CN115655978B - An experimental device and method for measuring the evolution of a disturbance shock wave front in a material - Google Patents
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Abstract
本发明涉及动高压冲击压缩技术领域,提供了一种测量材料中扰动冲击波波阵面演化的实验装置及方法,实验装置包括靶盘底座、实验样品、支架、固定后座以及测量系统,靶盘底座设置有样品容纳槽,靶盘底座的一端设置有靶盘缺口,靶盘缺口与样品容纳槽连通;实验样品放置于样品容纳槽内,实验样品的前界面呈曲面波纹状结构且面向靶盘底座的靶盘缺口。本发明利用高速飞片冲击实验样品,在其中产生扰动冲击波,测得样品后界面运动过程中的频谱信号,利用傅里叶变换等方法得到样品后界面粒子速度随时间的变化规律,进而可描绘出冲击波波阵面的演化过程,进一步地,选择连续压力点进行多次测量,利用粒子速度与压力的定量化关系分析被测实验样品的相变。
The invention relates to the technical field of dynamic high-pressure shock compression, and provides an experimental device and method for measuring the evolution of a disturbance shock wave front in a material. The experimental device includes a target plate base, an experimental sample, a bracket, a fixed back seat, and a measurement system, and the target plate The base is provided with a sample holding groove, and one end of the base of the target disk is provided with a target disk gap, and the target disk gap is connected with the sample holding groove; the experimental sample is placed in the sample holding groove, and the front interface of the experimental sample has a curved corrugated structure and faces the target disk The target plate notch of the base. In the present invention, the high-speed flyer is used to impact the experimental sample, a disturbance shock wave is generated in it, and the spectrum signal in the movement process of the interface behind the sample is measured, and the change law of the particle velocity at the interface behind the sample with time is obtained by using methods such as Fourier transform, and then it can be described The evolution process of the shock wave front is analyzed. Further, continuous pressure points are selected for multiple measurements, and the phase transition of the tested experimental sample is analyzed by using the quantitative relationship between particle velocity and pressure.
Description
技术领域technical field
本发明涉及动高压冲击压缩技术领域,具体而言,涉及一种测量材料中扰动冲击波波阵面演化的实验装置。The invention relates to the technical field of dynamic high-pressure shock compression, in particular to an experimental device for measuring the evolution of a disturbance shock wave front in a material.
背景技术Background technique
在高温高压条件下,凝聚态物质常作为流体处理,其动力学过程由流体力学方程组描述。物质的粘性系数对于研究任何实际流体的动力学运动过程都是一个重要的物性参数,通过粘性系数能够描述物质流场中粘应力与物质微元形变速率之间的相关性。能否精确的反映扰动冲击波在物质中的演化规律,决定着能否精确的测量出物质冲击高压下的粘性系数。因此,准确的反映出材料中扰动冲击波波阵面的演化规律具有至关重要的意义。Under high temperature and high pressure conditions, condensed matter is often treated as a fluid, and its dynamic process is described by a system of fluid mechanics equations. The viscosity coefficient of a substance is an important physical parameter for studying the dynamic process of any actual fluid. The viscosity coefficient can describe the correlation between the viscous stress in the flow field of a substance and the deformation rate of the microelement of the substance. Whether it can accurately reflect the evolution law of the disturbance shock wave in the material determines whether it can accurately measure the viscosity coefficient of the material shock under high pressure. Therefore, it is of great significance to accurately reflect the evolution law of the disturbance shock wave front in the material.
对于材料的粘性,由于材料强度部分效应的存在,目前所定义的粘性代表一种等效粘性,前人大量的研究证实,高温高压物质流场的等效粘性密切关系着流场中的动量扩散和能量耗散,耗散过程需要借助物质微观粒子的相互作用得以实现。因此,物质等效粘性的变化能够敏锐的反应物质的结构相变,极端条件下等效粘性系数的测量就为研究物质相变提供了新思路。Regarding the viscosity of the material, due to the existence of the partial effect of the material strength, the currently defined viscosity represents an equivalent viscosity. A large number of previous studies have confirmed that the equivalent viscosity of the high-temperature and high-pressure material flow field is closely related to the momentum diffusion in the flow field. And energy dissipation, the dissipation process needs to be realized by the interaction of material microscopic particles. Therefore, the change of material equivalent viscosity can sensitively reflect the structural phase transition of the material, and the measurement of the equivalent viscosity coefficient under extreme conditions provides a new idea for the study of material phase transition.
为了获得物质的粘性系数,早期主要是通过理论计算和静高压实验获得。理论计算因为其基于理想化模型和理想化条件,其分析结果很难得到公认。静高压实验因为实验条件的限制很难创造超高温高压的环境,使得高温高压条件下物质的粘性数据比较空缺。In order to obtain the viscosity coefficient of the material, it was mainly obtained through theoretical calculation and static high pressure experiment in the early stage. Theoretical calculations are difficult to be recognized because they are based on idealized models and idealized conditions. Due to the limitation of experimental conditions, it is difficult to create an environment of ultra-high temperature and high pressure in static high-pressure experiments, which makes the viscosity data of substances under high temperature and high pressure conditions relatively vacant.
