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CN114923848B - Device and method for evaluating flushing efficiency of high-temperature high-pressure well cementation two interfaces - Google Patents

Device and method for evaluating flushing efficiency of high-temperature high-pressure well cementation two interfaces Download PDF

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CN114923848B
CN114923848B CN202210451514.3A CN202210451514A CN114923848B CN 114923848 B CN114923848 B CN 114923848B CN 202210451514 A CN202210451514 A CN 202210451514A CN 114923848 B CN114923848 B CN 114923848B
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袁彬
杨朔
徐璧华
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Southwest Petroleum University
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    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
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Abstract

The invention discloses a method for detecting flushing efficiency of two interfaces of high-temperature high-pressure well cementation, which comprises the steps of selecting corresponding stirring cylinders through on-site annular gaps, installing the corresponding stirring cylinders on a magnetic stirrer, and sealing a kettle body; then pumping flushing liquid, determining flushing time according to experiment requirements, and adjusting the temperature and pressure of the kettle body to the temperature and pressure required by the experiment; according to different on-site flushing fluid types, different rotating speed formulas are adopted, the rotating speed of the outer cylinder is calculated according to the construction displacement and the annular space, and the initial fluid loss flow Q 0 of the artificial rock core is measured and recorded through a real-time flowmeter; pumping drilling fluid into the kettle body, heating and boosting, starting a magnetic stirrer, simulating the hydraulic filtration of the drilling fluid to form mud cakes, and measuring and recording the flow Q 1 of the drilling fluid through a real-time flowmeter. The invention has the characteristics of simple operation, real time and accuracy.

Description

一种高温高压固井二界面冲洗效率评价装置及方法A device and method for evaluating flushing efficiency of two interfaces of high temperature and high pressure cementing

技术领域Technical Field

本发明涉及石油工程技术领域,具体为一种检测高温高压固井二界面冲洗效率的方法。The invention relates to the technical field of petroleum engineering, in particular to a method for detecting flushing efficiency of a high-temperature and high-pressure cementing interface.

背景技术Background Art

钻井过程中,在压差作用下,钻井液会发生滤失在井壁上形成泥饼,它会使水泥环与地层岩石之间的胶结质量变差,在井筒内压变化的作用下,水泥环与地层岩石会剥离产生微裂缝,导致水泥环密封失效,引发油气水窜流。During the drilling process, under the action of pressure difference, the drilling fluid will be lost and form a mud cake on the well wall, which will deteriorate the bonding quality between the cement ring and the formation rock. Under the action of the change in wellbore internal pressure, the cement ring and the formation rock will peel off and produce microcracks, resulting in failure of the cement ring seal and triggering oil, gas and water channeling.

因此,在固井时必须将泥饼清除掉,通常采用冲洗液冲洗井壁的泥饼,改善固井二界面的胶结质量,提高胶结强度。冲洗液的冲洗效率决定着冲洗液的冲洗能力,通过对冲洗效率的评价能够实现对冲洗液体系的研发、优选。Therefore, the mud cake must be removed during cementing. Flushing fluid is usually used to flush the mud cake on the well wall to improve the bonding quality of the cementing interface and increase the bonding strength. The flushing efficiency of the flushing fluid determines the flushing capacity of the flushing fluid. The development and optimization of the flushing fluid system can be achieved through the evaluation of the flushing efficiency.

为此,国内外学者提出了一系列的评价固井二界面冲洗效率的装置及方法。国内评价二界面冲洗效率的装置和方法的专利有:“一种基于剪切速率相等原理的固井冲洗液评价装置及方法”(CN103541675B);“一种固井冲洗效率评价装置及方法”(CN104863533);“基于形成动态泥饼的固井冲洗液评价装置及其实验方法”(CN104849404);“一种钻井液滤饼压制及清洗效率一体化评价装置及方法”(CN110107235A);“固井注水泥钻井液滤饼冲洗效率评价装置及方法”(CN110617018A)。国内也有很多学者发表了评价二界面冲洗效率的相关论文,如:辜涛等.固井前置液冲洗效率评价方法——改进的旋转黏度计法[J].天然气工业,2020,40(11);李社坤等.页岩气水平井冲洗效率评价装置 [J].石油机械,2016,44(09);李韶利等.一种可视化冲洗液评价装置与方法[J]. 钻井液与完井液,2016,33(02);朱江林等.一种物理模拟冲洗液冲洗效率的评价方法[J].钻井液与完井液,2012,29(01);王广雷等.一种新型的冲洗效率评价方法[J].钻井液与完井液,2011,28(03);由福昌等.一种固井前置冲洗液冲洗效率的评价方法[J].钻井液与完井液,2009,26(06)等。国外学者有:Choi M等人通过荧光测量,确定了冲洗前后的泥饼厚度,进而评价冲洗效率(Choi M,etc. Novel methodology to evaluate displacement efficiency of drilling mudusing fluorescence in primary cementing[J].Journal of Petroleum Science &Engineering,2018,165:647-654)To this end, domestic and foreign scholars have proposed a series of devices and methods for evaluating the flushing efficiency of the two interfaces of cementing. The domestic patents for devices and methods for evaluating the flushing efficiency of the two interfaces include: "A cementing flushing fluid evaluation device and method based on the principle of equal shear rate" (CN103541675B); "A cementing flushing efficiency evaluation device and method" (CN104863533); "A cementing flushing fluid evaluation device and experimental method based on the formation of dynamic mud cake" (CN104849404); "A drilling fluid filter cake compression and cleaning efficiency integrated evaluation device and method" (CN110107235A); "Cementing cement drilling fluid filter cake flushing efficiency evaluation device and method" (CN110617018A). Many domestic scholars have also published papers on the evaluation of the flushing efficiency of the two interfaces, such as: Gu Tao et al. Evaluation method for flushing efficiency of cementing pre-flushing fluid-improved rotational viscometer method [J]. Natural Gas Industry, 2020, 40(11); Li Shekun et al. Shale gas horizontal well flushing efficiency evaluation device [J]. Petroleum Machinery, 2016, 44(09); Li Shaoli et al. A visual flushing fluid evaluation device and method [J]. Drilling Fluid and Completion Fluid, 2016, 33(02); Zhu Jianglin et al. A physical simulation flushing fluid evaluation method [J]. Drilling Fluid and Completion Fluid, 2012, 29(01); Wang Guanglei et al. A new flushing efficiency evaluation method [J]. Drilling Fluid and Completion Fluid, 2011, 28(03); You Fuchang et al. A method for evaluating the flushing efficiency of cementing pre-flushing fluid [J]. Drilling Fluid and Completion Fluid, 2009, 26(06), etc. Foreign scholars include: Choi M et al. determined the thickness of mud cake before and after flushing through fluorescence measurement, and then evaluated the flushing efficiency (Choi M, etc. Novel methodology to evaluate displacement efficiency of drilling mud using fluorescence in primary cementing [J]. Journal of Petroleum Science & Engineering, 2018, 165: 647-654)

