[go: up one dir, main page]

CN115553487B - Heated cigarette slice and manufacturing method thereof - Google Patents

Heated cigarette slice and manufacturing method thereof Download PDF

Info

Publication number
CN115553487B
CN115553487B CN202211253675.8A CN202211253675A CN115553487B CN 115553487 B CN115553487 B CN 115553487B CN 202211253675 A CN202211253675 A CN 202211253675A CN 115553487 B CN115553487 B CN 115553487B
Authority
CN
China
Prior art keywords
parts
pulp
sheet
tea
fruit pulp
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Active
Application number
CN202211253675.8A
Other languages
Chinese (zh)
Other versions
CN115553487A (en
Inventor
肖永银
杜超
刘劲芸
刘鑫
吴恒
徐世涛
陈永宽
尚善斋
赵立恒
蒋卓芳
高则睿
陈婉
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Yunnan China Tobacco New Material Technology Co ltd
Original Assignee
Yunnan China Tobacco New Material Technology Co ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Yunnan China Tobacco New Material Technology Co ltd filed Critical Yunnan China Tobacco New Material Technology Co ltd
Priority to CN202211253675.8A priority Critical patent/CN115553487B/en
Publication of CN115553487A publication Critical patent/CN115553487A/en
Application granted granted Critical
Publication of CN115553487B publication Critical patent/CN115553487B/en
Active legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Classifications

    • AHUMAN NECESSITIES
    • A24TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24BMANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
    • A24B3/00Preparing tobacco in the factory
    • A24B3/14Forming reconstituted tobacco products, e.g. wrapper materials, sheets, imitation leaves, rods, cakes; Forms of such products
    • AHUMAN NECESSITIES
    • A24TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24BMANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
    • A24B15/00Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
    • A24B15/18Treatment of tobacco products or tobacco substitutes

Landscapes

  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Manufacture Of Tobacco Products (AREA)

Abstract

The invention relates to the technical field of heating non-combustible tobacco products, in particular to a heating cigarette sheet and a manufacturing method thereof. The heated cigarette slice comprises water, an adhesive, a smoke agent, tobacco powder, wood pulp, tea fruit pulp and animal fat, wherein the tea fruit pulp comprises tannin and tea saponin, and the animal fat comprises glyceride. The tea fruit pulp and animal fat are added in the sheet raw material, and the moisture absorption problem of the sheet is effectively improved and the tensile strength of the sheet is improved through the synergistic effect among cellulose, tannin, tea saponin and glyceride.

