CN116076529B - Antibacterial moisture-proof Tibetan incense and preparation method thereof - Google Patents
Antibacterial moisture-proof Tibetan incense and preparation method thereof Download PDFInfo
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- CN116076529B CN116076529B CN202211663228.XA CN202211663228A CN116076529B CN 116076529 B CN116076529 B CN 116076529B CN 202211663228 A CN202211663228 A CN 202211663228A CN 116076529 B CN116076529 B CN 116076529B
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Abstract
The invention discloses a bacteriostatic moisture-proof Tibetan incense and a preparation method thereof, and the bacteriostatic moisture-proof Tibetan incense mainly comprises the following raw materials: 70-80 parts of sandalwood, 20-30 parts of frankincense, 700-800 parts of rhizoma nardostachyos, 70-80 parts of fructus tsaoko, 80-120 parts of fine She Yaju, 30-60 parts of cinnamon, 20-30 parts of nutmeg, 60-70 parts of camphor, 30-45 parts of clove, 40-70 parts of Tibetan costustoot, 40-70 parts of costustoot, 20-30 parts of valerian parviflora, 70-90 parts of Gao Shanbai peel, 200-300 parts of pterocarpus santalinus, 1-3 parts of borneol, 20-30 parts of mukul myrrh, 20-30 parts of temple, 5-10 parts of beeswax, 40-60 parts of tarragon, 30-60 parts of azulene, 40-70 parts of boat-leaf celery, 40-60 parts of rhizoma acori graminei, 30-60 parts of pyrrosia lingua, 30-70 parts of large seed artemisia, 1-4 parts of artificial musk and 20-30 parts of small-leaved lemonade. The antibacterial moisture-proof Tibetan incense provided by the invention has the effects of inhibiting the growth of bacteria in the air, purifying the air and the like, and can calm the heart, nourish the mind, clear the heart and nourish the nature and relieve fatigue.
Description
Technical Field
The invention belongs to the technical field of Tibetan incense preparation, and particularly relates to a bacteriostatic moisture-proof Tibetan incense and a preparation method thereof.
Background
Tibetan incense is one of daily necessities of Tibetan people living in Qinghai-Tibet plateau. To date, tibetan incense has a history of 1300 years, the formula of the Tibetan incense is firstly carried in four medical classics of the name of Tibetan medicine, tibetan citizens undergo multiple proved recipe arrangement of the substitute of the famous Tibetan medicine according to the Tibetan medicine theory and the Tibetan medicine compatibility technology, and various pure natural raw materials are reasonably prepared and carefully developed by taking the Tibetan medicine theory as a guide. The books record that the product can achieve the effects of purifying qi and regulating heart, making people feel calm and pleasant no matter in worry Buddha or daily life, and is a good product for preventing and treating various epidemic diseases.
The Tibetan incense takes the five-element theory in Tibetan culture and Tibetan medicine culture as a root, combines the heavy, stable, hard and sticky effects of the earth element, the heavy, cold, wet and moist effects of the water element, the heat, light, sharp and greasy effects of the fire element, the light, moving, rough and dry effects of the wind element and the empty and deficiency effects of the empty element, so that the raw materials of the Tibetan incense are taken from five elements, the manufacturing technology follows the five elements, and the shape, taste and effect of the Tibetan incense and the five elements of a human body form a function in the using process, and the function of the Tibetan incense is better played. Meanwhile, due to the unique fragrance and continuous smoke form, people can feel calm and safe in mind and feel comfortable at the light place when burning the Tibetan incense.
The scientific research results show that the fragrance is beneficial to the health of human bodies, and the scholars in the psychophysics center of the university of Yersinia indicate that the fragrance of the aromatherapy apples can promote metabolism and improve vigilance of people. The related tests of the university of cincinnati show that if fragrance is added into the air, the working efficiency can be improved. In the 90 s of the 20 th century, foreign developers purchase or artificially plant perfume raw materials in large quantities, develop and produce various products, and obtain great economic benefits. Especially, the health-care tea has the pure nature and the health-care function, caters for the pursuit of people for returning to nature, and is popular in North America, europe, southeast Asia and other countries. It is known that part of perfume research and development institutions in China are carrying out development and research on similar products to different degrees, and even part of products are popular at home and abroad, and the Tibetan perfume has wider market and is popular in the markets at home and abroad due to the increasing population focusing on the special efficacy exerted by the Tibetan perfume.
At present, the Tibetan incense products have different quality, the manufacturing process is also different, the waterwheel or the mill is used for grinding cypress into powder to prepare the incense brick, and then the incense brick is added with other 3 to 4 components to prepare the Tibetan incense, and a certain amount of chemical spices are added for increasing the incense, but the Tibetan incense is not environment-friendly in raw materials, the manufactured Tibetan incense has insufficient strong smell and short retention time, and the research on functional Tibetan incense (such as bacteriostasis, sleep quality improvement and mental stress relief) is less, so that the Tibetan incense is unfavorable for popularization.
Therefore, according to the Tibetan incense quality standard requirement of DB54-T0080-2014, a series of scientific researches are carried out by consulting Tibetan incense ancient book name prescription, raw material standard condition, prescription and production process parameters, harmful substance detection, microorganism inhibition rate, package design content and the like, 26 natural Tibetan medicinal materials such as sandalwood, rhizoma nardostachyos, clove, red sandalwood, canba and the like are taken as raw materials, and are processed by a strict Tibetan medicinal material processing method, and then the Tibetan incense is prepared by combining a traditional Tibetan incense preparation method and a modern incense forming process, so that the Tibetan incense is prepared, and the Tibetan incense has the advantages of safety, controllable quality, unique fragrance, bacteriostasis and moisture prevention, and important effects in market development, national brand characteristic enhancement, national culture connotation and the like, and is promoted to be continuously and pioneered.