现有的检测方法无法真实的模拟井下的实际环境,无法真实的模拟泥饼的形成过程,只能测量某一时间的冲洗效率,并且测出来的结果与井下的实际值差距较大。The existing detection methods cannot truly simulate the actual environment downhole, cannot truly simulate the mud cake formation process, can only measure the flushing efficiency at a certain time, and the measured results are far from the actual values downhole.

因此,设计操作简单、实时、准确的一种检测高温高压固井二界面冲洗效率的方法是很有必要的。Therefore, it is necessary to design a method that is simple to operate, real-time and accurate to detect the flushing efficiency of the second interface of high-temperature and high-pressure cementing.

发明内容Summary of the invention

本发明的目的在于提供一种检测高温高压固井二界面冲洗效率的方法,以解决上述背景技术中提出的问题。The object of the present invention is to provide a method for detecting the flushing efficiency of the second interface of high-temperature and high-pressure cementing, so as to solve the problems raised in the above-mentioned background technology.

为了解决上述技术问题,本发明提供如下技术方案:一种检测高温高压固井二界面冲洗效率的方法,该方法采用冲洗效率评价装置,该冲洗效率评价装置包括:釜体、人造岩心、岩心夹持器、搅拌筒、磁力搅拌器、金属滤网以及实时流量计;其中,所述釜体与冲洗液仓和钻井液仓均连通,其上设置有用于检测釜体内温度的温度传感器以及用于检测釜体内压力的压力传感器,该温度传感器和压力传感器均与电脑通过总线连接;所述人造岩心通过岩心夹持器可拆卸地固定在所述釜体的内部底部,岩心夹持器可拆卸地固定在釜体的内部底部;所述搅拌筒倒扣至所述人造岩心上,且其内部顶部未与人造岩心接触,其用于模拟钻井液动滤失形成泥饼以及不同的环空间隙下的转速;所述磁力搅拌器位于釜体顶部,其搅拌杆穿过釜体顶部固定在所述搅拌筒顶部,用于带动所述搅拌筒的转动;所述金属滤网套置在人造岩心上;所述釜体安装岩心夹持器的位置处设置有排液孔,该排液孔与人造岩心相连通;所述实时流量计设置于所述釜体的排液孔上,与电脑通过总线连接,用于测得排出的液体的流量;In order to solve the above technical problems, the present invention provides the following technical solutions: a method for detecting the flushing efficiency of the second interface of high-temperature and high-pressure cementing, the method adopts a flushing efficiency evaluation device, the flushing efficiency evaluation device comprises: a kettle, an artificial core, a core clamp, a mixing drum, a magnetic stirrer, a metal filter and a real-time flow meter; wherein the kettle is connected to both the flushing fluid tank and the drilling fluid tank, and is provided with a temperature sensor for detecting the temperature in the kettle and a pressure sensor for detecting the pressure in the kettle, the temperature sensor and the pressure sensor are both connected to a computer through a bus; the artificial core is detachably fixed to the inner bottom of the kettle through the core clamp, and the core clamp is used to fix the core of the kettle to the inner bottom of the kettle. The core holder is detachably fixed to the inner bottom of the kettle body; the mixing drum is inverted onto the artificial core, and the inner top thereof is not in contact with the artificial core, and is used to simulate the dynamic filtration of drilling fluid to form mud cakes and the rotation speed under different annular gaps; the magnetic stirrer is located at the top of the kettle body, and its stirring rod passes through the top of the kettle body and is fixed to the top of the mixing drum to drive the rotation of the mixing drum; the metal filter is sleeved on the artificial core; a drainage hole is provided at the position where the core holder is installed on the kettle body, and the drainage hole is connected to the artificial core; the real-time flow meter is provided on the drainage hole of the kettle body, and is connected to the computer through a bus to measure the flow rate of the discharged liquid;

