CN116210947A - A method for preparing a drop-type tobacco stick-shaped aerosol-generating product - Google Patents
A method for preparing a drop-type tobacco stick-shaped aerosol-generating product Download PDFInfo
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- A24B15/10—Chemical features of tobacco products or tobacco substitutes
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Abstract
本发明公开一种落料式烟草棒型气溶胶生成制品的制备方法,其特征在于,其包括以下步骤:(A)于湿度小于15%的环境下,在烟草颗粒表面包覆包衣层,得到具有包衣层的烟草颗粒;(B)落料装置(N1)将具有包衣层的烟草颗粒装入预留有空腔的气溶胶生成制品中,然后将气溶胶生成制品转移至湿度大于40%的环境下静置,静置过程中包衣层被活化,将烟草颗粒粘结成烟草棒(9),得到烟草棒型气溶胶生成制品,其中预留的空腔即为烟草棒(9)所在位置。本发明在烟草颗粒表面包覆包衣层后直接落料装填入气溶胶生成制品的空腔中,然后将气溶胶生成制品转移至湿度大于40%的环境下静置,静置过程中包衣层被活化,将烟草颗粒粘结成烟草棒(9),该方法既实现了外管内烟草颗粒成棒,也解决了落料对位困难的问题。
The invention discloses a method for preparing a blanking tobacco rod-type aerosol-generating product, which is characterized in that it comprises the following steps: (A) coating the surface of tobacco particles with a coating layer in an environment with a humidity less than 15%, Tobacco particles with a coating layer are obtained; (B) the blanking device (N1) packs the tobacco particles with a coating layer into an aerosol generating product with a cavity reserved, and then the aerosol generating product is transferred to a place with a humidity greater than Stand still under 40% environment, the coating layer is activated during the standing process, the tobacco particles are bonded into a tobacco rod (9), and a tobacco rod-shaped aerosol-generating product is obtained, wherein the reserved cavity is the tobacco rod ( 9) Location. In the present invention, after coating the coating layer on the surface of the tobacco particles, the material is directly filled into the cavity of the aerosol generating product, and then the aerosol generating product is transferred to an environment with a humidity greater than 40% to stand still. The coating layer is activated, and the tobacco particles are bonded into a tobacco rod (9). This method not only realizes the tobacco particles in the outer tube into a rod, but also solves the problem of difficult positioning of blanking.
Description
技术领域technical field
本发明涉及加热不燃烧卷烟技术领域,具体涉及一种落料式烟草棒型气溶胶生成制品的制备方法。The invention relates to the technical field of heat-not-burn cigarettes, in particular to a method for preparing a blanking tobacco stick-type aerosol-generating product.
背景技术Background technique
随着消费者对于健康问题的重视及对卷烟产品个性化体验的需求提升,烟草行业不断响应消费者的需求升级,开发出各种具有降焦减害的吸烟制品。其中,加热卷烟由于其卷烟加热方式不同于传统卷烟制品,使其能够在满足消费者对于卷烟产品的感官需求的同时提供更加健康的抽吸体验。As consumers pay more attention to health issues and demand for personalized experience of cigarette products, the tobacco industry continues to respond to the upgrading of consumer demand and develops various smoking products with reduced tar and harm. Among them, heated cigarettes can provide a healthier smoking experience while satisfying consumers' sensory needs for cigarette products because their cigarette heating methods are different from traditional cigarette products.
现有技术中颗粒型加热卷烟的发烟材料通常为松散的烟草颗粒,由于松散的烟草颗粒无法固定,必须用灌装的方式装入外管中,灌装的方法限制其只能针对单独管材批量灌装,生产效率低。另外,烟草颗粒段两侧需要通过封口纸和封堵件的方式固定颗粒,次品率高。The smoking material of granular heating cigarettes in the prior art is usually loose tobacco particles. Since the loose tobacco particles cannot be fixed, they must be filled into the outer tube by filling. The filling method is limited to a single tube. Batch filling, low production efficiency. In addition, both sides of the tobacco particle section need to fix the particles by means of sealing paper and plugging parts, and the defective rate is high.
为了解决散装烟草颗粒的问题,部分研究者将松散的烟草颗粒通过粘接剂粘合到一起形成圆柱状形式的烟芯棒,然后在烟芯棒包裹上卷烟纸后,单独作为气溶胶发生基质棒,然后通过灌装、卷接或复合的工艺将其和其他元件组合制作为气溶胶产生制品。由于这种发烟段已经是一个整体的圆柱状烟芯棒,不会出现烟草颗粒掉落散落的问题,所以也就无需再设置位于发烟段两侧的封口膜或者封堵件。另外,也就不限定灌装的形式将其和其他元件组合制作气溶胶产生制品。In order to solve the problem of loose tobacco particles, some researchers bonded loose tobacco particles together through an adhesive to form a cylindrical form of cigarette core rod, and then used it as an aerosol-generating substrate alone after the cigarette core rod was wrapped with cigarette paper rod, and then combine it with other components to make aerosol-generating products through filling, rolling or compounding processes. Since the smoking section is already a whole cylindrical cigarette core rod, there will be no problem of falling and scattering of tobacco particles, so there is no need to set sealing films or blocking parts on both sides of the smoking section. In addition, the form of filling is not limited and it can be combined with other components to make aerosol-generating products.
