CN115127327A - A kind of triazole sodium salt drying device and operation technique thereof - Google Patents
A kind of triazole sodium salt drying device and operation technique thereof Download PDFInfo
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- CN115127327A CN115127327A CN202110328639.2A CN202110328639A CN115127327A CN 115127327 A CN115127327 A CN 115127327A CN 202110328639 A CN202110328639 A CN 202110328639A CN 115127327 A CN115127327 A CN 115127327A
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- 238000001035 drying Methods 0.000 title claims abstract description 47
- UYXAHRLPUPVSNJ-UHFFFAOYSA-N sodium;2h-triazole Chemical compound [Na].C=1C=NNN=1 UYXAHRLPUPVSNJ-UHFFFAOYSA-N 0.000 title claims abstract description 27
- 238000000034 method Methods 0.000 title claims abstract description 10
- 238000010438 heat treatment Methods 0.000 claims abstract description 64
- 238000005192 partition Methods 0.000 claims abstract description 8
- 238000004140 cleaning Methods 0.000 claims description 6
- 238000007599 discharging Methods 0.000 claims description 6
- 239000000463 material Substances 0.000 claims description 5
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 5
- 238000006243 chemical reaction Methods 0.000 claims description 4
- 239000011521 glass Substances 0.000 claims description 3
- 239000000428 dust Substances 0.000 abstract 1
- 238000004519 manufacturing process Methods 0.000 description 3
- 238000012824 chemical production Methods 0.000 description 1
- 239000013064 chemical raw material Substances 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- 238000005265 energy consumption Methods 0.000 description 1
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- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F26—DRYING
- F26B—DRYING SOLID MATERIALS OR OBJECTS BY REMOVING LIQUID THEREFROM
- F26B17/00—Machines or apparatus for drying materials in loose, plastic, or fluidised form, e.g. granules, staple fibres, with progressive movement
- F26B17/10—Machines or apparatus for drying materials in loose, plastic, or fluidised form, e.g. granules, staple fibres, with progressive movement with movement performed by fluid currents, e.g. issuing from a nozzle, e.g. pneumatic, flash, vortex or entrainment dryers
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D46/00—Filters or filtering processes specially modified for separating dispersed particles from gases or vapours
- B01D46/02—Particle separators, e.g. dust precipitators, having hollow filters made of flexible material
- B01D46/023—Pockets filters, i.e. multiple bag filters mounted on a common frame
-
- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F26—DRYING
- F26B—DRYING SOLID MATERIALS OR OBJECTS BY REMOVING LIQUID THEREFROM
- F26B21/00—Arrangements or duct systems, e.g. in combination with pallet boxes, for supplying and controlling air or gases for drying solid materials or objects
- F26B21/001—Drying-air generating units, e.g. movable, independent of drying enclosure
-
- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F26—DRYING
- F26B—DRYING SOLID MATERIALS OR OBJECTS BY REMOVING LIQUID THEREFROM
- F26B23/00—Heating arrangements
-
- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F26—DRYING
- F26B—DRYING SOLID MATERIALS OR OBJECTS BY REMOVING LIQUID THEREFROM
- F26B25/00—Details of general application not covered by group F26B21/00 or F26B23/00
- F26B25/005—Treatment of dryer exhaust gases
- F26B25/007—Dust filtering; Exhaust dust filters
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- Engineering & Computer Science (AREA)
- Mechanical Engineering (AREA)
- General Engineering & Computer Science (AREA)
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Life Sciences & Earth Sciences (AREA)
- Sustainable Development (AREA)
- Drying Of Solid Materials (AREA)
Abstract
Description
技术领域technical field
本发明涉及一种化工生产设备及其操作工艺,特别是一种三氮唑钠盐烘干装置及其操作工艺。The invention relates to a chemical production equipment and an operation process thereof, in particular to a triazole sodium salt drying device and an operation process thereof.
