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CN114558073A - Essential oil with dehumidifying function - Google Patents

Essential oil with dehumidifying function Download PDF

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Publication number
CN114558073A
CN114558073A CN202210310460.9A CN202210310460A CN114558073A CN 114558073 A CN114558073 A CN 114558073A CN 202210310460 A CN202210310460 A CN 202210310460A CN 114558073 A CN114558073 A CN 114558073A
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raw materials
essential oil
extraction
root
compatible
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陈伟
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Individual
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    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/18—Magnoliophyta (angiosperms)
    • A61K36/185—Magnoliopsida (dicotyledons)
    • A61K36/48—Fabaceae or Leguminosae (Pea or Legume family); Caesalpiniaceae; Mimosaceae; Papilionaceae
    • A61K36/481—Astragalus (milkvetch)
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K35/00—Medicinal preparations containing materials or reaction products thereof with undetermined constitution
    • A61K35/56—Materials from animals other than mammals
    • A61K35/58—Reptiles
    • A61K35/583—Snakes; Lizards, e.g. chameleons
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/18—Magnoliophyta (angiosperms)
    • A61K36/185—Magnoliopsida (dicotyledons)
    • A61K36/23—Apiaceae or Umbelliferae (Carrot family), e.g. dill, chervil, coriander or cumin
    • A61K36/237—Notopterygium
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/18—Magnoliophyta (angiosperms)
    • A61K36/185—Magnoliopsida (dicotyledons)
    • A61K36/28—Asteraceae or Compositae (Aster or Sunflower family), e.g. chamomile, feverfew, yarrow or echinacea
    • A61K36/284—Atractylodes
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/18—Magnoliophyta (angiosperms)
    • A61K36/185—Magnoliopsida (dicotyledons)
    • A61K36/28—Asteraceae or Compositae (Aster or Sunflower family), e.g. chamomile, feverfew, yarrow or echinacea
    • A61K36/286—Carthamus (distaff thistle)
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/18—Magnoliophyta (angiosperms)
    • A61K36/185—Magnoliopsida (dicotyledons)
    • A61K36/48—Fabaceae or Leguminosae (Pea or Legume family); Caesalpiniaceae; Mimosaceae; Papilionaceae
    • A61K36/484—Glycyrrhiza (licorice)
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/18—Magnoliophyta (angiosperms)
    • A61K36/185—Magnoliopsida (dicotyledons)
    • A61K36/48—Fabaceae or Leguminosae (Pea or Legume family); Caesalpiniaceae; Mimosaceae; Papilionaceae
    • A61K36/486—Millettia
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/18—Magnoliophyta (angiosperms)
    • A61K36/185—Magnoliopsida (dicotyledons)
    • A61K36/53—Lamiaceae or Labiatae (Mint family), e.g. thyme, rosemary or lavender
    • A61K36/537—Salvia (sage)
    • A—HUMAN NECESSITIES
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    • A61K36/18—Magnoliophyta (angiosperms)
    • A61K36/185—Magnoliopsida (dicotyledons)
    • A61K36/54—Lauraceae (Laurel family), e.g. cinnamon or sassafras
    • A—HUMAN NECESSITIES
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    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/18—Magnoliophyta (angiosperms)
    • A61K36/185—Magnoliopsida (dicotyledons)
    • A61K36/71—Ranunculaceae (Buttercup family), e.g. larkspur, hepatica, hydrastis, columbine or goldenseal
    • A61K36/716—Clematis (leather flower)
    • A—HUMAN NECESSITIES
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    • A61K36/18—Magnoliophyta (angiosperms)
    • A61K36/88—Liliopsida (monocotyledons)
    • A61K36/889—Arecaceae, Palmae or Palmaceae (Palm family), e.g. date or coconut palm or palmetto
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    • A61K36/18—Magnoliophyta (angiosperms)
    • A61K36/88—Liliopsida (monocotyledons)
    • A61K36/896—Liliaceae (Lily family), e.g. daylily, plantain lily, Hyacinth or narcissus
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    • A61P—SPECIFIC THERAPEUTIC ACTIVITY OF CHEMICAL COMPOUNDS OR MEDICINAL PREPARATIONS
    • A61P29/00—Non-central analgesic, antipyretic or antiinflammatory agents, e.g. antirheumatic agents; Non-steroidal antiinflammatory drugs [NSAID]
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61P—SPECIFIC THERAPEUTIC ACTIVITY OF CHEMICAL COMPOUNDS OR MEDICINAL PREPARATIONS
    • A61P39/00—General protective or antinoxious agents
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B9/00—Essential oils; Perfumes
    • C11B9/02—Recovery or refining of essential oils from raw materials
    • C11B9/022—Refining
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B9/00—Essential oils; Perfumes
    • C11B9/02—Recovery or refining of essential oils from raw materials
    • C11B9/025—Recovery by solvent extraction
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B9/00—Essential oils; Perfumes
    • C11B9/02—Recovery or refining of essential oils from raw materials
    • C11B9/027—Recovery of volatiles by distillation or stripping
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2236/00—Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
    • A61K2236/10—Preparation or pretreatment of starting material
    • A61K2236/15—Preparation or pretreatment of starting material involving mechanical treatment, e.g. chopping up, cutting or grinding
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
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    • A61K2236/00—Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
    • A61K2236/10—Preparation or pretreatment of starting material
    • A61K2236/19—Preparation or pretreatment of starting material involving fermentation using yeast, bacteria or both; enzymatic treatment
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    • A61K2236/30—Extraction of the material
    • A61K2236/33—Extraction of the material involving extraction with hydrophilic solvents, e.g. lower alcohols, esters or ketones
    • A61K2236/331—Extraction of the material involving extraction with hydrophilic solvents, e.g. lower alcohols, esters or ketones using water, e.g. cold water, infusion, tea, steam distillation or decoction
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Abstract