轻气炮技术的发展为研究物质高温高压条件下的粘性提供了新的方法,在动高压领域研究物质粘性的方法主要有:The development of light gas gun technology provides a new method for studying the viscosity of substances under high temperature and high pressure conditions. The methods for studying the viscosity of substances in the field of dynamic high pressure mainly include:
1.间接测量法,间接测量法包括冲击加载下的金属圆柱运动法、离子导电率测量方法、荧光寿命方法和扩散凝聚法等。然而,由于这些测量方法需要提前标定,并与待测物质参数结果作比较,使得这些方法存在不确定性,所得结果很难被学术界接受。1. Indirect measurement method, indirect measurement method includes metal cylinder movement method under impact loading, ionic conductivity measurement method, fluorescence lifetime method and diffusion condensation method, etc. However, since these measurement methods need to be calibrated in advance and compared with the results of the parameters of the substance to be measured, there are uncertainties in these methods, and the results obtained are difficult to be accepted by the academic community.
2.直接测量法,直接测量法包括冲击波阵面厚度测量法与扰动冲击波振幅衰减测量法。对于冲击波阵面厚度测量法,由于实验仪器精度不高,使得测量结果只是一个粗略的平均值;目前利用扰动冲击波振幅衰减思路测量物质粘性系数的实验方法包括Sakharov小扰动实验与飞片碰撞扰动实验,对于Sakharov小扰动实验,由于实验中基板后界面波纹振幅设置过大,使得正弦冲击波引入到样品材料中时出现喷射而导致波形畸变,使得实验结果具有一定的不确定性;而飞片碰撞扰动实验实验装置装配难度较高,并且由于电探针测量端位置在装配和检测过程中可能出现不确定的变化,使得实验结果存在较大误差。2. Direct measurement method, direct measurement method includes shock wave front thickness measurement method and disturbance shock wave amplitude attenuation measurement method. For the shock wave front thickness measurement method, due to the low precision of the experimental equipment, the measurement result is only a rough average value; the current experimental methods for measuring the viscosity coefficient of materials using the idea of perturbed shock wave amplitude attenuation include Sakharov small perturbation experiment and flyer collision perturbation experiment , for the Sakharov small disturbance experiment, because the amplitude of the corrugation at the rear interface of the substrate is set too large in the experiment, when the sinusoidal shock wave is introduced into the sample material, ejection occurs and the waveform is distorted, which makes the experimental results have certain uncertainties; while the flyer collision disturbance It is difficult to assemble the experimental device, and because the position of the measuring end of the electric probe may change uncertainly during the assembly and detection process, there are large errors in the experimental results.
鉴于以上方法的缺点,本发明提出了一种基于多普勒效应来测量材料中扰动冲击波波阵面演化的实验装置及方法,以至少克服上述方法存在的缺陷。In view of the shortcomings of the above methods, the present invention proposes an experimental device and method for measuring the evolution of the disturbance shock wave front in materials based on the Doppler effect, so as to at least overcome the shortcomings of the above methods.
发明内容Contents of the invention
本发明的目的在于提供一种测量材料中扰动冲击波波阵面演化的实验装置及方法,以至少克服现有动高压领域研究物质粘性的方法所存在的测量结果不够准确、实验装置装配难度较高等技术问题。The object of the present invention is to provide an experimental device and method for measuring the evolution of the shock wave front in the material, so as to at least overcome the inaccurate measurement results and the high difficulty of assembling the experimental device in the existing methods for studying the viscosity of substances in the field of dynamic high pressure. technical problem.
本发明的目的通过以下技术方案实现:The object of the present invention is achieved through the following technical solutions:
一方面,本发明提供了一种测量材料中扰动冲击波波阵面演化的实验装置,用于测量扰动冲击波在实验样品中波阵面的演化过程,该实验装置包括:On the one hand, the present invention provides an experimental device for measuring the evolution of a disturbance shock wave front in a material, for measuring the evolution process of a disturbance shock wave wave front in an experimental sample, the experimental device comprising:
靶盘底座,所述靶盘底座设置有样品容纳槽,所述靶盘底座的一端设置有靶盘缺口,所述靶盘缺口与样品容纳槽连通;A target disk base, the target disk base is provided with a sample holding tank, one end of the target disk base is provided with a target disk gap, and the target disk gap communicates with the sample holding groove;
实验样品,所述实验样品放置于样品容纳槽内,所述实验样品的前界面呈曲面波纹状结构且面向靶盘底座的靶盘缺口;An experimental sample, the experimental sample is placed in the sample holding tank, the front interface of the experimental sample has a curved corrugated structure and faces the target plate gap of the target plate base;
支架,所述支架固定于实验样品的后端,且所述支架的前端面与实验样品的后界面接触,所述支架上设置有光纤孔;A bracket, the bracket is fixed on the rear end of the experimental sample, and the front surface of the bracket is in contact with the rear interface of the experimental sample, and the bracket is provided with an optical fiber hole;
固定后座,所述固定后座设置于靶盘底座远离靶盘缺口的一端,所述固定后座的前端面与支架的后端面接触,所述固定后座与靶盘底座可拆卸地连接;The fixed back seat is arranged on the end of the target plate base away from the target plate gap, the front end surface of the fixed back seat is in contact with the rear end surface of the bracket, and the fixed back seat is detachably connected to the target plate base;
测量系统,所述测量系统包括测量光纤、多普勒位移测速系统以及示波器,所述测量光纤的一端与支架上的光纤孔相连,所述测量光纤的另一端与多普勒位移测速系统相连,所述多普勒位移测速系统与示波器相连,所述示波器用于记录实验过程中实验样品后界面的运动过程。A measuring system, the measuring system comprising a measuring fiber, a Doppler displacement velocimetry system and an oscilloscope, one end of the measuring fiber is connected to the fiber hole on the support, and the other end of the measuring fiber is connected to the Doppler displacement velocimetry system, The Doppler displacement velocimetry system is connected with an oscilloscope, and the oscilloscope is used to record the movement process of the rear interface of the experimental sample during the experiment.
