CN115317412A - Oil-control itching-relieving anti-dandruff shampoo and preparation method thereof - Google Patents
Oil-control itching-relieving anti-dandruff shampoo and preparation method thereof Download PDFInfo
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Abstract
The invention relates to the field of cosmetic manufacture, and relates to A61Q5/00; the invention discloses an oil-control itching-relieving anti-dandruff traditional Chinese medicine shampoo which comprises the following raw materials in percentage by weight: 6-43% of surfactant, 0.06-7% of conditioner, 5-25% of traditional Chinese medicine liquid, pH regulator and the balance of water to 100%; wherein the Chinese medicinal liquid is prepared from at least one of cortex Mori, folium Platycladi, radix Polygoni Multiflori Preparata, radix Sophorae Flavescentis, rhizoma Zingiberis recens, radix Stemonae, fructus Cnidii, and herba Menthae. The shampoo has good effects of controlling oil, removing dandruff and relieving itching, the recurrence rate is obviously lower than that of a control group, and adverse reactions do not occur after long-term use.
Description
Technical Field
The invention relates to the field of cosmetic manufacture, and relates to A61Q5/00; in particular to a traditional Chinese medicine shampoo for controlling oil, relieving itching and removing dandruff and a preparation method thereof.
Background
The seborrheic dermatitis of the scalp is a common and frequent disease, the main symptoms of the seborrheic dermatitis are scalp itch, dandruff and oily hair, which seriously troubles patients and affects the life, work and social contact of the patients, and the products in the domestic washing and chemical industry at present are added with western antifungal medicines and other chemical components, so that the treatment effect is not lasting and certain side effects are caused.
The shampoo oil control in the market is generally solved by adopting powerful cleaning components for cleaning, if a great amount of shampoo adopts a super-strong cleaning agent, the cleaning power and the foaming power are very strong, the price is low, and the defects are as follows: the scalp and hair are excessively drained due to the strong cleaning, and after the scalp system is stimulated, more scalp oil can be secreted for self-protection, so that the repeated vicious circle can bring about more hair problems.
With the gradual clearness of the pathogenic mechanism of malassezia, an antimicrobial agent is widely applied to an anti-dandruff product, and the western anti-dandruff itching relieving principle is that an antifungal agent is added into shampoo to directly kill the malassezia, for example, copper zinc pyridinium (called as active zinc, ZPT factor and the like are mixed), ketoconazole with stronger bactericidal power is used, or selenium disulfide is used, the bactericidal power is stronger, although the side effects are more, the shampoo for removing dandruff and relieving itching is forbidden for children under the age of eight years, the shampoo for removing dandruff and relieving itching can only temporarily relieve the symptoms of dandruff and can damage scalp hair follicles due to the long-term use of a chemical anti-dandruff agent.
Symptoms of patients with scalp seborrheic dermatitis are shown as follows: greasy scales or scabs are attached to the surface of the scalp, and subjective symptoms are mainly mild and moderate pruritus. The silicon oil shampoo which is mainstream for many years can smooth and beautify hair and reduce static electricity caused by friction among hairs, but the silicon oil chemical is waterproof, and if the silicon oil shampoo is used for a long time, even if the content of the silicon oil is not over standard, the hair shampoo can stimulate the scalp and can cause scalp itching, scurf and the like and even alopecia. In patients with seborrheic dermatitis of the scalp, the condition is clearly exacerbated. Therefore, the invention provides a novel oil-control itching-relieving anti-dandruff shampoo, which is a problem to be solved urgently at present.
Disclosure of Invention
In order to solve the problems, the invention provides an oil-control itching-relieving anti-dandruff traditional Chinese medicine shampoo which comprises the following raw materials in percentage by weight: 6-43% of surfactant, 0.06-7% of conditioner, 5-25% of traditional Chinese medicine liquid, pH regulator and the balance of water to 100%; wherein the Chinese medicinal liquid is prepared from at least one of cortex Mori, folium Platycladi, radix Polygoni Multiflori Preparata, radix Sophorae Flavescentis, rhizoma Zingiberis recens, radix Stemonae, fructus Cnidii, and herba Menthae.
