moisture content and hot pressing parameters. The size and thickness of hot-milled fibers and hot-pressing parameters affect the strength of ultra-thin fiberboard, and the dry moisture content affects whether the ultra-thin fiberboard will burst. layered. The performance tests of the 0.8mm ultra-thin fiberboard prepared by this process all meet the China Forestry Products Industry Association T/CNFPIA3007-2019 "ultra-thin high-density fiberboard".

具体实施方式Detailed ways

实施方式中没有特别声明的情况下,数值范围“A~B”指A以上(大于或等于A)B以下(小于或等于B),当提到常温或室温,通常指22~25℃之间,根据不同工艺有时还会指20~28℃之间。有些工艺为做温度限定时,一般认为在所述常温或室温下进行。If there is no special statement in the implementation, the numerical range "A~B" refers to above A (greater than or equal to A) and below B (less than or equal to B). , According to different processes, it sometimes refers to between 20 and 28 °C. Some processes are generally considered to be carried out at the normal temperature or room temperature when the temperature is limited.

实际产业中不同领域对常温或室温存在不同的理解,但就专利法的实施应用来看,应以能实现发明目的为根据对待具体的适用范围,不局限于某一领域的狭义经验。本领域技术人员还应理解,当提到某一温度下的实际意义是,对温度的控制并非绝对的恒温,往往会出现一定的浮动性,该浮动在某种场景下可能会超过一度,甚至更多,只要可以达到实验目的都应视为在该温度下。Different fields in the actual industry have different understandings of normal temperature or room temperature, but from the perspective of the implementation and application of the patent law, the specific scope of application should be treated on the basis of the realization of the purpose of the invention, not limited to the narrow experience of a certain field. Those skilled in the art should also understand that when referring to a certain temperature, the actual meaning is that the control of the temperature is not an absolute constant temperature, and there will often be a certain degree of fluctuation, which may exceed one degree in certain scenarios, or even More, as long as the purpose of the experiment can be achieved, it should be regarded as being at this temperature.

所限定的温度,可以是对所用设备上的温度控制输入,实际中某时点的温度取决于机器设备的特殊性和反应当时的情况。所限定的温度也可以是人员指令的目标,实际控制中可能涉及温度变化的一段时间,甚至包括一个上下反复浮动的过程,例如当检测到温度低于所限定温度,对反应器加热,当高于所限定温度,对反应器冷却,整体上维持指令的温度。除了温度,实施方式中还将出现有关厚度、密度或压力、工艺变化速率等的工艺,对其本质的理解参照上述温度的界定原理。The defined temperature can be the temperature control input on the equipment used. In practice, the temperature at a certain point depends on the particularity of the equipment and the situation at that time. The defined temperature can also be the target of personnel instructions. The actual control may involve a period of temperature change, even including a process of repeated fluctuations. For example, when the temperature is detected to be lower than the defined temperature, the reactor is heated. At the defined temperature, the reactor is cooled to maintain the commanded temperature overall. In addition to temperature, there will also be processes related to thickness, density or pressure, process change rate, etc. in the embodiment. For the understanding of its essence, refer to the above-mentioned definition principle of temperature.

本实施方式提供超薄纤维板的制备工艺,所述超薄纤维板是指厚度<1.5mm的纤维板,尤其指厚度<1.5mm的纤维板的高密度纤维板,其中高密度的要求特指密度≥0.8g/m3。根据本工艺,尤其用于制备薄至0.8mm、密度可达0.9g/m3以上的超薄高密度纤维板。This embodiment provides a preparation process for ultra-thin fiberboards. The ultra-thin fiberboards refer to fiberboards with a thickness of <1.5mm, especially high-density fiberboards with a thickness of <1.5mm. m 3 . According to this process, it is especially used for preparing ultra-thin high-density fiberboards as thin as 0.8mm and with a density of more than 0.9g/m 3 .

在某些研究中,出现了无醛超薄纤维板的提案,但是无醛胶承受高成本的缺陷,另一方面在纤维板的制备中添加脲醛树脂胶往往面临对纤维板性能的影响。相对于此,本发明采用一种制备低醛释放率的超薄纤维板的方案。根据该制备方案,不但可以达到更薄更高密度纤维板的目标,还能满足力学性能要求,尤其符合中国林产工业协会T/CNFPIA3007-2019《超薄高密度纤维板》中多项标准要求。In some studies, there have been proposals for formaldehyde-free ultra-thin fiberboards, but formaldehyde-free glue suffers from high costs. On the other hand, adding urea-formaldehyde resin glue in the preparation of fiberboards often faces the impact on the performance of fiberboards. In contrast, the present invention adopts a scheme for preparing ultra-thin fiberboards with low aldehyde release rate. According to this preparation scheme, not only the goal of thinner and higher density fiberboard can be achieved, but also the mechanical performance requirements can be met, especially in line with the requirements of multiple standards in China Forest Products Industry Association T/CNFPIA3007-2019 "Ultra Thin High Density Fiberboard".