背景技术Background technique
三氮唑钠盐是一种重要的化工原料,但生产中用目前的烘干设备和工艺进行烘干,则干燥速度慢、物料受热不均匀、能耗大、热效率低,已不能满足现实大生产的要求,直接影响到企业产品的质量和市场竞争力。Triazole sodium salt is an important chemical raw material, but drying with the current drying equipment and process in production results in slow drying speed, uneven heating of materials, high energy consumption, and low thermal efficiency, which can no longer meet the needs of practical needs. Production requirements directly affect the quality and market competitiveness of enterprise products.
发明内容SUMMARY OF THE INVENTION
为了克服现有技术的不足,本发明提供了一种结构简单、生产效率高的三氮唑钠盐烘干装置及其操作工艺。In order to overcome the deficiencies of the prior art, the present invention provides a triazole sodium salt drying device with a simple structure and high production efficiency and an operation process thereof.
本发明采用如下技术方案。The present invention adopts the following technical solutions.
一种三氮唑钠盐烘干装置,它有烘干装置本体,烘干装置本体内有筛板,筛板上面分别连接两块上隔板,把烘干装置分隔成初加热室、中间加热室和终加热室,筛板下面分别连接两块下隔板,把烘干装置相应分成三个热风室,每个热风室通过热风支管和热风控制阀与热风主管相连,热风主管与蒸汽换热器相连,蒸汽换热器通过管道与热风鼓风机相连,热风鼓风机的电机为变频电机,蒸汽换热器的蒸汽入口与蒸汽控制阀相连,初加热室与螺旋送料机相连,螺旋送料机的电机为变频电机,初加热室通过管道与冷风鼓风机相连,初加热室有进料清理口,进料清理口设置有插板阀,终加热室有出料口,出料口设置有插板阀,初加热室、中间加热室和终加热室的上部有布袋除尘器,布袋除尘器上面的烘干装置本体有排风口和压缩空气进口,初加热室、中间加热室和终加热室的烘干装置本体都装有视镜、温度传感器和湿度传感器,冷风鼓风机的电机、热风鼓风机的电机、螺旋送料机的电机、蒸汽控制阀、所有热风控制阀和所有温度传感器及湿度传感器都与控制器电气相连。A drying device for triazole sodium salt, which has a drying device body, a sieve plate is arranged in the drying device body, and two upper partitions are respectively connected on the sieve plate, and the drying device is divided into an initial heating chamber and an intermediate heating chamber. Two lower partitions are connected under the sieve plate respectively, and the drying device is divided into three hot air chambers, each hot air chamber is connected with the hot air main pipe through the hot air branch pipe and the hot air control valve, and the hot air main pipe exchanges heat with the steam The steam heat exchanger is connected to the hot air blower through a pipeline. The motor of the hot air blower is a frequency conversion motor, the steam inlet of the steam heat exchanger is connected to the steam control valve, and the primary heating chamber is connected to the screw feeder. The motor of the screw feeder is Frequency conversion motor, the initial heating chamber is connected with the cold air blower through pipes, the initial heating chamber is provided with a feeding cleaning port, the feeding cleaning port is provided with a flapper valve, the final heating chamber is provided with a discharging port, and the discharging port is provided with a flapper valve. The upper parts of the heating chamber, the intermediate heating chamber and the final heating chamber are provided with a bag filter. The drying device body above the bag filter has an air outlet and a compressed air inlet. The drying devices of the initial heating chamber, the intermediate heating chamber and the final heating chamber The main body is equipped with sight glass, temperature sensor and humidity sensor, the motor of the cold air blower, the motor of the hot air blower, the motor of the screw feeder, the steam control valve, all the hot air control valves and all the temperature sensors and humidity sensors are electrically connected to the controller .
