CN115553487B - Heated cigarette slice and manufacturing method thereof - Google Patents
Heated cigarette slice and manufacturing method thereof Download PDFInfo
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- CN115553487B CN115553487B CN202211253675.8A CN202211253675A CN115553487B CN 115553487 B CN115553487 B CN 115553487B CN 202211253675 A CN202211253675 A CN 202211253675A CN 115553487 B CN115553487 B CN 115553487B
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- 235000019504 cigarettes Nutrition 0.000 title claims abstract description 27
- 238000004519 manufacturing process Methods 0.000 title claims abstract description 10
- 235000013399 edible fruits Nutrition 0.000 claims abstract description 80
- 241000208125 Nicotiana Species 0.000 claims abstract description 71
- 235000002637 Nicotiana tabacum Nutrition 0.000 claims abstract description 71
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 52
- 235000019737 Animal fat Nutrition 0.000 claims abstract description 44
- 239000000843 powder Substances 0.000 claims abstract description 43
- 239000003795 chemical substances by application Substances 0.000 claims abstract description 29
- 229920001131 Pulp (paper) Polymers 0.000 claims abstract description 26
- 239000000853 adhesive Substances 0.000 claims abstract description 25
- 230000001070 adhesive effect Effects 0.000 claims abstract description 25
- 239000000779 smoke Substances 0.000 claims abstract description 22
- 238000010438 heat treatment Methods 0.000 claims abstract description 14
- 125000005456 glyceride group Chemical group 0.000 claims abstract description 13
- 239000001397 quillaja saponaria molina bark Substances 0.000 claims abstract description 12
- 229930182490 saponin Natural products 0.000 claims abstract description 12
- 150000007949 saponins Chemical class 0.000 claims abstract description 12
- 229920001864 tannin Polymers 0.000 claims abstract description 9
- 235000018553 tannin Nutrition 0.000 claims abstract description 9
- 239000001648 tannin Substances 0.000 claims abstract description 9
- 241001122767 Theaceae Species 0.000 claims description 63
- DNIAPMSPPWPWGF-UHFFFAOYSA-N Propylene glycol Chemical compound CC(O)CO DNIAPMSPPWPWGF-UHFFFAOYSA-N 0.000 claims description 51
- 238000002156 mixing Methods 0.000 claims description 39
- 239000000203 mixture Substances 0.000 claims description 38
- 239000002904 solvent Substances 0.000 claims description 26
- 238000003756 stirring Methods 0.000 claims description 18
- 239000002002 slurry Substances 0.000 claims description 16
- 229910000831 Steel Inorganic materials 0.000 claims description 14
- 239000010959 steel Substances 0.000 claims description 14
- 238000001035 drying Methods 0.000 claims description 12
- 244000299461 Theobroma cacao Species 0.000 claims description 10
- 235000009470 Theobroma cacao Nutrition 0.000 claims description 10
- 238000004537 pulping Methods 0.000 claims description 10
- 238000005507 spraying Methods 0.000 claims description 10
- 238000001914 filtration Methods 0.000 claims description 8
- 238000010345 tape casting Methods 0.000 claims description 8
- 244000060011 Cocos nucifera Species 0.000 claims description 7
- 235000013162 Cocos nucifera Nutrition 0.000 claims description 7
- 238000012216 screening Methods 0.000 claims description 7
- 238000000034 method Methods 0.000 claims description 6
- 238000000855 fermentation Methods 0.000 claims description 4
- 230000004151 fermentation Effects 0.000 claims description 4
- 238000000465 moulding Methods 0.000 claims description 2
- 230000000391 smoking effect Effects 0.000 claims description 2
- 238000010521 absorption reaction Methods 0.000 abstract description 15
- 239000002994 raw material Substances 0.000 abstract description 11
- 229920002678 cellulose Polymers 0.000 abstract description 4
- 239000001913 cellulose Substances 0.000 abstract description 4
- 235000019505 tobacco product Nutrition 0.000 abstract description 4
- 230000002195 synergetic effect Effects 0.000 abstract description 2
- 244000269722 Thea sinensis Species 0.000 abstract 5
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 description 15
- 230000000052 comparative effect Effects 0.000 description 9
- 239000000835 fiber Substances 0.000 description 8
- 238000002360 preparation method Methods 0.000 description 7
- 238000004806 packaging method and process Methods 0.000 description 6
- 239000000047 product Substances 0.000 description 6
- 238000007789 sealing Methods 0.000 description 6
- 241000196324 Embryophyta Species 0.000 description 5
- 238000005516 engineering process Methods 0.000 description 5
- 239000000463 material Substances 0.000 description 5
- 239000003921 oil Substances 0.000 description 5
- 235000019198 oils Nutrition 0.000 description 5
- 239000002245 particle Substances 0.000 description 5
- 244000070406 Malus silvestris Species 0.000 description 4
- 230000015572 biosynthetic process Effects 0.000 description 4