Description

Heated cigarette slice and manufacturing method thereof
Technical Field
The invention relates to the technical field of heating non-combustible tobacco products, in particular to a heating cigarette sheet and a manufacturing method thereof.
Background
The heating non-burning tobacco product is a new-type product combining heating appliance and cigarette bullet, it is a "low-temp. cigarette" designed by using "heating only and non-burning" as thought, and utilizes special-purpose heating device to heat the treated cut tobacco and cigarette bullet to a certain temp., and heat the cigarette bullet to a degree sufficient for giving out smoke gas for smoking.
The cartridges of the heated non-combustible tobacco products are mainly divided into two types, namely a particle technology and a sheet technology. The particle technology has the advantages that the residues are some dry carbonized particles after the heating core is heated, so that the particles can be removed easily, but the particle technology has the defects of uneven heating, small smoke quantity, easy generation of burnt smell, inconsistent front and rear smoke quantity and incapability of keeping the fragrance of cigarettes. The sheet technology is that the herbal plant or tobacco-like component is crushed and mixed with natural fiber, and then added with adhesive and the like to be uniformly stirred, and the sheet product is prepared after constant-pressure drying. But the disadvantage is that the thin sheet is easy to absorb moisture, which affects the adaptability of the machine.
In order to solve the moisture absorption problem of the sheet, a moisture-proof layer is generally formed on the surface of the sheet in the prior art, such as a moisture-proof humectant disclosed in patent document with publication number CN113907409a for preventing moisture absorption of the tobacco sheet, and is characterized by comprising polyalcohol, beta-cyclodextrin and polyglucosamine (1-4) -2-amino-B-D glucose, and moisture absorption of the sheet is prevented by spraying the moisture-proof humectant. Another example of such a heated cigarette core material is disclosed in the publication CN114009826a and a method of making the same, comprising the steps of: pretreatment of a fuming agent, configuration of perfume, pretreatment of sizing material, preparation of substrate slurry, treatment of powder material, forming of a substrate, powder spraying, rolling of a sheet, film coating and drying forming. The porous solid adsorbent is added into the smoke agent, and the smoke agent is mixed with the glue system to be embedded in the base material slurry, so that the moisture absorption problem of the prepared smoke core material can be effectively solved by matching with the film coating process.
In the scheme, on one hand, the moisture-proof layer has the problem of easy falling off, and the long-term preservation effect of the thin sheet is affected; on the other hand, the sheet itself has the problem of low tensile strength, and the material used for the moisture-proof layer does not positively influence the tensile strength of the sheet.
Disclosure of Invention
The present invention has been made to solve the above problems, and provides a heated cigarette sheet and a method for manufacturing the same.
The technical scheme for solving the problems is that the invention firstly provides a heating cigarette slice which comprises water, an adhesive, a smoke agent, tobacco powder, wood pulp, tea fruit pulp and animal fat, wherein the tea fruit pulp comprises tannin and tea saponin, and the animal fat comprises glyceride.
Wherein water, adhesive, smoke agent, tobacco powder and wood pulp are common components of the flake.
The fuming agent is used for atomizing and generating smoke when heating, and common fuming agents such as propylene glycol and glycerol are selected. Preferably, the smoke generating agent comprises 10-60 parts by mass of propylene glycol and 40-90 parts by mass of glycerol.
The wood pulp is mainly used for providing supporting fibers for the thin sheet and ensuring the basic strength of the thin sheet, and is generally prepared by chemically pulping and physically pulping plant raw materials, wherein the plant raw materials can be woody plants such as needle wood, broad-leaved wood and the like, can also be herbaceous plants such as Chinese alpine rush, tobacco stems and the like, and can be directly purchased in the market.
The tobacco powder is used for providing traditional cigarette aroma for the thin sheet and also providing a certain amount of supporting fiber, and is usually prepared by directly fermenting tobacco leaves and then freezing and crushing the tobacco leaves.
The adhesive is used for combining the solid components, is preferably a nontoxic and non-pungent odor adhesive, and as a preferable mode of the invention, the adhesive comprises one or more of guar gum, chitosan, sodium carboxymethyl cellulose and pectin.
Water is generally used to dilute the above components for subsequent sheeting.
In order to solve the moisture absorption problem and the low tensile strength problem of the thin sheet, tea fruit pulp and animal fat are creatively added into the thin sheet raw material.