在一些可能的实施例中,所述实验样品的后界面呈阶梯状结构,所述支架的前端面也呈阶梯状结构,所述支架前端面的阶梯状结构与实验样品后界面的阶梯状结构相吻合;In some possible embodiments, the rear interface of the experimental sample has a stepped structure, and the front surface of the support also has a stepped structure, and the stepped structure of the front surface of the support is the same as the stepped structure of the rear interface of the experimental sample. match;
所述支架通过前端面的阶梯状结构与实验样品的后界面紧密接触,并固定于所述实验样品的后端。The bracket is in close contact with the rear interface of the experimental sample through the stepped structure of the front face, and is fixed to the rear end of the experimental sample.
在一些可能的实施例中,所述实验样品为固体样品或粉末样品;In some possible embodiments, the experimental sample is a solid sample or a powder sample;
当所述实验样品为粉末样品时,所述粉末样品呈阶梯状结构的一侧表面镀有铝箔,所述支架通过前端面的阶梯状结构与粉末样品后界面的铝箔紧密接触。When the experimental sample is a powder sample, one side surface of the powder sample with a stepped structure is coated with aluminum foil, and the bracket is in close contact with the aluminum foil at the rear interface of the powder sample through the stepped structure of the front surface.
在一些可能的实施例中,当所述实验样品为粉末样品时,该实验装置还包括压制装置,所述压制装置包括:In some possible embodiments, when the experimental sample is a powder sample, the experimental device also includes a pressing device, and the pressing device includes:
压制座,所述压制座设有压制腔,所述压制腔贯穿压制座的顶部设置;A pressing seat, the pressing seat is provided with a pressing cavity, and the pressing cavity is set through the top of the pressing seat;
成形模具,所述成形模具设置于压制腔的内底部,所述成形模具的顶部呈曲面波纹状结构;A forming die, the forming die is arranged at the inner bottom of the pressing cavity, and the top of the forming die is in a curved corrugated structure;
压机顶砧,所述压机顶砧的底部呈阶梯状结构,所述压机顶砧与压制腔适配。The top anvil of the press, the bottom of the top anvil of the press is in a stepped structure, and the top anvil of the press is adapted to the pressing chamber.
在一些可能的实施例中,所述支架上开设的光纤孔为多个,所述测量光纤与光纤孔一一对应,所述测量光纤与支架相连的一端延伸至光纤孔内;In some possible embodiments, there are multiple optical fiber holes on the support, the measuring optical fibers correspond to the optical fiber holes one by one, and the end of the measuring optical fiber connected to the support extends into the optical fiber hole;
多个所述光纤孔分别对应曲面波纹状结构中波峰和波谷在实验样品不同厚度处的后界面。The multiple optical fiber holes respectively correspond to the back interfaces of the crests and troughs of the curved surface corrugated structure at different thicknesses of the experimental samples.
在一些可能的实施例中,所述测量光纤的接头采用UPC接头,所述多普勒位移测速系统所使用的光源为波长1550nm的激光。In some possible embodiments, the connector of the measuring optical fiber adopts a UPC connector, and the light source used by the Doppler displacement velocimetry system is a laser with a wavelength of 1550 nm.
另一方面,本发明提供了一种测量材料中扰动冲击波波阵面演化的实验方法,采用上述所述的测量材料中扰动冲击波波阵面演化的实验装置,该实验方法包括以下步骤:In another aspect, the present invention provides an experimental method for measuring the evolution of a disturbance shock wave front in a material, using the above-mentioned experimental device for measuring the evolution of a disturbance shock wave front in a material, the experimental method comprising the following steps:
步骤S1.制备实验样品;Step S1. Prepare experimental samples;
当所述实验样品为固体样品时,将所述固体样品的前界面加工成曲面波纹状结构;将所述固体样品后界面加工成阶梯状结构;When the experimental sample is a solid sample, the front interface of the solid sample is processed into a curved corrugated structure; the rear interface of the solid sample is processed into a stepped structure;
当所述实验样品为粉末样品时,将所述粉末样品放入压制装置中压制成形,保证所述粉末样品的形状与固体样品的形状相同,并在所述粉末样品呈阶梯状结构的一侧表面镀上均匀的铝箔;When the experimental sample is a powder sample, the powder sample is put into a pressing device and pressed into shape to ensure that the shape of the powder sample is the same as that of the solid sample, and on the side where the powder sample has a stepped structure The surface is coated with uniform aluminum foil;
步骤S2.放置实验样品;Step S2. place the experimental sample;
当所述实验样品为固体样品时,将所述固体样品放置于靶盘底座的样品容纳槽内,并使得所述固体样品的前界面面向靶盘底座的靶盘缺口,随后安装所述支架,保证所述支架的前端面与固体样品的后界面紧密接触;When the experimental sample is a solid sample, the solid sample is placed in the sample holding groove of the target disc base, and the front interface of the solid sample faces the target disc gap of the target disc base, and then the bracket is installed, Ensure that the front surface of the support is in close contact with the rear interface of the solid sample;
当所述实验样品为粉末样品时,将所述粉末样品放置于靶盘底座的样品容纳槽内,并使得所述粉末样品的前界面面向靶盘底座的靶盘缺口,随后安装所述支架,保证所述支架的前端面与粉末样品后界面的铝箔紧密接触;When the experimental sample is a powder sample, place the powder sample in the sample holding tank of the target disc base, and make the front interface of the powder sample face the target disc notch of the target disc base, and then install the bracket, Ensure that the front end of the support is in close contact with the aluminum foil at the rear interface of the powder sample;