本实施方式将详细介绍发明所提供的低醛超薄纤维板的制备工艺,并且在要求保护的技术方案内可以根据本领域技术人员的理解包含相应的限定内容。本发明同时还要求,据此工艺所制备的低醛超薄纤维板产品的保护。This implementation mode will introduce the preparation process of the low-aldehyde ultra-thin fiberboard provided by the invention in detail, and the corresponding limitations may be included in the claimed technical solution according to the understanding of those skilled in the art. The invention also requires the protection of the low-aldehyde ultra-thin fiberboard products prepared according to the process.

刨片:Planer:

对原木材料进行刨片,工艺要求是木片长、宽尺寸范围均为5cm~8cm,厚为1cm~2cm。可采用刨片机对原木材料进行刨片,但本发明对原材和刨片机不做限定,实施例中将以新西兰辐射松原木材料进行验证。刨片方法不限于对木材的直接刨片,也可以和削片机以及打碎机配合利用。也可从市场上采购要求工艺的刨花。Plane the log material, the technical requirements are that the length and width of the wood chips are both 5cm-8cm, and the thickness is 1cm-2cm. A flaking machine can be used to plan the log material, but the present invention does not limit the raw material and the flaking machine. In the embodiment, the New Zealand radiata pine log material will be used for verification. The planing method is not limited to direct planing of wood, and can also be used in conjunction with chippers and chippers. Wood shavings with required craftsmanship can also be purchased from the market.

水洗:Washing:

刨片送至水洗机,从水洗机中出来后直接进入螺旋脱水机,螺旋脱水机脱出水可回流水洗工段。通过对木片进行水洗可清除附者在木片上的泥沙、污垢和非金属杂物,且在一定程度上可取代磁选工序,很好地降低污染物和沉淀物。The shavings are sent to the washing machine, and directly enter the screw dehydrator after coming out of the washing machine, and the water from the screw dehydrator can be returned to the washing section. Washing the wood chips can remove the silt, dirt and non-metallic impurities attached to the wood chips, and to a certain extent, it can replace the magnetic separation process to reduce pollutants and sediments.

另一方面对木片进行水洗还可提高或控制木片的含水率。木片的含水率过高,易在热磨前获得较长的纤维,长纤维易翘曲,在成型时易熱聚、结团,不利于纤维之间的交织络合,影响湿板坯的铺装质量。木片的含水率过低,容易出现木片软化不透,纤维分离困难,且纤维切断几率大,导致粗短、过细纤维增多,降低了纤维分离质量。On the other hand, washing wood chips can also improve or control the moisture content of wood chips. If the moisture content of wood chips is too high, it is easy to obtain longer fibers before thermal grinding. Long fibers are easy to warp, and they are easy to heat aggregate and agglomerate during molding, which is not conducive to interweaving and complexing between fibers, and affects the laying of wet slabs. Install quality. If the moisture content of wood chips is too low, it is easy to soften and impervious to wood chips, and it is difficult to separate fibers, and the probability of fiber cutting is high, resulting in an increase in thick, short, and ultra-fine fibers, which reduces the quality of fiber separation.

通过水洗和脱水过程,可以将木片含水率控制在含水率55%~65%,优选控制在53%~62%,更优选在50%左右。水洗工序利于调整水洗参数,木片的含水率可以得到有效控制。另外,热磨时纤维间相互摩擦起主导作用,磨盘接触变成次要因素,通过控制水洗木片含水率在50%左右,可避免纤维过度压溃和切断,保证纤维分离质量。Through the water washing and dehydration process, the moisture content of the wood chips can be controlled at a moisture content of 55%-65%, preferably 53%-62%, more preferably about 50%. The water washing process is beneficial to adjust the washing parameters, and the moisture content of wood chips can be effectively controlled. In addition, the friction between fibers plays a dominant role during thermal grinding, and the contact with the grinding disc becomes a secondary factor. By controlling the moisture content of washed wood chips at about 50%, excessive crushing and cutting of fibers can be avoided, and the quality of fiber separation can be guaranteed.

预处理:Preprocessing:

作为优选或可选的实施方式,水洗和脱水后的合格木片可进行预热处理。具体地,将合格木片经密闭传送带进入热磨机前的预热缓冲料仓临时储存,控制预热温度在90℃~98℃。所述合格木片指经清洗后的干净木片,尤其指木片长、宽尺寸范围均为5cm~8cm,厚为1cm~2cm,且含水率在55%~65%范围内的木片。As a preferred or optional implementation, the qualified wood chips after washing and dehydration can be preheated. Specifically, the qualified wood chips are temporarily stored in the preheated buffer bin before the heat refiner through the closed conveyor belt, and the preheating temperature is controlled at 90°C to 98°C. The qualified wood chips refer to cleaned wood chips, especially wood chips with a length and width of 5 cm to 8 cm, a thickness of 1 cm to 2 cm, and a moisture content of 55% to 65%.

根据需求,在将木片送入蒸煮器软化处理前还可以由变径螺旋挤压形成木塞。值得一提的是,木片含水率过高,会降低木片与进料螺旋间的摩擦力,且木材在受压缩时挤出水分,这些水分相当于润滑剂,使木片与螺旋面间产生打滑现象,不利于木塞的形成。木片的含水率过低,增加了进料螺旋的轴向力,加速轴承的磨损,且木塞不密实易造成反喷。According to the requirement, before the wood chip is sent to the digester for softening treatment, it can also be extruded by a variable diameter screw to form a cork. It is worth mentioning that if the moisture content of the wood chips is too high, the friction between the wood chips and the feeding screw will be reduced, and when the wood is compressed, water will be squeezed out. The water is equivalent to a lubricant, causing slippage between the wood chips and the screw , is not conducive to the formation of cork. The moisture content of the wood chips is too low, which increases the axial force of the feeding screw and accelerates the wear of the bearing, and the cork is not dense and may cause back spraying.

