CN114948828A - Whole-plant anhydrous lip glaze and preparation method thereof - Google Patents

Abstract

The application discloses an all-plant anhydrous lip glaze and a preparation method thereof. The all-plant anhydrous lip glaze provided by this application includes by weight percentage: vegetable oil: 40%-60%, vegetable wax: 0.1-5%, vegetable powder: 10%-30%, vegetable dispersant: 10%- 30%, Plant Antioxidants: 0.1%‑1%, Plant Preservatives: 0.1%‑1%, Plant Essential Oils: 0.1%‑1%, Plant Extracts: 0.1%‑1%. The all-plant anhydrous lip glaze provided by the application has fine texture, uniform color, good moisturizing and moisturizing effects, strong antiseptic and anti-inflammatory properties, and high safety. In addition, the preparation method of the all-plant anhydrous lip glaze provided by the present application is simple in procedure, short in time consumption, low in equipment requirements, well compatible with existing processes, and has great potential for large-scale application.

Description

A kind of whole plant anhydrous lip glaze and preparation method thereof

technical field

The application belongs to the technical field of daily cosmetics, and in particular relates to an all-plant anhydrous lip glaze and a preparation method thereof.

Background technique

Lip beauty products are used to make the lips rosy and shiny, moisturizing and maintaining the lips, and giving the lips color, increasing the facial beauty and correcting the contour of the lips. It is one of the essential beauty makeup products for women. . As one of the lip beauty products, lip glaze can combine the saturated color of lipstick and the bright texture of lip gloss into one, realizing a new progress in makeup.

With the improvement of living standards and the accumulation of human scientific knowledge, people have higher and higher requirements for the safety of cosmetics, and lip glazes with natural plant ingredients have been widely favored. However, most of the currently declared plant lip glaze (natural lip glaze) products only introduce some plant-derived raw materials, and there are still non-plant-derived oils, functional polymer materials, non-natural preservatives, and colorants. Wait. The ingredients of non-plant-derived raw materials are complex and easy to cause allergic reactions, such as chapped lip mucous membranes, peeling, cheilitis, etc., and even contain carcinogens and seriously endanger health.

SUMMARY OF THE INVENTION

In view of this, the present application provides an all-plant anhydrous lip glaze and a preparation method thereof, aiming at solving the problems of non-plant raw materials and low safety in the lip glaze.

On the one hand, the embodiment of the present application provides a kind of full-plant component lip glaze, which comprises by weight percentage:

Vegetable oils and fats: 40%-60%,

Vegetable wax: 0.1-5%,

Plant powder: 10%-30%,

Plant dispersant: 10%-30%,

Plant antioxidants: 0.1%-1%,

Plant preservatives: 0.1%-1%,

Plant essential oils: 0.1%-1%,

Plant extract: 0.1%-1%.

According to an embodiment of one aspect of the present application, the vegetable oil is selected from the group consisting of vegetable squalane, jojoba oil, sunflower seed oil, castor oil, white chia seed oil, coconut oil, shea butter, grape seed oil, and macadamia nut oil , olive oil, palm oil, cocoa butter, jojoba butter, sugar gum, one or more of octyldodecanol, caprylic capric triglyceride and coco-caprylic capric triglyceride.

According to an embodiment of one aspect of the present application, the vegetable wax is selected from one of candelilla wax, sunflower wax, carnauba wax, rice bran wax, jasmine wax, dextrin palmitate and dextrin isostearate or variety.

According to an embodiment of one aspect of the present application, the plant powder includes an oil-soluble toner and a filler,

Wherein, the oil-soluble toner is selected from one or more of lycopene, beet red, safflower red, purple sweet potato, elderberry and radish red;

The filler is selected from corn starch and/or rice starch.

According to an embodiment of one aspect of the present application, the vegetable dispersant is selected from the group consisting of soy lecithin, polyglycerol-3 diisostearate, polyglycerol-2 triisostearate, polyglycerol 2-dipolyhydroxystearin esters and one or more of oleic/linoleic/linolenic polyglycerides.

According to an embodiment of one aspect of the present application, the plant antioxidant is selected from one or more of vitamin E, tea polyphenols and rice bran oil.

According to an embodiment of one aspect of the present application, the plant preservative is selected from one or more of anisic acid, peony root bark extract and Magnolia bark extract.

According to an embodiment of one aspect of the present application, the plant essential oil is selected from one or more of tea tree essential oil, rose essential oil, jasmine essential oil, sweet orange essential oil, chamomile essential oil and lavender essential oil.

According to an embodiment of one aspect of the present application, the plant extract is selected from the group consisting of jasmine flower extract, camellia flower extract, Bletilla striata root extract, Atractylodes Rhizoma root extract, Atractylodes Rhizoma root extract, peach blossom extract, cherry extract and Cactus spinosa stem extract one or more of these.

On the other hand, the embodiment of the present application provides a kind of preparation method of whole plant anhydrous lip glaze, comprising:

Heat the vegetable oil and vegetable wax to 60-90℃, add it to the mixture containing vegetable oil, plant powder and plant dispersant, stir and cool to 40-45℃, then add plant antioxidant, plant preservative, plant The essential oils and plant extracts are stirred well to obtain the all-plant anhydrous lip gloss.