目前,将散落的烟草颗粒通过热熔胶粘合制备圆柱状烟芯棒的方法是,直接将散落的烟草颗粒放到搅拌器中,再向搅拌器中加入大量的粘接剂,然后搅拌混合均匀后挤出成型或者模压成型,然后在烟芯棒包裹上卷烟纸后,单独作为气溶胶发生基质棒,然后通过灌装、卷接或复合的工艺将其和其他元件组合制作为气溶胶产生制品。这种方法制备出的烟芯棒存在两个方面的问题,第一方面是烟草棒孔隙率低的问题:1、由于搅拌过程中加入了大量的包衣层材料,在冷却后,烟芯棒中相邻烟草颗粒之间的间隙中也存在冷却后的包衣层材料,这导致烟芯棒孔隙率低,轴向的透气量小;2、如果为了避免第一个问题,直接在搅拌混合的过程中加入较少的包衣层材料,又会导致包衣层材料分散不均匀,表面均没有包覆包衣层的烟草颗粒相邻,导致无法粘合,出现烟草颗粒散落的问题;3、还有一个更关键的问题是,加入了大量的包衣层材料还会导致每个烟草颗粒表面的施加了大量的包衣层材料,从而严重影响烟草颗粒受热后气溶胶的释放,其实本质上,包衣层的目的仅仅是为了让散落的烟草颗粒粘合,但是并不希望烟草颗粒不粘合的地方也被包衣层材料覆盖,而影响气溶胶释放。第二方面是挤压或者模压成型后再卷烟纸卷制耗时耗力的问题:1、如果采用挤压的方法成型,则需要另配备挤出装置,而采用模压的方法成型,则需要另外设置脱模的工序;2、成型得到烟草棒后需要再另行加卷制工序,即成棒和卷制需要两步工序,耗时耗力;3、如果成棒后利用灌装的工艺将其和其他元件组合制作为气溶胶产生制品,由于松散的烟草颗粒已经成型为一体的烟草棒,其再罐装入气溶胶生成制品的空腔中时,存在对位困难的问题,如果烟草棒没有与空管完全对位准确,则会出现外管变形或者烟草棒散开的情况,降低成品率。At present, the method of preparing cylindrical cigarette core rods by bonding scattered tobacco particles by hot melt adhesive is to directly put the scattered tobacco particles in the blender, then add a large amount of adhesive to the blender, and then stir and mix Extruded or molded after uniformity, and then after the cigarette core rod is wrapped with cigarette paper, it is used as an aerosol generating matrix rod alone, and then combined with other components to produce aerosol generating by filling, rolling or compounding products. There are two problems in the smoke core rod prepared by this method, the first aspect is the problem of low porosity of the tobacco rod: 1, due to adding a large amount of coating material in the stirring process, after cooling, the smoke core rod There is also a cooled coating layer material in the gap between adjacent tobacco particles in the middle, which leads to low porosity of the smoke core rod and small axial air flow; 2. If in order to avoid the first problem, directly stir and mix Adding less coating layer material in the process will cause the coating layer material to disperse unevenly, and the tobacco particles that are not coated with the coating layer on the surface are adjacent to each other, resulting in failure to bond and the problem of tobacco particles scattering; 3 , Another more critical issue is that adding a large amount of coating material will also cause a large amount of coating material to be applied on the surface of each tobacco particle, which will seriously affect the release of aerosol after the tobacco particle is heated. In general, the purpose of the coating layer is only to bind the scattered tobacco particles, but it is not expected that the non-adhesive parts of the tobacco particles will also be covered by the coating layer material, which will affect the release of aerosol. The second aspect is the problem of time-consuming and labor-intensive rolling of cigarette paper after extrusion or molding: 1. If the extrusion method is used to form, an additional extrusion device is required, and the molding method is used. Set the process of demoulding; 2. After forming the tobacco rod, another rolling process is required, that is, two steps are required for forming the rod and rolling, which is time-consuming and labor-intensive; 3. If the rod is formed and filled with the process Combined with other components to make an aerosol-generating product, since the loose tobacco particles have been formed into an integrated tobacco rod, when it is re-packed into the cavity of the aerosol-generating product, there is a problem of alignment difficulties. If the tobacco rod does not If the alignment with the empty tube is accurate, the outer tube will be deformed or the tobacco rod will be scattered, which will reduce the yield.
因此,如何将散状烟草颗粒粘合形成发烟棒,又保证发烟棒孔隙率和烟雾量,且可以通过落料罐装的方式制备,是人们关心的问题。Therefore, how to bond loose tobacco particles to form a smoking rod, and ensure the porosity and smoke volume of the smoking rod, and how to prepare it by blanking and canning is a problem that people care about.
为了解决以上问题,提出本发明。In order to solve the above problems, the present invention has been proposed.
发明内容Contents of the invention
为了进行区分,本发明中包裹有纸管的称之为气溶胶发生基质棒,而卷烟纸内的发烟材料称之为烟草棒。In order to distinguish, in the present invention, the one wrapped with the paper tube is called aerosol generating matrix rod, while the smoking material in the cigarette paper is called tobacco rod.
本发明第一方面提供一种落料式烟草棒型气溶胶生成制品的制备方法,其包括以下步骤:The first aspect of the present invention provides a method for preparing a drop-type tobacco stick-type aerosol-generating product, which includes the following steps:
(A)于湿度小于15%的环境下,在烟草颗粒表面包覆包衣层,得到具有包衣层的烟草颗粒;(A) coating the surface of the tobacco particles with a coating layer in an environment with a humidity of less than 15%, to obtain tobacco particles with a coating layer;
(B)落料装置N1将具有包衣层的烟草颗粒装入预留有空腔的气溶胶生成制品中,然后将气溶胶生成制品转移至湿度大于40%的环境下静置,静置过程中所述包衣层被活化,将烟草颗粒粘结成烟草棒9,得到烟草棒型气溶胶生成制品,其中预留的空腔即为烟草棒9所在位置。(B) The blanking device N1 packs the tobacco particles with a coating layer into the aerosol generating product with a cavity reserved, and then transfers the aerosol generating product to an environment with a humidity greater than 40% to stand still. The standing process The coating layer described above is activated, and the tobacco particles are bonded into a
烟草颗粒表面可以仅部分包覆包衣层,也可以全部包覆包衣层。The surface of the tobacco particles may be only partially covered with the coating layer, or may be completely covered with the coating layer.