蒸煮:Cooking:

预处理或水洗后的合格木片送入立式蒸煮器进行蒸煮软化处理。0.8mm超薄纤维板所需纤维制备时,蒸煮压力为7.5bar~8.0bar,温度160℃~165℃,蒸煮处理时间为3.5min~4.0min。Qualified wood chips after pretreatment or washing are sent to the vertical digester for cooking and softening treatment. When preparing the fibers required for 0.8mm ultra-thin fiberboard, the cooking pressure is 7.5bar to 8.0bar, the temperature is 160°C to 165°C, and the cooking time is 3.5min to 4.0min.

经过蒸煮软化木材,可以利用水对纤维素的非结晶区、半纤维素和木素进行润胀,为分子剧烈运动提供自由体积空间,木材经水热处理后,一部分半纤维素易分解溶解成液态,纤维素无定型区分子链上的游离羟基吸附水分,使纤维素间隙中水膜增厚,分子间距离增大,吸引力减小,便于在外力作用下产生相对滑移。After cooking and softening the wood, water can be used to swell the amorphous region of cellulose, hemicellulose and lignin, providing free volume space for the violent movement of molecules. After the wood is hydrothermally treated, part of the hemicellulose is easily decomposed and dissolved into a liquid state. , The free hydroxyl groups on the molecular chains of the cellulose amorphous region absorb water, which thickens the water film in the cellulose gap, increases the distance between molecules, and reduces the attractive force, which is convenient for relative slippage under the action of external force.

热磨:Hot grinding:

蒸煮好的木片送入热磨机中,并向其中添加融化后的58#全精炼石蜡,依据成品纤维板的体积控制添加量,本申请提供的实施例中控制为8~10kg/m3。经蒸煮后的纤维原料在热磨机的压力和转动作用下,得到50-100目的木纤维。热磨时间一般不必严格限定,但优选控制在2.8min~3min。合格纤维送入干燥管道。The cooked wood chips are put into a heat refiner, and the melted 58# fully refined paraffin wax is added thereto, and the amount of addition is controlled according to the volume of the finished fiberboard, which is controlled at 8-10kg/m 3 in the examples provided by this application. The fibrous raw material after cooking is under the pressure and rotation of the heat mill to obtain 50-100 mesh wood fibers. Generally, the heat grinding time does not need to be strictly limited, but it is preferably controlled at 2.8 minutes to 3 minutes. Qualified fibers are sent into the drying pipeline.

通过热磨处理,均化木片含水率,获得适于后段工序的纤维分离效率和纤维分离均匀性。已知分离纤维是一个十分复杂的物理力学和化学转化过程,由于其理论十分复杂,加之难于观察和模拟,分离纤维机理的研究,很难进行量化,但良好的热磨质量考虑是纤维制板的重要因素。Through thermal grinding treatment, the moisture content of wood chips is homogenized, and the fiber separation efficiency and fiber separation uniformity suitable for the subsequent process are obtained. It is known that separating fibers is a very complicated physical, mechanical and chemical transformation process. Due to its complex theory, coupled with difficulties in observation and simulation, it is difficult to quantify the research on the mechanism of separating fibers, but good thermal grinding quality considerations are important factor.

调施胶:Adjust glue:

将胶黏剂及助剂通过各自的计量管道以喷雾状进行施加,使其与干燥管道中的纤维流形成冲击式的搅混状态,保证物料均匀分布在纤维表面。本发明胶黏剂采用脲醛树脂胶,固体含量49~53%,优选51%,相对绝干纤维比重其施加量11~13%,优选12.5%。所述助剂包括固化剂和石蜡。Adhesives and additives are sprayed through their respective metering pipes to form an impact mixing state with the fiber flow in the drying pipe to ensure that the materials are evenly distributed on the fiber surface. The adhesive of the present invention adopts urea-formaldehyde resin glue, with a solid content of 49-53%, preferably 51%, and an applied amount of 11-13%, preferably 12.5%, relative to the dry fiber specific gravity. The auxiliary agent includes curing agent and paraffin.

对固化剂的种类不做限制,在本领域技术人员能够理解本发明的范围内可以适当选择,具体可以选用单组分固化剂,也可以选用多组分固化剂,或者复合型固化剂,相对绝干纤维比重添加量为0.40%~0.50%,优选0.45%,本发明所提供实施例中优选采用氯化铵。另外,石蜡的固含量为100%,相对绝干纤维比重其添加量为0.7~0.9%,优选0.8%。The type of curing agent is not limited, and can be appropriately selected within the scope of the understanding of the present invention by those skilled in the art. Specifically, a single-component curing agent can be selected, a multi-component curing agent, or a composite curing agent can be selected. The added amount of dry fiber specific gravity is 0.40%-0.50%, preferably 0.45%, and ammonium chloride is preferably used in the examples provided by the present invention. In addition, the paraffin wax has a solid content of 100%, and its added amount is 0.7-0.9%, preferably 0.8%, relative to the dry fiber specific gravity.