完成所述实验样品和支架的安装之后,安装所述固定后座,并保证所述固定后座的前端面与支架的后端面紧密接触;After completing the installation of the experimental sample and the bracket, install the fixed back seat, and ensure that the front end of the fixed back seat is in close contact with the rear end face of the bracket;
步骤S3.靶盘底座安装;Step S3. Target disc base installation;
将所述靶盘底座安装至轻气炮的靶架上,并使得所述靶盘底座的靶盘缺口与轻气炮的飞片正对;Install the target disc base on the target frame of the light gas gun, and make the target disc notch of the target disc base face the flyer of the light gas gun;
步骤S4.测量系统连接;Step S4. Measurement system connection;
将所述测量光纤的一端插入至支架对应的光纤孔内,所述测量光纤的另一端与多普勒位移测速系统相连,所述多普勒位移测速系统与示波器相连;Inserting one end of the measuring fiber into the corresponding fiber hole of the bracket, the other end of the measuring fiber is connected to a Doppler displacement velocimetry system, and the Doppler displacement velocimetry system is connected to an oscilloscope;
步骤S5.测量;Step S5. Measurement;
所述轻气炮发射飞片,利用所述飞片冲击实验样品的曲面波纹状结构,以实现在所述实验样品中产生扰动冲击波,随后,利用所测得样品后界面运动过程中的频谱信号,利用傅里叶变换等方法得到样品后界面粒子速度随时间的变化规律,进而描绘出冲击波波阵面的演化过程;并选择连续压力点进行多次测量,利用粒子速度与压力的定量化关系分析被测实验样品的相变。The light gas cannon emits flying pieces, and uses the flying pieces to impact the corrugated surface of the experimental sample to generate a disturbance shock wave in the experimental sample, and then uses the measured frequency spectrum signal during the rear interface movement of the sample , using methods such as Fourier transform to obtain the change law of particle velocity at the back of the sample with time, and then describe the evolution process of the shock wave front; and select continuous pressure points for multiple measurements, using the quantitative relationship between particle velocity and pressure Analyze the phase transition of the tested experimental samples.
本发明实施例的技术方案至少具有如下优点和有益效果:The technical solutions of the embodiments of the present invention have at least the following advantages and beneficial effects:
1、本发明提供的测量材料中扰动冲击波波阵面演化的实验装置及方法,基于轻气炮加载,通过高速飞片冲击,在实验样品中产生扰动冲击波,利用所测得样品后界面运动过程中测得的频谱信号,经过傅里叶变换等方法得到样品后界面粒子速度随时间的变化规律,进而可描绘出冲击波波阵面的演化过程,进一步地,选择连续压力点进行多次测量,利用粒子速度与压力的定量化关系分析被测实验样品的相变。1. The experimental device and method for measuring the evolution of the disturbance shock wave front in the material provided by the present invention is based on the loading of a light gas cannon, through the impact of high-speed flyers, a disturbance shock wave is generated in the experimental sample, and the interface movement process of the measured sample is used The spectrum signal measured in the sample is obtained by Fourier transform and other methods to obtain the change law of the particle velocity at the interface of the sample with time, and then the evolution process of the shock wave front can be described. Further, continuous pressure points are selected for multiple measurements. The phase transition of the tested experimental sample is analyzed by using the quantitative relationship between particle velocity and pressure.
2、本发明提供的实验装置结构相比于电探针实验装置结构更简单,相比于电探针实验装置具有更多的优势。在宏观角度,该实验装置能够测得实验样品不同厚度处的扰动冲击波波阵面特征点,利用扰动波阵面的演化规律获得被测实验样品的粘性系数;在微观角度,该实验装置能够测得实验样品不同厚度处对应界面的运动情况,并获得对应界面的粒子速度,进一步地,获得被测实验样品的可能相变信息。因此,该实验装置能够满足被测实验样品中冲击波波阵面、粘性系数、界面粒子速度以及相变信息的测量工作,实验成功率更高并且实验成本更低,具有更加广泛的应用前景。2. The structure of the experimental device provided by the present invention is simpler than that of the electrical probe experimental device, and has more advantages compared with the electrical probe experimental device. From a macroscopic point of view, the experimental device can measure the characteristic points of the disturbance shock wave front at different thicknesses of the experimental sample, and use the evolution law of the disturbance wave front to obtain the viscosity coefficient of the tested experimental sample; from a microscopic point of view, the experimental device can measure The movement of the corresponding interface at different thicknesses of the experimental sample is obtained, and the particle velocity of the corresponding interface is obtained, and further, the possible phase transition information of the tested experimental sample is obtained. Therefore, the experimental device can meet the measurement work of shock wave front, viscosity coefficient, interface particle velocity and phase change information in the tested experimental sample, with higher experimental success rate and lower experimental cost, and has wider application prospects.