The tea fruit pulp is mainly prepared by extracting tea fruits under the condition of a solvent, wherein the tea fruits comprise outer shells and tea seeds therein, the shells contain higher-content tannin, and the tea seeds contain higher-content tea saponin and vegetable oil. The solvent for extracting the tea fruits is not limited, and as the preferable choice of the invention, a mixed solvent of propylene glycol and water is selected. The ratio of the propylene glycol to the water is not limited, and the solvent preferably includes 10 to 60 parts by mass of propylene glycol and 20 to 90 parts by mass of water. The ratio of the amount of the tea fruit to the amount of the solvent is not limited, and in order to improve the extraction yield, it is preferable to mix 10 to 80 parts by mass of the tea fruit and 10 to 80 parts by mass of the solvent at the time of extraction.
The main components of animal fat are triglycerides of palmitic acid and stearic acid. Preferably, the animal fat comprises one or more of lard, beef tallow and mutton tallow.
When the tea fruit pulp and the animal fat are mixed for use, first, the tea fruit pulp and the animal fat can respectively act: tea fruit pulp: the wood pulp cellulose is subjected to condensation reaction with active hydrogen on tannin molecules through aldehyde groups (bleaching agents used in the process of preparing the wood pulp oxidize cellulose hydroxyl groups into aldehyde, general acid groups and the like), and the tannin is anchored on the fibers through covalent bonds, so that a hydrogen bond connection structure between the cellulose is replaced, the hydrophobicity of the sheet is improved, moisture absorption is avoided, and the bonding strength between the fibers, namely the tensile strength of the sheet is improved to a certain extent; the vegetable oil can form a layer of hydrophobic film on the surface of the flake through the hydrophobic group, so that the hydrophobic property is improved to realize moisture resistance, and the internal stress of the flake can be improved to increase the tensile strength of the flake. Animal fat: the hydrophobic property is also improved by the hydrophobic group, and the internal stress is improved.
Second, tea fruit pulp and animal fat may act synergistically: because of the existence of water and animal fat, before the sheet is formed, the slurry obtained by mixing all the raw materials is an oil-water mixture, and the tea saponin has good interfacial activity, can help the emulsification of the oil-water mixture, improves the uniformity of the slurry, and improves the moisture-proof uniformity of the sheet. Meanwhile, the tea saponin can also self-assemble to form micelles, the micelles form ordered fibrous aggregates in an oil-water interface in a self-assembly way, and as the tea saponin molecules are adsorbed perpendicular to the interface, the tea saponin has extremely high elastic modulus and viscosity, shows viscoelastic behavior, and improves the tensile strength of the thin sheet through the viscoelasticity. And glyceride is also an amphipathic molecule, glyceride in the oil phase tends to be adsorbed on the surface of oil drops, and at a certain concentration, glyceride crystals can pierce the fiber interface film of the tea saponin and enter the water phase, at the moment, glyceride part participates in interface formation, the glyceride and the tea saponin cooperatively reduce interfacial tension, formed emulsion drops are smaller, the accumulation is tighter, the strength of the constructed three-dimensional network structure is larger, and therefore the mechanical property is improved.
In the process, the ratio of the tea fruit pulp to the animal fat has a certain influence on the final hydrophobicity and tensile strength, and the excessive use of the animal fat and the excessive use of glyceride can influence the viscoelasticity of the fiber interface film and the tensile strength of the thin sheet; animal fat and oil are too low in dosage, so that the dosage of glyceride is too low, on one hand, the hydrophobicity is insufficient, and on the other hand, the glyceride is insufficient to pierce the fiber interface membrane, and the synergistic effect of the glyceride and the tea saponin is affected. Preferably, the animal fat is used in an amount of 3-5wt% of the tea fruit pulp.
The content of other raw materials also has a certain influence, and the preferred part of the invention is that the heating cigarette slice comprises 10-60 parts of tobacco powder, 5-60 parts of tea fruit pulp, 10-40 parts of water, 0.2-5 parts of adhesive, 10-60 parts of fumigant, 1-4 parts of wood pulp and 0.5-4 parts of animal fat.
In order to further improve the moisture absorption problem and the tensile strength of the sheet, the tobacco powder is preferably prepared by baking a mixture of pulp and fermented tobacco leaves at 140-160 ℃ and pulverizing.
The traditional tobacco powder only comprises tobacco leaves after fermentation, and fruit pulp is added for co-baking. The fruit pulp is mainly prepared by extracting fruit raw materials under the condition of a solvent, and contains saccharide compounds such as fructose and the like. The method can reduce harmful components in tobacco leaves by fermenting the tobacco leaves, and can obtain amino acid by fermenting. The amino acid can generate Maillard reaction with the saccharide compound at a certain temperature, so that the aroma of the flake is further improved, and the miscellaneous gas and the irritation are reduced; and the obtained product comprises furfural, can be covalently condensed with tannin in tea fruit pulp, improves the hydrophobicity and tensile strength of the flake, and has better compatibility of tobacco powder and wood pulp under the intermediate action of tannin.