干燥:dry:

热磨磨出纤维加上施胶使得纤维含水率达到58%~62%,需要通过干燥系统将纤维中的水分由液相转变成气相而蒸发掉,控制干燥系统入口管道温度100℃~110℃,控制出口管道温度55℃~68℃,控制最终纤维含水率为6.0%~6.5%。干燥含水率影响超薄纤维板是否发生爆板现象,含水率过高超薄纤维板表面容易鼓泡,含水率过低超薄纤维板上下表面容易分层。The fiber is ground by heat grinding and sizing to make the moisture content of the fiber reach 58% to 62%. The moisture in the fiber needs to be transformed from liquid phase to gas phase through the drying system and evaporated. , control the temperature of the outlet pipeline at 55°C to 68°C, and control the moisture content of the final fiber to 6.0% to 6.5%. The dry moisture content affects whether the ultra-thin fiberboard will burst. If the moisture content is too high, the surface of the ultra-thin fiberboard is prone to bubbling, and if the moisture content is too low, the upper and lower surfaces of the ultra-thin fiberboard are prone to delamination.

铺装:Paving:

通过铺装成型机将纤维铺成连续的板坯带,以目标板材厚度0.8mm,纤维板密度1050Kg/m3,板坯带宽度1250mm控制铺装工艺。根据密度要求,铺装机通过螺旋下料装置进行下料,铺装高度偏差为±3mm。Lay the fiber into a continuous slab belt by a paving forming machine, and control the paving process with a target board thickness of 0.8mm, a fiberboard density of 1050Kg/m 3 , and a slab belt width of 1250mm. According to the density requirement, the paving machine unloads through the screw unloading device, and the pavement height deviation is ±3mm.

预压:Preload:

铺装好的板坯带通过输送带运送至预压机,设置预压压力为95bar~130bar。The paved slab belt is transported to the pre-pressing machine through the conveyor belt, and the pre-pressing pressure is set at 95bar to 130bar.

热压:Hot pressing:

进行预压后的板坯带输送至热压机,板坯入口处设置为6.8mm,热压机分为4个连续压力区间,按板坯带前进的方向,设置1区热压温度175℃、2区热压温度165℃、3区热压温度140℃、4区热压温度130℃。热压速度为105m/min。1区压力为35bar~50bar、2区压力为25bar~55bar、3区压力为55bar~80bar、4区压力为120bar~150bar。表现The pre-pressed slab belt is transported to the hot press machine. The slab entrance is set to 6.8mm. The hot press machine is divided into 4 continuous pressure zones. According to the direction of the slab belt, set the hot pressing temperature in Zone 1 to 175°C , The hot-pressing temperature in Zone 2 is 165°C, the hot-pressing temperature in Zone 3 is 140°C, and the hot-pressing temperature in Zone 4 is 130°C. The hot pressing speed is 105m/min. The pressure in zone 1 is 35bar-50bar, the pressure in zone 2 is 25bar-55bar, the pressure in zone 3 is 55bar-80bar, and the pressure in zone 4 is 120bar-150bar. Performance

后处理:Post-processing:

根据需要,热压成型的板材经过输送带传至翻板架上,进行冷却,后续进行堆垛打包。According to needs, the hot-pressed plates are transferred to the turnover frame through the conveyor belt, cooled, and then stacked and packed.

根据发明构思提供以下实施例。各实施例中未单独提及的工艺采用了上述各工段中记载的优选方式。各实施例的性能指标依据以下测试方法测试。The following examples are provided in accordance with the inventive concept. For the processes not mentioned separately in each embodiment, the preferred methods described in the above-mentioned sections were adopted. The performance index of each embodiment is tested according to the following test methods.

密度测定:按GB/T 17657-2013中4.2密度测定方法进行。含水率测定:按GB/T17657-2013中4.3规定的含水率测定方法进行。静曲强度、弹性模量测定:按GB/T 17657-2013中4.7规定的静曲强度、弹性模量测定方法进行。内结合强度测定:按GB/T 17657-2013中4.11规定的内胶合强度测定方法进行。吸水率测定:按GB/T17657-2013中4.6规定的24h吸水率测定方法进行。甲醛释放量:按GB18580-2017中甲醛释放量的测定规定进行。Density measurement: according to GB/T 17657-2013 in 4.2 Density measurement method. Determination of moisture content: according to the determination method of moisture content specified in 4.3 of GB/T17657-2013. Determination of static bending strength and elastic modulus: according to the determination method of static bending strength and elastic modulus specified in 4.7 of GB/T 17657-2013. Determination of internal bonding strength: according to the determination method of internal bonding strength specified in 4.11 of GB/T 17657-2013. Determination of water absorption: according to the 24h water absorption determination method specified in 4.6 of GB/T17657-2013. Formaldehyde release: According to the determination of formaldehyde release in GB18580-2017.