优选地,所述包衣层选自羟丙基甲基纤维素、羟丙基纤维素、聚维酮、羧甲基纤维素钠、微晶纤维素、聚乙二醇、聚乙烯醇、瓜尔胶中的一种或多种。Preferably, the coating layer is selected from the group consisting of hydroxypropylmethylcellulose, hydroxypropylcellulose, povidone, sodium carboxymethylcellulose, microcrystalline cellulose, polyethylene glycol, polyvinyl alcohol, guarana One or more of Er gum.
优选地,步骤(A)中在烟草颗粒表面形成包衣层的方法为:将烟草颗粒加入搅拌桶内,边喷洒包衣层材料边进行搅拌,搅拌5-25分钟后停止喷洒包衣层材料,继续搅拌5-20分钟;然后将表面具有包衣层材料的烟草颗粒输送至流化床中用冷风进行风干,风干时间为5-10分钟,直至包衣层材料在烟草颗粒表面干燥并形成包衣层;其中包衣层材料占烟草颗粒重量的百分比为40-75%。Preferably, the method for forming a coating layer on the surface of the tobacco particles in step (A) is: adding the tobacco particles into the mixing tank, stirring while spraying the coating layer material, and stopping spraying the coating layer material after stirring for 5-25 minutes , and continue to stir for 5-20 minutes; then transport the tobacco particles with the coating layer material on the surface to the fluidized bed for air-drying with cold wind for 5-10 minutes until the coating layer material is dried on the surface of the tobacco particles and forms Coating layer; wherein the coating material accounts for 40-75% of the weight of the tobacco particles.
优选地,步骤(A)中还可以向搅拌桶内加入烟草提取物、发烟剂、香精香料与烟草颗粒和包衣层材料一并搅拌。加入烟草提取物、发烟剂、香精香料可以进一步提高烟雾量,烟气浓度和香气量,从而提高烟气品质。Preferably, in the step (A), the tobacco extract, smoking agent, flavor and fragrance can also be added into the mixing barrel together with the tobacco particles and the coating material and stirred together. Adding tobacco extracts, fumigants, flavors and fragrances can further increase the amount of smoke, the concentration of smoke and the amount of aroma, thereby improving the quality of smoke.
优选地,所述烟草棒9的孔隙率为40-80%。Preferably, the porosity of the
优选地,步骤(A),向经过流化床干燥后表面具有包衣层的烟草颗粒中加入表面没有包衣层的第二部分烟草颗粒,继续搅拌5-15分钟,其中第二部分烟草颗粒占烟草颗粒总重量的5-30%。Preferably, in step (A), a second part of tobacco particles without a coating layer on the surface is added to the tobacco particles having a coating layer on the surface after fluidized bed drying, and the stirring is continued for 5-15 minutes, wherein the second part of tobacco particles 5-30% of the total weight of tobacco particles.
通过分批搅拌的方法目的在于提高烟草棒的孔隙率。如果采用一批搅拌,即直接将散落的烟草颗粒放到搅拌器中,再向搅拌器中加入大量的包衣层材料,然后搅拌混合均匀,待包衣后活化包衣层将烟草颗粒粘接成棒,该方法存在的问题是:烟芯棒中相邻烟草颗粒之间的间隙中也存在冷却后的包衣层材料,这导致烟芯棒孔隙率低,轴向的透气量小。另外,每个烟草颗粒表面的施加了大量的包衣层材料,从而严重影响烟草颗粒受热后气溶胶的释放。The method by batch stirring aims at increasing the porosity of the tobacco rod. If a batch of stirring is used, that is, the scattered tobacco particles are directly put into the blender, and then a large amount of coating material is added to the blender, and then stirred and mixed evenly, after coating, the coating layer is activated to bond the tobacco particles The problem with this method is that the cooled coating layer material also exists in the gap between adjacent tobacco particles in the smoke core rod, which leads to low porosity of the smoke core rod and small axial air flow. In addition, a large amount of coating material is applied on the surface of each tobacco particle, thereby seriously affecting the release of aerosol after the tobacco particle is heated.
本发明向烟草颗粒表面包覆包衣层可以采用分批搅拌的方法,先取一部分烟草颗粒和包衣层材料放置到搅拌器内搅拌,待这部分烟草颗粒表面部分有包衣层材料后,再将第二部分烟草颗粒加入搅拌器中进行搅拌,这样可以保证只有一部分烟草颗粒表面有包衣层材料,第二部分烟草颗粒在第二批加入,其表面没有包衣层材料,或者包衣层材料很少,在粘合过程中,混合后的烟草颗粒接触,只要其中一个烟草颗粒表面有包衣层材料就可以实现两者的粘合,无需两个颗粒上面都有包衣层材料,这样可以避免两个颗粒粘合后,两者之间形成的缝隙中的包衣层材料冷却后堵塞孔隙,本发明在实现粘合的基础上保证烟芯棒轴向的通气量和孔隙率。In the present invention, the coating layer can be applied to the surface of the tobacco particles by stirring in batches. First, take a part of the tobacco particles and the coating material and place them in the mixer for stirring. After the coating layer material is present on the surface of the tobacco particles, then Add the second part of the tobacco particles into the stirrer and stir, so that only a part of the tobacco particles has the coating layer material on the surface, and the second part of the tobacco particles is added in the second batch, and there is no coating layer material on the surface, or the coating layer There are few materials. During the bonding process, the mixed tobacco particles are in contact. As long as one of the tobacco particles has a coating layer material on the surface, the bonding of the two can be achieved. There is no need for coating layer materials on both particles, so that After the two particles are bonded, the coating layer material in the gap formed between the two particles will be prevented from blocking the pores after cooling, and the invention ensures the axial ventilation and porosity of the cigarette core rod on the basis of bonding.
