CN114921956A - A kind of manufacturing method of ultra-thin down jacket fabric with waterproof and constant temperature function - Google Patents
A kind of manufacturing method of ultra-thin down jacket fabric with waterproof and constant temperature function Download PDFInfo
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- CN114921956A CN114921956A CN202210620131.4A CN202210620131A CN114921956A CN 114921956 A CN114921956 A CN 114921956A CN 202210620131 A CN202210620131 A CN 202210620131A CN 114921956 A CN114921956 A CN 114921956A
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- 239000004744 fabric Substances 0.000 title claims abstract description 99
- 238000004519 manufacturing process Methods 0.000 title claims abstract 12
- 239000003795 chemical substances by application Substances 0.000 claims abstract description 98
- 238000006243 chemical reaction Methods 0.000 claims abstract description 30
- 229920002101 Chitin Polymers 0.000 claims abstract description 29
- 239000002245 particle Substances 0.000 claims abstract description 29
- 239000000835 fiber Substances 0.000 claims abstract description 28
- 229920000742 Cotton Polymers 0.000 claims abstract description 20
- 230000006870 function Effects 0.000 claims abstract description 18
- 230000006386 memory function Effects 0.000 claims abstract description 15
- 238000000034 method Methods 0.000 claims abstract description 15
- 238000009987 spinning Methods 0.000 claims abstract description 14
- 238000002156 mixing Methods 0.000 claims abstract description 12
- 238000005507 spraying Methods 0.000 claims abstract description 10
- FXHOOIRPVKKKFG-UHFFFAOYSA-N N,N-Dimethylacetamide Chemical compound CN(C)C(C)=O FXHOOIRPVKKKFG-UHFFFAOYSA-N 0.000 claims abstract description 9
- 238000010521 absorption reaction Methods 0.000 claims abstract description 9
- 239000002270 dispersing agent Substances 0.000 claims abstract description 7
- 238000002166 wet spinning Methods 0.000 claims abstract description 7
- 239000000084 colloidal system Substances 0.000 claims abstract 2
- 239000011347 resin Substances 0.000 claims description 41
- 229920005989 resin Polymers 0.000 claims description 41
- 239000000080 wetting agent Substances 0.000 claims description 30
- 238000002360 preparation method Methods 0.000 claims description 22
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 claims description 18
- PCHJSUWPFVWCPO-UHFFFAOYSA-N gold Chemical compound [Au] PCHJSUWPFVWCPO-UHFFFAOYSA-N 0.000 claims description 18
- 239000010931 gold Substances 0.000 claims description 18
- 229910052737 gold Inorganic materials 0.000 claims description 18
- 239000002105 nanoparticle Substances 0.000 claims description 18
- HRPVXLWXLXDGHG-UHFFFAOYSA-N Acrylamide Chemical compound NC(=O)C=C HRPVXLWXLXDGHG-UHFFFAOYSA-N 0.000 claims description 17
- 229910021389 graphene Inorganic materials 0.000 claims description 17
- 229910021420 polycrystalline silicon Inorganic materials 0.000 claims description 15
- QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 claims description 14
- JKNCOURZONDCGV-UHFFFAOYSA-N 2-(dimethylamino)ethyl 2-methylprop-2-enoate Chemical compound CN(C)CCOC(=O)C(C)=C JKNCOURZONDCGV-UHFFFAOYSA-N 0.000 claims description 12
- 239000007788 liquid Substances 0.000 claims description 12
- 238000003756 stirring Methods 0.000 claims description 11
- 239000004902 Softening Agent Substances 0.000 claims description 7
- 238000001035 drying Methods 0.000 claims description 7
- 229920005610 lignin Polymers 0.000 claims description 6
- 229920001610 polycaprolactone Polymers 0.000 claims description 6
- 239000004632 polycaprolactone Substances 0.000 claims description 6
- 229920000193 polymethacrylate Polymers 0.000 claims description 6
- 229920002635 polyurethane Polymers 0.000 claims description 6
- 239000004814 polyurethane Substances 0.000 claims description 6
- 238000009941 weaving Methods 0.000 claims description 6
- 239000002120 nanofilm Substances 0.000 claims 2
- XUIMIQQOPSSXEZ-UHFFFAOYSA-N Silicon Chemical compound [Si] XUIMIQQOPSSXEZ-UHFFFAOYSA-N 0.000 claims 1
- 239000012530 fluid Substances 0.000 claims 1
- 229910052710 silicon Inorganic materials 0.000 claims 1
- 239000010703 silicon Substances 0.000 claims 1
- 238000002791 soaking Methods 0.000 claims 1
- 238000005406 washing Methods 0.000 claims 1
- 238000009413 insulation Methods 0.000 abstract description 9
- 230000031700 light absorption Effects 0.000 description 22
- 239000000243 solution Substances 0.000 description 22
- 229920005591 polysilicon Polymers 0.000 description 13
- 230000000052 comparative effect Effects 0.000 description 10
- 229920000642 polymer Polymers 0.000 description 10
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 6
- 229920001296 polysiloxane Polymers 0.000 description 5
- DPBJAVGHACCNRL-UHFFFAOYSA-N 2-(dimethylamino)ethyl prop-2-enoate Chemical compound CN(C)CCOC(=O)C=C DPBJAVGHACCNRL-UHFFFAOYSA-N 0.000 description 4
- 125000002496 methyl group Chemical group [H]C([H])([H])* 0.000 description 4
- 239000000203 mixture Substances 0.000 description 4
- 239000011550 stock solution Substances 0.000 description 4
- 230000002706 hydrostatic effect Effects 0.000 description 3
- 238000012360 testing method Methods 0.000 description 3
- 230000006872 improvement Effects 0.000 description 2
- 238000004321 preservation Methods 0.000 description 2
- 239000004753 textile Substances 0.000 description 2
- 230000009286 beneficial effect Effects 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 238000011156 evaluation Methods 0.000 description 1
- 238000002474 experimental method Methods 0.000 description 1
- 229910002804 graphite Inorganic materials 0.000 description 1
- 239000010439 graphite Substances 0.000 description 1
- 229920002521 macromolecule Polymers 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 238000011056 performance test Methods 0.000 description 1
- 230000035699 permeability Effects 0.000 description 1
- 230000003068 static effect Effects 0.000 description 1
- 230000009466 transformation Effects 0.000 description 1
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- D—TEXTILES; PAPER