Disclosure of Invention
Aiming at the defects of the prior art, the invention aims to provide the antibacterial moisture-proof Tibetan incense which has the effects of inhibiting the growth of bacteria in the air, purifying the air and the like, and can calm the heart and nourish the mind, clear the heart and nourish the nature and relieve fatigue.
In order to achieve the above purpose, the present invention provides the following technical solutions:
The antibacterial moisture-proof Tibetan incense comprises the following raw materials in parts by weight:
70-80 parts of sandalwood, 20-30 parts of frankincense, 700-800 parts of rhizoma et radix Valerianae, 70-80 parts of fructus tsaoko, 80-120 parts of fine She Yaju, 30-60 parts of cinnamon, 20-30 parts of nutmeg, 60-70 parts of Cinnamomum camphora, 30-45 parts of clove, 40-70 parts of Tibetan costus root, 40-70 parts of costus root, 20-30 parts of valerian, 70-90 parts of Gao Shanbai skin, 200-300 parts of pterocarpus santalinus, 1-3 parts of borneol, 20-30 parts of Mokul myrrh, 20-30 parts of temple, 5-10 parts of beeswax, 20-40 parts of rhizoma pini powder, 40-60 parts of tarragon, 30-60 parts of azure blue, 40-70 parts of herba perillae, 10-30 parts of guar gum, 40-60 parts of calamus, 30-60 parts of pyrrosia lingua, 30-70 parts of sweet wormwood, 1-4 parts of musk and 20-30 parts of small-leaved lemons.
Preferably, the adhesive comprises the following raw materials in parts by weight: 73-78 parts of sandalwood, 23-28 parts of frankincense, 720-770 parts of rhizoma et radix Valerianae, 72-77 parts of fructus tsaoko, 90-110 parts of fine She Yaju, 40-50 parts of cinnamon, 23-27 parts of nutmeg, 63-67 parts of Yunnan camphor, 35-40 parts of clove, 40-60 parts of Tibetan costustoot, 45-60 parts of costustoot, 23-28 parts of valerian, 75-85 parts of Gao Shanbai peel, 220-280 parts of pterocarpus santalinus, 1-2 parts of borneol, 22-27 parts of mukul myrrh, 23-28 parts of temple, 6-9 parts of beeswax, 25-35 parts of pine powder, 45-55 parts of tarragon, 40-55 parts of azure blue, 45-65 parts of boat-leaf celery, 15-25 parts of guar gum, 45-55 parts of calamus, 40-55 parts of pyrrosia lingua, 40-60 parts of artemisia rupestris, 2-3 parts of musk and 23-28 parts of small-18 parts of small-leaved lemons.
Preferably, the adhesive comprises the following raw materials in parts by weight: 75 parts of sandalwood, 25 parts of frankincense, 750 parts of rhizoma et radix Valerianae, 75 parts of fructus tsaoko, she Yaju parts of fine, 50 parts of cinnamon, 25 parts of nutmeg, 65 parts of Yunnan camphor, 37 parts of clove, 50 parts of Tibetan costustoot, 50 parts of costustoot, 25 parts of valerian, 75 parts of Gao Shanbai skin, 250 parts of pterocarpus santalinus, 2 parts of borneol, 25 parts of mukul myrrh, 25 parts of temple, 7.5 parts of beeswax, 30 parts of shi pine powder, 50 parts of tarragon, 50 parts of azure, 50 parts of boat-leaf celery, 20 parts of guar gum, 50 parts of Tibetan calamus, 50 parts of pyrrosia lingua, 50 parts of tarragon, 2 parts of artificial musk and 25 parts of small-leaved lemons.
The Tibetan incense raw materials are properly proportioned, so that the odor generated by the raw materials is pure and odorless, and the flammability and health-care function of the Tibetan incense can be effectively ensured.
The invention also provides a preparation method of the bacteriostatic moisture-proof Tibetan incense, which comprises the following steps of:
S1, weighing raw materials according to a formula, respectively grinding sandalwood, frankincense, rhizoma et radix Valerianae, fructus Tsaoko, cinnamon, nutmeg, yunnan camphor, tibetan radix aucklandiae, cortex Cupressi, pterocarpus santalinus, borneol, mukul myrrh, templa, sweet wax, tibetan calamus, valis, tarragon, fine She Yaju, clove, valerian, tarragon, azure blue and boat-leaf celery into powder, and uniformly mixing to obtain mixed powder for standby;
s2, stir-frying small-leaved lemmaples to light yellow, grinding the small-leaved lemmaples into powder, adding highland barley wine, mixing and grinding to obtain a mixed solution A for later use;
s3, grinding the musk into fine powder, adding the fine powder into water, then adding guar gum, and uniformly stirring to obtain a mixed solution B for later use;
s4, uniformly mixing the mixed powder obtained in the S1, the mixed solution A obtained in the S2 and the mixed solution B obtained in the S3, soaking the mixture in water, and then stirring the mixture in a stirrer for the first time, and then adding the shi pinang powder, and uniformly stirring the mixture for the second time to obtain Tibetan incense mud;
s5, using a fragrance making machine to obtain a molded Tibetan fragrance, and drying the molded Tibetan fragrance in the shade indoors to obtain the antibacterial moisture-proof Tibetan fragrance.
Preferably, the particle size of the powder ground in step S1 is 80-200 mesh.