进一步的,本发明通过控制添加的包衣层材料量,还可以保证第一部分烟草颗粒只有部分表面具有包衣层材料,由于烟草颗粒部分表面未施加包衣层材料,可以很好的保证烟草颗粒受热后气溶胶的释放,保证烟雾量。Further, the present invention can also ensure that only part of the surface of the first part of the tobacco particles has the coating layer material by controlling the amount of the coating layer material added. Since the coating layer material is not applied to the surface of the tobacco particle part, it can be well ensured that the tobacco particles The release of aerosol after heating ensures the amount of smoke.
优选地,步骤(B)中可利用蒸汽施加装置提供湿度大于40%的环境。Preferably, in step (B), a steam application device can be used to provide an environment with a humidity greater than 40%.
实际生产过程中是否设置蒸汽施加装置依据实际情况而定,如果环境空气中的水蒸气已经足以保证烟草颗粒表面的包衣层被活化,且粘接性已经足够将散状的发烟颗粒粘接,这不需要额外的再设置蒸汽施加装置。如果环境空气中的水蒸气量不足,这可以额外设置蒸汽施加装置以提供水蒸气,保证环境湿度。Whether to install a steam application device in the actual production process depends on the actual situation. If the water vapor in the ambient air is sufficient to ensure that the coating layer on the surface of the tobacco particles is activated, and the adhesiveness is sufficient to bond the loose smoke particles , which does not require additional resetting of the steam applicator. If the amount of water vapor in the ambient air is insufficient, an additional steam application device can be provided to provide water vapor to ensure the ambient humidity.
环境湿度的控制需要和静置时长相匹配,两者共同作用以达到烟草颗粒经静置后粘接成棒。如果静置一定时间后,未粘接成型还是松散的发烟颗粒则可以通过延长静置时间或者提高环境湿度两个手段,保证散装烟草颗粒粘接成型。The control of the ambient humidity needs to match the length of the standing time, and the two work together to achieve the bonding of the tobacco particles into a stick after standing. If after standing for a certain period of time, the smoke particles that are not bonded and formed are still loose, you can ensure that the bulk tobacco particles are bonded and formed by prolonging the standing time or increasing the ambient humidity.
本发明第二方面提供一种包含本发明第一方面所述的方法制备得到的烟草棒的气溶胶产生制品,其包括外管3,以及位于所述外管3内的包裹管4、封堵部件5、和过滤部件6;The second aspect of the present invention provides an aerosol-generating product comprising the tobacco rod prepared by the method described in the first aspect of the present invention, which includes an
所述包裹管4的空腔内具有烟草棒9,所述包裹管4由复合型纸材卷制而成;所述复合型纸材包括纸层1和靠近所述烟草棒9的吸附层2。There is a
优选地,所述吸附层2包括多孔材料,所述多孔材料选自活性炭、分子筛、碳分子筛、氧化铝、硅酸钙粉末;所述吸附层2的施加量为20-90g/cm3;所述复合型纸材制备方法为,先制备所述纸层1,然后将包含多孔材料和粘合剂的混合物通过压延涂布的方法涂覆到所述纸层1上;或者,在所述纸层1制备过程中的抄纸工艺中将包含多孔材料和粘合剂的混合物涂覆到所述纸层1上。所述粘结剂选自CMC、CM80、壳聚糖、羟丙基甲基纤维素、羟丙基纤维素、聚维酮、羧甲基纤维素钠、微晶纤维素、聚乙二醇、聚乙烯醇、瓜尔胶中的一种或多种。Preferably, the
本发明复合型纸材上的吸附层不是薄薄一层,而是具有一定厚度的。本发明复合型纸材用于包裹烟草棒9的优点有:1、为了使包1层具有粘性需要在湿度多大的环境下对其进行活化,而吸附层可以吸收环境中的水分防止纸层受潮另一方面吸附层还可以吸附粘发烟草棒中包衣粘接剂中的水分。2、在烟支存放过程中发烟材料内的水分,渗到所述卷烟纸管外侧,产生黄斑。此外,发烟材料中会添加发烟剂、香精香料等,长时间放置过程中,发烟材料中的发烟剂会携带香精香料渗透到纸管外侧,产生黄斑,影响纸管外观,吸附层可以吸附发烟材料中渗出的水分或者发烟剂等物质,防止其向纸管外壁渗透,从而防止黄斑的产生。The adsorption layer on the composite paper material of the present invention is not a thin layer, but has a certain thickness. The advantages of the composite paper material of the present invention for wrapping
本发明中,烟草颗粒的制备方法可以借鉴现有技术,比如将烟粉、发烟剂等混合成浆料之后再造粒。In the present invention, the preparation method of tobacco granules can refer to the existing technology, for example, mixing tobacco powder, smoking agent, etc. into a slurry and then granulating.