Compared with the prior art, the present application at least has the following beneficial effects:

(1) The all-plant anhydrous lip glaze provided by this application has fine texture, uniform color, good moisturizing and moisturizing effects, strong antiseptic and anti-inflammatory properties, high safety, and is also very friendly to users with sensitive skin, It fits the current concept of "pure beauty" very well.

First of all, the all-plant anhydrous lip glaze of the present application uses 100% all-plant-derived materials as raw materials, replacing chemical synthesis or non-natural ingredients in traditional beauty products, making the lip glaze safer and satisfying consumers' expectations for natural products. need. Secondly, since there is no water phase component in the raw material of the all-plant anhydrous lip glaze, there are no problems such as uneven color and poor moisturizing effect caused by the difficulty of mutual dissolution of water and oil. In addition, by adding efficient plant powder and plant dispersant, the application can improve the stability of the whole plant anhydrous lip glaze, and improve the color saturation of the whole plant anhydrous lip glaze; at the same time, the use of plant preservatives can Further enhance the safety level of the all-plant anhydrous lip glaze.

(2) The preparation method of the all-plant anhydrous lip glaze provided by the present application is simple in process, short in time consumption, low in equipment requirements, well compatible with existing processes, and has great potential for large-scale application.

Detailed ways

In order to make the application purpose, technical solutions and beneficial technical effects of the present application clearer, the present application will be further described in detail below with reference to the embodiments. It should be understood that the embodiments described in this specification are only for explaining the present application, but not for limiting the present application.

For the sake of brevity, this application only explicitly discloses some numerical ranges. However, any lower limit can be combined with any upper limit to form an unspecified range; and any lower limit can be combined with any other lower limit to form an unspecified range, and likewise any upper limit can be combined with any other upper limit to form an unspecified range. Furthermore, every point or single value between the endpoints of a range is included within the range, even if not expressly recited. Thus, each point or single value may serve as its own lower or upper limit in combination with any other point or single value or with other lower or upper limits to form a range not expressly recited.

In the description of the present application, it should be noted that, unless otherwise specified, "above" and "below" are inclusive of numbers, and "multiple" in "one or more" means two or both. above.

The above summary of this application is not intended to describe each disclosed embodiment or every implementation in this application. The following description illustrates exemplary embodiments in more detail. In various places throughout this application, guidance is provided through a series of examples, which examples can be used in various combinations. In various instances, the enumeration is merely a representative group and should not be construed as exhaustive.

The raw materials of the existing lip glaze are complex, often containing many chemical synthetic or non-natural ingredients, low safety, easy to cause allergic reactions, such as chapped lips, peeling, cheilitis, etc., and even contain carcinogens and seriously endanger health. .

Based on this, the inventor has conducted a lot of research and found that the safety performance of the lip glaze can be improved by preparing a water-free all-plant anhydrous lip glaze, and then under the synergistic effect of each plant component, the all-plant anhydrous lip glaze can be made The glaze has excellent safety, skin fit, ductility and smoothness.

All plant anhydrous lip gloss

On the one hand, the embodiment of the present application provides a kind of whole plant anhydrous lip glaze, which comprises by weight percentage:

Vegetable oils and fats: 40%-60%,

Vegetable wax: 0.1-5%,

Plant powder: 10%-30%,

Plant dispersant: 10%-30%,

Plant antioxidants: 0.1%-1%,

Plant preservatives: 0.1%-1%,

Plant essential oils: 0.1%-1%,

Plant extract: 0.1%-1%.

According to the embodiment of the present application, the above-mentioned all-plant anhydrous lip glaze is mainly composed of vegetable oil, and by adding a certain content of plant raw materials such as vegetable wax, plant powder, plant dispersant, etc., it can obtain fine texture, uniform color, moisturizing, moisturizing and safety. High all plant anhydrous lip gloss.

According to the embodiments of the present application, the all-plant anhydrous lip glaze of the present application uses 100% whole plant-derived materials as raw materials, replacing chemical synthesis or non-natural ingredients in traditional beauty products, making the lip glaze safer and satisfying consumption. demand for natural products. Secondly, because the raw materials of the all-plant anhydrous lip glaze do not contain water, there are no problems such as uneven color and poor moisturizing effect caused by the difficulty of mutual dissolution of water and oil.

In some embodiments, the vegetable oil may be selected from vegetable squalane, jojoba oil, sunflower seed oil, castor oil, white chia seed oil, coconut oil, shea butter, grapeseed oil, macadamia nut oil, olive oil , one or more of palm oil, cocoa butter, jojoba butter, sugar gum, octyldodecanol, caprylic capric triglyceride and coco-caprylic capric triglyceride. Illustratively, the vegetable oil can be sugar gum, can also be coconut oil, can also be a mixture of caprylic capric triglyceride and coco-caprylic capric triglyceride, or can be sunflower seed oil, castor oil and coconut oil. Vegetable oils and fats may also be selected from any of the above vegetable oils or mixtures consisting of any of the above vegetable oils and fats.