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- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/322—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing nitrogen
- D06M13/402—Amides imides, sulfamic acids
- D06M13/432—Urea, thiourea or derivatives thereof, e.g. biurets; Urea-inclusion compounds; Dicyanamides; Carbodiimides; Guanidines, e.g. dicyandiamides
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- D06M11/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising
- D06M11/07—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with halogens; with halogen acids or salts thereof; with oxides or oxyacids of halogens or salts thereof
- D06M11/11—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with halogens; with halogen acids or salts thereof; with oxides or oxyacids of halogens or salts thereof with halogen acids or salts thereof
- D06M11/13—Ammonium halides or halides of elements of Groups 1 or 11 of the Periodic Table
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- D06M11/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising
- D06M11/07—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with halogens; with halogen acids or salts thereof; with oxides or oxyacids of halogens or salts thereof
- D06M11/11—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with halogens; with halogen acids or salts thereof; with oxides or oxyacids of halogens or salts thereof with halogen acids or salts thereof
- D06M11/155—Halides of elements of Groups 2 or 12 of the Periodic Table
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- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
- D06M15/19—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with synthetic macromolecular compounds
- D06M15/37—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
- D06M15/643—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds containing silicon in the main chain
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- D06N3/00—Artificial leather, oilcloth or other material obtained by covering fibrous webs with macromolecular material, e.g. resins, rubber or derivatives thereof
- D06N3/0002—Artificial leather, oilcloth or other material obtained by covering fibrous webs with macromolecular material, e.g. resins, rubber or derivatives thereof characterised by the substrate
- D06N3/0006—Artificial leather, oilcloth or other material obtained by covering fibrous webs with macromolecular material, e.g. resins, rubber or derivatives thereof characterised by the substrate using woven fabrics
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- D06N3/00—Artificial leather, oilcloth or other material obtained by covering fibrous webs with macromolecular material, e.g. resins, rubber or derivatives thereof
- D06N3/0056—Artificial leather, oilcloth or other material obtained by covering fibrous webs with macromolecular material, e.g. resins, rubber or derivatives thereof characterised by the compounding ingredients of the macro-molecular coating
- D06N3/0059—Organic ingredients with special effects, e.g. oil- or water-repellent, antimicrobial, flame-resistant, magnetic, bactericidal, odour-influencing agents; perfumes
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- D06N3/00—Artificial leather, oilcloth or other material obtained by covering fibrous webs with macromolecular material, e.g. resins, rubber or derivatives thereof
- D06N3/0056—Artificial leather, oilcloth or other material obtained by covering fibrous webs with macromolecular material, e.g. resins, rubber or derivatives thereof characterised by the compounding ingredients of the macro-molecular coating
- D06N3/0063—Inorganic compounding ingredients, e.g. metals, carbon fibres, Na2CO3, metal layers; Post-treatment with inorganic compounds
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- D06N3/00—Artificial leather, oilcloth or other material obtained by covering fibrous webs with macromolecular material, e.g. resins, rubber or derivatives thereof
- D06N3/12—Artificial leather, oilcloth or other material obtained by covering fibrous webs with macromolecular material, e.g. resins, rubber or derivatives thereof with macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds, e.g. gelatine proteins
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- D06M2101/00—Chemical constitution of the fibres, threads, yarns, fabrics or fibrous goods made from such materials, to be treated
- D06M2101/02—Natural fibres, other than mineral fibres
- D06M2101/04—Vegetal fibres
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Abstract
Description
技术领域technical field
本发明涉及羽绒服面料技术领域，特别涉及一种防水恒温功能的超薄羽绒服面料的制作方法。The invention relates to the technical field of down jacket fabrics, in particular to a method for making ultra-thin down jacket fabrics with waterproof and constant temperature functions.
背景技术Background technique
随着人们生活水平的不断提高，人们对衣物的质量要求也越来越高，而对于羽绒服面料来说，面料的保暖性往往具有较高要求，目前市场上大部分的恒温面料主要是保温面料，提高面料在寒冷环境中保温性能，但是并不适用于较高温度环境中，在较高温度环境中无法降低面料温度，因此在高温环境下使用会造成人体闷热，给人体带来不适，另外现有面料在寒冷天气其保温性能往往不佳，不能满足现代人们的使用需求。With the continuous improvement of people's living standards, people's requirements for the quality of clothing are also getting higher and higher. For down jacket fabrics, the warmth of the fabrics often has higher requirements. At present, most of the thermostatic fabrics on the market are mainly thermal insulation fabrics. , to improve the thermal insulation performance of the fabric in a cold environment, but it is not suitable for a higher temperature environment, and the fabric temperature cannot be lowered in a higher temperature environment, so using it in a high temperature environment will cause the human body to be stuffy and uncomfortable. Existing fabrics often have poor thermal insulation performance in cold weather and cannot meet the needs of modern people.
发明内容SUMMARY OF THE INVENTION
本发明的主要目的在于提供一种防水恒温功能的超薄羽绒服面料的制作方法，可以有效解决背景技术中的问题。The main purpose of the present invention is to provide a method for making an ultra-thin down jacket fabric with a waterproof and constant temperature function, which can effectively solve the problems in the background technology.