- IPCSVZSSVZVIGE-UHFFFAOYSA-N hexadecanoic acid Chemical compound CCCCCCCCCCCCCCCC(O)=O IPCSVZSSVZVIGE-UHFFFAOYSA-N 0.000 description 4
- 239000011162 core material Substances 0.000 description 3
- 239000000839 emulsion Substances 0.000 description 3
- 238000000605 extraction Methods 0.000 description 3
- 230000002209 hydrophobic effect Effects 0.000 description 3
- 125000001165 hydrophobic group Chemical group 0.000 description 3
- 239000003760 tallow Substances 0.000 description 3
- 229920002907 Guar gum Polymers 0.000 description 2
- 241001349804 Juncus alpinoarticulatus Species 0.000 description 2
- 235000021314 Palmitic acid Nutrition 0.000 description 2
- 244000126002 Ziziphus vulgaris Species 0.000 description 2
- DPXJVFZANSGRMM-UHFFFAOYSA-N acetic acid;2,3,4,5,6-pentahydroxyhexanal;sodium Chemical compound [Na].CC(O)=O.OCC(O)C(O)C(O)C(O)C=O DPXJVFZANSGRMM-UHFFFAOYSA-N 0.000 description 2
- 150000001413 amino acids Chemical class 0.000 description 2
- 235000021016 apples Nutrition 0.000 description 2
- 235000015278 beef Nutrition 0.000 description 2
- 239000001768 carboxy methyl cellulose Substances 0.000 description 2
- GHVNFZFCNZKVNT-UHFFFAOYSA-N decanoic acid Chemical compound CCCCCCCCCC(O)=O GHVNFZFCNZKVNT-UHFFFAOYSA-N 0.000 description 2
- POULHZVOKOAJMA-UHFFFAOYSA-N dodecanoic acid Chemical compound CCCCCCCCCCCC(O)=O POULHZVOKOAJMA-UHFFFAOYSA-N 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 238000009501 film coating Methods 0.000 description 2
- 239000007888 film coating Substances 0.000 description 2
- 239000000796 flavoring agent Substances 0.000 description 2
- 235000019634 flavors Nutrition 0.000 description 2
- HYBBIBNJHNGZAN-UHFFFAOYSA-N furfural Chemical compound O=CC1=CC=CO1 HYBBIBNJHNGZAN-UHFFFAOYSA-N 0.000 description 2
- 239000007789 gas Substances 0.000 description 2
- 239000000665 guar gum Substances 0.000 description 2
- 229960002154 guar gum Drugs 0.000 description 2
- 235000010417 guar gum Nutrition 0.000 description 2
- 239000003906 humectant Substances 0.000 description 2
- 239000001257 hydrogen Substances 0.000 description 2
- 229910052739 hydrogen Inorganic materials 0.000 description 2
- 238000005259 measurement Methods 0.000 description 2
- 235000013372 meat Nutrition 0.000 description 2
- 239000000693 micelle Substances 0.000 description 2
- WQEPLUUGTLDZJY-UHFFFAOYSA-N n-Pentadecanoic acid Natural products CCCCCCCCCCCCCCC(O)=O WQEPLUUGTLDZJY-UHFFFAOYSA-N 0.000 description 2
- 235000019476 oil-water mixture Nutrition 0.000 description 2
- 239000001814 pectin Substances 0.000 description 2
- 235000010987 pectin Nutrition 0.000 description 2
- 229920001277 pectin Polymers 0.000 description 2
- -1 saccharide compounds Chemical class 0.000 description 2
- 235000019812 sodium carboxymethyl cellulose Nutrition 0.000 description 2
- 229920001027 sodium carboxymethylcellulose Polymers 0.000 description 2
- 239000007787 solid Substances 0.000 description 2
- 239000000758 substrate Substances 0.000 description 2
- 235000015112 vegetable and seed oil Nutrition 0.000 description 2
- 239000008158 vegetable oil Substances 0.000 description 2
- WRIDQFICGBMAFQ-UHFFFAOYSA-N (E)-8-Octadecenoic acid Natural products CCCCCCCCCC=CCCCCCCC(O)=O WRIDQFICGBMAFQ-UHFFFAOYSA-N 0.000 description 1
- LQJBNNIYVWPHFW-UHFFFAOYSA-N 20:1omega9c fatty acid Natural products CCCCCCCCCCC=CCCCCCCCC(O)=O LQJBNNIYVWPHFW-UHFFFAOYSA-N 0.000 description 1
- QSBYPNXLFMSGKH-UHFFFAOYSA-N 9-Heptadecensaeure Natural products CCCCCCCC=CCCCCCCCC(O)=O QSBYPNXLFMSGKH-UHFFFAOYSA-N 0.000 description 1
- 108010005094 Advanced Glycation End Products Proteins 0.000 description 1
- 239000005632 Capric acid (CAS 334-48-5) Substances 0.000 description 1
- 229920001661 Chitosan Polymers 0.000 description 1
- 229920000858 Cyclodextrin Polymers 0.000 description 1
- 239000001116 FEMA 4028 Substances 0.000 description 1
- 229930091371 Fructose Natural products 0.000 description 1
- 239000005715 Fructose Substances 0.000 description 1
- RFSUNEUAIZKAJO-ARQDHWQXSA-N Fructose Chemical compound OC[C@H]1O[C@](O)(CO)[C@@H](O)[C@@H]1O RFSUNEUAIZKAJO-ARQDHWQXSA-N 0.000 description 1
- 241001397809 Hakea leucoptera Species 0.000 description 1
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 description 1
- 239000005639 Lauric acid Substances 0.000 description 1
- 239000005642 Oleic acid Substances 0.000 description 1
- ZQPPMHVWECSIRJ-UHFFFAOYSA-N Oleic acid Natural products CCCCCCCCC=CCCCCCCCC(O)=O ZQPPMHVWECSIRJ-UHFFFAOYSA-N 0.000 description 1
- 244000046052 Phaseolus vulgaris Species 0.000 description 1
- 235000010627 Phaseolus vulgaris Nutrition 0.000 description 1
- 235000021355 Stearic acid Nutrition 0.000 description 1
- 235000006545 Ziziphus mauritiana Nutrition 0.000 description 1
- 235000008529 Ziziphus vulgaris Nutrition 0.000 description 1
- 238000009825 accumulation Methods 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 238000007792 addition Methods 0.000 description 1
