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CN114720171A - Explosive security inspection sampling device and detection method - Google Patents

Explosive security inspection sampling device and detection method Download PDF

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Publication number
CN114720171A
CN114720171A CN202110009298.2A CN202110009298A CN114720171A CN 114720171 A CN114720171 A CN 114720171A CN 202110009298 A CN202110009298 A CN 202110009298A CN 114720171 A CN114720171 A CN 114720171A
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sampling
polyimide tape
high temperature
explosives
temperature resistant
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王爱博
黄卫
李海洋
王卫国
李京华
张远智
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Dalian Institute of Chemical Physics of CAS
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Dalian Institute of Chemical Physics of CAS
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    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N1/00Sampling; Preparing specimens for investigation
    • G01N1/02Devices for withdrawing samples
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N1/00Sampling; Preparing specimens for investigation
    • G01N1/02Devices for withdrawing samples
    • G01N2001/022Devices for withdrawing samples sampling for security purposes, e.g. contraband, warfare agents

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  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Chemical & Material Sciences (AREA)
  • Analytical Chemistry (AREA)
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  • General Health & Medical Sciences (AREA)
  • General Physics & Mathematics (AREA)
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  • Sampling And Sample Adjustment (AREA)

Abstract

本发明公开了一种爆炸物安检采样装置及检测方法,目前,基于离子迁移谱的爆炸物探测仪,需要使用采样试纸擦取采样,然后放入探测仪中检测分析。而采样试纸多为聚四氟乙烯材料,其表面极为光滑,虽增加纹理,但采样效果极为不佳。为此,本发明公开了一种方便高效的爆炸物安检采样装置及其使用方法,可用于爆炸物安检仪的高效采样。该装置主要包括:耐高温聚亚酰胺胶带、采样载体、手柄。The invention discloses an explosive security inspection sampling device and a detection method. At present, an explosive detector based on ion mobility spectrum needs to use a sampling test paper to wipe the sample, and then put it into the detector for detection and analysis. The sampling test paper is mostly made of polytetrafluoroethylene, and its surface is extremely smooth. Although the texture is increased, the sampling effect is extremely poor. To this end, the present invention discloses a convenient and efficient explosive security inspection sampling device and a use method thereof, which can be used for efficient sampling of explosive security inspection instruments. The device mainly includes: high temperature resistant polyimide tape, sampling carrier and handle.

Description

一种爆炸物安检采样装置及检测方法A kind of explosive security inspection sampling device and detection method

技术领域technical field

发明涉及一种爆炸物安检采样装置及方法。The invention relates to an explosive security inspection sampling device and method.

背景技术Background technique

离子迁移谱(Ion Mobility Spectrometry,IMS)是根据大气压下离子迁移率的差异,通过均匀弱电场对样品离子进行分离和检测的技术。具有检测速度快(单个检测周期<20ms)、灵敏度高、易实现小型化、成本低等优点,广泛应用与军事、安检等领域。其中,在爆炸物安全检测的应用最为常见。Ion Mobility Spectrometry (IMS) is a technology that separates and detects sample ions through a uniform weak electric field according to the difference in ion mobility under atmospheric pressure. It has the advantages of fast detection speed (single detection period < 20ms), high sensitivity, easy miniaturization, and low cost, and is widely used in military, security inspection and other fields. Among them, the application of explosive safety detection is the most common.

但目前,基于离子迁移谱的爆炸物探测仪,需要使用采样试纸擦取采样,然后放入探测仪中检测分析。而采样试纸多为聚四氟乙烯材料,其表面极为光滑,虽增加纹理,但采样效果极为不佳。But at present, explosives detectors based on ion mobility spectrometry need to use sampling test paper to wipe the samples, and then put them into the detector for detection and analysis. The sampling test paper is mostly made of polytetrafluoroethylene, and its surface is extremely smooth. Although the texture is increased, the sampling effect is extremely poor.

为此,本发明公开了一种方便高效的爆炸物安检采样装置及其使用方法,使用耐高温的聚酰亚胺胶带为采样试纸,粘取物体表面、深层的爆炸物残留样品,使爆炸物采样的更为高效。To this end, the present invention discloses a convenient and efficient explosive security inspection sampling device and a method of using the same. The high temperature-resistant polyimide tape is used as the sampling test paper, and the explosive residue samples on the surface and deep layers of the object are adhered to make the explosives Sampling is more efficient.