该方法包含:The method includes:

(S1)通过现场环空间隙选择对应的搅拌筒,安装在磁力搅拌器上,封闭釜体;然后,泵入冲洗液,根据实验需要确定冲洗时间,将釜体的温度压力调整至实验所需的温度和压力;根据现场冲洗液类型的不同采用不同的转速公式,再根据施工排量和环空间隙计算外筒转速,通过实时流量计测量记录人造岩心的初始滤失流量Q0(S1) Select a mixing drum corresponding to the annular gap on site, install it on a magnetic stirrer, and seal the kettle body; then, pump in the flushing liquid, determine the flushing time according to the experimental needs, and adjust the temperature and pressure of the kettle body to the temperature and pressure required by the experiment; use different speed formulas according to the different types of flushing liquids on site, and then calculate the outer drum speed according to the construction displacement and the annular gap, and measure and record the initial filtration flow Q 0 of the artificial core through a real-time flow meter;

(S2)在釜体内泵入钻井液,升温升压,开启磁力搅拌器,模拟钻井液动滤失形成泥饼,通过实时流量计测量记录钻井液的流量Q1(S2) Pumping drilling fluid into the kettle, increasing the temperature and pressure, turning on the magnetic stirrer, simulating the dynamic filtration of the drilling fluid to form a mud cake, and measuring and recording the flow rate Q 1 of the drilling fluid by a real-time flow meter;

(S3)从釜体内泵出钻井液,泵入冲洗液,所设定的外筒转速、压力、温度、冲洗液用量及总体的冲洗时间参数与前面一致,进行冲洗,通过实时流量计可实时读取失水流量Q2,进而测得冲洗效率,为:(S3) Pumping out the drilling fluid from the kettle body and pumping in the flushing fluid. The outer cylinder speed, pressure, temperature, flushing fluid dosage and overall flushing time parameters are set to be consistent with the above parameters. Flushing is performed. The water loss flow Q 2 can be read in real time by the real-time flow meter, and the flushing efficiency is measured as follows:

所述外筒转速,为:The outer cylinder speed is:

(1)当冲洗液为宾汉流体时,外筒转速公式如下:(1) When the flushing fluid is Bingham fluid, the outer cylinder speed formula is as follows:

式中,λ为人造岩心与旋转外筒半径之比;D1为井眼直径,单位为m;D2为套管外径,单位为m;w为环空间隙,单位为m;Q为施工排量,单位为m3/min; n为外筒转速,单位为r/min;τ0为宾汉流体的动切力,单位为Pa;η为塑性黏度,单位为mPa·s;Wherein, λ is the ratio of the radius of the artificial core to the rotating outer cylinder; D1 is the borehole diameter, in m; D2 is the outer diameter of the casing, in m; w is the annular gap, in m; Q is the operation displacement, in m3 /min; n is the outer cylinder rotation speed, in r/min; τ0 is the dynamic shear force of the Bingham fluid, in Pa; η is the plastic viscosity, in mPa·s;

(2)当冲洗液为幂律流体时,外筒转速公式如下:(2) When the flushing fluid is a power-law fluid, the outer cylinder speed formula is as follows:

式中,λ为人造岩心与旋转外筒半径之比;D1为井眼直径,单位为m;D2为套管外径,单位为m;w为环空间隙,单位为m;Q为施工排量,单位为m3/min; n为外筒转速,单位为r/min;nm为幂律流体的流性指数;Where, λ is the ratio of the radius of the artificial core to the rotating outer cylinder; D1 is the borehole diameter, in m; D2 is the outer diameter of the casing, in m; w is the annular gap, in m; Q is the construction displacement, in m 3 /min; n is the outer cylinder rotation speed, in r/min; nm is the flow index of the power-law fluid;

(3)当冲洗液为牛顿流体时,即nm为1,外筒转速公式如下:(3) When the flushing fluid is a Newtonian fluid, that is, nm is 1, the outer cylinder speed formula is as follows:

式中,λ为人造岩心与旋转外筒半径之比;D1为井眼直径,单位为m;D2为套管外径,单位为m;w为环空间隙,单位为m;Q为施工排量,单位为m3/min; n为外筒转速,单位为r/min;Where, λ is the ratio of the radius of the artificial core to the rotating outer cylinder; D1 is the borehole diameter, in m; D2 is the outer diameter of the casing, in m; w is the annular gap, in m; Q is the construction displacement, in m 3 /min; n is the outer cylinder rotation speed, in r/min;

上述该旋转外筒为所述搅拌筒;井眼直径、套管外径、环空间隙以及施工排量均为施工现场参数;The rotating outer cylinder is the mixing cylinder; the wellbore diameter, casing outer diameter, annular space gap and construction displacement are all construction site parameters;

通过井眼直径、套管外径和岩心半径可以确定搅拌筒(4)半径,其公式如下:The radius of the mixing drum (4) can be determined by the borehole diameter, casing outer diameter and core radius, and the formula is as follows:

式中,D2为井眼直径,其单位为mm;D1为套管外径,其单位为mm;R2为搅拌筒(4)半径,其单位为mm;R1为岩心半径,其单位为mm;上述单位在计算时需要将其换算一致。Wherein, D2 is the borehole diameter, in mm; D1 is the outer diameter of the casing, in mm; R2 is the radius of the mixing drum (4), in mm; R1 is the core radius, in mm; the above units need to be converted to be consistent during calculation.