- 239000003463 adsorbent Substances 0.000 description 1
- 125000003172 aldehyde group Chemical group 0.000 description 1
- 150000001299 aldehydes Chemical class 0.000 description 1
- 229940058573 b-d glucose Drugs 0.000 description 1
- 230000006399 behavior Effects 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- WHGYBXFWUBPSRW-FOUAGVGXSA-N beta-cyclodextrin Chemical compound OC[C@H]([C@H]([C@@H]([C@H]1O)O)O[C@H]2O[C@@H]([C@@H](O[C@H]3O[C@H](CO)[C@H]([C@@H]([C@H]3O)O)O[C@H]3O[C@H](CO)[C@H]([C@@H]([C@H]3O)O)O[C@H]3O[C@H](CO)[C@H]([C@@H]([C@H]3O)O)O[C@H]3O[C@H](CO)[C@H]([C@@H]([C@H]3O)O)O3)[C@H](O)[C@H]2O)CO)O[C@@H]1O[C@H]1[C@H](O)[C@@H](O)[C@@H]3O[C@@H]1CO WHGYBXFWUBPSRW-FOUAGVGXSA-N 0.000 description 1
- 235000011175 beta-cyclodextrine Nutrition 0.000 description 1
- 229960004853 betadex Drugs 0.000 description 1
- 239000007844 bleaching agent Substances 0.000 description 1
- 238000006243 chemical reaction Methods 0.000 description 1
- 235000019864 coconut oil Nutrition 0.000 description 1
- 239000003240 coconut oil Substances 0.000 description 1
- 238000006482 condensation reaction Methods 0.000 description 1
- 239000013078 crystal Substances 0.000 description 1
- 230000007547 defect Effects 0.000 description 1
- 238000001514 detection method Methods 0.000 description 1
- 235000014113 dietary fatty acids Nutrition 0.000 description 1
- 238000004945 emulsification Methods 0.000 description 1
- 239000000194 fatty acid Substances 0.000 description 1
- 229930195729 fatty acid Natural products 0.000 description 1
- 150000004665 fatty acids Chemical class 0.000 description 1
- 239000003205 fragrance Substances 0.000 description 1
- 235000021588 free fatty acids Nutrition 0.000 description 1
- 238000007710 freezing Methods 0.000 description 1
- 230000008014 freezing Effects 0.000 description 1
- 239000002316 fumigant Substances 0.000 description 1
- 239000003292 glue Substances 0.000 description 1
- 125000002887 hydroxy group Chemical group [H]O* 0.000 description 1
- 230000007794 irritation Effects 0.000 description 1
- QXJSBBXBKPUZAA-UHFFFAOYSA-N isooleic acid Natural products CCCCCCCC=CCCCCCCCCC(O)=O QXJSBBXBKPUZAA-UHFFFAOYSA-N 0.000 description 1
- 230000007774 longterm Effects 0.000 description 1
- 238000000691 measurement method Methods 0.000 description 1
- 239000012528 membrane Substances 0.000 description 1
- 235000013336 milk Nutrition 0.000 description 1
- 239000008267 milk Substances 0.000 description 1
- 210000004080 milk Anatomy 0.000 description 1
- 239000012046 mixed solvent Substances 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 231100000252 nontoxic Toxicity 0.000 description 1
- 230000003000 nontoxic effect Effects 0.000 description 1
- QIQXTHQIDYTFRH-UHFFFAOYSA-N octadecanoic acid Chemical compound CCCCCCCCCCCCCCCCCC(O)=O QIQXTHQIDYTFRH-UHFFFAOYSA-N 0.000 description 1
- OQCDKBAXFALNLD-UHFFFAOYSA-N octadecanoic acid Natural products CCCCCCCC(C)CCCCCCCCC(O)=O OQCDKBAXFALNLD-UHFFFAOYSA-N 0.000 description 1
- ZQPPMHVWECSIRJ-KTKRTIGZSA-N oleic acid Chemical compound CCCCCCCC\C=C/CCCCCCCC(O)=O ZQPPMHVWECSIRJ-KTKRTIGZSA-N 0.000 description 1
- 235000021313 oleic acid Nutrition 0.000 description 1
- 239000002304 perfume Substances 0.000 description 1
- 238000004321 preservation Methods 0.000 description 1
- 238000010298 pulverizing process Methods 0.000 description 1
- 230000001105 regulatory effect Effects 0.000 description 1
- 238000005096 rolling process Methods 0.000 description 1
- 238000001338 self-assembly Methods 0.000 description 1
- 238000004513 sizing Methods 0.000 description 1
- 239000008117 stearic acid Substances 0.000 description 1
- 238000006467 substitution reaction Methods 0.000 description 1
- 150000005846 sugar alcohols Polymers 0.000 description 1
- 150000003626 triacylglycerols Chemical class 0.000 description 1
- 239000002569 water oil cream Substances 0.000 description 1
- 239000002023 wood Substances 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B3/00—Preparing tobacco in the factory
- A24B3/14—Forming reconstituted tobacco products, e.g. wrapper materials, sheets, imitation leaves, rods, cakes; Forms of such products
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
Landscapes
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Manufacture Of Tobacco Products (AREA)
Abstract
The invention relates to the technical field of heating non-combustible tobacco products, in particular to a heating cigarette sheet and a manufacturing method thereof. The heated cigarette slice comprises water, an adhesive, a smoke agent, tobacco powder, wood pulp, tea fruit pulp and animal fat, wherein the tea fruit pulp comprises tannin and tea saponin, and the animal fat comprises glyceride. The tea fruit pulp and animal fat are added in the sheet raw material, and the moisture absorption problem of the sheet is effectively improved and the tensile strength of the sheet is improved through the synergistic effect among cellulose, tannin, tea saponin and glyceride.