优选地,所述封堵部件5和所述过滤部件6之间还具有空腔结构7。Preferably, there is a
优选地,所述空腔结构7内还包含功能材料;和/或,Preferably, the
所述空腔结构7内还包含空管功能件8。功能材料可以为现有技术中任何形式的具有降温增香功能的物质。The
本发明复合型纸材卷制成纸管后作为空管功能件8。吸附层可以吸附香精香料或者发烟剂等功能物质,由于功能物质是吸附到吸附层内部,其在抽吸过程种可以起到缓慢释放的效果,保证抽吸前后香气一致。The composite paper material of the present invention is rolled into a paper tube as an empty tube
优选地,所述外管3上具有径向贯穿所述外管3的通气孔31。当空腔结构内具有空管功能件8时,通气孔同时贯穿所述外管和所述空管功能件8。通气孔的目的在于将空气引入气溶胶生成制品内,一方面降低气溶胶的温度,另一方面降低吸阻,所以根据实际气溶胶温度和吸阻确定是否需要通气孔。当然通气孔在轴向的位置可以在封堵部件上也可以在冷却部件(即空腔结构)上。当需要设置通气孔时,优选地是打穿形成通气孔,当然也可以不打穿而是选用透气纸作为外管,只要是能够向气溶胶生成制品引入空气即可。Preferably, the
本发明因为落料时装入气溶胶生成制品的时未粘结成棒的松散的烟草颗粒,所以发烟颗粒下游的封堵部件需要对散装的烟草颗粒进行封堵,本发明封堵部件可以选用本领域常用的齿轮件。更优选地,封堵部件选自内部具有聚拢片材棒的沟槽瓦楞件或者多层的瓦楞结构等,可选择的封堵件结构可以参考本申请人申请的申请号为202210706093.4,名称为一种具有复合形式封堵件的气溶胶发生制品的专利申请,或者申请号为202210706095.3,名称为一种具有多层沟槽瓦楞结构的气溶胶发生制品的专利申请,或者申请号为202210707599.7,名称为一种具有变径气流通道封堵件的气溶胶发生制品的专利申请,或者申请号为202211037571.3,名称为一种具有多孔气溶胶生成基质棒形式封堵件的气溶胶发生制品的专利申请。In the present invention, because the loose tobacco particles that are not bonded into rods are loaded into the aerosol generating product during blanking, the plugging parts downstream of the smoke particles need to block the bulk tobacco particles, and the plugging parts of the present invention can be selected Gear parts commonly used in this field. More preferably, the plugging part is selected from grooved corrugated parts with gathered sheet rods inside or multi-layer corrugated structures, etc. The optional plugging part structure can refer to the applicant's application number 202210706093.4, named one A patent application for an aerosol generating product with a composite plugging part, or the application number is 202210706095.3, and the name is a patent application for an aerosol generating product with a multi-layer grooved corrugated structure, or the application number is 202210707599.7, and the name is A patent application for an aerosol-generating product with a variable-diameter airflow channel blocking member, or application number 202211037571.3, titled a patent application for an aerosol-generating product with a porous aerosol-generating matrix rod-shaped blocking member.
优选地,预留有空腔的气溶胶生成制品的制备方法为:通过复合卷制的方法,利用外管卷制包裹管4、封堵部件和过滤部件,得到预留有空腔的气溶胶生成制品。当封堵部件和过滤部件之间具有空管功能件8时,卷制时依次复合包裹管4、封堵部件5、空管功能件8和过滤部件6即可。Preferably, the preparation method of the aerosol generating product with a reserved cavity is as follows: through the composite rolling method, the outer tube is used to wrap the
相对于现有技术,本发明具有以下有益效果:Compared with the prior art, the present invention has the following beneficial effects:
1、烟草颗粒上包覆包衣层后,如果采用常规的方法,先挤压或者模压成型烟草棒,再卷制卷烟纸,则需要两步工序,耗时耗力。如果通过落料方法罐装入气溶胶生成制品的空腔中时,又存在对位困难的问题,但是如果不成棒,直接装填入烟草颗粒后再成棒,又存在烟草颗粒已经在外管内,无法成棒的问题。此外由于包衣层材料对于湿度很敏感,空气中水蒸气的湿度就可以将其活化提高粘性,如果烟草颗粒上包覆包衣层后不立即成烟草棒,则需要对具有包衣层的烟草颗粒密封保存,保存条件严格,且容易出现由于保存不当造成的材料浪费。本发明在烟草颗粒表面包覆包衣层后直接落料装填入气溶胶生成制品的空腔中,然后将气溶胶生成制品转移至湿度大于15%的环境下静置,静置过程中所述包衣层被活化,将烟草颗粒粘结成烟草棒9,该方法既实现了外管内烟草颗粒成棒,也解决了落料对位困难的问题。1. After the coating layer is coated on the tobacco particles, if the conventional method is used to first extrude or mold the tobacco rod, and then roll the cigarette paper, it requires two steps, which is time-consuming and labor-intensive. If the can is loaded into the cavity of the aerosol generating product by the blanking method, there is a problem of alignment difficulty, but if it cannot be formed into a rod, it is directly filled with tobacco particles and then formed into a rod, and the tobacco particles are already in the outer tube. Unable to become a stick problem. In addition, because the coating layer material is very sensitive to humidity, the humidity of water vapor in the air can activate it to improve the viscosity. If the tobacco particles are not coated with the coating layer and become a tobacco rod immediately, it is necessary to use the coating layer on the tobacco. Granules are sealed and stored under strict storage conditions, and material waste due to improper storage is prone to occur. In the present invention, after coating the coating layer on the surface of the tobacco particles, the material is directly filled into the cavity of the aerosol-generating product, and then the aerosol-generating product is transferred to an environment with a humidity greater than 15% for standing. The above-mentioned coating layer is activated, and the tobacco particles are bonded into a
2、本发明通过调控湿度调控包衣层的粘接力,从而控制具有包衣层的烟草颗粒的流动性。当于湿度小于15%的干燥环境下,包衣层没有粘接力,具有包衣层的烟草颗粒是完全松散的、流动的,可以完成落料的工序,但是当湿度大于40%后,包衣层潮解活化粘性增加,将松散的烟草颗粒粘接成发烟体,此时烟草颗粒又是不可流动的。另外,包衣层的潮解是不可逆的,当包衣层潮解粘性增加,将松散的烟草颗粒粘接成发烟体后,即便湿度在下降,其也不会丧失粘性重回包衣层的形状。2. The present invention regulates the adhesive force of the coating layer by adjusting the humidity, thereby controlling the fluidity of the tobacco particles with the coating layer. When the humidity is less than 15% in a dry environment, the coating layer has no adhesive force, and the tobacco particles with the coating layer are completely loose and fluid, and the blanking process can be completed, but when the humidity is greater than 40%, the coating layer The deliquescence activation viscosity of the coating layer increases, and the loose tobacco particles are bonded into a smoke body. At this time, the tobacco particles are immobile again. In addition, the deliquescence of the coating layer is irreversible. When the deliquescent viscosity of the coating layer increases and the loose tobacco particles are bonded into a smoke body, even if the humidity drops, it will not lose its viscosity and return to the shape of the coating layer. .