实施例1Example 1

将新西兰辐射松原木材料用刨片机刨片,刨片后木片长、宽尺寸范围均为5cm~8cm,厚为1cm~2cm。将刨好的木片经水洗脱水后经密闭传送带进入热磨机前的预热缓冲料仓临时储存,经变径螺旋挤压后形成木塞送入立式蒸煮器进行蒸煮软化处理,蒸煮压力为7.5bar,蒸煮温度为162℃,蒸煮处理时间为3.5min。蒸煮好的木片被送入热磨机中进行热磨,向其中添加融化后的58#全精炼石蜡,添加量为8kg/m3,得到50-100目的松木纤维,合格的纤维进入干燥管道。脲醛树脂胶、氯化铵和石蜡通过各自的计量管道以喷雾状进行施加,使其与管道的纤维流形成冲击式的搅混状态,物料均匀分布在纤维表面,其中脲醛树脂胶固体含量51%、施加量12.5%,氯化铵固体含量20%、添加比例0.4%,石蜡固含量100%、添加量0.8%。热磨磨出纤维加上施胶使得纤维通过干燥系统进行干燥,控制干燥系统入口管道温度100℃,控制出口管道温度60℃,纤维含水率为7%,通过铺装成型机将纤维铺成连续的板坯带,设置目标板材0.8mm超薄纤维板密度为1050Kg/m3,板坯带宽度为1250mm,根据密度要求,铺装机通过螺旋下料装置进行下料,铺装高度偏差为±3mm。将铺装好的板坯带通过输送带运送至预压机,预压压力为100bar。预压后的板坯带输送至热压机,板坯入口处设置6.8mm,热压机分为4个连续压力区间,按照板坯带前进的方向,设置1区热压温度175℃、2区热压温度165℃、3区热压温度140℃、4区热压温度130℃,热压速度为105m/min,1区压力为50bar、2区压力为55bar、3区压力为80bar、4区压力为150bar。热压成型的板材经过输送带传至翻板架上,进行冷却,后续进行堆垛打包。The New Zealand radiata pine log material is planed with a planer. After planing, the length and width of the wood chips range from 5 cm to 8 cm, and the thickness is 1 cm to 2 cm. After the planed wood chips are washed and dehydrated, they enter the preheated buffer silo in front of the thermal mill through a closed conveyor belt for temporary storage, and are extruded by a variable diameter screw to form a cork and sent to a vertical digester for cooking and softening treatment. The cooking pressure is 7.5bar, the cooking temperature is 162°C, and the cooking time is 3.5min. The cooked wood chips are sent to a thermal grinder for thermal grinding, and the melted 58# fully refined paraffin wax is added therein in an amount of 8kg/ m3 to obtain 50-100 mesh pine fibers, and qualified fibers enter the drying pipeline. The urea-formaldehyde resin glue, ammonium chloride and paraffin are sprayed through their respective metering pipelines to form an impact mixing state with the fiber flow in the pipeline, and the materials are evenly distributed on the fiber surface. The solid content of the urea-formaldehyde resin glue is 51%, The application amount is 12.5%, the ammonium chloride solid content is 20%, the addition ratio is 0.4%, the paraffin wax solid content is 100%, and the addition amount is 0.8%. The fiber is ground by heat grinding and sizing is used to make the fiber dry through the drying system. The temperature of the inlet pipe of the drying system is controlled at 100°C, the temperature of the outlet pipe is controlled at 60°C, and the moisture content of the fiber is 7%. For the slab belt, set the density of the target 0.8mm ultra-thin fiberboard to 1050Kg/m 3 , and the width of the slab belt to 1250mm. According to the density requirements, the paving machine will be unloaded through the screw feeding device, and the paving height deviation will be ±3mm . The paved slab belt is transported to the pre-pressing machine through the conveyor belt, and the pre-pressing pressure is 100bar. The pre-pressed slab belt is transported to the hot press machine. The slab entrance is set at 6.8mm. The hot press machine is divided into 4 continuous pressure zones. According to the direction of the slab belt, set the hot pressing temperature in zone 1 to 175°C and 2 The hot-pressing temperature in zone 165°C, the hot-pressing temperature in zone 3 is 140°C, the hot-pressing temperature in zone 4 is 130°C, the hot-pressing speed is 105m/min, the pressure in zone 1 is 50bar, the pressure in zone 2 is 55bar, the pressure in zone 3 is 80bar, and the pressure in zone 4 is 105m/min. The zone pressure is 150 bar. The hot-pressed plates are transferred to the turnover frame through the conveyor belt, cooled, and then stacked and packed.