Description
Technical Field
The invention relates to the technical field of heating non-combustible tobacco products, in particular to a heating cigarette sheet and a manufacturing method thereof.
Background
The heating non-burning tobacco product is a new-type product combining heating appliance and cigarette bullet, it is a "low-temp. cigarette" designed by using "heating only and non-burning" as thought, and utilizes special-purpose heating device to heat the treated cut tobacco and cigarette bullet to a certain temp., and heat the cigarette bullet to a degree sufficient for giving out smoke gas for smoking.
The cartridges of the heated non-combustible tobacco products are mainly divided into two types, namely a particle technology and a sheet technology. The particle technology has the advantages that the residues are some dry carbonized particles after the heating core is heated, so that the particles can be removed easily, but the particle technology has the defects of uneven heating, small smoke quantity, easy generation of burnt smell, inconsistent front and rear smoke quantity and incapability of keeping the fragrance of cigarettes. The sheet technology is that the herbal plant or tobacco-like component is crushed and mixed with natural fiber, and then added with adhesive and the like to be uniformly stirred, and the sheet product is prepared after constant-pressure drying. But the disadvantage is that the thin sheet is easy to absorb moisture, which affects the adaptability of the machine.
In order to solve the moisture absorption problem of the sheet, a moisture-proof layer is generally formed on the surface of the sheet in the prior art, such as a moisture-proof humectant disclosed in patent document with publication number CN113907409a for preventing moisture absorption of the tobacco sheet, and is characterized by comprising polyalcohol, beta-cyclodextrin and polyglucosamine (1-4) -2-amino-B-D glucose, and moisture absorption of the sheet is prevented by spraying the moisture-proof humectant. Another example of such a heated cigarette core material is disclosed in the publication CN114009826a and a method of making the same, comprising the steps of: pretreatment of a fuming agent, configuration of perfume, pretreatment of sizing material, preparation of substrate slurry, treatment of powder material, forming of a substrate, powder spraying, rolling of a sheet, film coating and drying forming. The porous solid adsorbent is added into the smoke agent, and the smoke agent is mixed with the glue system to be embedded in the base material slurry, so that the moisture absorption problem of the prepared smoke core material can be effectively solved by matching with the film coating process.
In the scheme, on one hand, the moisture-proof layer has the problem of easy falling off, and the long-term preservation effect of the thin sheet is affected; on the other hand, the sheet itself has the problem of low tensile strength, and the material used for the moisture-proof layer does not positively influence the tensile strength of the sheet.
Disclosure of Invention
The present invention has been made to solve the above problems, and provides a heated cigarette sheet and a method for manufacturing the same.
The technical scheme for solving the problems is that the invention firstly provides a heating cigarette slice which comprises water, an adhesive, a smoke agent, tobacco powder, wood pulp, tea fruit pulp and animal fat, wherein the tea fruit pulp comprises tannin and tea saponin, and the animal fat comprises glyceride.
Wherein water, adhesive, smoke agent, tobacco powder and wood pulp are common components of the flake.
The fuming agent is used for atomizing and generating smoke when heating, and common fuming agents such as propylene glycol and glycerol are selected. Preferably, the smoke generating agent comprises 10-60 parts by mass of propylene glycol and 40-90 parts by mass of glycerol.
The wood pulp is mainly used for providing supporting fibers for the thin sheet and ensuring the basic strength of the thin sheet, and is generally prepared by chemically pulping and physically pulping plant raw materials, wherein the plant raw materials can be woody plants such as needle wood, broad-leaved wood and the like, can also be herbaceous plants such as Chinese alpine rush, tobacco stems and the like, and can be directly purchased in the market.
The tobacco powder is used for providing traditional cigarette aroma for the thin sheet and also providing a certain amount of supporting fiber, and is usually prepared by directly fermenting tobacco leaves and then freezing and crushing the tobacco leaves.
The adhesive is used for combining the solid components, is preferably a nontoxic and non-pungent odor adhesive, and as a preferable mode of the invention, the adhesive comprises one or more of guar gum, chitosan, sodium carboxymethyl cellulose and pectin.
Water is generally used to dilute the above components for subsequent sheeting.
In order to solve the moisture absorption problem and the low tensile strength problem of the thin sheet, tea fruit pulp and animal fat are creatively added into the thin sheet raw material.
The tea fruit pulp is mainly prepared by extracting tea fruits under the condition of a solvent, wherein the tea fruits comprise outer shells and tea seeds therein, the shells contain higher-content tannin, and the tea seeds contain higher-content tea saponin and vegetable oil. The solvent for extracting the tea fruits is not limited, and as the preferable choice of the invention, a mixed solvent of propylene glycol and water is selected. The ratio of the propylene glycol to the water is not limited, and the solvent preferably includes 10 to 60 parts by mass of propylene glycol and 20 to 90 parts by mass of water. The ratio of the amount of the tea fruit to the amount of the solvent is not limited, and in order to improve the extraction yield, it is preferable to mix 10 to 80 parts by mass of the tea fruit and 10 to 80 parts by mass of the solvent at the time of extraction.
The main components of animal fat are triglycerides of palmitic acid and stearic acid. Preferably, the animal fat comprises one or more of lard, beef tallow and mutton tallow.