根据上述技术方案,本方法(S1)、(S3)中,温度20~200℃,压力0.1~ 30MPa,岩心尺寸24.5mm*75mm。According to the above technical solution, in the method (S1) and (S3), the temperature is 20-200°C, the pressure is 0.1-30MPa, and the core size is 24.5mm*75mm.

与现有技术相比,本发明所达到的有益效果是:Compared with the prior art, the beneficial effects achieved by the present invention are:

本发明可以在高温高压的环境下进行实验,通过壁面剪切速率相等的原理,模拟不同高温高压以及环空间隙、顶替排量下的冲洗效率,采用失水法得到一系列数据,可以实时测量,计算冲洗效率。The present invention can carry out experiments under high temperature and high pressure environment, and simulate the flushing efficiency under different high temperature and high pressure, annular space gap and displacement through the principle of equal wall shear rate. A series of data is obtained by using water loss method, and the flushing efficiency can be measured and calculated in real time.

附图说明BRIEF DESCRIPTION OF THE DRAWINGS

附图用来提供对本发明的进一步理解,并且构成说明书的一部分,与本发明的实施例一起用于解释本发明,并不构成对本发明的限制。在附图中:The accompanying drawings are used to provide a further understanding of the present invention and constitute a part of the specification. Together with the embodiments of the present invention, they are used to explain the present invention and do not constitute a limitation of the present invention. In the accompanying drawings:

图1是本发明整体装置的结构示意图;FIG1 is a schematic structural diagram of the overall device of the present invention;

图2是本发明冲洗液为牛顿流体且温度为60℃时冲洗效率随时间变化曲线示意图;FIG2 is a schematic diagram of a curve showing the change of flushing efficiency over time when the flushing liquid of the present invention is a Newtonian fluid and the temperature is 60° C.;

图3是本发明冲洗液为牛顿流体且温度为75℃时冲洗效率随时间变化曲线示意图;FIG3 is a schematic diagram of a curve showing the change of flushing efficiency over time when the flushing liquid of the present invention is a Newtonian fluid and the temperature is 75° C.;

图4是本发明冲洗液为牛顿流体且温度为90℃时冲洗效率随时间变化曲线示意图;FIG4 is a schematic diagram of a curve showing the change of flushing efficiency over time when the flushing liquid of the present invention is a Newtonian fluid and the temperature is 90° C.;

图5是本发明冲洗液为宾汉流体且温度为60℃时冲洗效率随时间变化曲线示意图;5 is a schematic diagram of a curve showing the change of flushing efficiency over time when the flushing fluid of the present invention is a Bingham fluid and the temperature is 60° C.;

图6是本发明冲洗液为宾汉流体且温度为75℃时冲洗效率随时间变化曲线示意图;FIG6 is a schematic diagram of a curve showing the change of flushing efficiency over time when the flushing fluid of the present invention is a Bingham fluid and the temperature is 75° C.;

图7是本发明冲洗液为宾汉流体且温度为90℃时冲洗效率随时间变化曲线示意图;7 is a schematic diagram of a curve showing the change of flushing efficiency over time when the flushing fluid of the present invention is a Bingham fluid and the temperature is 90° C.;

图8是本发明的装置原理图;Fig. 8 is a schematic diagram of the device of the present invention;

图中:1、釜体;2、人造岩心;3、岩心夹持器;4、搅拌筒;5、磁力搅拌器;6、实时流量计。In the figure: 1. kettle body; 2. artificial core; 3. core holder; 4. stirring drum; 5. magnetic stirrer; 6. real-time flow meter.

具体实施方式DETAILED DESCRIPTION

下面将结合本发明实施例中的附图,对本发明实施例中的技术方案进行清楚、完整地描述,显然,所描述的实施例仅仅是本发明一部分实施例,而不是全部的实施例。基于本发明中的实施例,本领域普通技术人员在没有做出创造性劳动前提下所获得的所有其他实施例,都属于本发明保护的范围。The following will be combined with the drawings in the embodiments of the present invention to clearly and completely describe the technical solutions in the embodiments of the present invention. Obviously, the described embodiments are only part of the embodiments of the present invention, not all of the embodiments. Based on the embodiments of the present invention, all other embodiments obtained by ordinary technicians in this field without creative work are within the scope of protection of the present invention.