As a preferred technical scheme, the preparation raw materials of the traditional Chinese medicine liquid comprise raw white mulberry root-bark, cacumen biotae, prepared fleece flower root and radix sophorae flavescentis; the weight ratio of the white mulberry root-bark, the cacumen biotae, the prepared fleece flower root and the radix sophorae flavescentis is 1-2:1-2:1-2:1-2; preferably, the weight ratio of the white mulberry root-bark, the cacumen biotae, the prepared fleece-flower root and the radix sophorae flavescentis is 1.5:1.5:1.5:1.
and (3) raw white mulberry root-bark: in this application, refers to unprocessed cortex mori; cortex Mori is dry root bark of cortex Mori of Moraceae of dicotyledonous plants after removing embolus; latin's name: morus alba L. The mulberry bark comprises the following main components: benzofuran compounds, stilbene compounds, flavonoids, phenylpropanoids, triterpenes, alkaloids, etc.
Cacumen biotae: is dried shoot and leaf of Franco of Thuja orientalis L.
The radix polygoni multiflori preparata in the application is processed radix polygoni multiflori, and the radix polygoni multiflori is processed by vinegar and/or processed by black bean juice; preferably, the application is the polygonum multiflorum after processing the black bean juice. Polygonum multiflorum (famous name: fallopia multiflora (Thunb.) Harald.), and Polygonum multiflorum, stephania cochinchinensis, and caulis Polygoni Multiflori are perennial entwiny vine plants of Polygonum genus of Polygonaceae family.
Sophora flavescens ait is a plant of the family Leguminosae, genus Sophora, or a plant of the sub-shrub.
As a preferred technical scheme, the preparation method of the traditional Chinese medicine liquid comprises the following steps: mixing the raw materials, soaking in water for a certain time, and reflux-extracting in a Chinese medicinal extraction tank to obtain medicinal liquid; liquid retention and residue extraction are carried out on the liquid medicine, the extracted liquid is cooled and then is kept stand, and the supernatant is taken to obtain the extracted liquid medicine; and carrying out post-treatment on the extracted liquid medicine to obtain the traditional Chinese medicine liquid.
As a preferred technical scheme, the preparation method of the traditional Chinese medicine liquid comprises the following steps: mixing the preparation raw materials, adding 3-10 times of water by weight, soaking for 0.5-3h, and reflux-extracting for 0.5-1.5h in a Chinese medicinal extraction tank to obtain medicinal liquid; the liquid medicine is subjected to liquid retention and slag extraction, the extracted liquid is cooled and then is kept stand for 3-5h, and the supernatant is taken to obtain the extracted liquid medicine; and carrying out post-treatment on the extracted liquid medicine to obtain the traditional Chinese medicine liquid.
The post-treatment of the extracted liquid medicine is conventional operation in the field, namely, the extracted liquid medicine is concentrated, and impurities are removed by a decoloring and impurity removing process.
The specific operation of the liquid retention and slag removal is not particularly limited, and for example, a filter sieve and a liquid storage bottle can be adopted.
The reflux extraction is preferably carried out with mild fire, which means that the water is the minimum fire for boiling during the boiling process.
As a preferable technical scheme, the hydrophobic end of the surfactant has 10-15 carbon atoms, and the weight part of the anionic surfactant is 1-6 times of that of the non-anionic surfactant.
As a preferable technical scheme, the sodium lauryl polyether sulfate, cocamidopropyl betaine, cocamide DEA, cocamide MEA, sodium lauroyl sarcosinate and sodium methyl cocoyl taurate are selected from at least one of the following raw materials. Preferably, the traditional Chinese medicine shampoo comprises the following components in percentage by weight: the surfactant includes: 5-25% of sodium laureth sulfate, 0.5-10% of cocamidopropyl betaine, 0.5-8% of cocamide DEA and 0.5-8% of sodium lauroyl sarcosinate.
The invention forms a stable aqueous solution system by compounding a surfactant and citric acid through compatibility with sodium laureth sulfate, sodium lauroyl sarcosinate, cocamidopropyl betaine, sodium chloride and the like; especially, the raw white mulberry root-bark, the Chinese arborvitae twig, the prepared fleece flower root and the lightyellow sophora root are extracted together by reflux, so that the traditional Chinese medicine liquid can be promoted to play a role, and the effects of relieving itching and removing dandruff with a more lasting oil control effect are achieved.