3、本发明向烟草颗粒表面包覆包衣层可以采用分批搅拌的方法,先取一部分烟草颗粒和包衣层材料放置到搅拌器内搅拌,待这部分烟草颗粒表面部分有包衣层材料后,再将第二部分烟草颗粒加入搅拌器中进行搅拌,这样可以保证只有一部分烟草颗粒表面有包衣层材料,第二部分烟草颗粒在第二批加入,其表面没有包衣层材料,或者包衣层材料很少,在粘合过程中,混合后的烟草颗粒接触,只要其中一个烟草颗粒表面有包衣层材料就可以实现两者的粘合,无需两个颗粒上面都有包衣层材料,这样可以避免两个颗粒粘合后,两者之间形成的缝隙中的包衣层材料冷却后堵塞孔隙,本发明在实现粘合的基础上保证烟芯棒轴向的通气量和孔隙率。3, the present invention can adopt the method for batch stirring to coat the coating layer on the surface of the tobacco particles, first get a part of the tobacco particles and the coating layer material and place them in the stirrer for stirring, and wait for the coating layer material to be present on the surface of this part of the tobacco particles , and then add the second part of tobacco particles into the agitator for stirring, so that only a part of the tobacco particles have the coating material on the surface, and the second part of the tobacco particles is added in the second batch, and there is no coating layer material on the surface, or coated There are very few coating materials. During the bonding process, the mixed tobacco particles are in contact. As long as one of the tobacco particles has a coating layer material on the surface, the two can be bonded, and there is no need for two particles to have a coating layer material. In this way, after the two particles are bonded, the coating layer material in the gap formed between the two will block the pores after cooling. The present invention ensures the axial ventilation and porosity of the cigarette core rod on the basis of achieving bonding. .
4、本发明通过控制添加的包衣层材料量,还可以保证第一部分烟草颗粒只有部分表面具有包衣层材料,由于烟草颗粒部分表面未施加包衣层材料,可以很好的保证烟草颗粒受热后气溶胶的释放,保证烟雾量。4. The present invention can also ensure that only part of the surface of the first part of the tobacco particles has the coating layer material by controlling the amount of the coating layer material added. Since the coating layer material is not applied to the surface of the tobacco particle part, it can be well ensured that the tobacco particles are heated After the release of aerosol, the amount of smoke is guaranteed.
5、本发明复合型纸材用到气溶胶生成制品上具有两种形式,第一种是包裹烟草棒,在烟支存放过程中发烟材料内的水分,渗到所述卷烟纸管外侧,产生黄斑。此外,发烟材料中会添加发烟剂、香精香料等,长时间放置过程中,发烟材料中的发烟剂会携带香精香料渗透到纸管外侧,产生黄斑,影响纸管外观,吸附层可以吸附发烟材料中渗出的水分或者发烟剂等物质,防止其向纸管外壁渗透,从而防止黄斑的产生。另一种是卷制成纸管后作为空管功能件8用到冷却元件,本发明复合型纸材上的吸附层不是薄薄一层,而是具有一定厚度的。吸附层可以吸附香精香料或者发烟剂等功能物质,由于功能物质是吸附到吸附层内部,其在抽吸过程种可以起到缓慢释放的效果,保证抽吸前后香气一致。5. The composite paper material of the present invention has two forms when used in aerosol-generating products. The first one is to wrap tobacco sticks. During the storage of cigarettes, the moisture in the smoking material penetrates to the outside of the cigarette paper tube. produce macula. In addition, smoking agents, flavors and fragrances will be added to the smoking materials. During the long-term storage process, the smoking agents in the smoking materials will carry flavors and fragrances and penetrate to the outside of the paper tube, resulting in macula, affecting the appearance of the paper tube. It can absorb the moisture or smoking agent and other substances exuded from the smoking material to prevent it from penetrating into the outer wall of the paper tube, thereby preventing the occurrence of macula. The other is to use the cooling element as the empty tube
6、一方面吸附层可以避免发烟材料中的发烟剂或者香精香料外渗产生的黄斑问题,另一方面发烟材料中的发烟剂或者香精香料被吸附到吸附层的多孔材料中,随着烟草棒的继续受热,多孔材料中的发烟剂或者香精香料进一步被释放,从而起到保香的作用。6. On the one hand, the adsorption layer can avoid the macula problem caused by the extravasation of the fuming agent or flavor and fragrance in the smoking material; on the other hand, the smoking agent or flavor and fragrance in the smoking material are absorbed into the porous material of the adsorption layer As the tobacco rod continues to be heated, the smoking agent or flavor and fragrance in the porous material is further released, thereby playing the role of maintaining fragrance.