附图说明Description of drawings
图1为本发明实施例提供的测量固体样品时实验装置的正视剖视图;Fig. 1 is the front sectional view of the experimental device when measuring the solid sample provided by the embodiment of the present invention;
图2为本发明实施例提供的测量固体样品时实验装置的俯视剖视图;Fig. 2 is the top sectional view of the experimental device when measuring solid samples provided by the embodiment of the present invention;
图3为本发明实施例提供的靶盘底座与固定后座的结构剖视图;Fig. 3 is a structural cross-sectional view of the target plate base and the fixed back seat provided by the embodiment of the present invention;
图4为本发明实施例提供的测量固体样品时实验装置部分组件的爆炸图;Figure 4 is an exploded view of some components of the experimental device when measuring solid samples provided by an embodiment of the present invention;
图5为本发明实施例提供的测量固体样品时实验装置部分组件装配后的结构半剖视图;5 is a half-sectional view of the assembled structure of some components of the experimental device when measuring solid samples provided by the embodiment of the present invention;
图6为本发明实施例提供的测量粉末样品时实验装置的正视剖视图;Fig. 6 is the front cross-sectional view of the experimental device when measuring the powder sample provided by the embodiment of the present invention;
图7为本发明实施例提供的测量粉末样品时实验装置的俯视剖视图;Figure 7 is a top sectional view of the experimental device for measuring powder samples provided by the embodiment of the present invention;
图8为本发明实施例提供的测量粉末样品时实验装置部分组件的爆炸图;Figure 8 is an exploded view of some components of the experimental device when measuring powder samples provided by the embodiment of the present invention;
图9为本发明实施例提供的测量粉末样品时实验装置部分组件装配后的结构半剖视图;9 is a half-sectional view of the assembled structure of some components of the experimental device when measuring the powder sample provided by the embodiment of the present invention;
图10为本发明实施例提供的实验过程中其中一个测量光纤所对应的实验样品后界面的频谱信号图;Fig. 10 is a spectrum signal diagram of the rear interface of the experimental sample corresponding to one of the measurement optical fibers during the experiment provided by the embodiment of the present invention;
图11为本发明实施例提供的实验过程中实验样品后界面的粒子速度随时间变化的变换关系图。Fig. 11 is a diagram of the transformation relationship of the particle velocity at the interface behind the experimental sample with time during the experiment provided by the embodiment of the present invention.
图标:a-固体样品,b-粉末样品,10-靶盘底座,10a-样品容纳槽,10b-靶盘缺口,20-支架,20a-光纤孔,30-测量光纤,40-固定后座,50-多普勒位移测速系统,60-示波器,70-铝箔。Icons: a-solid sample, b-powder sample, 10-target plate base, 10a-sample holding groove, 10b-target plate gap, 20-bracket, 20a-fiber hole, 30-measurement fiber, 40-fixed back seat, 50-Doppler displacement velocity measurement system, 60-oscilloscope, 70-aluminum foil.
具体实施方式Detailed ways
请参照图1至图9,本实施例提供了一种测量材料中扰动冲击波波阵面演化的实验装置,用于实现测量扰动冲击波在实验样品中波阵面的演化过程,通过冲击波的波阵面演化过程可以获得冲击波的振荡衰减曲线,结合数值模拟方法进而得出被测样品在不同压力下的粘性系数。可以理解的是,本实施例中待测的实验样品包括固体样品a和粉末样品b,针对不同类型的实验样品,该实验装置略有不同,下面将对实验装置的具体结构做详细的阐述。Please refer to Figures 1 to 9, this embodiment provides an experimental device for measuring the evolution of the wave front of the disturbance shock wave in the material, which is used to measure the evolution of the wave front of the disturbance shock wave in the experimental sample, through the wave front of the shock wave The surface evolution process can obtain the shock wave oscillation attenuation curve, combined with the numerical simulation method to obtain the viscosity coefficient of the tested sample under different pressures. It can be understood that the experimental samples to be tested in this embodiment include solid sample a and powder sample b, and the experimental device is slightly different for different types of experimental samples, and the specific structure of the experimental device will be described in detail below.
在本实施例中,用于测量固体样品a和粉末样品b中扰动冲击波波阵面演化过程的实验装置均包括靶盘底座10、支架20、固定后座40以及测量系统。In this embodiment, the experimental devices for measuring the evolution process of the disturbance shock wave front in the solid sample a and the powder sample b all include a
结合图1、图2、图3、图6和图7所示的内容,在本实施例中,靶盘底座10设置有样品容纳槽10a,样品容纳槽10a贯穿靶盘底座10的一侧侧壁设置,样品容纳槽10a用于放置并固定实验中的固体样品a或粉末样品b,此时,靶盘底座10的一端开设有与样品容纳槽10a连通的靶盘缺口10b,以通过该靶盘缺口10b限制实验样品的位置。需要说明的是,本实施例的靶盘底座10可以但不局限于采用铝制成,且靶盘底座10的尺寸根据轻气炮靶架的尺寸确定,在此不做限定,通过靶盘底座10可以将该实验装置的固体样品a或粉末样品b、支架20以及固定后座40等组件固定至轻气炮的靶架上,以便后续进行实验样品材料中扰动冲击波波阵面演化的测量。1, 2, 3, 6 and 7, in this embodiment, the
结合图1、图2、图6或图7所示的内容,在本实施例中,支架20设置于靶盘底座10远离靶盘缺口10b的一侧,且当支架20安装完成后,支架20固定于实验样品的后端,以通过支架20限制实验样品的位置。可以理解的是,本实施例的支架20可以但不局限于采用铝制成,且支架20上设置有与样品容纳槽10a连通的光纤孔20a,以便于后续与测量系统相连。1, 2, 6 or 7, in this embodiment, the
结合图1、图2、图3、图6或图7所示的内容,在本实施例中,固定后座40设置于靶盘底座10远离靶盘缺口10b的一端,且固定后座40与靶盘底座10可拆卸地连接。其中,固定后座40可以但不局限于采用铝制成,固定后座40与靶盘底座10可以但不限于采用螺纹连接,即固定后座40的相应位置设置有外螺纹,靶盘底座10后端设置有内螺纹,且当固定后座40安装完成后,固定后座40的前端面能够伸入至样品容纳槽10a内并与支架20的后端面紧密接触,以通过固定后座40限制支架20的位置。1, FIG. 2, FIG. 3, FIG. 6 or FIG. 7, in this embodiment, the fixed
在本实施例中,若实验样品为固体样品a或粉末样品b,在实验前还需要将固体样品a或粉末样品b加工成特定形状。In this embodiment, if the experimental sample is a solid sample a or a powder sample b, the solid sample a or powder sample b needs to be processed into a specific shape before the experiment.