As a preferable technical scheme, the conditioning agent comprises at least one of guar hydroxypropyl trimethyl ammonium chloride, polyquaternium-7, polyquaternium-10, polyquaternium-67 and menthol. Preferably, the conditioner comprises 0.5-10% of acrylate copolymer, 0.01-2% of menthol and 0.05-5% of polyquaternium by total weight percentage of the traditional Chinese medicine shampoo.
As a preferred technical scheme, the method also comprises the following raw materials: 0.02-10% of preservative, 0.5-10% of film-forming agent, 0.002-10% of small molecular dihydric alcohol, 0.001-2% of sodium chloride and 0.01-5% of essence.
As a preferable technical scheme, the small-molecule dihydric alcohol is hexanediol and/or butanediol.
Preferably, the shampoo further comprises the following raw materials in percentage by weight based on the total weight of the traditional Chinese medicine shampoo: salicylic acid 0.01-5%, sodium benzoate 0.01-5%, hexylene glycol 0.001-5%, butanediol 0.001-5%, disodium EDTA 0.01-2%, sodium chloride 0.001-2%, and essence 0.01-5%.
The pH adjuster is not particularly limited, and is citric acid and/or sodium hydroxide.
The second aspect of the invention also provides a preparation method of the traditional Chinese medicine shampoo for controlling oil, relieving itching and removing dandruff, which comprises the following steps: mixing all the raw materials uniformly, and defoaming completely to obtain the product.
Preferably, the preparation method of the oil-control itching-relieving anti-dandruff traditional Chinese medicine shampoo comprises the following steps: placing the raw materials in a separate container, adding acrylic acid (ester) copolymer, adding water, stirring for 10-30min, dispersing uniformly, heating to 50-70 deg.C, adding sodium laureth sulfate, stirring uniformly to dissolve completely, cooling to about 40-60 deg.C, adding salicylic acid and sodium benzoate, stirring uniformly to dissolve, keeping the temperature to about 45-55 deg.C, sequentially adding the rest materials, stirring for 15-25min to dissolve all the raw materials completely, adding Chinese medicinal liquid, keeping the temperature for 25-35min to defoam completely, sampling, inspecting, detecting color, fragrance, viscosity, pH, state, skin feel, etc., and discharging after the detection is qualified.
Compared with the prior art, the invention has the following advantages:
1. the traditional Chinese medicine shampoo provided by the invention adopts a traditional Chinese medicine compatibility formula, takes traditional Chinese medicines such as cacumen biotae, raw cortex mori radicis, radix polygoni multiflori preparata and radix sophorae flavescentis as main components, has synergistic effect in many aspects, and has the effects of removing dampness and clearing heat, removing dandruff and relieving itching, improving scalp environment, promoting scalp metabolism, enhancing the resistance of scalp to external environment stimulation and the like.
2. The mild and low-irritation traditional Chinese medicine shampoo without silicone oil is a weakly acidic surfactant amino acid, is closer to the pH value of the scalp, is mild in property and free of irritation, effectively cleans scalp stains, and improves the scalp environment.
3. The problem of rareness of the traditional Chinese medicine shampoo is solved, the traditional shampoo is a shampoo which is boiled into a water shape by traditional Chinese medicines and achieves the effect of cleaning by soaking hair, and the product is added into a mild and low-irritation sulfate-free and salt-free amino acid shampoo system, so that the traditional soaking type washing method is changed into the usage of the shampoo which is more suitable for modern people.
4. Compared with the existing shampoo, the traditional Chinese medicine shampoo provided by the embodiment of the invention has the advantages of small stimulation, milder temperature, better oil control and itching relieving effects and moisture retention.
5. The traditional Chinese medicine shampoo regulates scalp environment through active ingredients of traditional Chinese medicine fluid extract, promotes organism balanced metabolism, gradually normalizes grease secretion, enables malassezia to lose an environment where excessive breeding and propagation is caused, and naturally scurf and scalp itch and the like are not found, so that oil control, scurf removal and itching relieving are carried out by regulating scalp metabolic environment, and the traditional Chinese medicine shampoo is an integral solution of the traditional Chinese medicine strengthening principle.
Detailed Description
The present invention will be specifically described below by way of examples. The starting materials used are all commercially available, unless otherwise stated.