When the tea fruit pulp and the animal fat are mixed for use, first, the tea fruit pulp and the animal fat can respectively act: tea fruit pulp: the wood pulp cellulose is subjected to condensation reaction with active hydrogen on tannin molecules through aldehyde groups (bleaching agents used in the process of preparing the wood pulp oxidize cellulose hydroxyl groups into aldehyde, general acid groups and the like), and the tannin is anchored on the fibers through covalent bonds, so that a hydrogen bond connection structure between the cellulose is replaced, the hydrophobicity of the sheet is improved, moisture absorption is avoided, and the bonding strength between the fibers, namely the tensile strength of the sheet is improved to a certain extent; the vegetable oil can form a layer of hydrophobic film on the surface of the flake through the hydrophobic group, so that the hydrophobic property is improved to realize moisture resistance, and the internal stress of the flake can be improved to increase the tensile strength of the flake. Animal fat: the hydrophobic property is also improved by the hydrophobic group, and the internal stress is improved.
Second, tea fruit pulp and animal fat may act synergistically: because of the existence of water and animal fat, before the sheet is formed, the slurry obtained by mixing all the raw materials is an oil-water mixture, and the tea saponin has good interfacial activity, can help the emulsification of the oil-water mixture, improves the uniformity of the slurry, and improves the moisture-proof uniformity of the sheet. Meanwhile, the tea saponin can also self-assemble to form micelles, the micelles form ordered fibrous aggregates in an oil-water interface in a self-assembly way, and as the tea saponin molecules are adsorbed perpendicular to the interface, the tea saponin has extremely high elastic modulus and viscosity, shows viscoelastic behavior, and improves the tensile strength of the thin sheet through the viscoelasticity. And glyceride is also an amphipathic molecule, glyceride in the oil phase tends to be adsorbed on the surface of oil drops, and at a certain concentration, glyceride crystals can pierce the fiber interface film of the tea saponin and enter the water phase, at the moment, glyceride part participates in interface formation, the glyceride and the tea saponin cooperatively reduce interfacial tension, formed emulsion drops are smaller, the accumulation is tighter, the strength of the constructed three-dimensional network structure is larger, and therefore the mechanical property is improved.
In the process, the ratio of the tea fruit pulp to the animal fat has a certain influence on the final hydrophobicity and tensile strength, and the excessive use of the animal fat and the excessive use of glyceride can influence the viscoelasticity of the fiber interface film and the tensile strength of the thin sheet; animal fat and oil are too low in dosage, so that the dosage of glyceride is too low, on one hand, the hydrophobicity is insufficient, and on the other hand, the glyceride is insufficient to pierce the fiber interface membrane, and the synergistic effect of the glyceride and the tea saponin is affected. Preferably, the animal fat is used in an amount of 3-5wt% of the tea fruit pulp.
The content of other raw materials also has a certain influence, and the preferred part of the invention is that the heating cigarette slice comprises 10-60 parts of tobacco powder, 5-60 parts of tea fruit pulp, 10-40 parts of water, 0.2-5 parts of adhesive, 10-60 parts of fumigant, 1-4 parts of wood pulp and 0.5-4 parts of animal fat.
In order to further improve the moisture absorption problem and the tensile strength of the sheet, the tobacco powder is preferably prepared by baking a mixture of pulp and fermented tobacco leaves at 140-160 ℃ and pulverizing.
The traditional tobacco powder only comprises tobacco leaves after fermentation, and fruit pulp is added for co-baking. The fruit pulp is mainly prepared by extracting fruit raw materials under the condition of a solvent, and contains saccharide compounds such as fructose and the like. The method can reduce harmful components in tobacco leaves by fermenting the tobacco leaves, and can obtain amino acid by fermenting. The amino acid can generate Maillard reaction with the saccharide compound at a certain temperature, so that the aroma of the flake is further improved, and the miscellaneous gas and the irritation are reduced; and the obtained product comprises furfural, can be covalently condensed with tannin in tea fruit pulp, improves the hydrophobicity and tensile strength of the flake, and has better compatibility of tobacco powder and wood pulp under the intermediate action of tannin.
In view of the formation amount of Maillard reaction products, as a preferred aspect of the present invention, the tobacco powder comprises 10-99 parts by mass of fermented tobacco leaves and 1-30 parts by mass of fruit pulp.
The pulp may be a solvent extract of any fruit material, such as apple pulp, jujube pulp, coconut pulp, etc., and preferably, coconut pulp is used in the present invention. Because the oil content of coconut meat is 35%, the oil is rich in capric acid, palmitic acid, lauric acid, oleic acid, fatty acid and free fatty acid, and the moisture absorption problem of the slice can be further improved by utilizing the hydrophobic group in the coconut oil. The solvent for extracting the fruit pulp is not limited, and preferably comprises 10-50 parts by mass of propylene glycol and 30-80 parts by mass of water. The ratio of the fruit to the solvent is not limited, and preferably, the fruit is mixed with 10 to 60 parts by mass and 20 to 90 parts by mass of the solvent during extraction.
The fermented tobacco leaves can be the product of fermenting fresh tobacco leaves in any mode, and are mixed fermentation products of tobacco leaves and cocoa pulp as the preferable mode of the invention. The color of the tobacco leaves can be regulated by fermenting the tobacco leaves and the cocoa pulp together, so that the milk flavor and the bean flavor of the tobacco leaves are improved. Preferably, 10-80 parts of cocoa pulp and 30-90 parts of tobacco leaf are mixed and fermented according to parts by mass.
It is yet another object of the present application to provide a method of manufacturing a heated cigarette sheet comprising the steps of:
s1, uniformly mixing smoke powder, tea fruit pulp, water, adhesive, smoke agent, wood pulp and animal fat according to parts by mass, and stirring at 50-60 ℃ to obtain thick pulp;
s2, uniformly spraying thick slurry on the steel belt through a slit of a tape casting forming device, forming and drying to obtain the sheet.
In the application, thick slurry is prepared by stirring at a specific temperature range of 50-60 ℃ so as to promote the stable formation of the oil-water emulsion, thereby ensuring the subsequent hydrophobicity and tensile strength.