实施例2Example 2

将新西兰辐射松原木材料用刨片机刨片,刨片后木片长、宽尺寸范围均为5cm~8cm,厚为1cm~2cm。将刨好的木片经水洗脱水后经密闭传送带进入热磨机前的预热缓冲料仓临时储存,经变径螺旋挤压后形成木塞送入立式蒸煮器进行蒸煮软化处理,蒸煮压力为8.0bar,蒸煮温度为160℃,蒸煮处理时间为4.0min。蒸煮好后的木片被送入热磨机中进行热磨,向其中添加融化后的58#全精炼石蜡,添加量为10kg/m3,得到50-100目的松木纤维,合格的纤维进入干燥管道。脲醛树脂胶、氯化铵和石蜡通过各自的计量管道以喷雾状进行施加,使其与管道的纤维流形成冲击式的搅混状态,物料均匀分布在纤维表面,其中脲醛树脂胶固体含量51%、施加量12.5%,氯化铵固体含量20%、添加比例0.45%,石蜡固含量100%、添加量0.8%。热磨磨出纤维通过干燥系统进行干燥,控制干燥系统入口管道温度110℃,控制出口管道温度55℃,纤维含水率为6.7%。通过铺装成型机将纤维铺成连续的板坯带,设置目标板材0.8mm超薄纤维板密度为1050Kg/m3,板坯带宽度为1250mm,根据密度要求,铺装机通过螺旋下料装置进行下料,铺装高度偏差为±3mm。将铺装好的板坯带通过输送带运送至预压机,预压压力为95bar。预压后的板坯带输送至热压机,板坯入口处设置6.8mm,热压机分为4个连续压力区间,按照板坯带前进的方向,设置1区热压温度175℃、2区热压温度165℃、3区热压温度140℃、4区热压温度130℃,热压速度为105m/min,1区压力为35bar、2区压力为40bar、3区压力为55bar、4区压力为130bar。热压成型的板材经过输送带传至翻板架上,进行冷却,后续进行堆垛打包。The New Zealand radiata pine log material is planed with a planer. After planing, the length and width of the wood chips range from 5 cm to 8 cm, and the thickness is 1 cm to 2 cm. After the planed wood chips are washed and dehydrated, they enter the preheated buffer silo in front of the thermal mill through a closed conveyor belt for temporary storage, and are extruded by a variable diameter screw to form a cork and sent to a vertical digester for cooking and softening treatment. The cooking pressure is 8.0bar, the cooking temperature is 160°C, and the cooking time is 4.0min. The cooked wood chips are sent to the thermal grinder for thermal grinding, and the melted 58# fully refined paraffin wax is added to it, and the addition amount is 10kg/ m3 to obtain 50-100 mesh pine fibers, and the qualified fibers enter the drying pipeline . The urea-formaldehyde resin glue, ammonium chloride and paraffin are sprayed through their respective metering pipelines to form an impact mixing state with the fiber flow in the pipeline, and the materials are evenly distributed on the fiber surface. The solid content of the urea-formaldehyde resin glue is 51%, The application amount is 12.5%, the ammonium chloride solid content is 20%, the addition ratio is 0.45%, the paraffin wax solid content is 100%, and the addition amount is 0.8%. The fibers produced by heat grinding are dried through the drying system. The temperature of the inlet pipe of the drying system is controlled at 110°C, the temperature of the outlet pipe is controlled at 55°C, and the moisture content of the fiber is 6.7%. Lay the fiber into a continuous slab belt through the paving forming machine, set the density of the target 0.8mm ultra-thin fiberboard to 1050Kg/m 3 , and set the width of the slab belt to 1250mm. For blanking, the pavement height deviation is ±3mm. The paved slab belt is transported to the pre-pressing machine through the conveyor belt, and the pre-pressing pressure is 95bar. The pre-pressed slab belt is transported to the hot press machine. The slab entrance is set at 6.8mm. The hot press machine is divided into 4 continuous pressure zones. According to the direction of the slab belt, set the hot pressing temperature in zone 1 to 175°C and 2 The hot-pressing temperature in zone 165°C, the hot-pressing temperature in zone 3 is 140°C, the hot-pressing temperature in zone 4 is 130°C, the hot-pressing speed is 105m/min, the pressure in zone 1 is 35bar, the pressure in zone 2 is 40bar, the pressure in zone 3 is 55bar, and the pressure in zone 4 is 105m/min. The zone pressure is 130 bar. The hot-pressed plates are transferred to the turnover frame through the conveyor belt, cooled, and then stacked and packed.