具体地,固体样品a或粉末样品b的尺寸由靶盘底座10和支架20的位置共同确定。其中,结合图2或图7所示的内容,当实验样品为固体样品a或粉末样品b时,固体样品a或粉末样品b位于样品容纳槽10a内,且固体样品a或粉末样品b的前界面(即固体样品a或粉末样品b位于样品容纳槽10a内面向靶盘缺口10b的一侧,该前界面为冲击加载条件下被飞片高速冲击的面)呈曲面波纹状结构,此时,曲面波纹状结构具有波峰和波谷。Specifically, the size of the solid sample a or the powder sample b is jointly determined by the positions of the
其中,对于固体样品a而言,固体样品a又分为金属固体样品和非金属固体样品,若为金属固体样品,则可以采用线切割装置在固体样品a的前界面加工出曲面波纹状结构,若为非金属固体样品,则可以采用雕刻机在固体样品a的前界面加工出曲面波纹状结构。对于粉末样品b而言,需要将粉末样品b压制为与样品容纳槽10a相匹配的形状,且压制成形后的粉末样品b与固体样品a的形状相同,以便于粉末样品b的安装与固定。Wherein, for the solid sample a, the solid sample a is further divided into metal solid samples and non-metal solid samples. If it is a metal solid sample, a curved corrugated structure can be processed on the front interface of the solid sample a by using a wire cutting device. If it is a non-metallic solid sample, an engraving machine can be used to process a curved corrugated structure on the front interface of the solid sample a. For the powder sample b, the powder sample b needs to be pressed into a shape that matches the
请参照图1或图6,在本实施例中,固体样品a或粉末样品b的后界面(即固体样品a或粉末样品b面向支架20的一侧)则加工成斜面,并在斜面上设置阶梯状结构,该阶梯状结构包括但不限于六级台阶,每一级台阶尺寸均相同。在本实施例中,支架20的前端面(即支架20面向固体样品a或粉末样品b一侧)同样设置为与实验样品的后界面相匹配的阶梯状结构,此时,支架20前端面的阶梯状结构与实验样品后界面的阶梯状结构相吻合,且当支架20安装在实验样品的后端时,支架20通过前端面的阶梯状结构与实验样品的后界面紧密接触,以保证支架20与固体样品a或粉末样品b能够匹配安装,从而实现既能保证支架20与固体样品a或粉末样品b相对位置的固定,又便于固定于支架20上光纤孔20a内的测量光纤30对不同厚度的扰动冲击波进行测量。Please refer to Fig. 1 or Fig. 6, in this embodiment, the rear interface of solid sample a or powder sample b (that is, the side of solid sample a or powder sample b facing the support 20) is then processed into a slope, and set on the slope The stepped structure includes but is not limited to six steps, and the size of each step is the same. In this embodiment, the front end of the support 20 (that is, the side of the
可以理解的是,为了实现粉末样品b的制备,当实验样品为粉末样品b时,该实验装置还包括压制装置(图中未示出),以通过压制装置将呈粉末状的粉末样品b压制成形,便于将粉末样品b放入靶盘底座10的样品容纳槽10a内并进行后续的测量实验。具体地,该压制装置包括压制座、成形模具以及压机顶砧,其中,压制座设有与粉末样品b的形状适配的压制腔,该压制腔贯穿压制座的顶部设置,成形模具设置于压制腔的内底部,且成形模具的顶部呈曲面波纹状结构,压机顶砧的底部则呈阶梯状结构且与压制腔适配,以使得压机顶砧能够伸入至压制腔内或伸出至压制腔外。在实际制备粉末样品b时,将粉末状的粉末样品b放入压制座的压制腔内,随后利用压机使得压机顶砧沿压制腔向下挤压粉末样品b,以实现粉末样品b的压制成形,最终压制成形且呈固体状态的粉末样品b与固体样品a的形状相同。It can be understood that, in order to realize the preparation of powder sample b, when the experimental sample is powder sample b, the experimental device also includes a pressing device (not shown in the figure), so that the powder sample b in powder form can be pressed by the pressing device It is convenient to put the powder sample b into the
此外,在实际实施时,制备支架20的材料也可以随实验压力的变化而变化,本实施例中支架20的材料采用铝,如果需要考虑多次冲击,制备支架20的材料可以根据实验压力不同分别选择石英玻璃、蓝宝石或氟化锂(LiF),具体地,当实验压力为低压力(10GPa以内)时,支架20可以采用石英玻璃制备而成,当实验压力为中压力(10-40GPa)时,支架20可以采用蓝宝石制备而成,当实验压力为高压力(大于40GPa)时,支架20可以采用氟化锂制备而成。In addition, in actual implementation, the material for preparing the
另一方面,当实验样品为粉末样品b时,考虑到粉末样品b疏松多孔,回光反射率较低,为此,结合图6或图7所示的内容,可以在粉末样品b呈阶梯状结构的一侧(即粉末样品b的后界面)表面镀上铝箔70,且支架20通过前端面的阶梯状结构与粉末样品b后界面的铝箔70紧密接触,通过增加铝箔70来进行反光,能够提高粉末样品b后界面的回光反射率,从而确保实验过程中粉末样品b每一级台阶的竖直后界面的运动规律均能够被测量系统探测到。On the other hand, when the experimental sample is powder sample b, considering that the powder sample b is loose and porous, and the retroreflectivity is low, for this reason, combined with the content shown in Figure 6 or Figure 7, the powder sample b can be stepped One side of the structure (that is, the rear interface of the powder sample b) is coated with
在本实施例中,测量系统可以测量在固体样品a或粉末样品b中扰动冲击波到达不同厚度界面的时间,对于同一厚度界面,利用扰动冲击波到达界面的时间差,可以算出对应界面的扰动振幅,通过多个不同厚度的界面测量信息就能得出扰动冲击波在实验样品中波阵面扰动的演化过程,进一步地,结合数值模拟方法就能够得出固体样品a或粉末样品b在对应实验压力下的粘性系数。In this embodiment, the measurement system can measure the time for the disturbance shock wave to reach the interface with different thicknesses in the solid sample a or the powder sample b. For the same thickness interface, the disturbance amplitude of the corresponding interface can be calculated by using the difference in the arrival time of the disturbance shock wave at the interface. The evolution process of the disturbance shock wave in the experimental sample can be obtained from the measurement information of multiple interfaces with different thicknesses. Further, combined with the numerical simulation method, the corresponding experimental pressure of the solid sample a or powder sample b can be obtained. Viscosity coefficient.