According to the embodiment of the present application, grease is an indispensable component in the lip glaze, and the above listed oils are all vegetable oils extracted from plants, and vegetable oils can ensure the safety, moisturizing, Fluidity and ductility, and ensure its moisturizing effect.

According to the embodiments of the present application, the sugar gum in the vegetable oil has excellent solubility and compatibility, and its water-binding ability is very strong, and the water-absorbing effect is good even in a low-humidity environment, so it can prevent skin moisture Evaporates again with instant and long-lasting hydration. In application, sugar gum not only has moisturizing and soothing effects, but also can give cosmetic products a soft and silky skin feel; in addition, it can also reduce the volatilization rate of essence, and bring long-lasting fragrance to products. At the same time, the sugar gum has a certain viscosity, and when combined with solid vegetable oils and vegetable waxes, it has a plastic effect and can improve the use texture of the lip glaze; at the same time, it can also form a breathable sugar film on the skin surface, which can better develop color. Provides a natural glow from the inside out.

According to the examples of the present application, octyldodecanol belongs to isomeric alcohols, has a smooth skin feel, and has an emollient effect. Absorption of functional active substances.

According to the embodiments of the present application, caprylic acid triglyceride is a vegetable oil with good skin feel, has good ductility, can make the skin feel slippery but not greasy, and has the effect of improving the uniformity and fineness of lip glaze. Very good effect.

According to the embodiment of the present application, coco-caprylic acid capric triglyceride is a mixture of natural coconut oil, caprylic acid and capric acid esterified, which is an emollient and emollient with good extensibility, and can be used as a cyclomethicone An alternative to silicone grease-based volatile silicones. Coco-Caprylic Capric Triglyceride provides extra oil to the skin, reduces moisture evaporation inside the skin, enhances skin hydration, leaves skin soft and elastic, and also makes the all-vegetable anhydrous lip gloss easier to apply.

In some embodiments, the vegetable wax may be selected from one or more of candelilla wax, sunflower wax, carnauba wax, rice wax, jasmine wax, dextrin palmitate, and dextrin isostearate. Illustratively, the vegetable wax can be candelilla wax, jasmine wax, or a mixture of dextrin palmitate and dextrin isostearate. The vegetable wax may also be selected from any one of the above vegetable waxes or a mixture of any of the above.

According to the embodiments of the present application, the above-mentioned vegetable wax is a pure natural material extracted from plants by methods such as pressing, extraction, etc., which is safe to use, has little damage to the skin, and has a high degree of fit with the skin. At the same time, the vegetable wax also maintains One of the important raw materials for the coagulation and moisturizing properties of all-plant anhydrous lip glaze.

According to the examples of the present application, dextrin palmitate and dextrin isostearate are composed of dextrin and higher fatty acid esters extracted from starch, when the amount of dextrin palmitate and dextrin isostearate is small in lip glaze (2- 4wt%), can increase the viscosity of the lip glaze system; when the dosage is larger (5-15wt%), it can make the liquid vegetable oil ester form translucent to transparent, thermally reversible gel, and improve the whole plant anhydrous lip glaze to the lip glaze. Skin affinity and stretchability when applied.

In some embodiments, the plant powder may include an oil-soluble toner and a filler, wherein the oil-soluble toner is selected from the group consisting of lycopene, beetroot, safflower, purple sweet potato, elderberry, and red radish One or more, the filler is selected from corn starch and/or rice starch.

According to the embodiments of the present application, the above-mentioned oil-soluble toner has strong hydrophilicity, and when it is modified by hydrophobization, it has good dispersibility in vegetable oils and fats, and has high color rendering and chromaticity, which is not easy to discoloration.

In some embodiments, the vegetable dispersant may be selected from the group consisting of soy lecithin, polyglycerol-3 diisostearate, polyglycerol-2 triisostearate, polyglycerol 2-dipolyhydroxystearate and One or more of oleic/linoleic/linolenic polyglycerides.

According to the embodiments of the present application, polyglycerol-3 diisostearate, polyglycerol-2 triisostearate and polyglycerol 2-dipolyhydroxystearate are compatible with oil phase systems of various polarities , has good toner dispersing ability, suitable for anhydrous, waterproof material system. Oleic/linoleic/linolenic polyglycerides are natural plant-derived products with excellent sensory benefits, deep moisturizing, water repellency and anti-wrinkle properties.

In some embodiments, the plant antioxidant may be selected from one or more of vitamin E, tea polyphenols and rice bran oil.

According to the embodiments of the present application, the plant antioxidant can prevent or delay the oxidation of the unsaturated components in the all-plant anhydrous lip glaze, and prolong the service life of the all-plant anhydrous lip glaze.

In some embodiments, the botanical preservative may be selected from one or more of anisic acid, Paeonia suffruticosa root bark extract and Magnolia bark extract.