一种三氮唑钠盐烘干装置的操作工艺如下:A kind of operation technique of triazole sodium salt drying device is as follows:
(1)三氮唑钠盐每个烘干周期分为第一阶段、第二阶段和第三阶段,第一阶段时长为二分之一烘干周期,第二阶段时长为四分之一烘干周期,第三阶段时长为四分之一烘干周期,在第一阶段,热风鼓风机的电机和螺旋送料机的电机的转速为每分钟1200-1400转,在第二阶段,热风鼓风机的电机和螺旋送料机的电机的转速为每分钟1000-1150转,在第三阶段,热风鼓风机的电机的转速为每分钟800-950转,螺旋送料机的电机不工作;(1) Each drying cycle of triazole sodium salt is divided into the first stage, the second stage and the third stage. The duration of the first stage is one half of the drying cycle, and the duration of the second stage is one quarter of the drying cycle. Dry cycle, the third stage is a quarter of the drying cycle. In the first stage, the motor of the hot air blower and the motor of the screw feeder rotate at 1200-1400 rpm. In the second stage, the motor of the hot air blower And the speed of the motor of the screw feeder is 1000-1150 revolutions per minute, in the third stage, the speed of the motor of the hot air blower is 800-950 revolutions per minute, and the motor of the screw feeder does not work;
(2)三氮唑钠盐进料含水率为45%-50%,初加热室温度控制在60±5℃,湿度20%-30%,三氮唑钠盐含水率为15%-20%,中间加热室温度控制在100±5℃,湿度5%-10%,三氮唑钠盐含水率为5%-8%,终加热室温度控制在140±5℃,湿度不大于2%,出料三氮唑钠盐含水率为≤0.1%;(2) The moisture content of triazole sodium salt feed is 45%-50%, the temperature of the initial heating chamber is controlled at 60±5℃, the humidity is 20%-30%, and the moisture content of triazole sodium salt is 15%-20% , the temperature of the intermediate heating chamber is controlled at 100±5℃, the humidity is 5%-10%, the moisture content of triazole sodium salt is 5%-8%, the temperature of the final heating chamber is controlled at 140±5℃, and the humidity is not more than 2%. The water content of triazole sodium salt in the discharge material is less than or equal to 0.1%;
(3)初加热室、中间加热室和终加热室的热风控制阀控制各自的温度,冷风鼓风机间歇工作,给各加热室送去新风,调节温度和湿度。(3) The hot air control valves of the initial heating chamber, the intermediate heating chamber and the final heating chamber control their respective temperatures, and the cold air blower works intermittently to send fresh air to each heating chamber to adjust the temperature and humidity.
与现有技术相比,本发明的优点在于结构简单,可靠性高,物料受热均匀,充分利用了热风的能源,提高了热效率。Compared with the prior art, the present invention has the advantages of simple structure, high reliability, uniform heating of materials, full utilization of the energy of hot air, and improved thermal efficiency.
附图说明Description of drawings
图1为本发明实施例的结构示意图。FIG. 1 is a schematic structural diagram of an embodiment of the present invention.
具体实施方式Detailed ways
以下结合附图和实施例对本发明作进一步详细描述。The present invention will be described in further detail below with reference to the accompanying drawings and embodiments.