The flakes themselves need to have a moisture content to avoid excessive drying of the flakes and to be brittle, and preferably according to the invention, the flakes are dried to a moisture content of 7-12% after molding.
As a preferred aspect of the present invention, the tobacco powder is prepared by: mixing fresh cocoa pulp and tobacco leaf, and fermenting at 40-50deg.C; taking out the fermentation product, baking at 90-110 ℃ until the water content is 10-20%, and obtaining the fermented tobacco leaves; mixing the fermented tobacco leaves and the pulp, baking at 140-160 ℃ until the water content is 4-7%, and then crushing and screening to obtain the tobacco powder.
The invention has the beneficial effects that:
1. in the application, by adding tea fruit pulp and animal fat into the sheet raw material, the moisture absorption problem of the sheet is effectively improved, and the tensile strength of the sheet is improved.
2. In this application, through the modified tradition tobacco powder of fruit pulp, can also cooperate the use of tea fruit pulp in order to further improve the slice moisture absorption problem and improve tensile strength when improving the suction taste of thin slice, can also improve the compatibility of tobacco powder and wood pulp in addition.
Detailed Description
The following is a specific embodiment of the present invention and further describes the technical solution of the present invention, but the present invention is not limited to these examples.
Example 1
A heated cigarette sheet prepared by the steps of: in the preparation process, the raw materials are calculated in parts by mass.
Preparing fruit pulp: uniformly mixing 20 parts of propylene glycol with 80 parts of water to obtain a solvent; mixing 20 parts of coconut meat and 80 parts of solvent, crushing, pulping and filtering to obtain fruit pulp.
Preparing tea fruit pulp: uniformly mixing 20 parts of propylene glycol with 80 parts of water to obtain a solvent; mixing 20 parts of tea fruits and 80 parts of solvent, crushing, pulping and filtering to obtain tea fruit pulp.
Preparing tobacco powder: uniformly mixing 30 parts of fresh cocoa pulp and 70 parts of tobacco leaves to obtain a mixture A; fermenting the mixture A at a constant temperature of 45 ℃ for 7 days; taking out the mixture A, putting the mixture A into a baking oven for baking at 100 ℃, and baking the mixture A until the moisture is 16%; then mixing 90 parts of the mixture A and 5 parts of fruit pulp, and uniformly stirring to obtain a mixture B; placing the mixture B into an oven at 145 ℃ for continuously baking until the water content is 7%; and (5) crushing and screening the mixture B to obtain the smoke powder.
Preparation of a smoke agent: and uniformly mixing 30 parts of propylene glycol and 70 parts of glycerol to obtain the fuming agent.
The animal fat is beef tallow. Pectin is used as the adhesive. Yang Mujiang is selected from wood pulp.
S1, uniformly mixing 25 parts of tobacco powder, 50 parts of tea fruit pulp, 10 parts of water, 1 part of adhesive, 11 parts of fuming agent, 2 parts of wood pulp and 1 part of animal fat, and stirring for 4 hours at the constant temperature of 55 ℃ to obtain thick pulp.
S2, uniformly spraying thick slurry on a steel belt through a slit of a tape casting forming device, and drying a formed sheet until the water content is 9%; and stripping the dried sheet from the steel belt, wrapping, sealing and packaging.
Example 2
This embodiment is substantially the same as embodiment 1, except that: increasing the dosage of animal fat.
In the step S1, 25 parts of tobacco powder, 50 parts of tea fruit pulp, 10 parts of water, 1 part of adhesive, 11 parts of fuming agent, 2 parts of wood pulp and 2 parts of animal fat are uniformly mixed, and then stirred for 4 hours at the constant temperature of 55 ℃ to obtain thick pulp.
Example 3
This embodiment is substantially the same as embodiment 1, except that: the dosage of animal fat is greatly increased.
In the step S1, 25 parts of tobacco powder, 50 parts of tea fruit pulp, 10 parts of water, 1 part of adhesive, 11 parts of fuming agent, 2 parts of wood pulp and 4 parts of animal fat are uniformly mixed, and then stirred for 4 hours at the constant temperature of 55 ℃ to obtain thick pulp.
Example 4
This embodiment is substantially the same as embodiment 1, except that: no fruit pulp is used.
Preparing tobacco powder: uniformly mixing 30 parts of fresh cocoa pulp and 70 parts of tobacco leaves to obtain a mixture A; fermenting the mixture A at a constant temperature of 45 ℃ for 7 days; taking out the mixture A, putting the mixture A into a baking oven for baking at 100 ℃, and baking the mixture A until the moisture is 16%; then, putting 90 parts of the mixture A into an oven at 145 ℃ to be continuously baked until the moisture is 7%, and finally crushing and screening to obtain the tobacco powder.
Example 5
This embodiment is substantially the same as embodiment 1, except that: the tobacco leaves are not fermented.
Preparing tobacco powder: 100 parts of tobacco leaves are put into an oven for baking at 100 ℃ until the moisture is 16%; then mixing 90 parts of tobacco leaves and 5 parts of fruit pulp, and uniformly stirring to obtain a mixture B; placing the mixture B into an oven at 145 ℃ for continuously baking until the water content is 7%; and (5) crushing and screening the mixture B to obtain the smoke powder.
Example 6
This embodiment is substantially the same as embodiment 1, except that: the pulp is replaced by pulp of coconut pulp and apple pulp.
Preparing fruit pulp: uniformly mixing 20 parts of propylene glycol with 80 parts of water to obtain a solvent; mixing 20 parts of apples and 80 parts of solvent, crushing, pulping and filtering to obtain fruit pulp.
Example 7
This embodiment is substantially the same as embodiment 1, except that: the stirring temperature was too high.