为实现上述目的，本发明采取的技术方案为：To achieve the above object, the technical scheme adopted in the present invention is:
一种防水恒温功能的超薄羽绒服面料的制作方法，包括以下步骤：A method for making an ultra-thin down jacket fabric with waterproof and constant temperature function, comprising the following steps:
S1：制备纤维丝：将棉纤维送入纺丝机中得到棉纤维丝，将二甲基乙酰胺、分散剂、成孔剂和甲壳素颗粒混合均匀，得到粘稠状的透明胶质纺丝原液，通过湿法纺丝得到甲壳素纤维丝；S1: Preparation of filaments: sending cotton fibers into a spinning machine to obtain cotton filaments, and mixing dimethylacetamide, dispersant, pore-forming agent and chitin particles uniformly to obtain viscous transparent colloidal spinning Dope solution, obtain chitin fiber by wet spinning;
S2：制备微孔纤维丝：将S1中制备的甲壳素纤维丝浸渍在温度为90-100℃的含水碱性浴中0.5-2h，取出，干燥后成孔剂从甲壳素纤维丝上洗脱，得微孔纤维丝；S2: Preparation of microporous filaments: immerse the chitin filaments prepared in S1 in an aqueous alkaline bath at a temperature of 90-100°C for 0.5-2 hours, take out, and elute the pore-forming agent from the chitin filaments after drying , to obtain microporous filaments;
S3：制备基布：以棉纤维丝为经线，以微孔纤维丝为纬线编织形成基布；S3: Preparation of base cloth: the base cloth is formed by weaving cotton fiber filaments as warp threads and microporous fiber filaments as weft threads;
S4：基布整理：通过处理液对基布进行液氨处理，35～45min后充分水洗，再通过整理剂对水洗后的基布进行树脂整理，干燥，得到具有形状记忆功能的基布；S4: Finishing of base fabric: The base fabric is treated with liquid ammonia through the treatment solution, fully washed with water after 35-45 minutes, and then the washed base fabric is resin-finished with a finishing agent and dried to obtain a base fabric with shape memory function;
S5：喷涂处理：将S4中获得的具有形状记忆功能的基布表面喷涂太阳光吸收转换剂。S5: Spraying treatment: The surface of the base fabric with shape memory function obtained in S4 is sprayed with a solar light absorption conversion agent.
作为本发明的进一步优化方案，所述二甲基乙酰胺、分散剂、成孔剂和甲壳素颗粒的重量比为3:(1-2):(2-3):9。As a further optimized solution of the present invention, the weight ratio of the dimethylacetamide, the dispersant, the pore-forming agent and the chitin particles is 3:(1-2):(2-3):9.
作为本发明的进一步优化方案，所述成孔剂由聚氨酯、木质素和聚甲基丙烯酸酯按照重量比1:1:(2-4)组成。As a further optimized solution of the present invention, the pore-forming agent is composed of polyurethane, lignin and polymethacrylate in a weight ratio of 1:1:(2-4).
作为本发明的进一步优化方案，所述分散剂为聚己内酯。As a further optimized solution of the present invention, the dispersant is polycaprolactone.
作为本发明的进一步优化方案，所述S4中液氨处理的处理液由2D树脂整理剂MgCl2·6H2O、NH4Cl、柔软剂和润湿剂组成，2D树脂整理剂的浓度为 92～95g/L、MgCl2·6H2O和NH4Cl的浓度为12～16g/L，柔软剂为30～40g/L，润湿剂为1～2g/L。As a further optimized solution of the present invention, the treatment solution of the liquid ammonia treatment in S4 is composed of 2D resin finishing agent MgCl 2 ·6H 2 O, NH 4 Cl, softener and wetting agent, and the concentration of 2D resin finishing agent is 92 ～95g/L, MgCl 2 ·6H 2 O and NH 4 Cl concentration of 12～16g/L, softener 30～40g/L, wetting agent 1～2g/L.
作为本发明的进一步优化方案，所述S4中树脂整理的树脂液由2D树脂整理剂、MgCl2·6H2O、NH4Cl、柔软剂和润湿剂组成，2D树脂整理剂的浓度为 80～90g/L、MgCl2·6H2O和NH4Cl的浓度为8～10g/L，柔软剂为40～50g/L，润湿剂为1～2g/L。As a further optimized solution of the present invention, the resin solution for resin finishing in the S4 is composed of 2D resin finishing agent, MgCl 2 ·6H 2 O, NH 4 Cl, softener and wetting agent, and the concentration of 2D resin finishing agent is 80 ～90g/L, MgCl 2 ·6H 2 O and NH 4 Cl concentrations are 8～10g/L, softener is 40～50g/L, wetting agent is 1～2g/L.
作为本发明的进一步优化方案，所述液氨处理的处理液和树脂整理的树脂液中MgCl2·6H2O和NH4Cl的浓度比为15：1，所述柔软剂为有机硅柔软剂，所述润湿剂为TRITONTMHW-1000。As a further optimized solution of the present invention, the concentration ratio of MgCl 2 ·6H 2 O and NH 4 Cl in the liquid ammonia-treated treatment solution and the resin-finished resin solution is 15:1, and the softener is a silicone softener , the wetting agent is TRITONTMHW-1000.
作为本发明的进一步优化方案，所述太阳光吸收转换剂制备方法为将甲基丙烯酸二甲基氨乙酯与丙烯酰胺混合搅拌至完全溶解，加入金纳米颗粒、石墨烯颗粒、多晶硅和高分子成膜剂后再次混合搅拌，得到太阳光吸收转换剂。As a further optimized solution of the present invention, the preparation method of the solar light absorption conversion agent is to mix and stir dimethylaminoethyl methacrylate and acrylamide until completely dissolved, add gold nanoparticles, graphene particles, polysilicon and macromolecules After the film-forming agent is mixed and stirred again, a solar light absorption conversion agent is obtained.
作为本发明的进一步优化方案，所述太阳光吸收转换剂中的组分按重量份计，包括：甲基丙烯酸二甲基氨乙酯30-45份、丙烯酰胺20-50份、金纳米颗粒5-10份、石墨烯颗粒5-10份、多晶硅5-10份和高分子成膜剂2-5份。As a further optimized solution of the present invention, the components in the solar light absorption conversion agent, in parts by weight, include: 30-45 parts of dimethylaminoethyl methacrylate, 20-50 parts of acrylamide, gold nanoparticles 5-10 parts, 5-10 parts of graphene particles, 5-10 parts of polysilicon and 2-5 parts of polymer film-forming agent.