In view of the formation amount of Maillard reaction products, as a preferred aspect of the present invention, the tobacco powder comprises 10-99 parts by mass of fermented tobacco leaves and 1-30 parts by mass of fruit pulp.
The pulp may be a solvent extract of any fruit material, such as apple pulp, jujube pulp, coconut pulp, etc., and preferably, coconut pulp is used in the present invention. Because the oil content of coconut meat is 35%, the oil is rich in capric acid, palmitic acid, lauric acid, oleic acid, fatty acid and free fatty acid, and the moisture absorption problem of the slice can be further improved by utilizing the hydrophobic group in the coconut oil. The solvent for extracting the fruit pulp is not limited, and preferably comprises 10-50 parts by mass of propylene glycol and 30-80 parts by mass of water. The ratio of the fruit to the solvent is not limited, and preferably, the fruit is mixed with 10 to 60 parts by mass and 20 to 90 parts by mass of the solvent during extraction.
The fermented tobacco leaves can be the product of fermenting fresh tobacco leaves in any mode, and are mixed fermentation products of tobacco leaves and cocoa pulp as the preferable mode of the invention. The color of the tobacco leaves can be regulated by fermenting the tobacco leaves and the cocoa pulp together, so that the milk flavor and the bean flavor of the tobacco leaves are improved. Preferably, 10-80 parts of cocoa pulp and 30-90 parts of tobacco leaf are mixed and fermented according to parts by mass.
It is yet another object of the present application to provide a method of manufacturing a heated cigarette sheet comprising the steps of:
s1, uniformly mixing smoke powder, tea fruit pulp, water, adhesive, smoke agent, wood pulp and animal fat according to parts by mass, and stirring at 50-60 ℃ to obtain thick pulp;
s2, uniformly spraying thick slurry on the steel belt through a slit of a tape casting forming device, forming and drying to obtain the sheet.
In the application, thick slurry is prepared by stirring at a specific temperature range of 50-60 ℃ so as to promote the stable formation of the oil-water emulsion, thereby ensuring the subsequent hydrophobicity and tensile strength.
The flakes themselves need to have a moisture content to avoid excessive drying of the flakes and to be brittle, and preferably according to the invention, the flakes are dried to a moisture content of 7-12% after molding.
As a preferred aspect of the present invention, the tobacco powder is prepared by: mixing fresh cocoa pulp and tobacco leaf, and fermenting at 40-50deg.C; taking out the fermentation product, baking at 90-110 ℃ until the water content is 10-20%, and obtaining the fermented tobacco leaves; mixing the fermented tobacco leaves and the pulp, baking at 140-160 ℃ until the water content is 4-7%, and then crushing and screening to obtain the tobacco powder.
The invention has the beneficial effects that:
1. in the application, by adding tea fruit pulp and animal fat into the sheet raw material, the moisture absorption problem of the sheet is effectively improved, and the tensile strength of the sheet is improved.
2. In this application, through the modified tradition tobacco powder of fruit pulp, can also cooperate the use of tea fruit pulp in order to further improve the slice moisture absorption problem and improve tensile strength when improving the suction taste of thin slice, can also improve the compatibility of tobacco powder and wood pulp in addition.
Detailed Description
The following is a specific embodiment of the present invention and further describes the technical solution of the present invention, but the present invention is not limited to these examples.
Example 1
A heated cigarette sheet prepared by the steps of: in the preparation process, the raw materials are calculated in parts by mass.
Preparing fruit pulp: uniformly mixing 20 parts of propylene glycol with 80 parts of water to obtain a solvent; mixing 20 parts of coconut meat and 80 parts of solvent, crushing, pulping and filtering to obtain fruit pulp.
Preparing tea fruit pulp: uniformly mixing 20 parts of propylene glycol with 80 parts of water to obtain a solvent; mixing 20 parts of tea fruits and 80 parts of solvent, crushing, pulping and filtering to obtain tea fruit pulp.
Preparing tobacco powder: uniformly mixing 30 parts of fresh cocoa pulp and 70 parts of tobacco leaves to obtain a mixture A; fermenting the mixture A at a constant temperature of 45 ℃ for 7 days; taking out the mixture A, putting the mixture A into a baking oven for baking at 100 ℃, and baking the mixture A until the moisture is 16%; then mixing 90 parts of the mixture A and 5 parts of fruit pulp, and uniformly stirring to obtain a mixture B; placing the mixture B into an oven at 145 ℃ for continuously baking until the water content is 7%; and (5) crushing and screening the mixture B to obtain the smoke powder.
Preparation of a smoke agent: and uniformly mixing 30 parts of propylene glycol and 70 parts of glycerol to obtain the fuming agent.
The animal fat is beef tallow. Pectin is used as the adhesive. Yang Mujiang is selected from wood pulp.
S1, uniformly mixing 25 parts of tobacco powder, 50 parts of tea fruit pulp, 10 parts of water, 1 part of adhesive, 11 parts of fuming agent, 2 parts of wood pulp and 1 part of animal fat, and stirring for 4 hours at the constant temperature of 55 ℃ to obtain thick pulp.
S2, uniformly spraying thick slurry on a steel belt through a slit of a tape casting forming device, and drying a formed sheet until the water content is 9%; and stripping the dried sheet from the steel belt, wrapping, sealing and packaging.