According to the embodiments of the present application, the plant preservative can inhibit the growth and reproduction of microorganisms in the whole plant anhydrous lip glaze, keep the properties of the whole plant anhydrous lip glaze stable, make it less likely to deteriorate after being opened and used, and prolong the storage time. Among them, the above-mentioned anisic acid has better antiseptic effect under acidic conditions. The root bark extract of peony has a certain inhibitory effect on Escherichia coli, Staphylococcus aureus, Salmonella, Aspergillus niger, Candida, acne pathogens and other bacteria, molds, and fungi. The main active components of Magnolia bark extract are honokiol and honokiol, which have good inhibitory effects on Escherichia coli, Staphylococcus aureus, Bacillus subtilis, etc.

In some embodiments, the plant essential oil may be selected from one or more of tea tree essential oil, rose essential oil, jasmine essential oil, sweet orange essential oil, chamomile essential oil, and lavender essential oil.

According to the embodiment of the present application, the plant essential oil can enhance the moisturizing and moisturizing feeling of the whole plant anhydrous lip glaze, and has a good repairing effect, and can nourish and relieve the dryness and peeling of the skin in time. Anhydrous lip gloss with specific fragrance.

In some embodiments, the plant extract may be selected from the group consisting of jasmine flower extract, camellia flower extract, Bletilla striata root extract, Atractylodes Rhizoma root extract, Atractylodes Rhizoma root extract, peach blossom extract, cherry extract, and Cactus spinosa stem extract one or more.

According to the embodiments of the present application, the above-mentioned plant extracts can prevent skin inflammation, and at the same time, can moisturize skin keratinocytes and help to keep the skin in a moist state.

According to the embodiments of the present application, the all-plant anhydrous lip glaze provided by the present application has fine texture, uniform color, good moisturizing and moisturizing effects, strong antiseptic and anti-inflammatory properties, and high safety, which is suitable for users with sensitive skin. Also very friendly.

Preparation method of whole plant anhydrous lip glaze

On the other hand, the present application also proposes a method for preparing an all-plant anhydrous lip glaze, comprising:

The vegetable oil and vegetable wax are heated to 60-90 ° C, and added to the mixture containing the vegetable oil, vegetable powder and vegetable dispersant, stirred and cooled to 40-45 ° C, and then the vegetable antioxidant, vegetable Preservatives, plant essential oils and plant extracts are mixed well to obtain the all-plant anhydrous lip gloss.

The preparation method of the all-plant anhydrous lip glaze provided by the present application is simple in procedure, short in time consumption, low in equipment requirements, well compatible with existing processes, and has great potential for large-scale application.

Example

The following examples describe the disclosure of the present application in more detail, and these examples are provided for illustrative purposes only, as various modifications and changes within the scope of the disclosure of the present application will be apparent to those skilled in the art. Unless otherwise stated, all parts, percentages, and ratios reported in the following examples are on a weight basis, and all reagents used in the examples are either commercially available or synthesized according to conventional methods, and can be directly Used without further processing, and the instruments used in the examples are commercially available.

Example 1

An all-plant anhydrous lip glaze, comprising the following components by mass percentage: sugar gum 36%, plant squalane 10%, sunflower seed oil 2%, jojoba butter 4.7%, sunflower wax 1.4%, polyglycerol- 3 Diisostearate 12%, Coco-Caprylic Capric Triglyceride 10%, Elderberry Color 17%, Corn Starch 6%, Rice Bran Oil 0.4%, Anisic Acid 0.05%, Paeonia Root Bark Extract 0.15%, jasmine essential oil 0.1%, camellia extract 0.2%;

The preparation method of whole plant anhydrous lip glaze is as follows:

(1) elderberry color powder, corn starch are dispersed in the mixture of polyglycerol-3 diisostearate, cocoyl-caprylic acid capric triglyceride and vegetable squalane, stir;

(2) sugar gum, sunflower seed oil, jojoba fat, sunflower wax are heated to 70 ℃, add in the color paste obtained in step (1) and stir well;

(3) After the mixture obtained in step (2) is cooled to 40-45° C., rice bran oil, anisic acid, Paeonia suffruticosa root bark extract, jasmine essential oil, and camellia flower extract are added thereto, and the whole plant source anhydrous can be obtained by mixing evenly. Lip Glaze.

Example 2

An all-plant anhydrous lip glaze, comprising the following components by mass percentage: sugar gum 24%, plant squalane 8%, jojoba oil 6%, jojoba grease 19.4%, sunflower wax 0.2%, polyglycerol- 2 Triisostearate 10%, Dextrin Palmitate 1%, Caprylic Capric Triglyceride 12%, Radish Red Powder 12.5%, Corn Starch 6%, Tea Polyphenols 0.4%, Anisic Acid 0.05%, Thick Hackberry Bark Extract 0.15%, Rose Essential Oil 0.1%, Atractylodes Rhizoma Root Extract 0.2%;

The preparation method of whole plant anhydrous lip glaze is as follows:

(1) radish red powder and corn starch are dispersed in polyglycerol-2 triisostearate, dextrin palmitate, caprylic capric triglyceride and vegetable squalane mixture, and stir well;

(2) sugar gum, jojoba oil, jojoba grease, sunflower wax are heated to 65 ℃, add in the color paste obtained in step (1) and stir well;

(3) The mixture obtained in step (2) is cooled to 40-45° C., to which tea polyphenols, anisic acid, Magnolia bark extract, rose essential oil and Atractylodes Rhizoma root extract are added, and the whole plant without Water Lip Glaze.