实施例3Example 3

将新西兰辐射松原木材料用刨片机刨片,刨片后木片长、宽尺寸范围均为5cm~8cm,厚为1cm~2cm。将刨好的木片经水洗脱水后经密闭传送带进入热磨机前的预热缓冲料仓临时储存,经变径螺旋挤压后形成木塞送入立式蒸煮器进行蒸煮软化处理,蒸煮压力为7.5bar,热磨温度为165℃,蒸煮处理时间为4.0min。蒸煮好后的木片被送入热磨机中进行热磨,向其中添加融化后的58#全精炼石蜡,添加量为9kg/m3,得到50-100目的松木纤维,合格的纤维进入干燥管道。脲醛树脂胶、氯化铵和石蜡通过各自的计量管道以喷雾状进行施加,使其与管道的纤维流形成冲击式的搅混状态,物料均匀分布在纤维表面,其中脲醛树脂胶固体含量51%、施加量12.5%,氯化铵固体含量20%、添加比例0.5%,石蜡固含量100%、添加量0.8%。通过干燥系统进行干燥,控制干燥系统入口管道温度110℃;控制出口管道温度68℃,纤维含水率为6.5%。通过铺装成型机将纤维铺成连续的板坯带,设置目标板材0.8mm超薄纤维板密度为1050Kg/m3,板坯带宽度为1250mm,根据密度要求,铺装机通过螺旋下料装置进行下料,铺装高度偏差为±3mm。将铺装好的板坯带通过输送带运送至预压机,预压压力为130bar。预压后的板坯带输送至热压机,板坯入口处设置6.8mm,热压机分为4个连续压力区间,按照板坯带前进的方向,设置1区热压温度175℃、2区热压温度165℃、3区热压温度140℃、4区热压温度130℃,热压速度为105m/min,1区压力为40bar、2区压力为25bar、3区压力为60bar、4区压力为120bar。热压成型的板材经过输送带传至翻板架上,进行冷却,后续进行堆垛打包。The New Zealand radiata pine log material is planed with a planer. After planing, the length and width of the wood chips range from 5 cm to 8 cm, and the thickness is 1 cm to 2 cm. After the planed wood chips are washed and dehydrated, they enter the preheated buffer silo in front of the thermal mill through a closed conveyor belt for temporary storage, and are extruded by a variable diameter screw to form a cork and sent to a vertical digester for cooking and softening treatment. The cooking pressure is 7.5bar, the heat grinding temperature is 165°C, and the cooking time is 4.0min. The cooked wood chips are sent to the thermal grinder for thermal grinding, and the melted 58# fully refined paraffin wax is added to it, and the addition amount is 9kg/ m3 to obtain 50-100 mesh pine fibers, and the qualified fibers enter the drying pipeline . The urea-formaldehyde resin glue, ammonium chloride and paraffin are sprayed through their respective metering pipelines to form an impact mixing state with the fiber flow in the pipeline, and the materials are evenly distributed on the fiber surface. The solid content of the urea-formaldehyde resin glue is 51%, The application amount is 12.5%, the ammonium chloride solid content is 20%, the addition ratio is 0.5%, the paraffin wax solid content is 100%, and the addition amount is 0.8%. Drying is carried out through the drying system, and the temperature of the inlet pipe of the drying system is controlled at 110°C; the temperature of the outlet pipe is controlled at 68°C, and the moisture content of the fiber is 6.5%. Lay the fiber into a continuous slab belt through the paving forming machine, set the density of the target 0.8mm ultra-thin fiberboard to 1050Kg/m 3 , and set the width of the slab belt to 1250mm. For blanking, the pavement height deviation is ±3mm. The paved slab belt is transported to the pre-pressing machine through the conveyor belt, and the pre-pressing pressure is 130bar. The pre-pressed slab belt is transported to the hot press machine. The slab entrance is set at 6.8mm. The hot press machine is divided into 4 continuous pressure zones. According to the direction of the slab belt, set the hot pressing temperature in zone 1 to 175°C and 2 The hot-pressing temperature in zone 165°C, the hot-pressing temperature in zone 3 is 140°C, the hot-pressing temperature in zone 4 is 130°C, the hot-pressing speed is 105m/min, the pressure in zone 1 is 40bar, the pressure in zone 2 is 25bar, the pressure in zone 3 is 60bar, and the pressure in zone 4 is 105m/min. The zone pressure is 120 bar. The hot-pressed plates are transferred to the turnover frame through the conveyor belt, cooled, and then stacked and packed.

根据实施例1~3制备得到的纤维板依据上文测试标准进行测试,结果如下表。The fiberboards prepared according to Examples 1-3 were tested according to the above test standards, and the results are shown in the following table.

表1Table 1

Figure BDA0004146805760000091
Figure BDA0004146805760000091

需理解的是,此处所描述的具体实施例仅仅用于解释相关发明,而非对该发明的限定。在权利要求所限定的范围内本发明可以进行各种变形。不同的实施方式或实施例、以及常用技术手段的组合获得的新的变形等也应视为包含在本发明范围之内。It should be understood that the specific embodiments described here are only used to explain related inventions, not to limit the invention. Various modifications can be made to the present invention within the scope defined by the claims. Different implementations or examples, and new deformations obtained by combining common technical means should also be considered to be included within the scope of the present invention.

Claims (10)