Example 2
This embodiment is substantially the same as embodiment 1, except that: increasing the dosage of animal fat.
In the step S1, 25 parts of tobacco powder, 50 parts of tea fruit pulp, 10 parts of water, 1 part of adhesive, 11 parts of fuming agent, 2 parts of wood pulp and 2 parts of animal fat are uniformly mixed, and then stirred for 4 hours at the constant temperature of 55 ℃ to obtain thick pulp.
Example 3
This embodiment is substantially the same as embodiment 1, except that: the dosage of animal fat is greatly increased.
In the step S1, 25 parts of tobacco powder, 50 parts of tea fruit pulp, 10 parts of water, 1 part of adhesive, 11 parts of fuming agent, 2 parts of wood pulp and 4 parts of animal fat are uniformly mixed, and then stirred for 4 hours at the constant temperature of 55 ℃ to obtain thick pulp.
Example 4
This embodiment is substantially the same as embodiment 1, except that: no fruit pulp is used.
Preparing tobacco powder: uniformly mixing 30 parts of fresh cocoa pulp and 70 parts of tobacco leaves to obtain a mixture A; fermenting the mixture A at a constant temperature of 45 ℃ for 7 days; taking out the mixture A, putting the mixture A into a baking oven for baking at 100 ℃, and baking the mixture A until the moisture is 16%; then, putting 90 parts of the mixture A into an oven at 145 ℃ to be continuously baked until the moisture is 7%, and finally crushing and screening to obtain the tobacco powder.
Example 5
This embodiment is substantially the same as embodiment 1, except that: the tobacco leaves are not fermented.
Preparing tobacco powder: 100 parts of tobacco leaves are put into an oven for baking at 100 ℃ until the moisture is 16%; then mixing 90 parts of tobacco leaves and 5 parts of fruit pulp, and uniformly stirring to obtain a mixture B; placing the mixture B into an oven at 145 ℃ for continuously baking until the water content is 7%; and (5) crushing and screening the mixture B to obtain the smoke powder.
Example 6
This embodiment is substantially the same as embodiment 1, except that: the pulp is replaced by pulp of coconut pulp and apple pulp.
Preparing fruit pulp: uniformly mixing 20 parts of propylene glycol with 80 parts of water to obtain a solvent; mixing 20 parts of apples and 80 parts of solvent, crushing, pulping and filtering to obtain fruit pulp.
Example 7
This embodiment is substantially the same as embodiment 1, except that: the stirring temperature was too high.
Step S1, uniformly mixing 25 parts of tobacco powder, 50 parts of tea fruit pulp, 10 parts of water, 1 part of adhesive, 11 parts of fuming agent, 2 parts of wood pulp and 1 part of animal fat, and stirring for 4 hours at the constant temperature of 40 ℃ to obtain thick pulp.
Example 8
This embodiment is substantially the same as embodiment 1, except that: the stirring temperature was too low.
Step S1, uniformly mixing 25 parts of tobacco powder, 50 parts of tea fruit pulp, 10 parts of water, 1 part of adhesive, 11 parts of fuming agent, 2 parts of wood pulp and 1 part of animal fat, and stirring for 4 hours at the constant temperature of 80 ℃ to obtain thick pulp.
Example 9
A heated cigarette sheet prepared by the steps of: in the preparation process, the raw materials are calculated in parts by mass.
Preparing fruit pulp: uniformly mixing 10 parts of propylene glycol with 90 parts of water to obtain a solvent; mixing 10 parts of apples and 80 parts of solvent, crushing, pulping and filtering to obtain fruit pulp.
Preparing tea fruit pulp: uniformly mixing 10 parts of propylene glycol with 90 parts of water to obtain a solvent; mixing 10 parts of tea fruits and 80 parts of solvent, crushing, pulping and filtering to obtain tea fruit pulp.
Preparing tobacco powder: uniformly mixing 20 parts of fresh cocoa pulp and 80 parts of tobacco leaves to obtain a mixture A; fermenting the mixture A at a constant temperature of 40 ℃ for 7 days; taking out the mixture A, putting the mixture A into an oven for baking at 110 ℃, and baking the mixture A until the moisture is 10%; then mixing 99 parts of the mixture A and 1 part of fruit pulp, and uniformly stirring to obtain a mixture B; putting the mixture B into an oven at 160 ℃ for continuously baking until the water content is 4%; and (5) crushing and screening the mixture B to obtain the smoke powder.
Preparation of a smoke agent: 10 parts of propylene glycol and 90 parts of glycerol are uniformly mixed to obtain the fuming agent.
The animal fat is lard. Guar gum is selected as the adhesive. Yang Mujiang is selected from wood pulp.
S1, uniformly mixing 60 parts of tobacco powder, 10 parts of tea fruit pulp, 40 parts of water, 5 parts of adhesive, 60 parts of fuming agent, 4 parts of wood pulp and 0.5 part of animal fat, and stirring for 4 hours at the constant temperature of 50 ℃ to obtain thick pulp.
S2, uniformly spraying thick slurry on a steel belt through a slit of a tape casting forming device, and drying a formed sheet until the water content is 7%; and stripping the dried sheet from the steel belt, wrapping, sealing and packaging.
Example 10
A heated cigarette sheet prepared by the steps of: in the preparation process, the raw materials are calculated in parts by mass.
Preparing fruit pulp: uniformly mixing 60 parts of propylene glycol with 40 parts of water to obtain a solvent; mixing 80 parts of Chinese date and 80 parts of solvent, crushing, pulping and filtering to obtain fruit pulp.