请参阅图1-8,本发明提供技术方案:一种检测高温高压固井二界面冲洗效率的方法,该方法采用冲洗效率评价装置,该冲洗效率评价装置包括:釜体 1、人造岩心2、岩心夹持器3、搅拌筒4、磁力搅拌器5、金属滤网以及实时流量计6;其中,所述釜体1与冲洗液仓和钻井液仓均连通,其上设置有用于检测釜体1内温度的温度传感器以及用于检测釜体1内压力的压力传感器,该温度传感器和压力传感器均与电脑通过总线连接;所述人造岩心2通过岩心夹持器3可拆卸地固定在所述釜体1的内部底部,岩心夹持器3可拆卸地固定在釜体1的内部底部;所述搅拌筒4倒扣至所述人造岩心2上,且其内部顶部未与人造岩心2接触,其用于模拟钻井液动滤失形成泥饼以及不同的环空间隙下的转速;所述磁力搅拌器5位于釜体1顶部,其搅拌杆穿过釜体1顶部固定在所述搅拌筒4顶部,用于带动所述搅拌筒4的转动;所述金属滤网套置在人造岩心2上;所述釜体1安装岩心夹持器3的位置处设置有排液孔,该排液孔与人造岩心2相连通;所述实时流量计6设置于所述釜体1的排液孔上,与电脑通过总线连接,用于测得排出的液体的流量;Please refer to Figures 1-8. The present invention provides a technical solution: a method for detecting the flushing efficiency of the second interface of high-temperature and high-pressure cementing, the method adopts a flushing efficiency evaluation device, the flushing efficiency evaluation device includes: a kettle 1, an artificial core 2, a core clamp 3, a mixing drum 4, a magnetic stirrer 5, a metal filter and a real-time flow meter 6; wherein the kettle 1 is connected to both the flushing fluid tank and the drilling fluid tank, and is provided with a temperature sensor for detecting the temperature in the kettle 1 and a pressure sensor for detecting the pressure in the kettle 1, and the temperature sensor and the pressure sensor are both connected to the computer through a bus; the artificial core 2 is detachably fixed to the inner bottom of the kettle 1 by the core clamp 3, and the core clamp 3 is detachably fixed to the inner bottom of the kettle 1; the mixing drum 4 is inverted onto the artificial core 2 , and the top of the interior thereof is not in contact with the artificial core 2, which is used to simulate the dynamic loss of drilling fluid to form mud cakes and the rotation speed under different annular gaps; the magnetic stirrer 5 is located at the top of the kettle body 1, and its stirring rod passes through the top of the kettle body 1 and is fixed to the top of the stirring drum 4, which is used to drive the rotation of the stirring drum 4; the metal filter is sleeved on the artificial core 2; a drainage hole is provided at the position where the core holder 3 is installed on the kettle body 1, and the drainage hole is connected to the artificial core 2; the real-time flowmeter 6 is provided on the drainage hole of the kettle body 1, and is connected to the computer through a bus, and is used to measure the flow rate of the discharged liquid;

该方法包含:The method includes:

(S1)通过现场环空间隙选择对应的搅拌筒4,安装在磁力搅拌器5上,封闭釜体1;然后,泵入冲洗液,根据实验需要确定冲洗时间,将釜体1的温度压力调整至实验所需的温度和压力;根据现场冲洗液类型的不同采用不同的转速公式,再根据施工排量和环空间隙计算外筒转速,通过实时流量计6测量记录人造岩心2的初始滤失流量Q0(S1) Select the corresponding mixing drum 4 according to the annular gap on site, install it on the magnetic stirrer 5, and close the kettle body 1; then, pump in the flushing liquid, determine the flushing time according to the experimental needs, and adjust the temperature and pressure of the kettle body 1 to the temperature and pressure required by the experiment; use different speed formulas according to the different types of flushing liquid on site, and then calculate the outer drum speed according to the construction displacement and the annular gap, and measure and record the initial filtration flow Q 0 of the artificial core 2 through the real-time flow meter 6;

(S2)在釜体1内泵入钻井液,升温升压,开启磁力搅拌器5,模拟钻井液动滤失形成泥饼,通过实时流量计6测量记录钻井液的流量Q1(S2) Pumping drilling fluid into the kettle 1, raising the temperature and pressure, turning on the magnetic stirrer 5, simulating the dynamic filtration of the drilling fluid to form a mud cake, and measuring and recording the flow rate Q1 of the drilling fluid through the real-time flow meter 6;

(S3)从釜体1内泵出钻井液,泵入冲洗液,所设定的外筒转速、压力、温度、冲洗液用量及总体的冲洗时间参数与前面一致,进行冲洗,通过实时流量计6可实时读取失水流量Q2,进而测得冲洗效率,为:(S3) Drilling fluid is pumped out from the kettle 1, and flushing fluid is pumped in. The outer cylinder speed, pressure, temperature, flushing fluid dosage and overall flushing time parameters are set to be consistent with the above parameters. Flushing is performed. The water loss flow rate Q 2 can be read in real time by the real-time flow meter 6, and the flushing efficiency is measured as follows:

所述外筒转速,为:The outer cylinder speed is:

(1)当冲洗液为宾汉流体时,外筒转速公式如下:(1) When the flushing fluid is Bingham fluid, the outer cylinder speed formula is as follows:

式中,λ为人造岩心2与旋转外筒半径之比;D1为井眼直径,单位为m;D2为套管外径,单位为m;w为环空间隙,单位为m;Q为施工排量,单位为m3/min; n为外筒转速,单位为r/min;τ0为宾汉流体的动切力,单位为Pa;η为塑性黏度,单位为mPa·s;Wherein, λ is the ratio of the radius of the artificial core 2 to the rotating outer cylinder; D1 is the borehole diameter, in m; D2 is the outer diameter of the casing, in m; w is the annular gap, in m; Q is the operation displacement, in m3 /min; n is the outer cylinder rotation speed, in r/min; τ0 is the dynamic shear force of the Bingham fluid, in Pa; η is the plastic viscosity, in mPa·s;

(2)当冲洗液为幂律流体时,外筒转速公式如下:(2) When the flushing fluid is a power-law fluid, the outer cylinder speed formula is as follows:

式中,λ为人造岩心2与旋转外筒半径之比;D1为井眼直径,单位为m;D2为套管外径,单位为m;w为环空间隙,单位为m;Q为施工排量,单位为m3/min; n为外筒转速,单位为r/min;nm为幂律流体的流性指数;Wherein, λ is the ratio of the radius of the artificial core 2 to the rotating outer cylinder; D1 is the borehole diameter, in m; D2 is the outer diameter of the casing, in m; w is the annular gap, in m; Q is the construction displacement, in m 3 /min; n is the outer cylinder rotation speed, in r/min; nm is the flow index of the power-law fluid;

(3)当冲洗液为牛顿流体时,即nm为1,外筒转速公式如下:(3) When the flushing fluid is a Newtonian fluid, that is, nm is 1, the outer cylinder speed formula is as follows:

式中,λ为人造岩心2与旋转外筒半径之比;D1为井眼直径,单位为m;D2为套管外径,单位为m;w为环空间隙,单位为m;Q为施工排量,单位为m3/min; n为外筒转速,单位为r/min;Wherein, λ is the ratio of the radius of the artificial core 2 to the rotating outer cylinder; D1 is the borehole diameter, in m; D2 is the outer diameter of the casing, in m; w is the annular gap, in m; Q is the construction displacement, in m 3 /min; n is the outer cylinder rotation speed, in r/min;

上述该旋转外筒为所述搅拌筒4;井眼直径、套管外径、环空间隙以及施工排量均为施工现场参数;The rotating outer cylinder is the mixing cylinder 4; the wellbore diameter, casing outer diameter, annular space gap and construction displacement are all construction site parameters;

通过井眼直径、套管外径和岩心半径可以确定搅拌筒(4)半径,其公式如下:The radius of the mixing drum (4) can be determined by the borehole diameter, casing outer diameter and core radius, and the formula is as follows:

式中,D2为井眼直径,其单位为mm;D1为套管外径,其单位为mm;R2为搅拌筒(4)半径,其单位为mm;R1为岩心半径,其单位为mm;上述单位在计算时需要将其换算一致。Wherein, D2 is the borehole diameter, in mm; D1 is the outer diameter of the casing, in mm; R2 is the radius of the mixing drum (4), in mm; R1 is the core radius, in mm; the above units need to be converted to be consistent during calculation.

本方法(S1)、(S3)中,温度20~200℃,压力0.1~30MPa,岩心尺寸 24.5mm*75mm。In the present method (S1) and (S3), the temperature is 20 to 200°C, the pressure is 0.1 to 30 MPa, and the core size is 24.5 mm*75 mm.

应用实例Application Examples

采用本发明的方法实际评价冲洗液针对川西地区页岩气井的冲洗效率,具体如下:The method of the present invention is used to actually evaluate the flushing efficiency of the flushing fluid for shale gas wells in western Sichuan, as follows:

实验所需的现场数据来自川西地区页岩气井,向装置的釜体内泵入一定体积的冲洗液,编辑温控和压力程序,升温升压至模拟的井下温度和压力,通过现场冲洗液类型、实际环空间隙与排量确定外筒转速,根据公式计算转速,直至流量计读数不变,将冲洗液泵回冲洗液仓,再泵入钻井液,启动磁力搅拌器模拟钻井时井内钻井液的循环,模拟泥饼形成,开始测量钻井液动滤失过程的失水量,待失水完成后,将钻井液泵回钻井液仓,此时再泵入冲洗液模拟井场冲洗泥饼的过程,通过公式和实时流量计可以计算出各个时间段的冲洗效率。The field data required for the experiment came from shale gas wells in western Sichuan. A certain volume of flushing fluid was pumped into the kettle of the device, and the temperature control and pressure programs were edited. The temperature and pressure were raised to the simulated downhole temperature and pressure. The outer cylinder speed was determined by the type of on-site flushing fluid, the actual annular space gap and the displacement. The speed was calculated according to the formula until the flow meter reading remained unchanged. The flushing fluid was pumped back to the flushing fluid tank, and then the drilling fluid was pumped in. The magnetic agitator was started to simulate the circulation of the drilling fluid in the well during drilling, the mud cake formation was simulated, and the water loss in the dynamic filtration process of the drilling fluid was measured. After the water loss was completed, the drilling fluid was pumped back to the drilling fluid tank. At this time, the flushing fluid was pumped in again to simulate the process of flushing the mud cake at the well site. The flushing efficiency of each time period can be calculated by the formula and the real-time flow meter.

首先,我们保持不同气井的排量为1.0m3/min不变,不同环空间隙对应的外筒半径和外筒转速见表1,测量不同温度、不同环空间隙在不同时间下的冲洗效率。冲洗液体系为多次实验得到的最佳配方且为牛顿流体,基本性能见表 2,实验所用钻井液来自川西地区某一页岩气井具体性能见表3。实验压力为 20MPa,温度为60℃、75℃、90℃,其冲洗效率随时间变化曲线分别见图2、图3、图4。First, we kept the displacement of different gas wells at 1.0m 3 /min. The outer cylinder radius and outer cylinder speed corresponding to different annular gaps are shown in Table 1. The flushing efficiency at different temperatures and different annular gaps at different times was measured. The flushing fluid system is the best formula obtained from multiple experiments and is a Newtonian fluid. The basic properties are shown in Table 2. The drilling fluid used in the experiment comes from a shale gas well in western Sichuan. The specific properties are shown in Table 3. The experimental pressure is 20MPa, and the temperature is 60℃, 75℃, and 90℃. The flushing efficiency curves over time are shown in Figures 2, 3, and 4, respectively.