发明内容SUMMARY OF THE INVENTION

一种爆炸物安检采样装置,其特征在于:An explosive security inspection sampling device, characterized in that:

所述装置包括:耐高温聚亚酰胺胶带(1)、采样载体(2)、手柄(3);所述手柄(3)一端与采样载体(2)相连;The device comprises: a high temperature resistant polyimide tape (1), a sampling carrier (2), and a handle (3); one end of the handle (3) is connected to the sampling carrier (2);

所述采样载体外周设有耐高温聚亚酰胺胶带(1);所述耐高温聚亚酰胺胶带(1)含胶面向外。The outer periphery of the sampling carrier is provided with a high temperature resistant polyimide tape (1); the adhesive surface of the high temperature resistant polyimide tape (1) is outward.

将耐高温聚亚酰胺胶带(1)不含胶面围绕载体(2)缠绕一周固定。手持手柄(3)粘取表面、深层的爆炸物残留样品。Wind the non-adhesive surface of the high-temperature resistant polyimide tape (1) around the carrier (2) for one week and fix it. Hold the handle (3) to take samples of explosive residues on the surface and deep.

进一步地,在上述技术方案中,耐高温聚亚酰胺胶带(1)厚度为0.5-2mm。Further, in the above technical solution, the thickness of the high temperature resistant polyimide tape (1) is 0.5-2 mm.

进一步地,在上述技术方案中,所述采样载体(2)与手柄(3)夹角为0-90°。Further, in the above technical solution, the angle between the sampling carrier (2) and the handle (3) is 0-90°.

本发明提供一种爆炸物安检采样检测方法,采用上述装置进行采样,手持采样装置手柄(3)通过耐高温聚亚酰胺胶带(1)粘取样品;通过高温聚亚酰胺胶带的粘性,粘取物体表面、深层的爆炸物残留样品,然后剪取适量采过样的耐高温聚亚酰胺胶带(1),放入爆炸物安检仪中检测。The invention provides a method for security inspection sampling and detection of explosives. The above device is used for sampling, and the handle (3) of the sampling device is held to take samples through high temperature resistant polyimide tape (1); Explosive residue samples on the surface and deep layers of the object, and then cut an appropriate amount of high-temperature polyimide tape (1) that has been sampled, and put it into the explosives security detector for detection.

本发明提供一种爆炸物安检采样检测方法,其特征在于:采用高温聚亚酰胺胶带作为采样试纸粘取采样,然后剪取适量采过样的高温聚亚酰胺胶带,放入爆炸物安检仪中检测。The invention provides a sampling and detection method for security inspection of explosives, which is characterized in that: a high-temperature polyimide tape is used as a sampling test paper to stick and take samples, and then an appropriate amount of the high-temperature polyimide tape that has been sampled is cut and placed in a security inspection apparatus for explosives detection.

进一步地,在上述技术方案中,将耐高温聚亚酰胺胶带平铺固定采样区或周边地面上,所述耐高温聚亚酰胺胶带胶面朝上,粘取出入该区域人员鞋底的样品,然后剪取适量采过样的耐高温聚亚酰胺胶带,放入爆炸物安检仪中检测。Further, in the above-mentioned technical scheme, the high temperature resistant polyimide tape is laid flat on the fixed sampling area or the surrounding ground, the adhesive surface of the high temperature resistant polyimide tape is facing up, and the samples of the personnel's soles in this area are glued and taken out, and then Cut an appropriate amount of sampled high temperature polyimide tape and put it into the explosives security detector for detection.

进一步地,在上述技术方案中,将耐高温聚亚酰胺胶带平铺固定在门前地板上。Further, in the above technical solution, the high temperature resistant polyimide tape is flatly fixed on the floor in front of the door.

进一步地,在上述技术方案中,耐高温聚亚酰胺胶带(1)可耐300℃高温,使用前在200-300℃高温下活化处理12h,以除去胶带残留物质干扰。Further, in the above technical solution, the high temperature resistant polyimide tape (1) can withstand a high temperature of 300°C, and is activated at a high temperature of 200-300°C for 12 hours before use to remove the interference of residual substances in the tape.

本发明的优点如下:The advantages of the present invention are as follows:

本发明方法,采样试纸可方便采购和定制,可成卷保存,携带方便。According to the method of the invention, the sampling test paper can be conveniently purchased and customized, can be stored in rolls, and is convenient to carry.

本发明方法,使用了聚亚酰胺胶带的粘性特征,可粘取物体表面、深层的爆炸物残留样品,采样效果更佳。The method of the invention uses the sticky characteristics of the polyimide tape, and can stick samples of explosive residues on the surface and deep layers of objects, and the sampling effect is better.