如图1 所示,一种三氮唑钠盐烘干装置,它有烘干装置本体31,烘干装置本体31内有筛板6,筛板6上面分别连接两块上隔板3,把烘干装置分隔成初加热室23、中间加热室4和终加热室5,筛板6下面分别连接两块下隔板21,把烘干装置相应分成热风室A22,热风室B20,热风室C9,热风室A22通过热风支管18和热风控制阀D19与热风主管15相连,热风室B20通过热风支管18和热风控制阀E17与热风主管15相连,热风室C9通过热风支管18和热风控制阀F16与热风主管15相连,热风主管15与蒸汽换热器14相连,蒸汽换热器14通过管道与热风鼓风机13相连,热风鼓风机13的电机12为变频电机,蒸汽换热器14的蒸汽入口11与蒸汽控制阀10相连,初加热室23与螺旋送料机29相连,螺旋送料机29的电机30为变频电机,初加热室23通过管道与冷风鼓风机24相连,初加热室23有进料清理口26,进料清理口26设置有右插板阀27,终加热室5有出料口8,出料口8有左插板阀7,初加热室23、中间加热室4和终加热室5的上部有布袋除尘器2,布袋除尘器2上面的烘干装置本体31有排风口1和压缩空气进口32,初加热室23、中间加热室4和终加热室5的烘干装置本体31都装有视镜28、温度传感器和湿度传感器(图中未画出),冷风鼓风机24的电机25、热风鼓风机13的电机12、螺旋送料机29的电机30、热风控制阀D19、热风控制阀E17、热风控制阀F16、蒸汽控制阀10和所有温度传感器及湿度传感器都与控制器(图中未画出)电气相连。As shown in Figure 1, a kind of triazole sodium salt drying device, it has a
一种三氮唑钠盐烘干装置的操作工艺如下:A kind of operation technique of triazole sodium salt drying device is as follows:
(1) 三氮唑钠盐每个烘干周期分为第一阶段、第二阶段和第三阶段,第一阶段时长为二分之一烘干周期,第二阶段时长为四分之一烘干周期,第三阶段时长为四分之一烘干周期,在第一阶段,热风鼓风机13的电机12和螺旋送料机29的电机30的转速为每分钟1200-1400转,在第二阶段,热风鼓风机13的电机12和螺旋送料机29的电机30的转速为每分钟1000-1150转,在第三阶段,热风鼓风机13的电机12的转速为每分钟800-950转,螺旋送料机29的电机30不工作;(1) Each drying cycle of triazole sodium salt is divided into the first stage, the second stage and the third stage, the duration of the first stage is one-half drying cycle, and the duration of the second stage is one-quarter drying In the drying cycle, the duration of the third stage is a quarter of the drying cycle. In the first stage, the rotational speed of the
(2) 三氮唑钠盐进料含水率为45%-50%,初加热室23温度控制在60±5℃,湿度20%-30%,三氮唑钠盐含水率为15%-20%,中间加热室4温度控制在100±5℃,湿度5%-10%,三氮唑钠盐含水率为5%-8%,终加热室5温度控制在140±5℃,湿度不大于2%,出料三氮唑钠盐含水率为≤0.1%;(2) The water content of triazole sodium salt feed is 45%-50%, the temperature of the
(3) 初加热室23、中间加热室4和终加热室5的热风控制阀D19、热风控制阀E17、热风控制阀F16控制各自的温度,冷风鼓风机24间歇工作,给各加热室送去新风,调节温度和湿度。(3) The hot air control valve D19, hot air control valve E17 and hot air control valve F16 of the
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Citations (5)
Publication number | Priority date | Publication date | Assignee | Title |
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CN101571341A (en) * | 2009-06-11 | 2009-11-04 | 陆文光 | Fluid-bed drying system |
CN201532081U (en) * | 2009-11-17 | 2010-07-21 | 山东天力干燥设备有限公司 | Novel high-efficiency chlorinated polypropylene fluidized bed drying system |
WO2011043541A2 (en) * | 2009-10-08 | 2011-04-14 | 한국에너지기술연구원 | Fluidized bed drying apparatus |
CN205536893U (en) * | 2016-01-20 | 2016-08-31 | 杭州万隆果干食品有限公司 | Fluid bed drying device |
CN214469943U (en) * | 2021-03-26 | 2021-10-22 | 长沙鑫本助剂有限公司 | Triazole sodium salt drying device |
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- 2021-03-26 CN CN202110328639.2A patent/CN115127327A/en active Pending
Patent Citations (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN101571341A (en) * | 2009-06-11 | 2009-11-04 | 陆文光 | Fluid-bed drying system |
WO2011043541A2 (en) * | 2009-10-08 | 2011-04-14 | 한국에너지기술연구원 | Fluidized bed drying apparatus |
CN201532081U (en) * | 2009-11-17 | 2010-07-21 | 山东天力干燥设备有限公司 | Novel high-efficiency chlorinated polypropylene fluidized bed drying system |
CN205536893U (en) * | 2016-01-20 | 2016-08-31 | 杭州万隆果干食品有限公司 | Fluid bed drying device |
CN214469943U (en) * | 2021-03-26 | 2021-10-22 | 长沙鑫本助剂有限公司 | Triazole sodium salt drying device |
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