表1--不同环空间隙对应的外筒半径和外筒转速Table 1 - Outer cylinder radius and outer cylinder speed corresponding to different annular gaps

环空间隙(mm)Annular space gap (mm) 搅拌筒半径(mm)Radius of mixing drum (mm) 外筒转速(r/min)External cylinder speed (r/min) 38.138.1 20.1520.15 370370 31.7531.75 18.6418.64 710710 25.425.4 17.2017.20 915915 19.0519.05 15.8315.83 854 854

表2--多次实验所得最佳冲洗液配方Table 2 - Optimal flushing solution formula obtained from multiple experiments

表3--川西地区某一页岩气井所用钻井液基本性能Table 3--Basic properties of drilling fluid used in a shale gas well in western Sichuan

然后,我们又单独选取了某一口页岩气井作为实验对象,该井井眼内径与套管外径为:215.9mm×139.7mm,环空间隙为38.1mm,所用钻井液性能见表3,冲洗液为乳化冲洗液+0.3%纤维且为宾汉流体,其动切力为6Pa,塑性黏度为18mPa·s,通过不同的排量确定外筒转速见表4,实验压力为20MPa,温度为60℃、75℃、90℃,其冲洗效率随时间变化曲线分别见图5、图6、图7。Then, we selected a shale gas well as the experimental object. The inner diameter of the wellbore and the outer diameter of the casing are: 215.9mm×139.7mm, the annular space gap is 38.1mm, and the properties of the drilling fluid used are shown in Table 3. The flushing fluid is an emulsified flushing fluid + 0.3% fiber and is a Bingham fluid. Its dynamic shear force is 6Pa, and its plastic viscosity is 18mPa·s. The outer cylinder speed is determined by different displacements as shown in Table 4. The experimental pressure is 20MPa, and the temperature is 60℃, 75℃, and 90℃. The flushing efficiency change curves over time are shown in Figures 5, 6, and 7, respectively.

表4--不同排量对应的外筒转速Table 4 - External cylinder speed corresponding to different displacements

排量(m3/min)Displacement (m 3 /min) 0.80.8 1.01.0 1.21.2 1.41.4 外筒转速(r/min)External cylinder speed (r/min) 279279 353353 427427 500 500

本发明装置中,确保实验数据对于现场应用的可靠性,人造岩心半径R1为12.25mm,搅拌筒的外径需要通过现场环空间隙来确定,例如:现场井眼×套管为215.9×139.7,那么通过公式计算得到搅拌筒的外径R2就应该为20.15mm,进一步的就可以通过施工排量计算出外筒转速。在实验过程中,冲洗液和钻井液加量应该尽可能高于人造岩心,这是为了防止离心力导致泥饼形成效果差。In the device of the present invention, the reliability of the experimental data for field application is ensured. The radius R1 of the artificial core is 12.25 mm. The outer diameter of the mixing drum needs to be determined by the field annular clearance. For example, if the field wellbore × casing is 215.9 × 139.7, then the outer diameter R2 of the mixing drum calculated by the formula should be 20.15 mm. Further, the outer drum speed can be calculated by the construction displacement. During the experiment, the amount of flushing fluid and drilling fluid added should be as high as possible compared to the artificial core to prevent the centrifugal force from causing poor mud cake formation.

需要说明的是,在本文中,诸如第一和第二等之类的关系术语仅仅用来将一个实体或者操作与另一个实体或操作区分开来,而不一定要求或者暗示这些实体或操作之间存在任何这种实际的关系或者顺序。而且,术语“包括”、“包含”或者其任何其他变体意在涵盖非排他性的包含,从而使得包括一系列要素的过程、方法、物品或者设备不仅包括那些要素,而且还包括没有明确列出的其他要素,或者是还包括为这种过程、方法、物品或者设备所固有的要素。It should be noted that, in this article, relational terms such as first and second, etc. are only used to distinguish one entity or operation from another entity or operation, and do not necessarily require or imply any such actual relationship or order between these entities or operations. Moreover, the terms "include", "comprise" or any other variants thereof are intended to cover non-exclusive inclusion, so that a process, method, article or device including a series of elements includes not only those elements, but also other elements not explicitly listed, or also includes elements inherent to such process, method, article or device.

最后应说明的是:以上所述仅为本发明的优选实施例而已,并不用于限制本发明,尽管参照前述实施例对本发明进行了详细的说明,对于本领域的技术人员来说,其依然可以对前述各实施例所记载的技术方案进行修改,或者对其中部分技术特征进行等同替换。凡在本发明的精神和原则之内,所作的任何修改、等同替换、改进等,均应包含在本发明的保护范围之内。Finally, it should be noted that the above is only a preferred embodiment of the present invention and is not intended to limit the present invention. Although the present invention has been described in detail with reference to the aforementioned embodiments, those skilled in the art can still modify the technical solutions described in the aforementioned embodiments or replace some of the technical features therein by equivalents. Any modification, equivalent replacement, improvement, etc. made within the spirit and principle of the present invention shall be included in the protection scope of the present invention.