与现有技术相比，本发明具有如下有益效果：Compared with the prior art, the present invention has the following beneficial effects:
1、本发明中，通过对纤维丝进行微孔处理，并对由微孔处理纤维丝织成的基布进行整理作业，使得微孔处理的基布具备形状记忆功能，使得该基布在较高温度下带动纤维丝发生形变，进而使得纤维上的微孔打开，在较高温度环境下降低面料温度，避免面料对人体造成闷热感，提高面料在较高温度环境下的舒适度。1. In the present invention, by performing microporous treatment on the fiber filaments and finishing the base fabric woven from the microporous treated fiber filaments, the microporous treated base fabric has a shape memory function, so that the base fabric has a relatively high performance. The high temperature drives the deformation of the fibers, thereby opening the micropores on the fibers, reducing the temperature of the fabric in a higher temperature environment, preventing the fabric from causing a sultry feeling to the human body, and improving the comfort of the fabric in a higher temperature environment.
2、本发明中，通过在具有形状记忆功能的基布表面喷涂由甲基丙烯酸二甲基氨乙酯、丙烯酰胺、金纳米颗粒、石墨烯颗粒、多晶硅和高分子成膜剂组成的太阳光吸收转换剂，可辅助基布在具备防水性能的同时提高面料的保温性能。2. In the present invention, by spraying the sunlight composed of dimethylaminoethyl methacrylate, acrylamide, gold nanoparticles, graphene particles, polysilicon and polymer film-forming agent on the surface of the base cloth with shape memory function The absorption conversion agent can assist the base fabric to improve the thermal insulation performance of the fabric while having the waterproof performance.
3、本发明中，通过在太阳光吸收转换剂加入金纳米颗粒和石墨烯颗粒，与添加单一的太阳光吸收颗粒相比，该金纳米颗粒和石墨烯颗粒共同添加可对不同波长的太阳光进行吸收转化，进而进一步提高了面料的保温性能。3. In the present invention, by adding gold nanoparticles and graphene particles to the solar light absorption conversion agent, compared with adding a single solar light absorbing particle, the gold nanoparticles and graphene particles can be added together to reduce sunlight of different wavelengths. Absorption and transformation are carried out, which further improves the thermal insulation performance of the fabric.
具体实施方式Detailed ways
下面对本申请作进一步详细描述，有必要在此指出的是，以下具体实施方式只用于对本申请进行进一步的说明，不能理解为对本申请保护范围的限制，该领域的技术人员可以根据上述申请内容对本申请作出一些非本质的改进和调整。The application will be described in further detail below. It is necessary to point out that the following specific embodiments are only used to further illustrate the application, and should not be construed as limiting the scope of protection of the application. Those skilled in the art can Some non-essential improvements and adjustments are made to this application.
实施例1Example 1
一种防水恒温功能的超薄羽绒服面料的制作方法，包括以下步骤：A method for making an ultra-thin down jacket fabric with waterproof and constant temperature function, comprising the following steps:
S1：制备纤维丝：将棉纤维送入纺丝机中得到棉纤维丝，将二甲基乙酰胺、聚己内酯、成孔剂和甲壳素颗粒按3:1:2:9的重量比混合均匀，得到粘稠状的透明胶质纺丝原液，通过湿法纺丝得到甲壳素纤维丝，其中成孔剂由聚氨酯、木质素和聚甲基丙烯酸酯按照重量比1:1:3组成；S1: Preparation of filaments: the cotton fibers are sent into a spinning machine to obtain cotton filaments, and dimethylacetamide, polycaprolactone, pore-forming agent and chitin particles are mixed in a weight ratio of 3:1:2:9 Mix evenly to obtain a viscous transparent colloidal spinning stock solution, and obtain chitin fiber by wet spinning, wherein the pore-forming agent is composed of polyurethane, lignin and polymethacrylate in a weight ratio of 1:1:3 ;
S2：制备微孔纤维丝：将S1中制备的甲壳素纤维丝浸渍在温度为90-100℃的含水碱性浴中1h，取出，干燥后成孔剂从甲壳素纤维丝上洗脱，得微孔纤维丝；S2: Preparation of microporous filaments: The chitin filaments prepared in S1 were immersed in an aqueous alkaline bath at a temperature of 90-100 °C for 1 h, taken out, and the pore-forming agent was eluted from the chitin filaments after drying to obtain Microporous filaments;
S3：制备基布：以棉纤维丝为经线，以微孔纤维丝为纬线编织形成基布；S3: Preparation of base cloth: the base cloth is formed by weaving cotton fiber filaments as warp threads and microporous fiber filaments as weft threads;
S4：基布整理：通过由2D树脂整理剂、MgCl2·6H2O、NH4Cl、柔软剂和润湿剂组成的处理液对基布进行液氨处理，40min后充分水洗，再通过由2D树脂整理剂、MgCl2·6H2O、NH4Cl、柔软剂和润湿剂组成的整理剂对水洗后的基布进行树脂整理，干燥，得到具有形状记忆功能的基布，其中处理液内2D树脂整理剂的浓度为80g/L、MgCl2·6H2O和NH4Cl的浓度为8g/L，柔软剂为40g/L，润湿剂为1g/L；其中整理剂内2D树脂整理剂的浓度为80g/L、MgCl2·6H2O和 NH4Cl的浓度为8g/L，柔软剂为40g/L，润湿剂为1g/L，且液氨处理的处理液和树脂整理的树脂液中MgCl2·6H2O和NH4Cl的浓度比为15：1，所述柔软剂为有机硅柔软剂，所述润湿剂为TRITONTMHW-1000；S4: Finishing of base fabric: The base fabric is treated with liquid ammonia through a treatment solution consisting of 2D resin finishing agent, MgCl 2 ·6H 2 O, NH 4 Cl, softener and wetting agent, fully washed with water after 40 minutes, and then passed through the The finishing agent composed of 2D resin finishing agent, MgCl 2 ·6H 2 O, NH 4 Cl, softener and wetting agent is used to perform resin finishing on the washed base cloth and dry to obtain a base cloth with shape memory function, wherein the treatment liquid The concentration of the inner 2D resin finishing agent is 80g/L, the concentration of MgCl 2 ·6H 2 O and NH 4 Cl is 8g/L, the softener is 40g/L, and the wetting agent is 1g/L; The concentration of finishing agent is 80g/L, the concentration of MgCl 2 ·6H 2 O and NH 4 Cl is 8g/L, the softener is 40g/L, the wetting agent is 1g/L, and the treatment liquid and resin treated with liquid ammonia The concentration ratio of MgCl 2 ·6H 2 O and NH 4 Cl in the finished resin solution is 15:1, the softener is a silicone softener, and the wetting agent is TRITONTMHW-1000;