具体地,请参照图1、图2、图6或图7,该测量系统包括测量光纤30、多普勒位移测速系统50以及示波器60。其中,测量光纤30的一端与支架20上的光纤孔20a相连,测量光纤30的另一端与多普勒位移测速系统50相连,多普勒位移测速系统50与示波器60相连,以通过示波器60记录实验过程中实验样品后界面的运动过程。可以理解的是,示波器60可以但不局限于采用高分辨率检测示波器,以提高测量结果的准确度。Specifically, referring to FIG. 1 , FIG. 2 , FIG. 6 or FIG. 7 , the measurement system includes a measurement
需要说明的是,为了便于测量光纤30与支架20相连,支架20上开设的光纤孔20a为多个,且测量光纤30与光纤孔20a一一对应,测量光纤30与支架20相连的一端延伸至光纤孔20a内,可以理解的是,为了使得测量光纤30能够更好的与支架20上的光纤孔20a匹配,测量光纤30的接头采用UPC接头,且开设在支架20上的光纤孔20a的尺寸根据测量光纤30的纤芯长度和纤径来确定,同时,多普勒位移测速系统50所使用的光源为波长1550nm的激光,多普勒位移测速系统50又包括激光发射系统和回光接收系统,激光发射系统用于发出波长为1550nm的激光,回光接收系统则用于将探测到的固体样品a或粉末样品b后界面的回光振幅信息传递至示波器60,通过示波器60记录整个实验过程中的回光振幅信号。It should be noted that, in order to facilitate the measurement of the
此外,在实际实施时,开设在支架20上的多个光纤孔20a需要分别对应固体样品a或粉末样品b的曲面波纹状结构中波峰和波谷在固体样品a或粉末样品b不同厚度处的后界面。In addition, in actual implementation, the plurality of
示例的,请参照图4或图8,本实施例中支架20上开设有十八个光纤孔20a,对应十八个测量光纤30通道,此时,光纤孔20a呈矩形阵列分布;其中,结合图1或图6所示的内容,位于同一竖直线上的六个光纤孔20a分别与固体样品a或粉末样品b的曲面波纹状结构的波峰或波谷对应,结合图2或图7所示的内容,位于同一水平线上的三个光纤孔20a则与固体样品a或粉末样品b的曲面波纹状结构的一个波峰与两个波谷对应。值得注意的是,在实际实施时还需要合理控制支架20的厚度,保证测量光纤30的端头与固体样品a或粉末样品b的后界面的距离一定,确保回光效果最佳。For example, please refer to Fig. 4 or Fig. 8, in the present embodiment, eighteen
另一方面,本实施例提供了一种测量材料中扰动冲击波波阵面演化的实验方法,采用上述所述的测量材料中扰动冲击波波阵面演化的实验装置,该实验方法包括以下步骤:On the other hand, this embodiment provides an experimental method for measuring the evolution of a disturbance shock wave front in a material, using the above-mentioned experimental device for measuring the evolution of a disturbance shock wave front in a material, and the experimental method includes the following steps:
步骤S1.制备实验样品;Step S1. Prepare experimental samples;
当实验样品为固体样品a时,将固体样品a的前界面(即固体样品a位于靶盘底座10内面向靶盘缺口10b的一侧)加工成曲面波纹状结构;将固体样品a的后界面(即固体样品a位于靶盘底座10内面向支架20的一侧)加工成阶梯状结构;When the experimental sample is a solid sample a, the front interface of the solid sample a (that is, the solid sample a is located on the side of the
当实验样品为粉末样品b时,先将粉末样品b放入压制装置中压制成形,以使得粉末样品b的形状与固体样品a的形状相同,并在粉末样品b呈阶梯状结构的一侧表面(即粉末样品b的后界面)镀上均匀的铝箔70;When the experimental sample is a powder sample b, the powder sample b is first put into a compacting device and pressed into shape, so that the shape of the powder sample b is the same as that of the solid sample a, and the surface of the powder sample b has a stepped structure. (i.e. the rear interface of the powder sample b) coated with a
步骤S2.放置实验样品;Step S2. place the experimental sample;
当实验样品为固体样品a时,将固体样品a放置于靶盘底座10的样品容纳槽10a内,并使得固体样品a的前界面面向靶盘底座10的靶盘缺口10b,随后安装支架20,让固体样品a位于支架20与靶盘底座10构成的样品容纳槽10a内,保证支架20的前端面与固体样品a的后界面紧密接触;When the experimental sample is a solid sample a, the solid sample a is placed in the
当实验样品为粉末样品b时,将压制成形的粉末样品b放置于靶盘底座10的样品容纳槽10a内,并使得粉末样品b的前界面面向靶盘底座10的靶盘缺口10b,随后安装支架20,让粉末样品b位于支架20与靶盘底座10构成的样品容纳槽10a内,铝箔70位于粉末样品b远离靶盘缺口10b的一侧,保证支架20的前端面与粉末样品b后界面的铝箔70紧密接触;When the experimental sample is a powder sample b, the pressed powder sample b is placed in the
步骤S3.靶盘底座10安装;Step S3.