附图说明Description of drawings
图1复合型纸材的结构示意图。Figure 1 Schematic diagram of the composite paper structure.
图2落料式烟草棒型气溶胶生成制品的制备工艺图。Figure 2 is a schematic diagram of the manufacturing process of the drop-type tobacco stick-shaped aerosol-generating product.
图3实施例1三段式烟支结构示意图。Fig. 3 is a schematic structural diagram of a three-stage cigarette stick in Example 1.
图4实施例2带有空腔结构的四段式烟支结构示意图。Fig. 4 is a schematic structural diagram of a four-section cigarette with a cavity structure in
附图标记在附图说明中的名称:1-纸层、2-吸附层、3-外管、4-包裹管、5-封堵部件、6-过滤部件、7-空腔结构、8-空管功能件、9-烟草棒、31-通气孔;The names of reference signs in the description of the drawings: 1-paper layer, 2-adsorption layer, 3-outer tube, 4-wrapped tube, 5-blocking component, 6-filter component, 7-cavity structure, 8- Empty pipe functional parts, 9-tobacco stick, 31-ventilation hole;
N1-落料装置。N1-Blanking device.
具体实施方式Detailed ways
下面结合实施例对本发明作进一步的详细描述。The present invention will be further described in detail below in conjunction with the examples.
本领域技术人员将会理解,下列实施例仅用于说明本发明,而不应视为限定本发明的范围。实施例中未注明具体技术或条件者,按照本领域内的文献所描述的技术或条件或者按照产品说明书进行。所用材料或设备未注明生产厂商者,均为可以通过购买获得的常规产品。Those skilled in the art will understand that the following examples are only for illustrating the present invention and should not be considered as limiting the scope of the present invention. If no specific technique or condition is indicated in the examples, it shall be carried out according to the technique or condition described in the literature in this field or according to the product specification. The materials or equipment used are not indicated by the manufacturer, and they are all conventional products that can be obtained through purchase.
本技术领域技术人员可以理解,除非特意声明,这里使用的单数形式“一”、“一个”、“所述”和“该”也可包括复数形式。应该进一步理解的是,本发明的说明书中使用的措辞“包括”是指存在所述特征、整数、步骤、操作、元件和/或组件,但是并不排除存在或添加一个或多个其他特征、整数、步骤、操作、元件、组件和/或它们的组。应该理解,当我们称元件被“连接”到另一元件时,它可以直接连接到其他元件,或者也可以存在中间元件。此外,这里使用的“连接”可以包括无线连接。Those skilled in the art will understand that unless otherwise stated, the singular forms "a", "an", "said" and "the" used herein may also include plural forms. It should be further understood that the word "comprising" used in the description of the present invention refers to the presence of said features, integers, steps, operations, elements and/or components, but does not exclude the presence or addition of one or more other features, Integers, steps, operations, elements, components, and/or groups thereof. It will be understood that when an element is referred to as being "connected" to another element, it can be directly connected to the other element or intervening elements may also be present. Additionally, "connection" as used herein may include wireless connections.
在本发明的描述中,除非另有说明,“多个”的含义是两个或两个以上。术语“内”、“上”、“下”等指示的方位或状态关系为基于附图所示的方位或状态关系,仅是为了便于描述本发明和简化描述,而不是指示或暗示所指的装置或元件必须具有特定的方位、以特定的方位构造和操作,因此不能理解为对本发明的限制。In the description of the present invention, unless otherwise specified, "plurality" means two or more. The orientation or state relationship indicated by the terms "inner", "upper", "lower" and the like are based on the orientation or status relationship shown in the drawings, and are only for the convenience of describing the present invention and simplifying the description, rather than indicating or implying the No device or element must have a specific orientation, be constructed, and operate in a specific orientation and therefore should not be construed as limiting the invention.
在本发明的描述中,需要说明的是,除非另有明确的规定和限定,术语“安装”、“连接”、“设有”应做广义理解,例如,可以是固定连接,也可以是可拆卸连接,或一体地连接;可以是机械连接,也可以是电连接;可以是直接相连,也可以通过中间媒介间接相连。对于本领域的普通技术人员而言,根据具体情况理解上述术语在本发明中的具体含义。In the description of the present invention, it should be noted that, unless otherwise specified and limited, the terms "installation", "connection" and "installation" should be interpreted in a broad sense, for example, it can be a fixed connection or an optional connection. Detachable connection, or integral connection; it can be mechanical connection or electrical connection; it can be direct connection or indirect connection through an intermediary. Those of ordinary skill in the art will understand the specific meanings of the above terms in the present invention according to specific situations.
本技术领域技术人员可以理解,除非另外定义,这里使用的所有术语包括技术术语和科学术语具有与本发明所属领域中的普通技术人员的一般理解相同的意义。还应该理解的是,诸如通用字典中定义的那些术语应该被理解为具有与现有技术的上下文中的意义一致的意义,并且除非像这里一样定义,不会用理想化或过于正式的含义来解释。Those skilled in the art can understand that, unless otherwise defined, all terms including technical terms and scientific terms used herein have the same meaning as commonly understood by one of ordinary skill in the art to which this invention belongs. It should also be understood that terms such as those defined in commonly used dictionaries should be understood to have a meaning consistent with the meaning in the context of the prior art, and unless defined as herein, are not to be interpreted in an idealized or overly formal sense explain.