S5：喷涂处理：将S4中获得的具有形状记忆功能的基布表面喷涂太阳光吸收转换剂；其中太阳光吸收转换剂制备方法为将甲基丙烯酸二甲基氨乙酯与丙烯酰胺混合搅拌至完全溶解，加入金纳米颗粒、石墨烯颗粒、多晶硅和高分子成膜剂后再次混合搅拌，得到太阳光吸收转换剂；且太阳光吸收转换剂中的组分按重量份计，包括：甲基丙烯酸二甲基氨乙酯30份、丙烯酰胺20 份、金纳米颗粒5份、石墨烯颗粒5份、多晶硅5份和高分子成膜剂2份。S5: Spraying treatment: the surface of the base fabric with shape memory function obtained in S4 is sprayed with a solar light absorption conversion agent; wherein the preparation method of the solar light absorption conversion agent is to mix and stir dimethylaminoethyl methacrylate and acrylamide to Completely dissolving, adding gold nanoparticles, graphene particles, polysilicon and polymer film-forming agent and then mixing and stirring again to obtain a solar light absorption conversion agent; and the components in the solar light absorption conversion agent are based on parts by weight, including: methyl 30 parts of dimethylaminoethyl acrylate, 20 parts of acrylamide, 5 parts of gold nanoparticles, 5 parts of graphene particles, 5 parts of polysilicon and 2 parts of polymer film-forming agent.
实施例2Example 2
一种防水恒温功能的超薄羽绒服面料的制作方法，包括以下步骤：A method for making an ultra-thin down jacket fabric with waterproof and constant temperature function, comprising the following steps:
S1：制备纤维丝：将棉纤维送入纺丝机中得到棉纤维丝，将二甲基乙酰胺、聚己内酯、成孔剂和甲壳素颗粒按3:2:3:9的重量比混合均匀，得到粘稠状的透明胶质纺丝原液，通过湿法纺丝得到甲壳素纤维丝，其中成孔剂由聚氨酯、木质素和聚甲基丙烯酸酯按照重量比1:1:3组成；S1: Preparation of filaments: sending cotton fibers into a spinning machine to obtain cotton filaments, and mixing dimethylacetamide, polycaprolactone, pore-forming agent and chitin particles in a weight ratio of 3:2:3:9 Mix evenly to obtain a viscous transparent colloidal spinning stock solution, and obtain chitin fiber by wet spinning, wherein the pore-forming agent is composed of polyurethane, lignin and polymethacrylate in a weight ratio of 1:1:3 ;
S2：制备微孔纤维丝：将S1中制备的甲壳素纤维丝浸渍在温度为90-100℃的含水碱性浴中1h，取出，干燥后成孔剂从甲壳素纤维丝上洗脱，得微孔纤维丝；S2: Preparation of microporous filaments: The chitin filaments prepared in S1 were immersed in an aqueous alkaline bath at a temperature of 90-100 °C for 1 h, taken out, and the pore-forming agent was eluted from the chitin filaments after drying to obtain Microporous filaments;
S3：制备基布：以棉纤维丝为经线，以微孔纤维丝为纬线编织形成基布；S3: Preparation of base cloth: the base cloth is formed by weaving cotton fiber filaments as warp threads and microporous fiber filaments as weft threads;
S4：基布整理：通过由2D树脂整理剂MgCl2·6H2O、NH4Cl、柔软剂和润湿剂组成的处理液对基布进行液氨处理，40min后充分水洗，再通过由2D树脂整理剂、MgCl2·6H2O、NH4Cl、柔软剂和润湿剂组成的整理剂对水洗后的基布进行树脂整理，干燥，得到具有形状记忆功能的基布，其中处理液内2D树脂整理剂的浓度为80g/L、MgCl2·6H2O和NH4Cl的浓度为8g/L，柔软剂为40g/L，润湿剂为1g/L；其中整理剂内2D树脂整理剂的浓度为80g/L、MgCl2·6H2O和NH4Cl的浓度为8g/L，柔软剂为40g/L，润湿剂为1g/L，且液氨处理的处理液和树脂整理的树脂液中MgCl2·6H2O和NH4Cl的浓度比为15：1，所述柔软剂为有机硅柔软剂，所述润湿剂为TRITONTMHW-1000；S4: Finishing of the base fabric: The base fabric is treated with liquid ammonia through a treatment solution composed of 2D resin finishing agent MgCl 2 ·6H 2 O, NH 4 Cl, softener and wetting agent, fully washed with water after 40 minutes, and then passed through the 2D The finishing agent consisting of resin finishing agent, MgCl 2 ·6H 2 O, NH 4 Cl, softener and wetting agent is used to carry out resin finishing on the washed base cloth and dry to obtain the base cloth with shape memory function, wherein the inside of the treatment liquid is The concentration of 2D resin finishing agent is 80g/L, the concentration of MgCl 2 ·6H 2 O and NH 4 Cl is 8g/L, the softening agent is 40g/L, and the wetting agent is 1g/L; the 2D resin finishing agent in the finishing agent The concentration of the agent is 80g/L, the concentration of MgCl 2 ·6H 2 O and NH 4 Cl is 8g/L, the softener is 40g/L, the wetting agent is 1g/L, and the treatment liquid and resin finishing of liquid ammonia treatment The concentration ratio of MgCl 2 ·6H 2 O and NH 4 Cl in the resin solution is 15:1, the softener is a silicone softener, and the wetting agent is TRITONTMHW-1000;
S5：喷涂处理：将S4中获得的具有形状记忆功能的基布表面喷涂太阳光吸收转换剂；其中太阳光吸收转换剂制备方法为将甲基丙烯酸二甲基氨乙酯与丙烯酰胺混合搅拌至完全溶解，加入金纳米颗粒、石墨烯颗粒、多晶硅和高分子成膜剂后再次混合搅拌，得到太阳光吸收转换剂；且太阳光吸收转换剂中的组分按重量份计，包括：甲基丙烯酸二甲基氨乙酯30份、丙烯酰胺20 份、金纳米颗粒5份、石墨烯颗粒5份、多晶硅5份和高分子成膜剂2份。S5: Spraying treatment: the surface of the base fabric with shape memory function obtained in S4 is sprayed with a solar light absorption conversion agent; wherein the preparation method of the solar light absorption conversion agent is to mix and stir dimethylaminoethyl methacrylate and acrylamide to Completely dissolving, adding gold nanoparticles, graphene particles, polysilicon and polymer film-forming agent and then mixing and stirring again to obtain a solar light absorption conversion agent; and the components in the solar light absorption conversion agent are based on parts by weight, including: methyl 30 parts of dimethylaminoethyl acrylate, 20 parts of acrylamide, 5 parts of gold nanoparticles, 5 parts of graphene particles, 5 parts of polysilicon and 2 parts of polymer film-forming agent.