Preparing tea fruit pulp: uniformly mixing 60 parts of propylene glycol with 40 parts of water to obtain a solvent; mixing 80 parts of tea fruits and 80 parts of solvent, crushing, pulping and filtering to obtain tea fruit pulp.
Preparing tobacco powder: uniformly mixing 70 parts of fresh cocoa pulp and 30 parts of tobacco leaves to obtain a mixture A; fermenting the mixture A at the constant temperature of 50 ℃ for 7 days; taking out the mixture A, putting the mixture A into an oven for baking at 90 ℃, and baking the mixture A until the moisture is 20%; then mixing 10 parts of the mixture A and 30 parts of fruit pulp, and uniformly stirring to obtain a mixture B; placing the mixture B into an oven at 140 ℃ for continuously baking until the water content is 5%; and (5) crushing and screening the mixture B to obtain the smoke powder.
Preparation of a smoke agent: 60 parts of propylene glycol and 40 parts of glycerol are uniformly mixed to obtain the fuming agent.
The animal fat is lard. The adhesive is sodium carboxymethyl cellulose. The wood pulp is selected from Chinese alpine rush pulp.
S1, uniformly mixing 10 parts of tobacco powder, 60 parts of tea fruit pulp, 10 parts of water, 0.2 part of adhesive, 10 parts of fuming agent, 1 part of wood pulp and 1.8 parts of animal fat, and stirring for 4 hours at the constant temperature of 60 ℃ to obtain thick slurry.
S2, uniformly spraying thick slurry on a steel belt through a slit of a tape casting forming device, and drying a formed sheet until the water content is 12%; and stripping the dried sheet from the steel belt, wrapping, sealing and packaging.
Comparative example 1
This comparative example is substantially the same as example 1, except that: the tea fruit pulp is not used, and the tea fruit pulp is replaced by water with the same quality.
S1, uniformly mixing 25 parts of tobacco powder, 60 parts of water, 1 part of adhesive, 11 parts of fuming agent, 2 parts of wood pulp and 1 part of animal fat, and stirring for 4 hours at the constant temperature of 55 ℃ to obtain thick slurry.
S2, uniformly spraying thick slurry on a steel belt through a slit of a tape casting forming device, and drying a formed sheet until the water content is 9%; and stripping the dried sheet from the steel belt, wrapping, sealing and packaging.
Comparative example 2
This comparative example is substantially the same as example 1, except that: animal fat is not used, and the animal fat is replaced by water with equal mass.
S1, uniformly mixing 25 parts of tobacco powder, 50 parts of tea fruit pulp, 11 parts of water, 1 part of adhesive, 11 parts of fuming agent and 2 parts of wood pulp, and stirring for 4 hours at the constant temperature of 55 ℃ to obtain thick pulp.
S2, uniformly spraying thick slurry on a steel belt through a slit of a tape casting forming device, and drying a formed sheet until the water content is 9%; and stripping the dried sheet from the steel belt, wrapping, sealing and packaging.
Comparative example 3
This comparative example is substantially the same as example 1, except that: the tea fruit pulp and the animal fat are not used, and the tea fruit pulp and the animal fat are replaced by water with the same quality.
S1, uniformly mixing 25 parts of tobacco powder, 61 parts of water, 1 part of adhesive, 11 parts of fuming agent and 2 parts of wood pulp, and stirring for 4 hours at the constant temperature of 55 ℃ to obtain thick slurry.
S2, uniformly spraying thick slurry on a steel belt through a slit of a tape casting forming device, and drying a formed sheet until the water content is 9%; and stripping the dried sheet from the steel belt, wrapping, sealing and packaging.
[ Performance detection ]
The tensile strength of the sheets prepared in examples and comparative examples was measured according to the measurement method 6 in YC/T16-2014 reconstituted tobacco, and the measurement results are shown in Table 1 below.
The sheets prepared in examples and comparative examples were placed in the same environment, and the moisture was measured at different time periods, and the measurement results are shown in table 1 below.
Table 1.
As shown in table 1, it can be seen from the comparison of examples and comparative examples that the combination of tea fruit pulp and animal fat is effective in improving the tensile strength of the sheet and reducing the moisture absorption of the sheet. Meanwhile, it can be seen from a comparison of example 2 and examples 1 and 3 that although the moisture absorption of the sheet is improved with an increase in the amount of animal fat, an excessively high amount of animal fat affects the tensile strength of the sheet. By comparing example 1 with examples 4 and 5, it can be seen that co-baking the pulp with the fermented tobacco leaves also increases the tensile strength and reduces the moisture absorption to some extent. From a comparison of example 1 and example 6, it can be seen that coconut pulp has better moisture absorption resistance than ordinary fruit pulp. From a comparison of example 1 with examples 7 and 8, it can be seen that stirring also affects to some extent the formation of the thick stock emulsion and thus the properties of the flakes formed by the thick stock emulsion.
The specific embodiments described herein are offered by way of example only to illustrate the spirit of the invention. Those skilled in the art may make various modifications or additions to the described embodiments or substitutions thereof without departing from the spirit of the invention or exceeding the scope of the invention as defined in the accompanying claims.