Step S1, uniformly mixing 25 parts of tobacco powder, 50 parts of tea fruit pulp, 10 parts of water, 1 part of adhesive, 11 parts of fuming agent, 2 parts of wood pulp and 1 part of animal fat, and stirring for 4 hours at the constant temperature of 40 ℃ to obtain thick pulp.
Example 8
This embodiment is substantially the same as embodiment 1, except that: the stirring temperature was too low.
Step S1, uniformly mixing 25 parts of tobacco powder, 50 parts of tea fruit pulp, 10 parts of water, 1 part of adhesive, 11 parts of fuming agent, 2 parts of wood pulp and 1 part of animal fat, and stirring for 4 hours at the constant temperature of 80 ℃ to obtain thick pulp.
Example 9
A heated cigarette sheet prepared by the steps of: in the preparation process, the raw materials are calculated in parts by mass.
Preparing fruit pulp: uniformly mixing 10 parts of propylene glycol with 90 parts of water to obtain a solvent; mixing 10 parts of apples and 80 parts of solvent, crushing, pulping and filtering to obtain fruit pulp.
Preparing tea fruit pulp: uniformly mixing 10 parts of propylene glycol with 90 parts of water to obtain a solvent; mixing 10 parts of tea fruits and 80 parts of solvent, crushing, pulping and filtering to obtain tea fruit pulp.
Preparing tobacco powder: uniformly mixing 20 parts of fresh cocoa pulp and 80 parts of tobacco leaves to obtain a mixture A; fermenting the mixture A at a constant temperature of 40 ℃ for 7 days; taking out the mixture A, putting the mixture A into an oven for baking at 110 ℃, and baking the mixture A until the moisture is 10%; then mixing 99 parts of the mixture A and 1 part of fruit pulp, and uniformly stirring to obtain a mixture B; putting the mixture B into an oven at 160 ℃ for continuously baking until the water content is 4%; and (5) crushing and screening the mixture B to obtain the smoke powder.
Preparation of a smoke agent: 10 parts of propylene glycol and 90 parts of glycerol are uniformly mixed to obtain the fuming agent.
The animal fat is lard. Guar gum is selected as the adhesive. Yang Mujiang is selected from wood pulp.
S1, uniformly mixing 60 parts of tobacco powder, 10 parts of tea fruit pulp, 40 parts of water, 5 parts of adhesive, 60 parts of fuming agent, 4 parts of wood pulp and 0.5 part of animal fat, and stirring for 4 hours at the constant temperature of 50 ℃ to obtain thick pulp.
S2, uniformly spraying thick slurry on a steel belt through a slit of a tape casting forming device, and drying a formed sheet until the water content is 7%; and stripping the dried sheet from the steel belt, wrapping, sealing and packaging.
Example 10
A heated cigarette sheet prepared by the steps of: in the preparation process, the raw materials are calculated in parts by mass.
Preparing fruit pulp: uniformly mixing 60 parts of propylene glycol with 40 parts of water to obtain a solvent; mixing 80 parts of Chinese date and 80 parts of solvent, crushing, pulping and filtering to obtain fruit pulp.
Preparing tea fruit pulp: uniformly mixing 60 parts of propylene glycol with 40 parts of water to obtain a solvent; mixing 80 parts of tea fruits and 80 parts of solvent, crushing, pulping and filtering to obtain tea fruit pulp.
Preparing tobacco powder: uniformly mixing 70 parts of fresh cocoa pulp and 30 parts of tobacco leaves to obtain a mixture A; fermenting the mixture A at the constant temperature of 50 ℃ for 7 days; taking out the mixture A, putting the mixture A into an oven for baking at 90 ℃, and baking the mixture A until the moisture is 20%; then mixing 10 parts of the mixture A and 30 parts of fruit pulp, and uniformly stirring to obtain a mixture B; placing the mixture B into an oven at 140 ℃ for continuously baking until the water content is 5%; and (5) crushing and screening the mixture B to obtain the smoke powder.
Preparation of a smoke agent: 60 parts of propylene glycol and 40 parts of glycerol are uniformly mixed to obtain the fuming agent.
The animal fat is lard. The adhesive is sodium carboxymethyl cellulose. The wood pulp is selected from Chinese alpine rush pulp.
S1, uniformly mixing 10 parts of tobacco powder, 60 parts of tea fruit pulp, 10 parts of water, 0.2 part of adhesive, 10 parts of fuming agent, 1 part of wood pulp and 1.8 parts of animal fat, and stirring for 4 hours at the constant temperature of 60 ℃ to obtain thick slurry.
S2, uniformly spraying thick slurry on a steel belt through a slit of a tape casting forming device, and drying a formed sheet until the water content is 12%; and stripping the dried sheet from the steel belt, wrapping, sealing and packaging.
Comparative example 1
This comparative example is substantially the same as example 1, except that: the tea fruit pulp is not used, and the tea fruit pulp is replaced by water with the same quality.
S1, uniformly mixing 25 parts of tobacco powder, 60 parts of water, 1 part of adhesive, 11 parts of fuming agent, 2 parts of wood pulp and 1 part of animal fat, and stirring for 4 hours at the constant temperature of 55 ℃ to obtain thick slurry.
S2, uniformly spraying thick slurry on a steel belt through a slit of a tape casting forming device, and drying a formed sheet until the water content is 9%; and stripping the dried sheet from the steel belt, wrapping, sealing and packaging.
Comparative example 2
This comparative example is substantially the same as example 1, except that: animal fat is not used, and the animal fat is replaced by water with equal mass.