Preferably, the granularity of the powder in the step S2 is 60-100 meshes, and the dosage of the highland barley wine is 2-4 times of the total amount of the small-leaved lemmaphylls.
Preferably, the frying method in step S2 uses butter or sand.
Preferably, the water is used in step S3 in an amount of 4-6 times the total amount of guar gum and artificial musk.
Preferably, the water is used in the step S4 in an amount of 40-80% of the mass of the powder in the step S1; the primary stirring time is 2-4h; the secondary stirring time is 0.5-1h.
Preferably, the drying in the shade in the step S5 is carried out for 15-20 days at room temperature, and the environment humidity of the drying in the shade is 20-30% and is protected from light.
The bacteriostatic moisture-proof Tibetan incense provided by the invention adopts natural raw materials, has various varieties without any chemical additives, is derived from natural raw materials, is mostly aromatic plants produced in the Tibetan places, is rich in fragrance, and has unique health care and health care effects of killing bacteria, expelling dirty gas, preventing epidemic diseases, enhancing sleep and the like, wherein a small amount of raw materials are from the inner places, india, nepal and the like.
The sandalwood is a dry core material of a trunk of the santalum album of the santaceae, has the effects of promoting circulation of qi, warming spleen and stomach, stimulating appetite and relieving pain, and is used for treating cold congealing, qi stagnation, chest diaphragma, chest pain, epigastric pain, vomiting and poor appetite;
The olibanum is resin oozed from bark of olibanum tree and other plant of Oleraceae, is in form of long oval dripping emulsion, round-like granule or bonded into irregular block with different sizes, has yellowish white surface, is semitransparent, is provided with yellowish white powder, and deepens color after long-term storage; crisp and softened when heated; the broken surface has glass-like or wax-like luster; has special fragrance. Pungent and bitter in taste and warm in nature; has effects in promoting blood circulation and activating qi-flowing; menstrual flow and pain are relieved; swelling-diminishing and tissue-regenerating effects. Is mainly used for treating heart and abdomen pain; rheumatalgia; amenorrhea dysmenorrhea; traumatic injury and blood stasis pain; carbuncle and abscess; acute appendicitis; sore and ulcer are not healed; stagnation of qi and blood, pain in heart and abdomen, carbuncle, sore, toxic swelling, traumatic injury, dysmenorrhea, postpartum blood stasis, and pain;
rhizoma et radix Valerianae has effects of regulating qi-flowing, relieving pain, resolving stagnation and activating spleen;
Fructus Tsaoko, tibetan language Gagaola, also known as miscellaneous Dong Zhaibu, yila glass cloth and the like, is used as a Tibetan incense patch additive and has the effects of eliminating dampness, warming middle-jiao, eliminating phlegm and checking malaria;
thin She Yaju, has hemostatic and repercussive effects;
Cinnamon, tibetan language, tower, and prick, etc. has the effects of dispelling wind and cold, and has the effects of eliminating bad effect, diarrhea and liver disease;
nutmeg has effects of warming spleen and stomach, activating qi-flowing, astringing intestine, and relieving diarrhea;
The camphor, tibetan name acarina, also called as stroma, alamar and the like, has the effect of clearing heat and has curative effects on heart diseases, dragon fever and the like;
flos Caryophylli, tibetan medicine named Lixi, labazaar, baken, etc. has effects of dispelling pathogenic wind-cold, warming stomach, resolving food stagnation, relieving pain, and can make the product fragrant and sweet in smell, and simultaneously has effects of promoting qi and tonifying yang;
The Tibetan costustoot is also called elecampane, contains volatile oil, and the main components in the oil are alantolactone, isoalantolactone, alantolol, alantolic acid, dihydroalantolactone and the like. Pungent and bitter in taste and warm in nature; has effects in invigorating spleen, regulating stomach function, regulating qi, resolving stagnation, relieving pain, preventing miscarriage, clearing away blood heat, and dispelling pathogenic wind, and can be used for treating chronic gastritis, gastrointestinal dysfunction, intercostal neuralgia, chest wall contusion, pain due to chest pain and fetal movement, wind-heat syndrome, blood heat syndrome, and expelling parasites;
Valerian, whole herb, has the effects of clearing heat and detoxicating, dissipating swelling, setting bone and expelling pus;
Gao Shanbai bark, bark of Cupressaceae Gao Shanbai, reddish brown and longitudinal split; the branches are flat. Leaf scale shape, small shape; the male and female plants are the same or different, and the globeflower has single branches. The cones are nearly oval; seed is oval and has no wing; the wood has moderate softness and hardness, delicateness, fragrance and strong corrosion resistance. The branches and leaves have the effects of cooling blood and stopping bleeding; is mainly used for treating hematemesis, epistaxis, hematochezia, hematuria, chronic tracheitis and other diseases;
pterocarpus santalinus has the effects of giving play to natural fragrance after ignition, sterilizing and dyeing;
borneol, tibetan Gabuh, nib, kava horses and the like are used for increasing fragrance, supporting combustion, diminishing inflammation, reducing fever, clearing heat and detoxicating, and preventing cold, encephalitis and epidemic heat diseases;
the mukul myrrh has the effects of removing blood stasis, relieving pain, and externally-applied detumescence and promoting granulation;
a gum of root of radix aucklandiae of Compositae;
the artemisia rupestris has the effects of clearing heat, cooling blood, detoxifying and killing insects;
ganqing blue has the effects of harmonizing stomach and soothing liver;
The cress has pungent taste and aromatic smell, and has the effects of clearing heat and detoxicating, and treating Chen Rebing, heart heat diseases and poisoning;
Rhizoma Acori Calami has effects of eliminating phlegm, inducing resuscitation, removing dampness, invigorating stomach, killing parasites, and relieving itching, and is commonly used for treating phlegm syncope coma, apoplexy, epilepsia, palpitation, amnesia, tinnitus, deafness, food stagnation abdominal pain, dysentery diarrhea, rheumatalgia, eczema, and scabies;
the pyrrosia lingua has the effects of clearing heat and detoxicating, promoting urination and treating stranguria and stopping bleeding;
the artemisia rupestris has the effects of clearing heat, detoxicating, eliminating swelling, stopping bleeding and benefiting kidney, and is slightly sweet, bitter and cold;
The artificial musk has the functions of stopping the syndrome of unconsciousness, extremely fragrant smell, extremely strong channeling, inducing resuscitation, dredging the orifices, stopping the sleep and refreshing, increasing the fragrance, fixing and prolonging the fragrance and the diffusing range of the channeling fragrance;
the small-leaved lemmaphylls have the effects of clearing heat and detoxicating and treating heat diseases and bone heat diseases.