附图说明Description of drawings

图1为一种爆炸物安检采样装置结构示意图,其中,1为耐高温聚亚酰胺胶带、2为采样载体、3为手柄。Figure 1 is a schematic structural diagram of an explosive security inspection sampling device, wherein 1 is a high temperature resistant polyimide tape, 2 is a sampling carrier, and 3 is a handle.

具体实施方式Detailed ways

以下实施例说明本发明的使用,但不限制所述的应用范围。The following examples illustrate the use of the present invention, but do not limit the scope of application described.

耐高温聚亚酰胺胶带(1)可耐300℃高温,使用前在200-300℃高温干净空气氛围下活化处理12h,以除去胶带残留物质干扰。The high temperature resistant polyimide tape (1) can withstand high temperature of 300 °C. Before use, it should be activated for 12 hours in a high temperature and clean air atmosphere of 200-300 °C to remove the interference of residual substances in the tape.

一种爆炸物安检采样装置,所述装置包括:耐高温聚亚酰胺胶带(1)、采样载体(2)、手柄(3);所述手柄(3)一端与采样载体(2)相连;所述采样载体外周设有耐高温聚亚酰胺胶带(1);所述耐高温聚亚酰胺胶带(1)含胶面向外。An explosive security inspection sampling device, the device comprises: a high temperature resistant polyimide tape (1), a sampling carrier (2), and a handle (3); one end of the handle (3) is connected to the sampling carrier (2); The outer periphery of the sampling carrier is provided with a high temperature resistant polyimide adhesive tape (1); the adhesive surface of the high temperature resistant polyimide adhesive tape (1) is outward.

实施例1Example 1

将耐高温聚亚酰胺胶带(1)不含胶面围绕载体(2)缠绕一周固定,含胶面向外,手持手柄(3)粘取可疑物品。Wrap the non-adhesive surface of the high temperature resistant polyimide tape (1) around the carrier (2) and fix it, with the adhesive-containing surface facing outwards, hold the handle (3) to stick the suspicious item.

实施例2Example 2

不用采样载体(2)和手柄(3),直接用高温聚亚酰胺胶带粘取采样,然后剪取适量采过样的胶带,放入爆炸物安检仪中检测。Without the sampling carrier (2) and the handle (3), directly stick the samples with high-temperature polyimide tape, and then cut an appropriate amount of the sampled tape and put it into the explosives security detector for detection.

实施例3Example 3

将较大面积的聚亚酰胺胶带平铺固定在门前地板上,粘取出入该门人员鞋底的样品,然后剪取适量采过样的胶带,放入爆炸物安检仪中检测。Lay and fix a large area of polyimide tape on the floor in front of the door, stick and take out the sample of the shoe sole of the door personnel, and then cut an appropriate amount of the sampled tape and put it into the explosive security detector for detection.

Claims (9)