将靶盘底座10安装至轻气炮的靶架上,并使得靶盘底座10的靶盘缺口10b与轻气炮的飞片正对;The
步骤S4.测量系统连接;Step S4. Measurement system connection;
将测量光纤30的一端插入至支架20上设置的光纤孔20a内,测量光纤30的另一端与多普勒位移测速系统50相连,多普勒位移测速系统50与示波器60相连;One end of the measuring
步骤S5.测量;Step S5. Measurement;
轻气炮发射飞片,利用飞片高速冲击实验样品的曲面波纹状结构,以实现在实验样品中产生扰动冲击波,利用所测得样品后界面运动过程中的频谱信号,利用傅里叶变换等方法得到样品后界面粒子速度随时间的变化规律,进而可描绘出冲击波波阵面的演化过程,进一步地,选择连续压力点进行多次测量,利用粒子速度与压力的定量化关系分析被测实验样品的相变。The light gas cannon fires the flying pieces, and uses the high-speed impact of the flying pieces on the corrugated surface of the experimental sample to generate a disturbance shock wave in the experimental sample. Using the measured spectrum signal during the movement of the interface behind the sample, Fourier transform, etc. The method obtains the change law of the particle velocity at the interface of the sample with time, and then can describe the evolution process of the shock wave front. Further, select continuous pressure points for multiple measurements, and use the quantitative relationship between particle velocity and pressure to analyze the measured experiment. Phase transition of the sample.
实验例Experimental example
在实测实验中,将金属铝作为实验样品,并将其加工成特定的形状(即前述所说的前界面呈曲面波纹状结构,后界面呈阶梯状结构)以满足实验装置要求。将实验装置固定于轻气炮的靶架上,利用铝飞片高速冲击实验样品,实测过程中,飞片的速度为1.51km/s。在实测实验中,其中一个测量光纤30所测实验信号图如图10所示,图10为该测量光纤30所对应实验样品后界面的频谱信号图,通过该图可以判断扰动冲击波到达该界面所对应的时间。In the actual measurement experiment, metal aluminum is used as the experimental sample, and it is processed into a specific shape (that is, the front interface is a curved corrugated structure, and the rear interface is a stepped structure) to meet the requirements of the experimental device. The experimental device was fixed on the target frame of the light gas gun, and the aluminum flyer was used to impact the experimental sample at high speed. During the actual measurement, the speed of the flyer was 1.51km/s. In the actual measurement experiment, one of the measured experimental signal diagrams of the measuring
为了进一步对图10所示的频谱信号图进行处理,需要用傅里叶变换进行数学变换。傅里叶变换关系式为:In order to further process the spectrum signal diagram shown in Fig. 10, it is necessary to use Fourier transform to perform mathematical transformation. The Fourier transform relation is:
式中:w为变换频率,是变换后的函数变量;t为变换时间,是原函数的函数变量;e -iwt 为复变函数;φ代表傅里叶变换;dt代表微分;函数F(w)为函数f(t)的傅里叶变换,f(t)为F(w)的傅里叶逆变换。In the formula: w is the transformation frequency, which is the function variable after transformation; t is the transformation time, which is the function variable of the original function; e -iwt is a complex variable function; φ represents Fourier transform; dt represents differential; function F ( w ) is the Fourier transform of the function f ( t ), and f ( t ) is the inverse Fourier transform of F ( w ).
通过傅里叶变换可以得到实验样品后界面频率随时间变化的变换关系,如图11所示。利用图11可以得出实验样品后界面的粒子速度随时间变化的变换关系。对比多个压力值下的测量结果,可用于分析实验样品的相变。Through the Fourier transform, the transformation relationship of the interface frequency of the experimental sample with time can be obtained, as shown in Figure 11. Figure 11 can be used to obtain the transformation relationship of the particle velocity at the rear interface of the experimental sample as a function of time. Comparing the measurement results under multiple pressure values can be used to analyze the phase transition of experimental samples.
以上所述仅是本发明的优选实施方式,应当理解本发明并非局限于本文所披露的形式,不应看作是对其他实施例的排除,而可用于各种其他组合、修改和环境,并能够在本文所述构想范围内,通过上述教导或相关领域的技术或知识进行改动。而本领域人员所进行的改动和变化不脱离本发明的精神和范围,则都应在本发明所附权利要求的保护范围内。The above descriptions are only preferred embodiments of the present invention, and it should be understood that the present invention is not limited to the forms disclosed herein, and should not be regarded as excluding other embodiments, but can be used in various other combinations, modifications and environments, and Modifications can be made within the scope of the ideas described herein, by virtue of the above teachings or skill or knowledge in the relevant art. However, changes and changes made by those skilled in the art do not depart from the spirit and scope of the present invention, and should all be within the protection scope of the appended claims of the present invention.
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