S1, uniformly mixing 25 parts of tobacco powder, 50 parts of tea fruit pulp, 11 parts of water, 1 part of adhesive, 11 parts of fuming agent and 2 parts of wood pulp, and stirring for 4 hours at the constant temperature of 55 ℃ to obtain thick pulp.
S2, uniformly spraying thick slurry on a steel belt through a slit of a tape casting forming device, and drying a formed sheet until the water content is 9%; and stripping the dried sheet from the steel belt, wrapping, sealing and packaging.
Comparative example 3
This comparative example is substantially the same as example 1, except that: the tea fruit pulp and the animal fat are not used, and the tea fruit pulp and the animal fat are replaced by water with the same quality.
S1, uniformly mixing 25 parts of tobacco powder, 61 parts of water, 1 part of adhesive, 11 parts of fuming agent and 2 parts of wood pulp, and stirring for 4 hours at the constant temperature of 55 ℃ to obtain thick slurry.
S2, uniformly spraying thick slurry on a steel belt through a slit of a tape casting forming device, and drying a formed sheet until the water content is 9%; and stripping the dried sheet from the steel belt, wrapping, sealing and packaging.
[ Performance detection ]
The tensile strength of the sheets prepared in examples and comparative examples was measured according to the measurement method 6 in YC/T16-2014 reconstituted tobacco, and the measurement results are shown in Table 1 below.
The sheets prepared in examples and comparative examples were placed in the same environment, and the moisture was measured at different time periods, and the measurement results are shown in table 1 below.
Table 1.
As shown in table 1, it can be seen from the comparison of examples and comparative examples that the combination of tea fruit pulp and animal fat is effective in improving the tensile strength of the sheet and reducing the moisture absorption of the sheet. Meanwhile, it can be seen from a comparison of example 2 and examples 1 and 3 that although the moisture absorption of the sheet is improved with an increase in the amount of animal fat, an excessively high amount of animal fat affects the tensile strength of the sheet. By comparing example 1 with examples 4 and 5, it can be seen that co-baking the pulp with the fermented tobacco leaves also increases the tensile strength and reduces the moisture absorption to some extent. From a comparison of example 1 and example 6, it can be seen that coconut pulp has better moisture absorption resistance than ordinary fruit pulp. From a comparison of example 1 with examples 7 and 8, it can be seen that stirring also affects to some extent the formation of the thick stock emulsion and thus the properties of the flakes formed by the thick stock emulsion.
The specific embodiments described herein are offered by way of example only to illustrate the spirit of the invention. Those skilled in the art may make various modifications or additions to the described embodiments or substitutions thereof without departing from the spirit of the invention or exceeding the scope of the invention as defined in the accompanying claims.
Claims (7)
1. A heated cigarette sheet comprising water, adhesive, smoking agent, tobacco powder, wood pulp, characterized in that: the tea fruit pulp comprises tannin and tea saponin, and animal fat comprises glyceride;
the tea fruit pulp is prepared by the following steps: mixing 10-80 parts of tea fruits and 10-80 parts of solvent according to parts by mass, crushing, pulping and filtering to obtain tea fruit pulp;
according to the mass parts, the solvent comprises 10-60 parts of propylene glycol and 20-90 parts of water;
the tea fruit comprises an outer shell and tea seeds therein;
according to the mass parts, the heating cigarette slice comprises 10-60 parts of tobacco powder, 5-60 parts of tea fruit pulp, 10-40 parts of water, 0.2-5 parts of adhesive, 10-60 parts of fuming agent, 1-4 parts of wood pulp and 0.5-4 parts of animal fat;
the tobacco powder is prepared by baking a mixture of fruit pulp and fermented tobacco leaves at 140-160 ℃ and crushing; the tobacco powder comprises 10-99 parts of fermented tobacco leaves and 1-30 parts of fruit pulp.
2. A heated cigarette sheet as in claim 1 wherein: the amount of animal fat is 3-5wt% of the amount of the tea fruit pulp.
3. A heated cigarette sheet as in claim 1 wherein: the fermented tobacco leaves are mixed fermented products of tobacco leaves and cocoa pulp.
4. A heated cigarette sheet as in claim 1 wherein: the fruit pulp comprises coconut pulp.
5. A method of manufacturing a heated cigarette sheet according to any of claims 1-4, wherein: the method comprises the following steps:
s1, uniformly mixing smoke powder, tea fruit pulp, water, adhesive, smoke agent, wood pulp and animal fat according to parts by mass, and stirring at 50-60 ℃ to obtain thick pulp;
s2, uniformly spraying thick slurry on the steel belt through a slit of a tape casting forming device, forming and drying to obtain the sheet.
6. A method of manufacturing a heated cigarette sheet as in claim 5 wherein: drying to water content of 7-12% after molding to obtain sheet.
7. A method of manufacturing a heated cigarette sheet as in claim 5 wherein: the tobacco powder is prepared by the following steps: mixing cocoa pulp and tobacco leaf, and fermenting at 40-50deg.C; taking out the fermentation product, baking at 90-110 ℃ until the water content is 10-20%, and obtaining the fermented tobacco leaves; mixing the fermented tobacco leaves and the fruit pulp, baking at 140-160 ℃ until the water content is 4-7%, and then crushing and screening to obtain the tobacco powder.
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CN114098134A (en) * | 2021-12-15 | 2022-03-01 | 云南中烟新材料科技有限公司 | Heating cigarette core material and preparation method thereof |
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CN110946320A (en) * | 2019-12-12 | 2020-04-03 | 河南卷烟工业烟草薄片有限公司 | Damp-proof heating non-combustion reconstituted tobacco, preparation method and application |
CN114098134A (en) * | 2021-12-15 | 2022-03-01 | 云南中烟新材料科技有限公司 | Heating cigarette core material and preparation method thereof |
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