1.一种爆炸物安检采样装置,其特征在于:1. An explosives security inspection sampling device is characterized in that: 所述装置包括:耐高温聚亚酰胺胶带(1)、采样载体(2)、手柄(3);所述手柄(3)一端与采样载体(2)相连;The device comprises: a high temperature resistant polyimide tape (1), a sampling carrier (2), and a handle (3); one end of the handle (3) is connected to the sampling carrier (2); 所述采样载体外周设有耐高温聚亚酰胺胶带(1);所述耐高温聚亚酰胺胶带(1)含胶面向外。The outer periphery of the sampling carrier is provided with a high temperature resistant polyimide tape (1); the adhesive surface of the high temperature resistant polyimide tape (1) is outward. 2.根据权利要求1所述的一种爆炸物安检采样装置,其特征在于:耐高温聚亚酰胺胶带(1)厚度为0.5-2mm。2 . The explosives security inspection sampling device according to claim 1 , wherein the thickness of the high temperature resistant polyimide tape (1) is 0.5-2 mm. 3 . 3.根据权利要求1所述的一种爆炸物安检采样装置,其特征在于:所述采样载体(2)与手柄(3)夹角为0-90°。3 . The explosives security inspection sampling device according to claim 1 , wherein the angle between the sampling carrier ( 2 ) and the handle ( 3 ) is 0-90°. 4 . 4.一种爆炸物安检采样检测方法,其特征在于:采用权利要求1或2所述装置进行采样,手持采样装置手柄(3)通过耐高温聚亚酰胺胶带(1)粘取样品;通过高温聚亚酰胺胶带的粘性,粘取物体表面、深层的爆炸物残留样品,然后剪取适量采过样的耐高温聚亚酰胺胶带(1),放入爆炸物安检仪中检测。4. An explosives security inspection sampling detection method is characterized in that: adopting the device according to claim 1 or 2 for sampling, holding the sampling device handle (3) to take samples by sticking with high temperature resistant polyimide tape (1); To determine the viscosity of the polyimide tape, stick samples of explosive residues on the surface and deep layers of the object, and then cut out an appropriate amount of high-temperature-resistant polyimide tape (1) that has been sampled, and put it into an explosives security detector for detection. 5.一种爆炸物安检采样检测方法,其特征在于:采用高温聚亚酰胺胶带作为采样试纸粘取采样,然后剪取适量采过样的高温聚亚酰胺胶带,放入爆炸物安检仪中检测。5. A method for sampling and detecting explosives security inspection, it is characterized in that: adopt high-temperature polyimide tape as sampling test paper to stick and take samples, then cut an appropriate amount of high-temperature polyimide tape that has been sampled, put into explosives security inspection instrument and detect . 6.根据权利要求5所述的方法,其特征在于:将耐高温聚亚酰胺胶带平铺固定采样区或周边地面上,所述耐高温聚亚酰胺胶带胶面朝上,粘取出入该区域人员鞋底的样品,然后剪取适量采过样的耐高温聚亚酰胺胶带,放入爆炸物安检仪中检测。6. The method according to claim 5, characterized in that: the high temperature resistant polyimide tape is laid flat on the fixed sampling area or the surrounding ground, the adhesive surface of the high temperature resistant polyimide tape is facing upward, and the adhesive tape is taken out into the area. Samples of the soles of the personnel, and then cut an appropriate amount of high-temperature polyimide tape that has been sampled, and put them into the explosives security detector for detection. 7.根据权利要求6所述的方法,其特征在于:将耐高温聚亚酰胺胶带平铺固定在门前地板上。7 . The method according to claim 6 , wherein the high temperature resistant polyimide tape is flatly fixed on the floor in front of the door. 8 . 8.根据权利要求4或5所述的方法,其特征在于:所述爆炸物安检仪为基于离子迁移谱的爆炸物探测仪。8. The method according to claim 4 or 5, wherein the explosives security detector is an explosive detector based on ion mobility spectrometry. 9.根据权利要求1~3任意一项所述装置,或权利要求4-8任意一项方法,其特征在于:耐高温聚亚酰胺胶带(1)可耐300℃高温,使用前在200-300℃高温下活化处理12h,以除去胶带残留物质干扰。9. The device according to any one of claims 1 to 3, or the method of any one of claims 4 to 8, characterized in that: the high temperature resistant polyimide tape (1) can withstand a high temperature of 300° C. Activation treatment at a high temperature of 300 ° C for 12 hours to remove the interference of residual substances in the tape.
CN202110009298.2A 2021-01-05 2021-01-05 Explosive security inspection sampling device and detection method Pending CN114720171A (en)

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Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101363778A (en) * 2007-08-10 2009-02-11 同方威视技术股份有限公司 Handheld sampling device and method capable of preventing sampling carrier from deforming
CN105548134A (en) * 2015-12-04 2016-05-04 山东大学 Wiping extraction-surface-enhanced Raman scattering film for on-site fast detection of explosive and its preparation method and use
CN105954067A (en) * 2016-04-26 2016-09-21 中南大学 Sampling film and method for detection and analysis of iron ore sintering flue gas ultrafine particles by using sampling film
CN209707139U (en) * 2019-03-12 2019-11-29 河南师范大学 A body surface heavy metal sampling device using tape method
CN210037346U (en) * 2019-05-21 2020-02-07 佛山量源环境与安全检测有限公司 Portable oil smoke detects sampling device
CN110790865A (en) * 2019-11-15 2020-02-14 中国科学院新疆理化技术研究所 A dual-network hydrogel for explosive particle sampling and preparation method thereof

Patent Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101363778A (en) * 2007-08-10 2009-02-11 同方威视技术股份有限公司 Handheld sampling device and method capable of preventing sampling carrier from deforming
CN105548134A (en) * 2015-12-04 2016-05-04 山东大学 Wiping extraction-surface-enhanced Raman scattering film for on-site fast detection of explosive and its preparation method and use
CN105954067A (en) * 2016-04-26 2016-09-21 中南大学 Sampling film and method for detection and analysis of iron ore sintering flue gas ultrafine particles by using sampling film
CN209707139U (en) * 2019-03-12 2019-11-29 河南师范大学 A body surface heavy metal sampling device using tape method
CN210037346U (en) * 2019-05-21 2020-02-07 佛山量源环境与安全检测有限公司 Portable oil smoke detects sampling device
CN110790865A (en) * 2019-11-15 2020-02-14 中国科学院新疆理化技术研究所 A dual-network hydrogel for explosive particle sampling and preparation method thereof

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