Compared with the prior art, the invention has the following beneficial effects:
(1) The antibacterial moisture-proof Tibetan incense is prepared by adopting natural plants as raw materials, and the sandalwood, the clove, the Tibetan costustoot, the red sandalwood and the Tibetan calamus are compounded, so that the odor emitted in the combustion process can inhibit and kill germs and prevent respiratory diseases; the powder prepared from the Nardostachys jatamansi, gao Shanbai skins and the Yunnan camphor leaves is matched with the guar gum, so that the Tibetan incense can be molded and can be used as a combustion matrix, and the guar gum burns without peculiar smell, so that the Tibetan incense smell is normally diffused, the powder does not have adverse effect on a human body after long-term use, and the powder has the effects of sterilizing, relieving mental stress and improving sleep.
(2) According to the antibacterial moisture-proof Tibetan incense, the prepared antibacterial moisture-proof Tibetan incense is prepared by uniformly mixing Tibetan incense raw materials, and the shi song powder is added after the Tibetan incense raw materials are uniformly mixed, so that the Tibetan incense can be ensured not to absorb moisture and become damp in the storage process, the service performance is influenced, and meanwhile, the shi song powder can also improve the porosity in a Tibetan incense finished product, so that the Tibetan incense is more stable in burning; the shi pine powder is odorless and tasteless when being ignited, and can not influence the odor emitted in the combustion process of the Tibetan incense, so that the Tibetan incense is pure in odor and odorless.
(3) The preparation method of the antibacterial moisture-proof Tibetan incense provided by the invention has the advantages that the preparation process is environment-friendly and pollution-free, the preparation is fine, and the grinding treatment is carried out on sandalwood, frankincense, spikenard, tsaoko cardamom, cinnamon, nutmeg, yunnan camphor, tibetan costus root, alpine cypress bark, red sandalwood, borneol, mukul myrrh, temple, sweet wax, tibetan calamus, pyrrosia lingua, tarragon, fine She Yaju, clove, valerian, tarragon, azure blue and boat-leaf celery, so that better raw material feeding is facilitated; parching small-leaved lemmaphylls, mixing with semen Avenae Nudae wine, grinding, and mixing with artificial Moschus and guar gum solution to adhere raw materials, so that Tibetan incense is not scattered, and adding semen Pini powder to improve hydrophobicity of Tibetan incense. The product retains most of effective components in the raw materials, so that the Tibetan incense has better effect, and the prepared Tibetan incense has effects of tranquillizing mind and body and heart, arresting convulsion, and tranquilizing mind and mind of a user.
Detailed Description
The technical solutions of the present invention will be clearly and completely described in connection with the embodiments, and it is obvious that the described embodiments are only some embodiments of the present invention, not all embodiments. All other embodiments, which can be made by those skilled in the art based on the embodiments of the invention without making any inventive effort, are intended to be within the scope of the invention.
The raw materials or instruments used are conventional products available commercially without identifying the manufacturer.
Example 1
A preparation method of antibacterial moisture-proof Tibetan incense comprises the following steps:
S1, weighing raw materials according to a formula, respectively grinding 75g of sandalwood, 25g of frankincense, 750g of rhizoma et radix Valerianae, 75g of fructus tsaoko, 50g of cinnamon, 25g of nutmeg, 65g of Yunnan camphor, 50g of Tibetan costus root, 50g of costus root, 75g of Gao Shanbai skin, 250g of pterocarpus santalinus, 2g of borneol, 25g of mukul myrrh, 25g of temple, 7.5g of sweet wax, 50g of Tibetan calamus, 50g of valis, 50g of artemisia apiacea, 100g of fine She Yaju, 37g of clove, 25g of valerian, 50g of artemisia rupestris, 50g of azulene and 50g of boat-shaped celery into 150-mesh powder, and uniformly mixing to obtain mixed powder for later use;
S2, parching 25g of small-leaved lemmaples with sand to light yellow, grinding into 80-mesh powder, adding 75g of highland barley wine, mixing and grinding to obtain a mixed solution A for later use;
s3, grinding 2g of artificial musk into fine powder, adding the fine powder into 100g of water, then adding 20g of guar gum, and uniformly stirring to obtain a mixed solution B for later use;
S4, uniformly mixing the powder obtained in the step S1, the mixed solution A obtained in the step S2 and the mixed solution B obtained in the step S3, soaking with 1000g of water, stirring in a stirrer for 3 hours, adding 30g of lycopodium clavatum powder, and stirring again for 1 hour to obtain Tibetan incense mud;
s5, using a perfume making machine to obtain the formed Tibetan incense by using the Tibetan incense mud obtained in the step 4, drying the formed Tibetan incense in the shade for 18d at room temperature, wherein the environment humidity of the shade is 20-30% and the formed Tibetan incense is protected from light, and thus the antibacterial moisture-proof Tibetan incense is obtained.