实施例3Example 3
一种防水恒温功能的超薄羽绒服面料的制作方法，包括以下步骤：A method for making an ultra-thin down jacket fabric with waterproof and constant temperature function, comprising the following steps:
S1：制备纤维丝：将棉纤维送入纺丝机中得到棉纤维丝，将二甲基乙酰胺、聚己内酯、成孔剂和甲壳素颗粒按3:1:3:9的重量比混合均匀，得到粘稠状的透明胶质纺丝原液，通过湿法纺丝得到甲壳素纤维丝，其中成孔剂由聚氨酯、木质素和聚甲基丙烯酸酯按照重量比1:1:3组成；S1: Preparation of filaments: sending cotton fibers into a spinning machine to obtain cotton filaments, and mixing dimethylacetamide, polycaprolactone, pore-forming agent and chitin particles in a weight ratio of 3:1:3:9 Mix evenly to obtain a viscous transparent colloidal spinning stock solution, and obtain chitin fiber by wet spinning, wherein the pore-forming agent is composed of polyurethane, lignin and polymethacrylate in a weight ratio of 1:1:3 ;
S2：制备微孔纤维丝：将S1中制备的甲壳素纤维丝浸渍在温度为90-100℃的含水碱性浴中1h，取出，干燥后成孔剂从甲壳素纤维丝上洗脱，得微孔纤维丝；S2: Preparation of microporous filaments: The chitin filaments prepared in S1 were immersed in an aqueous alkaline bath at a temperature of 90-100 °C for 1 h, taken out, and the pore-forming agent was eluted from the chitin filaments after drying to obtain Microporous filaments;
S3：制备基布：以棉纤维丝为经线，以微孔纤维丝为纬线编织形成基布；S3: Preparation of base cloth: the base cloth is formed by weaving cotton fiber filaments as warp threads and microporous fiber filaments as weft threads;
S4：基布整理：通过由2D树脂整理剂、MgCl2·6H2O、NH4Cl、柔软剂和润湿剂组成的处理液对基布进行液氨处理，40min后充分水洗，再通过由2D树脂整理剂、MgCl2·6H2O、NH4Cl、柔软剂和润湿剂组成的整理剂对水洗后的基布进行树脂整理，干燥，得到具有形状记忆功能的基布，其中处理液内2D树脂整理剂的浓度为80g/L、MgCl2·6H2O和NH4Cl的浓度为8g/L，柔软剂为40g/L，润湿剂为1g/L；其中整理剂内2D树脂整理剂的浓度为80g/L、MgCl2·6H2O和 NH4Cl的浓度为8g/L，柔软剂为40g/L，润湿剂为1g/L，且液氨处理的处理液和树脂整理的树脂液中MgCl2·6H2O和NH4Cl的浓度比为15：1，所述柔软剂为有机硅柔软剂，所述润湿剂为TRITONTMHW-1000；S4: Finishing of base fabric: The base fabric is treated with liquid ammonia through a treatment solution consisting of 2D resin finishing agent, MgCl 2 ·6H 2 O, NH 4 Cl, softener and wetting agent, fully washed with water after 40 minutes, and then passed through the The finishing agent composed of 2D resin finishing agent, MgCl 2 ·6H 2 O, NH 4 Cl, softener and wetting agent is used to perform resin finishing on the washed base cloth and dry to obtain a base cloth with shape memory function, wherein the treatment liquid The concentration of the inner 2D resin finishing agent is 80g/L, the concentration of MgCl 2 ·6H 2 O and NH 4 Cl is 8g/L, the softener is 40g/L, and the wetting agent is 1g/L; The concentration of finishing agent is 80g/L, the concentration of MgCl 2 ·6H 2 O and NH 4 Cl is 8g/L, the softener is 40g/L, the wetting agent is 1g/L, and the treatment liquid and resin treated with liquid ammonia The concentration ratio of MgCl 2 ·6H 2 O and NH 4 Cl in the finished resin solution is 15:1, the softener is a silicone softener, and the wetting agent is TRITONTMHW-1000;
S5：喷涂处理：将S4中获得的具有形状记忆功能的基布表面喷涂太阳光吸收转换剂；其中太阳光吸收转换剂制备方法为将甲基丙烯酸二甲基氨乙酯与丙烯酰胺混合搅拌至完全溶解，加入金纳米颗粒、石墨烯颗粒、多晶硅和高分子成膜剂后再次混合搅拌，得到太阳光吸收转换剂；且太阳光吸收转换剂中的组分按重量份计，包括：甲基丙烯酸二甲基氨乙酯30份、丙烯酰胺20 份、金纳米颗粒5份、石墨烯颗粒5份、多晶硅5份和高分子成膜剂2份。S5: Spraying treatment: the surface of the base fabric with shape memory function obtained in S4 is sprayed with a solar light absorption conversion agent; wherein the preparation method of the solar light absorption conversion agent is to mix and stir dimethylaminoethyl methacrylate and acrylamide to Completely dissolving, adding gold nanoparticles, graphene particles, polysilicon and polymer film-forming agent and then mixing and stirring again to obtain a solar light absorption conversion agent; and the components in the solar light absorption conversion agent are based on parts by weight, including: methyl 30 parts of dimethylaminoethyl acrylate, 20 parts of acrylamide, 5 parts of gold nanoparticles, 5 parts of graphene particles, 5 parts of polysilicon and 2 parts of polymer film-forming agent.