Example 1
The traditional Chinese medicine shampoo capable of controlling oil, relieving itching and removing dandruff comprises the following raw materials in percentage by weight: 10% of sodium laureth sulfate, 5% of cocamidopropyl betaine, 4% of cocamide DEA, 4% of sodium lauroyl amino acid, 5% of acrylic acid (ester) copolymer, 2% of salicylic acid, 3% of sodium benzoate, 10% of polyquaternium, 3% of hexanediol, 2% of butanediol, 0.5% of citric acid, 3% of sodium hydroxide, 1% of menthol, 1% of disodium EDTA, 1% of sodium chloride, 3% of essence, 15% of liquid medicine and the balance of water.
The Chinese medicinal liquid is prepared from cortex Mori, folium Platycladi, radix Polygoni Multiflori Preparata, and radix Sophorae Flavescentis; the application relates to fleece-flower root after black bean juice processing. The weight ratio of the white mulberry root-bark, the cacumen biotae, the prepared fleece flower root and the radix sophorae flavescentis is 1.5:1.5:1.5:1. the preparation method of the traditional Chinese medicine liquid comprises the following steps: mixing the preparation raw materials together, adding 5 times of water by weight, soaking for 2h, and then pouring into a traditional Chinese medicine extraction tank for reflux extraction for 1h to obtain liquid medicine; liquid retention and residue extraction are carried out on the liquid medicine, the extracted liquid is cooled and then is kept stand for 4 hours, and supernatant is taken to obtain extracted liquid medicine; concentrating the extractive solution, decolorizing, and removing impurities to obtain Chinese medicinal solution.
The preparation method of the traditional Chinese medicine shampoo capable of controlling oil, relieving itching and removing dandruff comprises the following steps: placing the raw materials in a separate container, adding acrylic acid (ester) copolymer, adding water, stirring for 20min for uniform dispersion, heating to 60 deg.C, adding sodium laureth sulfate, stirring for uniform dissolution, cooling to 50 deg.C, adding salicylic acid and sodium benzoate, stirring for uniform dissolution, maintaining the temperature to 50 deg.C, sequentially adding the rest materials, stirring for 20min until all raw materials are completely dissolved, adding Chinese medicinal liquid, keeping the temperature for 30min to completely defoam, sampling, inspecting, detecting color, fragrance, viscosity, pH, state and skin feel, and discharging after qualified detection.
Example 2
The traditional Chinese medicine shampoo capable of controlling oil, relieving itching and removing dandruff comprises the following raw materials in percentage by weight: 6% of sodium laureth sulfate, 1% of cocamidopropyl betaine, 1% of cocamide DEA, 2% of sodium lauroyl amide, 1% of acrylic acid (ester) copolymer, 1% of salicylic acid, 1% of sodium benzoate, 10% of polyquaternary ammonium salt, 1% of hexanediol, 1% of butanediol, 0.2% of citric acid, 0.02% of sodium hydroxide, 1% of menthol, 1% of disodium EDTA, 1% of sodium chloride, 2% of essence, 6% of Chinese medicinal liquid and the balance of water.
The Chinese medicinal liquid is prepared from cortex Mori, folium Platycladi, radix Polygoni Multiflori Preparata, and radix Sophorae Flavescentis; the application relates to fleece-flower root after black bean juice processing. The weight ratio of the white mulberry root-bark, the cacumen biotae, the prepared fleece flower root and the radix sophorae flavescentis is 1.5:1.5:1.5:1. the preparation method of the traditional Chinese medicine liquid comprises the following steps: mixing the preparation raw materials, adding 3 times of water by weight, soaking for 0.5h, and then pouring into a traditional Chinese medicine extraction tank for reflux extraction for 0.5h to obtain a liquid medicine; the liquid medicine is subjected to liquid retention and slag removal, the liquid taken out is cooled and then stands for 3 hours, and the supernatant is taken to obtain the extracted liquid medicine; concentrating the extractive solution, decolorizing, and removing impurities to obtain Chinese medicinal solution.
The specific steps of the preparation method of the traditional Chinese medicine shampoo for controlling oil, relieving itching and removing dandruff are the same as those in example 1.