Example 2
A preparation method of antibacterial moisture-proof Tibetan incense comprises the following steps:
s1, weighing raw materials according to a formula, respectively grinding 70g of sandalwood, 20g of frankincense, 700g of rhizoma et radix Valerianae, 70g of fructus tsaoko, 30g of cinnamon, 20g of nutmeg, 60g of Yunnan camphor, 40g of Tibetan costus root, 40g of costus root, 70g of Gao Shanbai skin, 200g of pterocarpus santalinus, 1g of borneol, 20g of mukul myrrh, 20g of temple, 5g of sweet wax, 40g of Tibetan calamus, 30g of valis, 30g of artemisia rupestris, 80g of fine She Yaju, 30g of clove, 20g of valerian, 40g of artemisia rupestris, 30g of azulensis and 40g of boat-shaped celery into 80-mesh powder, and uniformly mixing to obtain mixed powder for standby;
s2, parching 20g of small-leaved lemmaples with sand to light yellow, grinding into 60-mesh powder, adding 40g of highland barley wine, mixing and grinding to obtain a mixed solution A for later use;
S3, grinding 1g of artificial musk into fine powder, adding the fine powder into 50g of water, then adding 10g of guar gum, and uniformly stirring to obtain a mixed solution B for later use;
S4, uniformly mixing the powder obtained in the step S1, the mixed solution A obtained in the step S2 and the mixed solution B obtained in the step S3, soaking 1000g of water, stirring in a stirrer for 2 hours once, adding 25g of pinus koraiensis powder, and stirring for 0.5 hour again to obtain Tibetan incense mud;
s5, using a perfume making machine to obtain the formed Tibetan incense by using the Tibetan incense mud obtained in the step 4, drying the formed Tibetan incense in the shade for 15d at room temperature, wherein the environment humidity of the shade is 20-30% and the formed Tibetan incense is protected from light, and thus the antibacterial moisture-proof Tibetan incense is obtained.
Example 3
A preparation method of antibacterial moisture-proof Tibetan incense comprises the following steps:
S1, weighing raw materials according to a formula, respectively grinding 80g of sandalwood, 30g of frankincense, 800g of rhizoma et radix Valerianae, 80g of fructus tsaoko, 60g of cinnamon, 30g of nutmeg, 70g of Yunnan camphor, 70g of Tibetan costus root, 70g of costus root, 90g of Gao Shanbai skin, 300g of pterocarpus santalinus, 3g of borneol, 30g of mukul myrrh, 30g of temple, 10g of sweet wax, 60g of rhizoma acori graminei, 60g of pyrrosia lingua, 70g of artemisia rupestris, 120g of fine She Yaju, 45g of clove, 30g of valerian, 60g of artemisia rupestris, 60g of azulensis and 70g of boat-shaped celery into 200-mesh powder, and uniformly mixing to obtain mixed powder for standby;
S2, frying 30g of small-leaved lemmaples with butter to be light yellow, grinding into 100-mesh powder, adding 120g of highland barley wine, mixing and grinding to obtain a mixed solution A for later use;
s3, grinding 4g of artificial musk into fine powder, adding 200g of water, then adding 30g of guar gum, and uniformly stirring to obtain a mixed solution B for later use;
s4, uniformly mixing the powder obtained in the step S1, the mixed solution A obtained in the step S2 and the mixed solution B obtained in the step S3, soaking with 1600g of water, stirring in a stirrer for 4 hours once, adding 35g of shi song powder, and stirring for 1 hour again to obtain Tibetan incense mud;
S5, using a perfume making machine to obtain the formed Tibetan incense by using the Tibetan incense mud obtained in the step 4, drying the formed Tibetan incense in the shade for 20d at room temperature, and obtaining the antibacterial moisture-proof Tibetan incense by using the shade with the environment humidity of 20-30%.
Comparative example 1
A preparation method of antibacterial moisture-proof Tibetan incense comprises the following steps:
S1, weighing raw materials according to a formula, respectively grinding 25g of frankincense, 750g of rhizoma et radix Valerianae, 75g of fructus tsaoko, 50g of cinnamon, 25g of nutmeg, 50g of Tibetan costustoot, 50g of costustoot, 75g of Gao Shanbai bark, 2g of borneol, 25g of mukul myrrh, 25g of temple, 7.5g of sweet wax, 50g of Tibetan calamus, 50g of pyrrosia lingua, 50g of artemisia major seed, 100g of fine She Yaju, 25g of valerian, 50g of artemisia rupestris, 50g of azulene and 50g of boat-leaf celery into 150-mesh powder, and uniformly mixing to obtain mixed powder for later use;
S2, parching 25g of small-leaved lemmaples with sand to light yellow, grinding into 80-mesh powder, adding 75g of highland barley wine, mixing and grinding to obtain a mixed solution A for later use;
s3, grinding 2g of artificial musk into fine powder, adding the fine powder into 100g of water, then adding 20g of guar gum, and uniformly stirring to obtain a mixed solution B for later use;
S4, uniformly mixing the powder obtained in the step S1, the mixed solution A obtained in the step S2 and the mixed solution B obtained in the step S3, soaking with 800g of water, stirring in a stirrer for 3 hours, adding 30g of lycopodium clavatum powder, and stirring again for 1 hour to obtain Tibetan incense mud;
s5, using a perfume making machine to obtain the formed Tibetan incense by using the Tibetan incense mud obtained in the step 4, drying the formed Tibetan incense in the shade for 18d at room temperature, wherein the environment humidity of the shade is 20-30% and the formed Tibetan incense is protected from light, and thus the antibacterial moisture-proof Tibetan incense is obtained.