Example 3

An all-plant anhydrous lip glaze, comprising the following components by mass percentage: sugar gum 30%, jojoba oil 10%, castor oil 6%, cocoa butter 6.7%, candelilla wax 0.5%, polyglycerol-3 Diisostearate 12%, Octyldodecanol 10%, Purple Sweet Potato Color Powder 20%, Rice Starch 4%, Tea Polyphenols 0.4%, Paeonia Root Bark Extract 0.1%, Magnolia Bark Extract 0.1% , Sweet Orange Essential Oil 0.1%, Cherry Extract 0.1%;

The preparation method of whole plant anhydrous lip glaze is as follows:

(1) disperse purple sweet potato color powder and rice starch in polyglycerol-3 diisostearate, octyldodecanol and jojoba oil mixture, stir evenly;

(2) sugar gum, castor oil, cocoa butter, candelilla wax are heated to 70 ℃, add in the color paste obtained in step (1) and stir well;

(3) After the mixture obtained in step (2) is cooled to 40-45° C., tea polyphenols, Paeonia suffruticosa root bark extract, Magnolia bark extract, sweet orange essential oil, and cherry extract are added thereto, and the mixture is uniformly obtained. All plant anhydrous lip gloss.

Example 4

An all-plant anhydrous lip glaze, comprising the following components by mass percentage: sugar gum 26%, plant squalane 10%, white chia seed oil 8%, jojoba fat 14%, carnauba wax 0.2%, poly Glycerol 2-Dipolyhydroxystearate 8%, Dextrin Isostearate 1%, Coco-Caprylic Caprate Triglyceride 8%, Soy Lecithin 1%, Lycopene 20%, Rice Starch 3%, Tea Polyphenols 0.4%, Anisic Acid 0.05%, Magnolia Bark Extract 0.15%, Lavender Essential Oil 0.1%, Twisted Cactus Stem Extract 0.1%;

The preparation method of the whole plant source anhydrous lip glaze of the present embodiment is as follows:

(1) Disperse lycopene and rice starch in polyglycerol 2-dipolyhydroxystearate, dextrin isostearate, coco-caprylic acid capric triglyceride, soybean lecithin and vegetable squalane In the alkane mixture, stir well;

(2) sugar gum, white chia seed oil, jojoba fat, carnauba wax are heated to 75 ℃, add in the color paste obtained in step (1) and stir well;

(3) The mixture obtained in step (2) is cooled to 40-45° C., to which tea polyphenols, anisic acid, Magnolia bark extract, lavender essential oil, and thorn cactus stem extract are added, and the mixture is uniformly mixed. Botanical anhydrous lip gloss.

Comparative ratio

Comparative Example 1

A non-whole plant anhydrous lip glaze, comprising the following components by mass percentage: 36% of sugar gum, 11.25% of hydrogenated polyisobutylene, 2% of isododecane, 11.7% of polydimethylsiloxane, and synthetic wax 4.4%, Cetyl Macrogol/Polypropylene Glycol-10/1 Dimethicone 2.0%, Octyldodecanol 10%, Red Iron Oxide 17%, Nylon Powder 6%, Anisic Acid 0.05%, Paeonia suffruticosa root bark extract 0.15%, jasmine essential oil 0.15%, camellia extract 0.2%;

The preparation method of whole plant anhydrous lip glaze is as follows:

(1) Disperse red iron oxide and nylon powder in the mixture of cetyl polyethylene glycol/polypropylene glycol-10/1 dimethylsiloxane and octyldodecanol, and stir evenly;

(2) heating sugar gum, hydrogenated polyisobutylene, isododecane, polydimethylsiloxane, and synthetic wax to 70° C., adding to the color paste obtained in step (1) and stirring uniformly;

(3) The mixture obtained in step (2) is cooled to 40-45° C., anisic acid, peony root bark extract, jasmine essential oil, and camellia flower extract are added thereto, and the anhydrous lip glaze is obtained by mixing evenly. .