Example 2
The traditional Chinese medicine shampoo capable of controlling oil, relieving itching and removing dandruff comprises the following raw materials in percentage by weight: 20% of sodium lauryl polyether sulfate, 2% of cocamidopropyl betaine, 3% of cocamide DEA, 7% of sodium lauroyl amide, 2% of acrylic acid (ester) copolymer, 4% of salicylic acid, 3% of sodium benzoate, 10% of polyquaternary ammonium salt, 2% of hexanediol, 3% of butanediol, 0.6% of citric acid, 0.3% of sodium hydroxide, 0.5% of menthol, 1% of disodium EDTA (ethylene diamine tetraacetic acid), 1% of sodium chloride, 0.8% of essence, 20% of traditional Chinese medicine liquid and the balance of water;
the Chinese medicinal liquid is prepared from cortex Mori, folium Platycladi, radix Polygoni Multiflori Preparata, and radix Sophorae Flavescentis; the application relates to fleece-flower root after black bean juice processing. The weight ratio of the white mulberry root-bark, the cacumen biotae, the prepared fleece flower root and the radix sophorae flavescentis is 1.5:1.5:1.5:1. the preparation method of the traditional Chinese medicine liquid comprises the following steps: mixing the preparation raw materials together, adding 10 times of water by weight, soaking for 0.5h, and then pouring into a traditional Chinese medicine extraction tank for reflux extraction for 1.5h to obtain liquid medicine; liquid retention and residue extraction are carried out on the liquid medicine, the extracted liquid is cooled and then stands for 5 hours, and the supernatant is taken to obtain the extracted liquid medicine; concentrating the extractive solution, decolorizing, and removing impurities to obtain Chinese medicinal solution.
The specific steps of the preparation method of the traditional Chinese medicine shampoo for controlling oil, relieving itching and removing dandruff are the same as those in example 1.
Performance testing
(1) Properties of shampoos obtained in examples 1-3: color: a yellow transparent liquid; fragrance: special traditional Chinese medicine smell; viscosity: 1780mpa.s; pH:4.7-5.3; the state is as follows: a somewhat viscous liquid.
(2) The traditional Chinese medicine shampoo provided by the invention applies a traditional Chinese medicine compatibility formula and a mild and low-stimulation weak-acid amino acid shampoo formula, and has the effects of removing dampness and clearing heat, removing dandruff and relieving itching, improving scalp environment, promoting scalp metabolism, enhancing the resistance of scalp to external environment stimulation and the like. The traditional Chinese medicine external lotion for treating scalp seborrheic dermatitis is prepared by decocting traditional Chinese medicines into a traditional Chinese medicine liquid and then directly soaking and washing the traditional Chinese medicine liquid, although the traditional Chinese medicine external lotion has curative effect, the traditional Chinese medicine external lotion wastes time and labor and is very inconvenient, the traditional soaking type washing method is updated into modern shampoo, the traditional Chinese medicine external lotion has the function of adjuvant therapy, and relevant experimental data are proved by relevant experiments, and the relevant experimental data are as follows:
the population selection standard is as follows: patients with seborrheic dermatitis (with lesions on the head) who did not use antifungal drugs, hormones, and immunosuppressants for nearly 4 weeks; no medication contraindication; adults (18-60 years old).
The treatment method comprises the following steps:
100 patients with seborrheic dermatitis of the head to be included were randomly divided into a control group and a test group [ example 1 ] and 50 patients were included. The dispensed test product was used and the daily use of the shampoo and conditioner products was discontinued.
Control group: 2% ketoconazole lotion, 2 times/week, for 8 weeks. Experimental group [ example 1 ]: the shampoo is used for 2 times per week for 8 weeks. During the treatment period, patients need to ensure the daily work and rest rule, have light diet and avoid the intake of spicy, greasy and sweet foods.
The experimental results are as follows:
observation and therapeutic effect determination method: a method combining subjective feeling of a patient and objective evaluation of doctor's examination before and after treatment of the patient:
TABLE 1 Observation of clinical efficacy of 4 weeks for the treatment of seborrheic dermatitis of the head
TABLE 2 Observation of the clinical efficacy of 8 weeks for the treatment of seborrheic dermatitis of the head
By following the visit of 6 months after the treatment, 3 relapse cases appear in the patients of the example 1 group, 7 relapse cases appear in the patients of the control group, and the relapse rate of the patients of the research group is 6 percent (3/50) which is obviously lower than 24 percent (12/50) of the patients of the control group.