实施例4Example 4
一种防水恒温功能的超薄羽绒服面料的制作方法，包括以下步骤：A method for making an ultra-thin down jacket fabric with waterproof and constant temperature function, comprising the following steps:
S1：制备纤维丝：将棉纤维送入纺丝机中得到棉纤维丝，将二甲基乙酰胺、聚己内酯、成孔剂和甲壳素颗粒按3:1:3:9的重量比混合均匀，得到粘稠状的透明胶质纺丝原液，通过湿法纺丝得到甲壳素纤维丝，其中成孔剂由聚氨酯、木质素和聚甲基丙烯酸酯按照重量比1:1:3组成；S1: Preparation of filaments: sending cotton fibers into a spinning machine to obtain cotton filaments, and mixing dimethylacetamide, polycaprolactone, pore-forming agent and chitin particles in a weight ratio of 3:1:3:9 Mix evenly to obtain a viscous transparent colloidal spinning stock solution, and obtain chitin fiber by wet spinning, wherein the pore-forming agent is composed of polyurethane, lignin and polymethacrylate in a weight ratio of 1:1:3 ;
S2：制备微孔纤维丝：将S1中制备的甲壳素纤维丝浸渍在温度为90-100℃的含水碱性浴中1h，取出，干燥后成孔剂从甲壳素纤维丝上洗脱，得微孔纤维丝；S2: Preparation of microporous filaments: The chitin filaments prepared in S1 were immersed in an aqueous alkaline bath at a temperature of 90-100 °C for 1 h, taken out, and the pore-forming agent was eluted from the chitin filaments after drying to obtain Microporous filaments;
S3：制备基布：以棉纤维丝为经线，以微孔纤维丝为纬线编织形成基布；S3: Preparation of base cloth: the base cloth is formed by weaving cotton fiber filaments as warp threads and microporous fiber filaments as weft threads;
S4：基布整理：通过由2D树脂整理剂、MgCl2·6H2O、NH4Cl、柔软剂和润湿剂组成的处理液对基布进行液氨处理，40min后充分水洗，再通过由2D树脂整理剂、MgCl2·6H2O、NH4Cl、柔软剂和润湿剂组成的整理剂对水洗后的基布进行树脂整理，干燥，得到具有形状记忆功能的基布，其中处理液内2D树脂整理剂的浓度为80g/L、MgCl2·6H2O和NH4Cl的浓度为8g/L，柔软剂为40g/L，润湿剂为1g/L；其中整理剂内2D树脂整理剂的浓度为80g/L、MgCl2·6H2O和 NH4Cl的浓度为8g/L，柔软剂为40g/L，润湿剂为1g/L，且液氨处理的处理液和树脂整理的树脂液中MgCl2·6H2O和NH4Cl的浓度比为15：1，所述柔软剂为有机硅柔软剂，所述润湿剂为TRITONTMHW-1000；S4: Finishing of base fabric: The base fabric is treated with liquid ammonia through a treatment solution consisting of 2D resin finishing agent, MgCl 2 ·6H 2 O, NH 4 Cl, softener and wetting agent, fully washed with water after 40 minutes, and then passed through the The finishing agent composed of 2D resin finishing agent, MgCl 2 ·6H 2 O, NH 4 Cl, softener and wetting agent is used to perform resin finishing on the washed base cloth and dry to obtain a base cloth with shape memory function, wherein the treatment liquid The concentration of the inner 2D resin finishing agent is 80g/L, the concentration of MgCl 2 ·6H 2 O and NH 4 Cl is 8g/L, the softener is 40g/L, and the wetting agent is 1g/L; The concentration of finishing agent is 80g/L, the concentration of MgCl 2 ·6H 2 O and NH 4 Cl is 8g/L, the softener is 40g/L, the wetting agent is 1g/L, and the treatment liquid and resin treated with liquid ammonia The concentration ratio of MgCl 2 ·6H 2 O and NH 4 Cl in the finished resin solution is 15:1, the softener is a silicone softener, and the wetting agent is TRITONTMHW-1000;
S5：喷涂处理：将S4中获得的具有形状记忆功能的基布表面喷涂太阳光吸收转换剂；其中太阳光吸收转换剂制备方法为将甲基丙烯酸二甲基氨乙酯与丙烯酰胺混合搅拌至完全溶解，加入金纳米颗粒、石墨烯颗粒、多晶硅和高分子成膜剂后再次混合搅拌，得到太阳光吸收转换剂；且太阳光吸收转换剂中的组分按重量份计，包括：甲基丙烯酸二甲基氨乙酯40份、丙烯酰胺35 份、金纳米颗粒8份、石墨烯颗粒8份、多晶硅8份和高分子成膜剂4份。S5: Spraying treatment: the surface of the base fabric with shape memory function obtained in S4 is sprayed with a solar light absorption conversion agent; wherein the preparation method of the solar light absorption conversion agent is to mix and stir dimethylaminoethyl methacrylate and acrylamide to Completely dissolving, adding gold nanoparticles, graphene particles, polysilicon and polymer film-forming agent and then mixing and stirring again to obtain a solar light absorption conversion agent; and the components in the solar light absorption conversion agent are based on parts by weight, including: methyl 40 parts of dimethylaminoethyl acrylate, 35 parts of acrylamide, 8 parts of gold nanoparticles, 8 parts of graphene particles, 8 parts of polysilicon and 4 parts of polymer film-forming agent.