Comparative Example 2

A non-whole plant anhydrous lip glaze, comprising the following components by mass percentage: sugar gum 36%, olive oil squalane 10%, sunflower seed oil 2%, jojoba butter 4.7%, sunflower wax 1.4%, poly Glycerin-3 Diisostearate 12%, Coco-Caprylic Capric Triglyceride 10%, Elderberry Color 17%, Corn Starch 5.5%, Rice Bran Oil 0.4%, Caprylyl Glycol 0.05%, Phenoxy Ethanol 0.15%, ethylhexylglycerin 0.5%, jasmine essential oil 0.1%, camellia extract 0.2%;

The preparation method of whole plant anhydrous lip glaze is as follows:

(1) elderberry color powder, corn starch are dispersed in the mixture of polyglycerol-3 diisostearate, coco-caprylic acid capric triglyceride and olive oil squalane, stir;

(2) heating sugar gum, sunflower seed oil, jojoba fat, and sunflower wax to 70° C., adding to the color paste obtained in step (1) and stirring uniformly;

(3) The mixture obtained in step (2) is cooled to 40-45° C., and rice bran oil, caprylyl glycol, phenoxyethanol, ethylhexyl glycerin, jasmine essential oil, and camellia extract are added thereto, and the mixture is homogeneously obtained. Anhydrous lip gloss derived from plant preservatives.

Comparative Example 3

A non-whole plant anhydrous lip glaze, comprising the following components by mass percentage: octyldodecanol 35%, polydimethylsiloxane 10%, hydrogenated polyisobutylene 9%, synthetic wax 4.7%, microcrystalline Wax 6.4%, Cetyl Macrogol/Polypropylene Glycol-10/1 Dimethicone 2%, Caprylic/Capric Triglyceride 15%, Red Iron Oxide 10%, Talc 6%, Tocopherol 0.4%, phenoxyethanol 0.5%, ethylhexylglycerol 1%;

The preparation method of whole plant anhydrous lip glaze is as follows:

(1) Disperse red iron oxide and talc in the mixture of cetyl polyethylene glycol/polypropylene glycol-10/1 dimethylsiloxane, caprylic acid/capric acid triglyceride, and stir well;

(2) heating octyldodecanol, polydimethylsiloxane, hydrogenated polyisobutylene, synthetic wax, and microcrystalline wax to 70° C., adding to the color paste obtained in step (1) and stirring uniformly;

(3) After the mixture obtained in step (2) is cooled to 40-45° C., tocopherol, phenoxyethanol and ethylhexyl glycerol are added thereto, and the non-plant source anhydrous lip glaze can be obtained by mixing evenly.

Compared with Example 1, Comparative Example 1 contains non-plant raw materials, Comparative Example 2 contains non-plant raw materials and no plant preservatives are added, and Comparative Example 3 contains non-plant raw materials and no plant extracts are added. thing.

test section

1) Stability test: (1) Place in a 40-50 ℃ electric heating constant temperature incubator for 30-50 days, and observe after returning to room temperature; (2) within 24 hours, frequently change back and forth between 0-50 ℃, and so on repeatedly 15-30 days, observe after returning to room temperature, (3) store at -5°C and 40°C for 3 times, each time for 24h, that is, after storing at -5°C for 24h, store at room temperature for 24h, and then put in Stored in a 40°C incubator for 24h, cycled 3 times in turn, and observed its stability. (4) Store at -5°C for 1 week and observe its stability.

2) The centrifugation test method is as follows: add the sample to the centrifuge and rotate at 10000rpm for 10-15min or 3000rpm for 30min or 300rpm for 1h, observe the stratification and separation of the liquid to obtain the results in Table 1 below.

The all-plant anhydrous lip glazes of the above-mentioned Examples 1-4 and Comparative Examples 1-3 were subjected to relevant performance tests. The test results of Examples 1 to 4 and Comparative Examples 1 to 3 are shown in Table 1 below.

Table 1 The performance test results of the whole plant anhydrous lip glazes of Examples 1-4 and Comparative Examples 1-3

sample heat resistant hardy stability Example 1 No significant changes No significant changes No delamination Example 2 No significant changes No significant changes No delamination Example 3 No significant changes No significant changes No delamination Example 4 No significant changes No significant changes No delamination Comparative Example 1 No significant changes No significant changes No delamination Comparative Example 2 No significant changes No significant changes No delamination Comparative Example 3 No significant changes No significant changes No delamination

From the test results in Table 1 above, it can be seen that the all-plant anhydrous lip glazes of Examples 1-4 have good heat resistance, cold resistance and stability, and can achieve the same effect as the non-whole-plant anhydrous lip glazes of Comparative Examples 1-3.

3) Corrosion resistance test:

The selected strains were Staphylococcus aureus, Escherichia coli, Pseudomonas aeruginosa, Candida albicans and Aspergillus niger.

The medium is beef extract peptone medium and agar medium.

The configuration of the test bacteria liquid:

(1) Configuration of standard suspension

The concentration of the suspension prepared by mixing 9.9 mL of 1% sulfuric acid and 0.1 mL of 1% barium chloride is 3*10 ⁸ cfu/mL, and then the suspension is diluted 3 times.

(2) Preparation of bacterial suspension

Before the experiment, the strains were inoculated on the slants of each medium, and incubated at a constant temperature of 36 °C for 48 h. The cultured active strains were washed with sterilized saline into a sterilized conical flask, and shaken well. Use a pipette to draw the bacterial solution from the conical flask for dilution until the turbidity is the same as that of the standard suspension (3*10 ⁸ cfu/mL);

At this time, dilute the diluted bacterial solution by 3 times, that is, the bacterial suspension with a concentration of 1*10 ⁸ cfu/mL, to determine the number of bacteria.