Comparative example 1 in comparison with example 1, no sandalwood, clove, red sandalwood, and Yunnan camphor wood were added.
Comparative example 2
A preparation method of antibacterial moisture-proof Tibetan incense comprises the following steps:
S1, weighing raw materials according to a formula, respectively grinding 75g of sandalwood, 25g of frankincense, 750g of rhizoma et radix Valerianae, 75g of fructus tsaoko, 50g of cinnamon, 25g of nutmeg, 65g of Yunnan camphor, 50g of Tibetan costus root, 50g of costus root, 75g of Gao Shanbai skin, 250g of pterocarpus santalinus, 2g of borneol, 25g of mukul myrrh, 25g of temple, 7.5g of sweet wax, 50g of pyrrosia lingua, 50g of artemisia rupestris, 100g of fine She Yaju, 37g of clove, 50g of azulene and 50g of boat-shaped celery into 150-mesh powder, and uniformly mixing to obtain mixed powder for standby;
S2, parching 25g of small-leaved lemmaples with sand to light yellow, grinding into 80-mesh powder, adding 75g of highland barley wine, mixing and grinding to obtain a mixed solution A for later use;
S3, grinding 2g of artificial musk into fine powder, adding the fine powder into 100g of water, and uniformly stirring to obtain a mixed solution B for later use;
s4, uniformly mixing the powder obtained in the step S1, the mixed solution A obtained in the step S2 and the mixed solution B obtained in the step S3, soaking with 950g of water, and stirring in a stirrer for 3 hours to obtain Tibetan incense mud;
s5, using a perfume making machine to obtain the formed Tibetan incense by using the Tibetan incense mud obtained in the step 4, drying the formed Tibetan incense in the shade for 18d at room temperature, wherein the environment humidity of the shade is 20-30% and the formed Tibetan incense is protected from light, and thus the antibacterial moisture-proof Tibetan incense is obtained.
Comparative example 2 in comparison with example 1, no valerian, tarragon, calamus, guar gum and pinus koraiensis powder were added.
The bacteriostatic moisture-proof Tibetan incense prepared in the embodiment 1-3 and the comparative embodiment 1-2 is subjected to comparison of bacteriostatic experiments, and the specific experimental process is as follows:
Carrier bacteriostasis experiment
The method is suitable for measuring the microbial antibacterial effect of solid antibacterial products such as wet tissues, non-woven fabrics masks, sanitary napkins, protection pads, diapers and the like containing the dissoluble antibacterial components.
1. Reagent, culture medium and apparatus
1.1 Test strains
Staphylococcus aureus (ATCC 6538), escherichia coli (8099), candida albicans (ATCC 10231) and other strains used according to the specific use of the bacteriostatic agent.
1.2 Reagent(s)
Dilution liquid: 0.03 mol/L Phosphate Buffer (PBS) (pH 7.2-7.4), medium: the culture of staphylococcus aureus and escherichia coli uses a nutrient agar medium, and the culture of candida albicans uses a sand agar medium.
1.3 Equipment and method for manufacturing the same
Constant temperature water bath, timer, II level biosafety cabinet, etc.
2. Test procedure
The fresh slant culture of the test bacteria for 24 hours is washed by PBS, diluted to about 10 5CFU/mL～106 CFU/mL by PBS, and prepared into bacterial suspension for standby.
The test sample and the control sample were individually cut into 20 mm X30 mm pieces with sterile scissors under sterile conditions for use. 0.1mL bacterial suspension was added dropwise during the test. The control pieces were sterilized by steam under pressure prior to the bacterial contamination. Taking a sterile plate, taking 2 test pieces by sterile forceps, placing the test pieces in a water bath at 20+/-1 ℃ for 5min without overlapping, dripping 0.1mL of test bacterial suspension on each test piece, and immediately timing. And (3) respectively clamping the bacteria-contaminated sample slices to be added into a 5.0mLPBS test tube for uniformly mixing after the bacteria to be tested contacts with the sample slices for the specified time of the instruction book. Shaking and eluting, respectively sucking 1.0 mL sample solutions, and measuring the number of viable bacteria according to a viable bacteria culture counting method, wherein each sample solution is inoculated with 2 plates. If the number of colonies growing on the plate is large, the viable bacteria culture count can be performed after 10-fold serial dilution.
Meanwhile, 2 pieces of control sample pieces which are the same as the test sample and do not contain antibacterial components are used for replacing the test sample pieces to carry out the test, and the positive control recovered bacteria amount is 1.0 multiplied by 10 4 CFU/piece to 9.0 multiplied by 10 4 CFU/piece; the same batch of PBS and medium was used as negative control.
All test and control samples were incubated at 36 ℃ + -1deg.C, bacterial propagules were incubated for 48h and Candida albicans was incubated for 72h to observe the final results. The test was repeated 3 times and the bacteriostatic rate was calculated.
3. Calculation of the bacteriostatic Rate
Wherein, X-antibacterial rate,%;
A 0 -the positive control recovery bacterial load, the unit is CFU/mL;
a 1 -the amount of recovered bacteria in the test group is CFU/mL.
4. Test determination
The bacteriostasis rate is more than or equal to 50-90 percent, and the bacteriostasis effect is judged; the bacteriostasis rate is more than or equal to 90 percent, and the strong bacteriostasis effect is judged.