Claims (7)

1. A heated cigarette sheet comprising water, adhesive, smoking agent, tobacco powder, wood pulp, characterized in that: the tea fruit pulp comprises tannin and tea saponin, and animal fat comprises glyceride;
the tea fruit pulp is prepared by the following steps: mixing 10-80 parts of tea fruits and 10-80 parts of solvent according to parts by mass, crushing, pulping and filtering to obtain tea fruit pulp;
according to the mass parts, the solvent comprises 10-60 parts of propylene glycol and 20-90 parts of water;
the tea fruit comprises an outer shell and tea seeds therein;
according to the mass parts, the heating cigarette slice comprises 10-60 parts of tobacco powder, 5-60 parts of tea fruit pulp, 10-40 parts of water, 0.2-5 parts of adhesive, 10-60 parts of fuming agent, 1-4 parts of wood pulp and 0.5-4 parts of animal fat;
the tobacco powder is prepared by baking a mixture of fruit pulp and fermented tobacco leaves at 140-160 ℃ and crushing; the tobacco powder comprises 10-99 parts of fermented tobacco leaves and 1-30 parts of fruit pulp.
2. A heated cigarette sheet as in claim 1 wherein: the amount of animal fat is 3-5wt% of the amount of the tea fruit pulp.
3. A heated cigarette sheet as in claim 1 wherein: the fermented tobacco leaves are mixed fermented products of tobacco leaves and cocoa pulp.
4. A heated cigarette sheet as in claim 1 wherein: the fruit pulp comprises coconut pulp.
5. A method of manufacturing a heated cigarette sheet according to any of claims 1-4, wherein: the method comprises the following steps:
s1, uniformly mixing smoke powder, tea fruit pulp, water, adhesive, smoke agent, wood pulp and animal fat according to parts by mass, and stirring at 50-60 ℃ to obtain thick pulp;
s2, uniformly spraying thick slurry on the steel belt through a slit of a tape casting forming device, forming and drying to obtain the sheet.
6. A method of manufacturing a heated cigarette sheet as in claim 5 wherein: drying to water content of 7-12% after molding to obtain sheet.
7. A method of manufacturing a heated cigarette sheet as in claim 5 wherein: the tobacco powder is prepared by the following steps: mixing cocoa pulp and tobacco leaf, and fermenting at 40-50deg.C; taking out the fermentation product, baking at 90-110 ℃ until the water content is 10-20%, and obtaining the fermented tobacco leaves; mixing the fermented tobacco leaves and the fruit pulp, baking at 140-160 ℃ until the water content is 4-7%, and then crushing and screening to obtain the tobacco powder.
CN202211253675.8A 2022-10-13 2022-10-13 Heated cigarette slice and manufacturing method thereof Active CN115553487B (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN202211253675.8A CN115553487B (en) 2022-10-13 2022-10-13 Heated cigarette slice and manufacturing method thereof