(3) Preparation of fungal suspension

Wash the cultured active strains with sterilized saline into a sterilized conical flask, shake and shake well; use a pipette to dilute the bacterial solution from the conical flask by 10 times, and each dilution uses Counting on a hemocytometer, the total number of molds must be 190-210 in 5 medium cells. The bacterial suspension within this range is the required 1*10 ⁸ cfu/mL mold bacterial suspension to determine the number of molds.

Inoculation:

The inoculation method is single-bacteria inoculation: do a separate experiment for each test strain, and it is easy to understand the susceptibility of each microorganism to the preservative system.

The number of inoculations is one inoculation: it is only inoculated once at the beginning of the test, and the whole test period is 28 days (a 28-day microbiological experiment with one addition of bacteria).

Operation method:

Weigh 30 g of the sample to be tested, and add 0.3 mL of bacterial suspension and mold suspension with a concentration of 1*10 ⁷ to 1*10 ⁸ cfu/mL, stir evenly with a sterile key, and cover with plastic wrap. Culture in an incubator at 32.5 ± 2.5 °C, and mold in an incubator at 22.5 ± 2.5 °C.

Since the samples of this invention are all oil-soluble, take 10g of the sample, add 10mL of sterile Tween-80, 10mL of sterile white mineral oil and 70mL of sterile normal saline, and mix well with a sterile glass rod;

Aspirate 1mL of the diluted sample solution, add it to 9mL of sterile physiological saline, and dilute in sequence, respectively ^10-1 , ^10-2 , ^10-3 , ^10-4 , ^10-5 , ^10-6 , and ^10-7 , etc. Dilution: Take three sample solutions of appropriate dilution, pipette 1 mL respectively into sterilized plates, count the colonies, and do two parallels.

nourish:

Bacteria were cultured in an incubator at 32.5±2.5°C;

The mold is cultivated in an incubator at 22.5±2.5℃;

The mixed bacteria were cultured in an incubator at 28°C.

Colony count:

After 0, 7, 14, 21, and 28 days of separation and calculation of the total number of live bacteria and mold in the sample, put the plate back in the incubator for the next observation. Do not open the plate during the observation to avoid burning bacteria cannot be observed.

Standard method for colony counting:

1. First select the plate with the average number of colonies between 30 and 300 as the measurement range of the total number of bacterial colonies, and select the plate with the average number of colonies between 5 and 50 as the measurement range of the total number of mold colonies;

2. There are two dilutions between 30 and 300, and the ratio is calculated. If the ratio is less than or equal to 2, report the average number; if the ratio is greater than 2, calculate the total number of bacteria with the smaller dilution;

3. All dilutions are greater than 300, and the average colony with the highest dilution is calculated;

4. All dilutions are less than 30, and the number of evaluated colonies with the lowest dilution is calculated;

5. All dilutions are outside 30-300, one of them is greater than 300, and the adjacent dilution is less than 30, then the average number of colonies closest to 30 or 300 is calculated;

6. If there are continuous flaky or flower-like colonies in the plate, it should not be counted;

7. If the flaky colonies are less than half of the plate, but the colonies in the other half are uniform, you can count the plate colonies *2 to report the number of colonies in the whole plate.

The whole plant anhydrous lip glazes of the above-mentioned Examples 1-4 and Comparative Examples 1-3 were subjected to relevant performance tests. The test results of Examples 1 to 4 and Comparative Examples 1 to 3 are shown in Table 2 below.

The performance test results of table 2 embodiment 1～4 and comparative example 1～3 whole plant anhydrous lip glaze

From the test results in Table 2 above, it can be seen that the all-plant anhydrous lip glazes of Examples 1 to 4 have reached the standard of antiseptic effect of cosmetics after 1 day. The preservative effect of the non-whole plant anhydrous lip glaze of Comparative Examples 1 to 3 can also meet the preservative requirements of cosmetics, but its safety performance is low, which may cause problems such as cheilitis.

4) Anti-inflammatory test

Healthy male SD rats were randomly divided into model group, indomethacin group and example sample group, with 10 rats in each group. The skin was administered continuously for 3 days, and the model group was administered deionized water. One hour after the last administration, 0.05 mL of 1% carrageenan was subcutaneously injected into the right hind foot pad of the rats to induce inflammation. Before the inflammation and 1, 2, 4, 6, and 24 hours after the inflammation, the diameter of 0.5 cm below the bare joint of the right hind limb of each rat was measured by magnifying 8 times. The difference was taken as swelling degree.

The whole plant anhydrous lip glazes of the above-mentioned Examples 1-4 and Comparative Examples 1-3 were subjected to relevant performance tests. The test results of Examples 1-4 and Comparative Examples 1-3 are shown in Table 3 below.