实施例1Example 1
本实施例气溶胶产生制品包括外管3,以及位于所述外管3内的包裹管4、封堵部件5、和过滤部件6;The aerosol-generating product of this embodiment includes an
所述包裹管4的空腔内具有烟草棒9,所述包裹管4由复合型纸材卷制而成;所述复合型纸材包括纸层1和靠近所述烟草棒9的吸附层2。There is a
所述吸附层2为活性炭,所述吸附层2的施加量为40g/cm3;所述复合型纸材制备方法为,先制备所述纸层1,然后将包含多孔材料和粘合剂的混合物通过压延涂布的方法涂覆到所述纸层1上。所述粘结剂选自CMC。The
所述外管3上具有径向贯穿所述外管3的通气孔31。通气孔在轴向的位置在封堵部件上。The
本实施例落料式烟草棒型气溶胶生成制品的制备方法,其包括以下步骤:The preparation method of the blanking tobacco rod type aerosol generating product of this embodiment comprises the following steps:
(A)于湿度小于15%的环境下,在烟草颗粒表面包覆包衣层,得到具有包衣层的烟草颗粒;(A) coating the surface of the tobacco particles with a coating layer in an environment with a humidity of less than 15%, to obtain tobacco particles with a coating layer;
(B)落料装置N1将具有包衣层的烟草颗粒装入预留有空腔的气溶胶生成制品中,然后将气溶胶生成制品转移至湿度大于40%的环境下静置,静置过程中所述包衣层被活化,将烟草颗粒粘结成烟草棒9,得到烟草棒型气溶胶生成制品,其中预留的空腔即为烟草棒9所在位置。(B) The blanking device N1 packs the tobacco particles with a coating layer into the aerosol generating product with a cavity reserved, and then transfers the aerosol generating product to an environment with a humidity greater than 40% to stand still. The standing process The coating layer described above is activated, and the tobacco particles are bonded into a
烟草颗粒表面可以仅部分包覆包衣层,也可以全部包覆包衣层。The surface of the tobacco particles may be only partially covered with the coating layer, or may be completely covered with the coating layer.
所述包衣层选自羟丙基甲基纤维素。The coating layer is selected from hydroxypropyl methylcellulose.
步骤(A)中在烟草颗粒表面形成包衣层的方法为:将烟草颗粒加入搅拌桶内,边喷洒包衣层材料边进行搅拌,搅拌15分钟后停止喷洒包衣层材料,继续搅拌10分钟;然后将表面具有包衣层材料的烟草颗粒输送至流化床中用冷风进行风干,风干时间为10分钟,直至包衣层材料在烟草颗粒表面干燥并形成包衣层;其中包衣层材料占烟草颗粒重量的百分比为70%。The method for forming a coating layer on the surface of the tobacco particles in step (A) is as follows: adding the tobacco particles into the mixing tank, stirring while spraying the coating layer material, stopping spraying the coating layer material after stirring for 15 minutes, and continuing to stir for 10 minutes ; Then the tobacco particles with the coating layer material on the surface are transported to the fluidized bed and air-dried with cold wind for 10 minutes until the coating layer material is dried on the surface of the tobacco particles and forms a coating layer; wherein the coating layer material The percentage by weight of tobacco particles is 70%.
步骤(A)中还可以向搅拌桶内加入烟草提取物、发烟剂、香精香料与烟草颗粒和包衣层材料一并搅拌。加入烟草提取物、发烟剂、香精香料可以进一步提高烟雾量,烟气浓度和香气量,从而提高烟气品质。In the step (A), the tobacco extract, smoking agent, essence and fragrance can also be added into the mixing barrel together with the tobacco particles and the coating material and stirred together. Adding tobacco extracts, fumigants, flavors and fragrances can further increase the amount of smoke, the concentration of smoke and the amount of aroma, thereby improving the quality of smoke.
所述烟草棒9的孔隙率为70%。The porosity of the
步骤(A),向经过流化床干燥后表面具有包衣层的烟草颗粒中加入表面没有包衣层的第二部分烟草颗粒,继续搅拌10分钟,其中第二部分烟草颗粒占烟草颗粒总重量的5%。Step (A), adding a second part of tobacco particles without a coating layer on the surface to the tobacco particles having a coating layer on the surface after fluidized bed drying, and continuing to stir for 10 minutes, wherein the second part of tobacco particles accounts for the total weight of the
步骤(B)中可利用蒸汽施加装置提供湿度大于40%的环境。In step (B), a steam application device can be used to provide an environment with a humidity greater than 40%.
实施例2Example 2
本实施例气溶胶发生制品与实施例1的区别在于:The difference between the aerosol generating product of this embodiment and
所述封堵部件5和所述过滤部件6之间还具有空腔结构7。There is also a
所述空腔结构7内还包含空管功能件8。The
本实施例将复合型纸材卷制成纸管后作为空管功能件8。吸附层可以吸附香精香料或者发烟剂等功能物质,由于功能物质是吸附到吸附层内部,其在抽吸过程种可以起到缓慢释放的效果,保证抽吸前后香气一致。In this embodiment, the composite paper material is rolled into a paper tube as the empty tube
所述外管3上具有径向贯穿所述外管3的通气孔31。通气孔在轴向的位置在空腔结构上。The
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