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN202211253675.8A CN115553487B (en) 2022-10-13 2022-10-13 Heated cigarette slice and manufacturing method thereof

Publications (2)

Publication Number Publication Date
CN115553487A CN115553487A (en) 2023-01-03
CN115553487B true CN115553487B (en) 2024-03-08

Family

ID=84745012

Family Applications (1)

Application Number Title Priority Date Filing Date
CN202211253675.8A Active CN115553487B (en) 2022-10-13 2022-10-13 Heated cigarette slice and manufacturing method thereof

Country Status (1)

Country Link
CN (1) CN115553487B (en)

Families Citing this family (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN115428976A (en) * 2022-10-11 2022-12-06 南通烟滤嘴有限责任公司 Coconut-flavored heating cigarette sheet and preparation method thereof

Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110946320A (en) * 2019-12-12 2020-04-03 河南卷烟工业烟草薄片有限公司 Damp-proof heating non-combustion reconstituted tobacco, preparation method and application
CN114098134A (en) * 2021-12-15 2022-03-01 云南中烟新材料科技有限公司 Heating cigarette core material and preparation method thereof

Patent Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110946320A (en) * 2019-12-12 2020-04-03 河南卷烟工业烟草薄片有限公司 Damp-proof heating non-combustion reconstituted tobacco, preparation method and application
CN114098134A (en) * 2021-12-15 2022-03-01 云南中烟新材料科技有限公司 Heating cigarette core material and preparation method thereof

Non-Patent Citations (3)

* Cited by examiner, † Cited by third party
Title
基于单甘油酯和茶皂苷的多相结构化油脂构建研究;杜李阳;中国优秀硕士学位论文全文数据库工程科技Ⅰ辑(第01期);摘要,第29-32页 *
江用文.中国茶产品加工.上海科学技术出版社,2011,(第1版),第440-443页. *
纤维素基活性包装材料的制备及性能研究;姬云忠;中国优秀硕士学位论文全文数据库工程科技Ⅰ辑(第09期);摘要,第23-24页,第26页 *

Also Published As

Publication number Publication date
CN115553487A (en) 2023-01-03

Similar Documents

Publication Publication Date Title
FI104459B (en) Tobacco item and tobacco element
JP3212271B2 (en) Manufacturing method of tobacco flavored articles
CN102697168B (en) Additive for boosting maillard reaction of recombined tobacco leaves and method for preparing tobacco leaves by using additive
US5046514A (en) Smoking material and process for making same
CA3129119A1 (en) Reconstituted cannabis material for generating aerosols
CN109527635B (en) A kind of technological method and application of improving burley tobacco quality
CN109619650A (en) It is a kind of to heat the reconstituted tobacoo and preparation method thereof that do not burn
CN110693072B (en) Flavoring matrix for cigarette cartridge and preparation method thereof
RU2313999C1 (en) Smoking mixture
CN109156882A (en) Improve process and its application that thick slurry method heats reconstituted tobacco quality of not burning
US3867951A (en) Tobacco substitute
CN115553487B (en) Heated cigarette slice and manufacturing method thereof
KR20180088846A (en) Structurally enhanced crop sheet and method of making
US6499490B1 (en) Method for producing a heat-irreversibly coagulated glucan sheet containing a leaf tobacco extract and method for producing a tobacco flavor-generating medium using a heat-irreversibly coagulated glucan sheet
CN104082850A (en) Method for manufacturing middle aroma type buccal cigarette
WO2019153885A1 (en) Cigarette smoke generating carrier for electric heating without burning and preparation method therefor
WO2025086962A1 (en) New tobacco product having nicotine puff-by-puff release uniformity, and preparation method for nicotine regulator, thick slurry and thin sheet thereof
CN108936790A (en) The preparation method and the purposes in tobacco product of a kind of solid spice
CN109393568B (en) A kind of burley tobacco extract for heat not burn cigarette and preparation method thereof
CN115053982B (en) Preparation method and application of cigar core tobacco leaf aroma-enhancing quality-improving alcoholization medium
CN116602436A (en) Reconstituted tobacco leaf and its preparation process and heat-not-burn tobacco products
CN110522072A (en) A preparation method of recombined stem core material for heat-not-burn cigarettes
AU2021104993A4 (en) Tobacco flavor and preparation method thereof
CN109619651A (en) A kind of reconstituted tobacoo and preparation method thereof
CN104910444B (en) A kind of papermaking-method reconstituted tobaccos humectant and its application process

Legal Events

Date Code Title Description
PB01 Publication
PB01 Publication
SE01 Entry into force of request for substantive examination
SE01 Entry into force of request for substantive examination
GR01 Patent grant
GR01 Patent grant