Claims (2)

1. The method for detecting the flushing efficiency of the high-temperature high-pressure well cementation two interfaces is characterized by comprising the following steps of: the device comprises a kettle body (1), an artificial rock core (2), a rock core holder (3), a stirring cylinder (4), a magnetic stirrer (5), a metal filter screen and a real-time flowmeter (6); the kettle body (1) is communicated with the flushing fluid bin and the drilling fluid bin, a temperature sensor for detecting the temperature in the kettle body (1) and a pressure sensor for detecting the pressure in the kettle body (1) are arranged on the kettle body, and the temperature sensor and the pressure sensor are connected with a computer through buses; the artificial rock core (2) is detachably fixed at the inner bottom of the kettle body (1) through a rock core holder (3), and the rock core holder (3) is detachably fixed at the inner bottom of the kettle body (1); the stirring barrel (4) is reversely buckled on the artificial rock core (2), and the inner top of the stirring barrel is not contacted with the artificial rock core (2) and is used for simulating drilling fluid filtration to form mud cakes and rotating speeds under different annular gaps; the magnetic stirrer (5) is positioned at the top of the kettle body (1), and a stirring rod of the magnetic stirrer passes through the top of the kettle body (1) and is fixed at the top of the stirring cylinder (4) and is used for driving the stirring cylinder (4) to rotate; the metal filter screen is sleeved on the artificial rock core (2); a liquid discharge hole is formed in the position, where the core holder (3) is arranged, of the kettle body (1), and the liquid discharge hole is communicated with the artificial core (2); the real-time flowmeter (6) is arranged on the liquid discharge hole of the kettle body (1) and is connected with a computer through a bus for measuring the flow of discharged liquid;
The method comprises the following steps:
(S1) selecting corresponding stirring cylinders (4) through the on-site annular gap, installing the corresponding stirring cylinders on a magnetic stirrer (5), and sealing the kettle body (1); then pumping flushing liquid, determining flushing time according to experiment requirements, and adjusting the temperature and pressure of the kettle body (1) to the temperature and pressure required by the experiment; according to different on-site flushing fluid types, different rotating speed formulas are adopted, the rotating speed of the outer cylinder is calculated according to the construction displacement and the annular space, and the initial fluid loss flow Q 0 of the artificial rock core (2) is measured and recorded through a real-time flowmeter (6);
(S2) pumping drilling fluid into the kettle body (1), heating and boosting, starting the magnetic stirrer (5), simulating drilling fluid to filter out to form mud cakes, and measuring and recording the flow Q 1 of the drilling fluid through the real-time flowmeter (6);
(S3) pumping drilling fluid out of the kettle body (1), pumping flushing fluid, wherein the set rotating speed, pressure, temperature, flushing fluid consumption and general flushing time parameters of the outer barrel are consistent with those of the flushing fluid pumped in the front, flushing is performed, the water loss flow Q 2 can be read in real time through a real-time flowmeter (6), and the flushing efficiency is measured, and is:
The rotating speed of the outer cylinder is as follows:
(1) When the flushing fluid is a Bingham fluid, the rotating speed formula of the outer cylinder is as follows:
Wherein lambda is the ratio of the radius of the artificial core (2) to the radius of the rotary outer cylinder; d 1 is the diameter of the borehole in m; d 2 is the outer diameter of the sleeve, and the unit is m; w is an annular gap, and the unit is m; q is construction displacement, and the unit is m 3/min; n is the rotation speed of the outer cylinder, and the unit is t/min; τ 0 is the dynamic shear force of the Bingham fluid in Pa; η is plastic viscosity, and the unit is mPa.s;
(2) When the flushing fluid is power law fluid, the rotating speed formula of the outer cylinder is as follows:
Wherein lambda is the ratio of the radius of the artificial core (2) to the radius of the rotary outer cylinder; d 1 is the diameter of the borehole in m; d 2 is the outer diameter of the sleeve, and the unit is m; w is an annular gap, and the unit is m; q is construction displacement, and the unit is m 3/min; n is the rotation speed of the outer cylinder, and the unit is r/min; n m is the fluidity index of the power law fluid;
(3) When the flushing fluid is Newtonian fluid, namely n m is 1, the rotating speed formula of the outer cylinder is as follows:
Wherein lambda is the ratio of the radius of the artificial core (2) to the radius of the rotary outer cylinder; d 1 is the diameter of the borehole in m; d 2 is the outer diameter of the sleeve, and the unit is m; w is an annular gap, and the unit is m; q is construction displacement, and the unit is m 3/min; n is the rotation speed of the outer cylinder, and the unit is r/min;
The rotary outer cylinder is the stirring cylinder (4); the diameter of the well bore, the outer diameter of the sleeve, the annular clearance and the construction displacement are all construction site parameters;
the radius of the stirring cylinder (4) can be determined by the diameter of the well bore, the outer diameter of the casing and the radius of the core, and the formula is as follows:
Wherein D 2 is the diameter of the borehole in mm; d 1 is the outer diameter of the sleeve, and the unit is mm; r 2 is the radius of the stirring cylinder (4), and the unit is mm; r 1 is the radius of the core, and the unit is mm; the units need to be converted to be identical in calculation.
2. The method for detecting the flushing efficiency of the high-temperature high-pressure well cementation two interfaces according to claim 1, which is characterized by comprising the following steps: in the method (S1) and (S3), the temperature is 20-200 ℃, the pressure is 0.1-30 MPa, and the core size is 24.5mm 75mm.
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