对比例1Comparative Example 1
一种防水恒温功能的超薄羽绒服面料的制作方法，其唯一区别与实施例4 相比在于将步骤一中的成孔剂替换为等量的甲壳素颗粒，并去除步骤二。A method for making an ultra-thin down jacket fabric with waterproof and constant temperature function, the only difference compared with Example 4 is that the pore-forming agent in step 1 is replaced with the same amount of chitin particles, and step 2 is removed.
对比例2Comparative Example 2
一种防水恒温功能的超薄羽绒服面料的制作方法，其唯一区别与实施例4 相比在于将步骤五中的金纳米颗粒、石墨烯颗粒和多晶硅替换为等量的丙烯酰胺。A method for making an ultra-thin down jacket fabric with waterproof and constant temperature function, the only difference compared with Example 4 is that the gold nanoparticles, graphene particles and polysilicon in step 5 are replaced with the same amount of acrylamide.
对比例3Comparative Example 3
一种防水恒温功能的超薄羽绒服面料的制作方法，其区别与实施例4相比在于将步骤五中的甲基丙烯酸二甲基氨乙酯和丙烯酰胺替换为等量的金纳米颗粒和石墨烯颗粒。A method for making an ultra-thin down jacket fabric with waterproof and constant temperature function, the difference compared with Example 4 lies in that the dimethylaminoethyl methacrylate and acrylamide in step 5 are replaced with equal amounts of gold nanoparticles and graphite ene particles.
为了进一步说明本发明的技术进步性，现采用实验进一步说明。In order to further illustrate the technical progress of the present invention, experiments are now used to further illustrate.
分别采用上述实施例1-4和对比例1-3的方法制成7组防水恒温功能的超薄羽绒服面料样品，对这些样品进行性能测试，包括：(1)根据GB/T 11048 —2018《纺织品生理舒适性稳态条件下热阻和湿阻的测定》，采用静态平板法在YG606型平板式织物保温仪上测定织物的保温率，且试验温度分别为0℃和38℃；(2)对防水恒温功能的超薄羽绒服面料样品进行防水性能检测，其中，利用YG(B)812型织物渗水测定仪按照GB/T 4744-2013《纺织品防水性能的检测和评价》测试，测试结果以耐静水压/mm表示；得到数据如下表：7 groups of ultra-thin down jacket fabric samples with waterproof and constant temperature function were made by the methods of the above-mentioned Examples 1-4 and Comparative Examples 1-3 respectively, and performance tests were carried out on these samples, including: (1) According to GB/T 11048-2018 " Determination of Thermal Resistance and Moisture Resistance under Steady-State Conditions for Physiological Comfort of Textiles", the thermal insulation rate of fabrics was measured on a YG606 flat-panel fabric warmer by the static flat plate method, and the test temperatures were 0 °C and 38 °C; (2) The waterproof performance of the ultra-thin down jacket fabric samples with waterproof and constant temperature function was tested. Among them, the YG(B)812 fabric water permeability tester was used to test in accordance with GB/T 4744-2013 "Testing and Evaluation of Waterproof Performance of Textiles". The hydrostatic pressure/mm is expressed; the data obtained are as follows:
从上表可以看出，采用本发明制备方法所生产加工的防水恒温功能的超薄羽绒服面料其各方面性能均显著提升，保温率>90％，耐静水压值≧171mm。通过比较各对比例可以看出，利用成孔剂对纤维丝进行微孔处理，可在高温环境下降低面料温度，避免闷热；通过实施例1-4和对比例2可知，向太阳光吸收转换剂内加入金纳米颗粒、石墨烯颗粒和多晶硅材料可使其保温率得到提升；而实施例4与对比例3相比，加入甲基丙烯酸二甲基氨乙酯和丙烯酰胺的太阳光吸收转换剂，可使面料的防水性能提高。It can be seen from the above table that the performance of the ultra-thin down jacket fabric with waterproof and constant temperature function produced and processed by the preparation method of the present invention is significantly improved in all aspects, the heat preservation rate is >90%, and the hydrostatic pressure resistance value is ≧171mm. By comparing the comparative examples, it can be seen that the microporous treatment of fiber filaments with a pore-forming agent can reduce the temperature of the fabric in a high temperature environment and avoid sultry heat; it can be seen from Examples 1-4 and Comparative Example 2 that the conversion to sunlight absorption The addition of gold nanoparticles, graphene particles and polysilicon materials into the agent can improve the heat preservation rate; and Example 4 is compared with Comparative Example 3, adding dimethylaminoethyl methacrylate and acrylamide. The solar light absorption conversion agent, which can improve the waterproof performance of the fabric.
以上显示和描述了本发明的基本原理和主要特征和本发明的优点。本行业的技术人员应该了解，本发明不受上述实施例的限制，上述实施例和说明书中描述的只是说明本发明的原理，在不脱离本发明精神和范围的前提下，本发明还会有各种变化和改进，这些变化和改进都落入要求保护的本发明范围内。本发明要求保护范围由所附的权利要求书及其等效物界定。The basic principles and main features of the present invention and the advantages of the present invention have been shown and described above. Those skilled in the art should understand that the present invention is not limited by the above-mentioned embodiments, and the descriptions in the above-mentioned embodiments and the description are only to illustrate the principle of the present invention. Without departing from the spirit and scope of the present invention, the present invention will have Various changes and modifications fall within the scope of the claimed invention. The claimed scope of the present invention is defined by the appended claims and their equivalents.
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