5. Experimental results
1. In a relatively airtight environment, incense is ignited, a filter paper sheet soaked in pure water is placed at a position 3cm above the incense for fumigation for 1.5 hours, then filter paper is taken down to perform bacteriostasis experiments on staphylococcus aureus (ATCC 6538) and escherichia coli (8099), the bacteriostasis experiments are respectively performed for 30min and 60min, and the experimental results are shown in Table 1:
TABLE 1 antibacterial effects of Tibetan incense of examples 1-3 and comparative examples 1-2 (1.5 h)
2. In a relatively airtight environment, incense is ignited, a filter paper sheet soaked in pure water is placed at a position 3cm above the incense for fumigation for 2 hours, then filter paper is taken down to perform bacteriostasis experiments on staphylococcus aureus (ATCC 6538) and escherichia coli (8099), the bacteria are respectively acted for 30min and 60min, and the experimental results are shown in Table 2:
TABLE 2 antibacterial effects of Tibetan incense of examples 1-3 and comparative examples 1-2 (2 h)
The Tibetan incense prepared by the invention has the effects of inhibiting the growth of staphylococcus aureus and escherichia coli, and a carrier bacteriostasis test is carried out, and the result shows that the bacteriostasis effect of example 1 on staphylococcus aureus after 2 hours of incense has a maximum bacteriostasis rate of 74.5% after 60 minutes of action, which indicates that the bacteriostasis effect is achieved; the maximum antibacterial rate of the antibacterial agent after 60min of action on escherichia coli is 86.7%.
Antibacterial moisture-proof Tibetan incense moisture-proof the performance test method comprises the following steps: the finished Tibetan incense of example 1 and comparative examples 1-2 was placed in a constant temperature and humidity cabinet for 90 days to test its water absorption under the following test conditions: the temperature is 25+/-1 ℃ and the humidity is 90+/-2%; then, the water vapor on the surface of the sample was removed by taking out the filter paper, and the sample was then subjected to conditioning in an environment at 25.+ -. 1 ℃ and a humidity of 50.+ -. 2% for 10 minutes, and the water absorption was measured, and the measurement results were shown in Table 3 below.
The water absorption was calculated as follows:
wherein m 0 is the quality of Tibetan incense before testing; m 1 is the quality of the adjusted Tibetan incense.
Table 3 results of moisture resistance test of antibacterial moisture-proof Tibetan incense
As can be seen from the above Table 3, the bacteriostatic moisture-proof Tibetan incense prepared by the invention has good moisture resistance, low water absorption under the humid condition and good storage performance.
In conclusion, the Tibetan incense prepared by the invention can obviously inhibit the growth of bacteria in the air, and the formula of the Tibetan incense has the advantages of better growth inhibition effect on staphylococcus aureus and escherichia coli in the air, excellent moisture resistance, no moisture absorption and long fragrance preservation time.
Although embodiments of the present invention have been shown and described, it will be understood by those skilled in the art that various changes, modifications, substitutions and alterations can be made therein without departing from the principles and spirit of the invention, the scope of which is defined in the appended claims and their equivalents.
Claims (10)
1. The antibacterial moisture-proof Tibetan incense is characterized by comprising the following raw materials in parts by weight:
70-80 parts of sandalwood, 20-30 parts of frankincense, 700-800 parts of rhizoma et radix Valerianae, 70-80 parts of fructus tsaoko, 80-120 parts of fine She Yaju, 30-60 parts of cinnamon, 20-30 parts of nutmeg, 60-70 parts of Cinnamomum camphora, 30-45 parts of clove, 40-70 parts of Tibetan costus root, 40-70 parts of costus root, 20-30 parts of valerian, 70-90 parts of Gao Shanbai skin, 200-300 parts of pterocarpus santalinus, 1-3 parts of borneol, 20-30 parts of Mokul myrrh, 20-30 parts of oil head, 5-10 parts of beeswax, 20-40 parts of rhizoma pinellinae praeparata, 40-60 parts of tarragon, 30-60 parts of azulene, 40-70 parts of herba schizonepetae, 10-30 parts of guar gum, 40-60 parts of calamus, 30-60 parts of pyrrosia lingua, 30-70 parts of artemisia seed, 1-4 parts of artificial musk and 20-30 parts of small-leaved lemma;
The preparation method of the antibacterial moisture-proof Tibetan incense comprises the following steps of:
S1, weighing raw materials according to a formula, respectively grinding sandalwood, frankincense, rhizoma et radix Valerianae, fructus Tsaoko, cinnamon, nutmeg, cinnamomum camphora, tibetan radix aucklandiae, cortex Cupressi, pterocarpus Indicus, borneolum Syntheticum, mokuer myrrh, oil head, cera flava, tibetan rhizoma Acori Graminei, folium Pyrrosiae, herba Artemisiae Scopariae, fine She Yaju, flos Caryophylli, rhizoma et radix Valerianae, radix Rumicis Crispi, ganqinglan and herba Apii, mixing uniformly to obtain mixed powder for standby;
s2, stir-frying small-leaved lemmaples to light yellow, grinding the small-leaved lemmaples into powder, adding highland barley wine, mixing and grinding to obtain a mixed solution A for later use;
s3, grinding the musk into fine powder, adding the fine powder into water, then adding guar gum, and uniformly stirring to obtain a mixed solution B for later use;
s4, uniformly mixing the mixed powder obtained in the S1, the mixed solution A obtained in the S2 and the mixed solution B obtained in the S3, soaking the mixture in water, and then stirring the mixture in a stirrer for the first time, and then adding the shi pinang powder, and uniformly stirring the mixture for the second time to obtain Tibetan incense mud;
s5, using a fragrance making machine to obtain a molded Tibetan fragrance, and drying the molded Tibetan fragrance in the shade indoors to obtain the antibacterial moisture-proof Tibetan fragrance.