The result shows that the shampoo has better effects of controlling oil, removing dandruff and relieving itching, the recurrence rate is obviously lower than that of a control group, and adverse reactions do not occur after long-term use.
Claims (10)
1. The traditional Chinese medicine shampoo capable of controlling oil, relieving itching and removing dandruff is characterized by comprising the following raw materials in percentage by weight: 6-43% of surfactant, 0.06-7% of conditioner, 5-25% of traditional Chinese medicine liquid, pH regulator and the balance of water to 100%; wherein the Chinese medicinal liquid is prepared from at least one of cortex Mori, folium Platycladi, radix Polygoni Multiflori Preparata, radix Sophorae Flavescentis, rhizoma Zingiberis recens, radix Stemonae, fructus Cnidii, and herba Menthae.
2. The traditional Chinese medicine shampoo for controlling oil, relieving itching and removing dandruff as claimed in claim 1, wherein the traditional Chinese medicine liquid is prepared from raw materials including raw cortex mori radicis, cacumen biotae, radix polygoni multiflori preparata and radix sophorae flavescentis; the weight ratio of the white mulberry root-bark, the cacumen biotae, the prepared fleece flower root and the radix sophorae flavescentis is 1-2:1-2:1-2:1-2.
3. The traditional Chinese medicine shampoo for controlling oil, relieving itching and removing dandruff as claimed in claim 1 or 2, wherein the preparation method of the traditional Chinese medicine liquid comprises the following steps: mixing the raw materials, soaking in water for a certain time, and reflux-extracting in a Chinese medicinal extraction tank to obtain medicinal liquid; the liquid medicine is left for liquid retention and slag removal, the liquid taken out is cooled and then stands, and the supernatant is taken to obtain the extracted liquid medicine; and carrying out post-treatment on the extracted liquid medicine to obtain the traditional Chinese medicine liquid.
4. The traditional Chinese medicine shampoo with functions of controlling oil, relieving itching and removing dandruff as claimed in claim 3, wherein the preparation method of the traditional Chinese medicine liquid comprises the following steps: mixing the preparation raw materials, adding 3-10 times of water by weight, soaking for 0.5-3h, and reflux-extracting for 0.5-1.5h in a Chinese medicinal extraction tank to obtain medicinal liquid; the liquid medicine is subjected to liquid retention and slag extraction, the extracted liquid is cooled and then is kept stand for 3-5h, and the supernatant is taken to obtain the extracted liquid medicine; and carrying out post-treatment on the extracted liquid medicine to obtain the traditional Chinese medicine liquid.
5. The traditional Chinese medicine shampoo capable of controlling oil, relieving itching and removing dandruff as claimed in claim 4, wherein the number of carbon atoms of the hydrophobic end of the surfactant is 10-15, and the weight part of the anionic surfactant is 1-6 times that of the non-anionic surfactant.
6. The traditional Chinese medicine shampoo for controlling oil, relieving itching and removing dandruff as claimed in claim 5, which is characterized by being selected from at least one of sodium laureth sulfate, cocamidopropyl betaine, cocamide DEA, cocamide MEA, sodium lauroyl sarcosinate and sodium methylcocoyl taurate.
7. The traditional Chinese medicine shampoo capable of controlling oil, relieving itching and removing dandruff as claimed in claim 6, wherein the conditioner comprises at least one of guar hydroxypropyltrimonium chloride, polyquaternium-7, polyquaternium-10, polyquaternium-67 and menthol.
8. The traditional Chinese medicine shampoo for controlling oil, relieving itching and removing dandruff as claimed in claim 7, further comprising the following raw materials: 0.02-10% of preservative, 0.5-10% of film-forming agent, 0.002-10% of small molecular dihydric alcohol, 0.001-2% of sodium chloride and 0.01-5% of essence.
9. The traditional Chinese medicine shampoo for controlling oil, relieving itching and removing dandruff as claimed in claim 4, wherein the small molecular diol is hexanediol and/or butanediol.
10. The method for preparing the traditional Chinese medicine shampoo for controlling oil, relieving itching and removing dandruff as claimed in any one of claims 1 to 9, comprising the following steps: mixing all the raw materials uniformly, and defoaming completely to obtain the product.
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