1.一种低醛超薄纤维板的制备方法,1. A preparation method of low-aldehyde ultra-thin fiberboard, 其特征在于,包括步骤:It is characterized in that, comprising steps: 蒸煮处理:将合格木片进行蒸煮,蒸煮压力为7.5bar~8.0bar,蒸煮温度为160℃~165℃,蒸煮时间为3.5min~4.0min;Cooking treatment: Cook the qualified wood chips, the cooking pressure is 7.5bar~8.0bar, the cooking temperature is 160℃~165℃, and the cooking time is 3.5min~4.0min; 热磨处理:对蒸煮后的木片添加融化的58#全精炼石蜡并进行热磨,得到50-100目的木纤维;Thermal grinding treatment: add melted 58# fully refined paraffin wax to the cooked wood chips and perform thermal grinding to obtain 50-100 mesh wood fibers; 施胶处理:在干燥管道内对木纤维的表面均匀施加脲醛树脂胶和助剂;Glue sizing treatment: uniformly apply urea-formaldehyde resin glue and additives to the surface of wood fiber in the drying pipeline; 干燥处理:对施胶后的木纤维进行干燥,得到含水率6.0%~6.5%的铺装料;Drying treatment: dry the wood fiber after sizing to obtain a paving material with a moisture content of 6.0% to 6.5%; 铺装处理:将铺装料铺装成连续的板坯带,设置目标板材厚度0.8mm,纤维板密度1050Kg/m3Pavement treatment: Pave the pavement material into a continuous slab strip, set the target plate thickness to 0.8mm, and the fiberboard density to 1050Kg/m 3 ; 热压处理:将板坯带送至热压机进行热压,热压机布置四个连续的压力区间,按板坯带前进方向,设置四个压力区间的热压温度逐渐降低,并且至少后三个压力区间的热压压力逐渐增大,Hot-pressing treatment: Send the slab belt to a hot-pressing machine for hot-pressing. The hot-pressing machine arranges four continuous pressure zones. According to the advancing direction of the slab belt, the hot-pressing temperature in the four pressure zones is set to gradually decrease, and at least The hot pressing pressure in the three pressure ranges increases gradually, 其中,板坯入口处设置为6.8mm,并且按板坯带前进方向设置:第一区间的热压温度为175℃、第二区间的热压温度为165℃、第三区间的热压温度为140℃、第四区间的热压温度为130℃;第一区间的热压压力为35bar~50bar、第二区间的热压压力为25bar~55bar、第三区间的热压压力为55bar~80bar、第四区间的热压压力为120bar~150bar;热压速度均为105m/min。Among them, the slab entrance is set to 6.8mm, and is set according to the advancing direction of the slab belt: the hot-pressing temperature in the first section is 175°C, the hot-pressing temperature in the second section is 165°C, and the hot-pressing temperature in the third section is 140°C, the hot-pressing temperature in the fourth section is 130°C; the hot-pressing pressure in the first section is 35bar-50bar, the hot-pressing pressure in the second section is 25bar-55bar, the hot-pressing pressure in the third section is 55bar-80bar, The hot pressing pressure in the fourth section is 120bar-150bar; the hot pressing speed is 105m/min. 2.如权利要求1所述的制备方法,其中,2. preparation method as claimed in claim 1, wherein, 所述合格木片为长度5cm~8cm、宽度5cm~8cm、厚度1cm~2cm,且含水率55%~65%的木片。The qualified wood chips are wood chips with a length of 5 cm to 8 cm, a width of 5 cm to 8 cm, a thickness of 1 cm to 2 cm, and a moisture content of 55% to 65%. 3.如权利要求2所述的制备方法,其中,3. preparation method as claimed in claim 2, wherein, 所述合格木片的制备包括水洗处理:将长度5cm~8cm、宽度5cm~8cm、厚度1cm~2cm的刨片进行水洗和脱水,并控制木片含水率为55%~65%。The preparation of the qualified wood chips includes water washing: washing and dehydrating planed chips with a length of 5 cm to 8 cm, a width of 5 cm to 8 cm, and a thickness of 1 cm to 2 cm, and controlling the moisture content of the wood chips to 55% to 65%. 4.如权利要求3所述的制备方法,其中,4. preparation method as claimed in claim 3, wherein, 所述合格木片的制备还包括预热处理:将水洗后的木片进行预热,控制预热温度在90℃~98℃。The preparation of the qualified wood chips also includes preheating: preheating the washed wood chips, and controlling the preheating temperature at 90°C to 98°C. 5.如权利要求4所述的制备方法,其中,5. preparation method as claimed in claim 4, wherein, 所述合格木片的制备还包括压形处理:将预热后的木片由变径螺旋挤压形成木塞。The preparation of the qualified wood chips also includes pressing treatment: the preheated wood chips are extruded by a variable-diameter screw to form a cork. 6.如权利要求1所述的制备方法,其中,6. preparation method as claimed in claim 1, wherein, 58#全精炼石蜡相对成品纤维板体积其添加量为8kg/m3~10kg/m3The amount of 58# fully refined paraffin relative to the volume of the finished fiberboard is 8kg/m 3 -10kg/m 3 . 7.如权利要求1所述的制备方法,其中,7. preparation method as claimed in claim 1, wherein, 脲醛树脂胶的固含量为49%~53%,相对绝干纤维重量其施加量为11%~13%。The solid content of the urea-formaldehyde resin glue is 49%-53%, and its application amount is 11%-13% relative to the dry fiber weight. 8.如权利要求1所述的制备方法,其中,8. preparation method as claimed in claim 1, wherein, 所述助剂包括固化剂和石蜡,Described auxiliary agent comprises solidifying agent and paraffin, 固化剂为氯化铵,相对绝干纤维重量其添加量为0.40%~0.50%;The curing agent is ammonium chloride, and its addition amount is 0.40% to 0.50% relative to the dry fiber weight; 石蜡的固含量为100%,相对绝干纤维重量其添加量为0.7%~0.9%。The solid content of the paraffin wax is 100%, and its addition amount is 0.7% to 0.9% relative to the dry fiber weight. 9.如权利要求1所述的制备方法,其中,9. preparation method as claimed in claim 1, wherein, 所述热压处理前还包括预压处理:将铺装好的板坯带进行预压,预压压力为95bar~130bar。Before the hot-pressing treatment, pre-pressing treatment is also included: pre-pressing the paved slab belt, and the pre-pressing pressure is 95bar-130bar. 10.一种由权利要求1~9任一项所述的制备方法制备的低醛超薄纤维板。10. A low-aldehyde ultra-thin fiberboard prepared by the preparation method described in any one of claims 1-9.
CN202310305352.7A 2023-03-23 2023-03-23 Low-formaldehyde ultrathin fiber board and preparation method thereof Withdrawn CN116373063A (en)

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