2. The bacteriostatic moisture-proof Tibetan incense according to claim 1, which is characterized by comprising the following raw materials in parts by weight: 73-78 parts of sandalwood, 23-28 parts of frankincense, 720-770 parts of rhizoma et radix Valerianae, 72-77 parts of fructus tsaoko, 45-110 parts of fine She Yaju, 40-50 parts of cinnamon, 23-27 parts of nutmeg, 63-67 parts of Cinnamomum camphora, 35-40 parts of clove, 40-60 parts of Tibetan costus root, 45-60 parts of costus root, 23-28 parts of valerian, 75-85 parts of Gao Shanbai skin, 220-280 parts of pterocarpus santalinus, 1-2 parts of borneol, 22-27 parts of Mokul myrrh, 23-28 parts of oil head, 6-9 parts of beeswax, 25-35 parts of pine powder, 45-55 parts of tarragon, 40-55 parts of azure blue, 45-65 parts of boat-65 parts of celery, 15-25 parts of guar gum, 45-55 parts of calamus, 40-55 parts of pyrrosia lingua, 40-60 parts of artemisia rupestris, 2-3 parts of artificial musk and 23-28 parts of small-leaved lemons.
3. The bacteriostatic moisture-proof Tibetan incense according to claim 1, which is characterized by comprising the following raw materials in parts by weight: 75 parts of sandalwood, 25 parts of frankincense, 750 parts of rhizoma et radix Valerianae, 75 parts of fructus tsaoko, she Yaju parts of fine, 50 parts of cinnamon, 25 parts of nutmeg, 65 parts of Yunnan camphor, 37 parts of clove, 50 parts of Tibetan costustoot, 50 parts of costustoot, 25 parts of valerian, 75 parts of Gao Shanbai peel, 250 parts of pterocarpus santalinus, 2 parts of borneol, 25 parts of mukul myrrh, 25 parts of oil head, 7.5 parts of beeswax, 30 parts of shipinus koraiensis powder, 50 parts of tarragon, 50 parts of azure blue, 50 parts of boat-leaf celery, 20 parts of guar gum, 50 parts of Tibetan calamus, 50 parts of pyrrosia lingua, 50 parts of tarragon, 2 parts of artificial musk and 25 parts of small-leaved lemons.
4. A method for preparing a bacteriostatic moisture-proof Tibetan incense according to any one of claims 1-3, comprising the steps of:
S1, weighing raw materials according to a formula, respectively grinding sandalwood, frankincense, rhizoma et radix Valerianae, fructus Tsaoko, cinnamon, nutmeg, cinnamomum camphora, tibetan radix aucklandiae, cortex Cupressi, pterocarpus Indicus, borneolum Syntheticum, mokuer myrrh, oil head, cera flava, tibetan rhizoma Acori Graminei, folium Pyrrosiae, herba Artemisiae Scopariae, fine She Yaju, flos Caryophylli, rhizoma et radix Valerianae, radix Rumicis Crispi, ganqinglan and herba Apii, mixing uniformly to obtain mixed powder for standby;
s2, stir-frying small-leaved lemmaples to light yellow, grinding the small-leaved lemmaples into powder, adding highland barley wine, mixing and grinding to obtain a mixed solution A for later use;
s3, grinding the musk into fine powder, adding the fine powder into water, then adding guar gum, and uniformly stirring to obtain a mixed solution B for later use;
s4, uniformly mixing the mixed powder obtained in the S1, the mixed solution A obtained in the S2 and the mixed solution B obtained in the S3, soaking the mixture in water, and then stirring the mixture in a stirrer for the first time, and then adding the shi pinang powder, and uniformly stirring the mixture for the second time to obtain Tibetan incense mud;
s5, using a fragrance making machine to obtain a molded Tibetan fragrance, and drying the molded Tibetan fragrance in the shade indoors to obtain the antibacterial moisture-proof Tibetan fragrance.
5. The process according to claim 4, wherein the particle size of the powder ground in step S1 is 80 to 200 mesh.
6. The preparation method according to claim 4, wherein the powder in the step S2 has a particle size of 60-100 meshes, and the amount of the highland barley wine is 2-4 times of the total amount of the small-leaved lemmaphyllum.
7. The method according to claim 4, wherein the frying method in step S2 uses butter or sand.
8. The method according to claim 4, wherein the amount of water used in step S3 is 4-6 times the total amount of guar gum and artificial musk.
9. The preparation method according to claim 4, wherein the amount of water used in the step S4 is 40-80% of the mass of the powder in the step S1; the primary stirring time is 2-4h; the secondary stirring time is 0.5-1h.
10. The preparation method according to claim 4, wherein the shade-drying condition in step S5 is a shade-drying condition at room temperature for 15-20d, and the shade-drying environment has a humidity of 20-30% and is protected from light.
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| CN104800878A (en) * | 2015-05-14 | 2015-07-29 | 西藏朗卓工贸有限公司 | Tibetan incense and preparation method thereof |
| CN110432735A (en) * | 2018-05-04 | 2019-11-12 | 仁庆欧珠 | A kind of joss stick produced in Xizang and preparation method thereof |
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| CN104800878A (en) * | 2015-05-14 | 2015-07-29 | 西藏朗卓工贸有限公司 | Tibetan incense and preparation method thereof |
| CN110432735A (en) * | 2018-05-04 | 2019-11-12 | 仁庆欧珠 | A kind of joss stick produced in Xizang and preparation method thereof |
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