The performance test results of table 3 embodiment 1～4 and comparative example 1～3 whole plant anhydrous lip glaze

It can be seen from the above Table 3 that the anti-inflammatory effects of the all-plant anhydrous lip glazes of Examples 1 to 4 are good, while in Comparative Examples 1 to 3, since there are no substances containing anti-inflammatory effects such as plant extracts, the right hindlimb of the rats is naked. The swelling degree of the joint is relatively large, so the anti-inflammatory effect of the non-full plant anhydrous lip glaze in Comparative Examples 1 to 3 is low, which is not conducive to the use of sensitive skin consumers.

It can be seen from the above test results that the all-plant anhydrous lip glazes of Examples 1 to 4 have good heat resistance, cold resistance and stability, and both anti-corrosion and anti-inflammatory effects can meet actual requirements, and are innovative and novel in the beauty market. It has strong product competitiveness. From the test results of Comparative Examples 1 to 3, it can be seen that the stability, anti-corrosion, anti-inflammatory and other safety properties of the non-whole plant anhydrous lip glaze are poor.

To sum up, the all-plant anhydrous lip glaze of the present application uses 100% all-plant-derived materials as raw materials, which replaces chemical synthesis or non-natural ingredients in traditional beauty products, making the lip glaze safer and satisfying consumers. Demand for natural products. Secondly, because the raw materials of the all-plant anhydrous lip glaze do not contain water, there are no problems such as uneven color and poor moisturizing effect caused by the difficulty of mutual dissolution of water and oil. In addition, by adding efficient plant powder and plant dispersant, the application can improve the stability of the whole plant anhydrous lip glaze, and improve the color saturation of the whole plant anhydrous lip glaze; at the same time, the use of plant preservatives can Further enhance the safety level of the all-plant anhydrous lip glaze.

The above are only specific embodiments of the present application, but the protection scope of the present application is not limited thereto. Any person skilled in the art can easily think of various equivalents within the technical scope disclosed in the present application. Modifications or substitutions shall be covered by the protection scope of this application. Therefore, the protection scope of the present application shall be subject to the protection scope of the claims.

Claims (10)

1. a whole plant anhydrous lip glaze, is characterized in that, described whole plant anhydrous lip glaze comprises by weight percentage: Vegetable oils and fats: 40%-60%, Vegetable wax: 0.1-5%, Plant powder: 10%-30%, Plant dispersant: 10%-30%, Plant antioxidants: 0.1%-1%, Plant preservatives: 0.1%-1%, Plant essential oils: 0.1%-1%, Plant extract: 0.1%-1%. 2. whole plant anhydrous lip glaze according to claim 1 is characterized in that, described vegetable oil is selected from vegetable squalane, jojoba oil, sunflower seed oil, castor oil, white chia seed oil, coconut oil, Shea Butter, Grapeseed Oil, Macadamia Oil, Olive Oil, Palm Oil, Cocoa Butter, Jojoba Butter, Gum Gum, Caprylyl Dodecanol, Caprylic Triglyceride and Coco-Capric Capric Glycerin one or more of the triester. 3. The whole plant anhydrous lip glaze according to claim 1, wherein the vegetable wax is selected from candelilla wax, sunflower wax, carnauba wax, rice bran wax, jasmine wax, dextrin palmitate and One or more of dextrin isostearates. 4. all-plant anhydrous lip glaze according to claim 1, is characterized in that, described plant powder comprises oil-soluble toner and filler, Wherein, the oil-soluble toner is selected from one or more of lycopene, beet red, safflower red, purple sweet potato, elderberry and radish red; The filler is selected from corn starch and/or rice starch. 5. whole plant anhydrous lip glaze according to claim 1 is characterized in that, described plant dispersant is selected from soybean lecithin, polyglycerol-3 diisostearate, polyglycerol-2 triisostearate one or more of polyglycerol 2-dipolyhydroxystearate and oleic/linoleic/linolenic acid esters. 6 . The whole plant anhydrous lip glaze according to claim 1 , wherein the plant antioxidant is selected from one or more of vitamin E, tea polyphenols and rice bran oil. 7 . 7. The whole plant anhydrous lip glaze according to claim 1, wherein the plant preservative is selected from one or more of anisic acid, peony root bark extract and Magnolia bark extract. 8. whole plant anhydrous lip glaze according to claim 1, is characterized in that, described plant essential oil is selected from one or more in tea tree essential oil, rose essential oil, jasmine essential oil, sweet orange essential oil, chamomile essential oil and lavender essential oil kind. 9. The whole plant anhydrous lip glaze according to claim 1, wherein the plant extract is selected from the group consisting of jasmine flower extract, camellia flower extract, Bletilla striata root extract, Atractylodes Rhizoma root extract, Atractylodes Rhizoma root extract, peach blossom One or more of extract, cherry extract, and Twisted Cactus stem extract. 10. a method for preparing the whole plant anhydrous lip glaze described in any one of claims 1-9, is characterized in that, comprising: The vegetable oil and vegetable wax are heated to 60-90°C, and added to the mixture containing the vegetable oil, vegetable powder and vegetable dispersant, stirred and cooled to 40-45°C, and then the vegetable antioxidant is added , plant preservatives, plant essential oils and plant extracts are stirred evenly to obtain the all-plant anhydrous lip glaze.