The invention discloses conditioning essential oil with a dehumidifying function, which comprises the following raw materials; astragalus root, spatholobus stem, safflower, black-tail snake, notopterygium root, clematis root, white atractylodes rhizome, salvia root, cassia twig, dragon's blood resin and honey-fried licorice root, according to the preparation method, raw materials for treating rheumatism are selected from compatibility, so that the raw materials are reasonably matched, physical conflict among the raw materials is prevented, essential oil prepared from the raw materials has strong damp-clearing property, and then the raw materials are subjected to three key steps of raw material pretreatment, crude extraction and fine extraction through the preparation process matching of material weighing, material pretreatment, boiling and crushing, residue removal and filtration, digestion and enzymolysis, crude extraction and fine extraction, so that the refined dehumidifying and conditioning essential oil with the dehumidifying function is obtained.

Description

Essential oil with dehumidifying function
Technical Field
The invention relates to the technical field of essential oil preparation, in particular to conditioning essential oil with a dehumidifying function.
Background
The essential oil is volatile aromatic substances extracted from flowers, leaves, stems, roots or fruits of plants by a steam distillation method, an extrusion method, a cold soaking method or a solvent extraction method, and is diluted (compound essential oil) and undiluted (single essential oil) such as cactus seed oil, and the essential oil has strong volatility and can be quickly volatilized once contacting air, so the essential oil must be stored in a sealed dark bottle.
Essential oil is often used in people's daily life, and the essential oil that exists on the market does not have the dehumidification function for caring and maintaining skin effect mostly, daubs the essential oil on the market at people after, can't carry out dehumidification to internal moisture or joint moisture and handle, reduces the recuperation effect of essential oil to the human body, for this reason, proposes dehumidification function recuperation essential oil.
Disclosure of Invention
The invention aims to provide essential oil with a dehumidifying function, and aims to solve the problems that most of the essential oil in the market provided by the background art has the functions of caring and maintaining skin, does not have the dehumidifying function, and reduces the nursing effect of the essential oil on human bodies.
In order to achieve the purpose, the invention provides the following technical scheme: a conditioning essential oil with dehumidifying function comprises the following raw materials;
astragalus root, spatholobus stem, safflower, zaocys dhumnade, notopterygium root, clematis root, bighead atractylodes rhizome, salvia miltiorrhiza, cassia twig, dragon's blood and honey-fried licorice root;
and the mass ranges of the raw material components are as follows:
25-35g of astragalus membranaceus, 20-40g of caulis spatholobi, 25-40g of safflower, 15-25g of zaocys dhumnade, 18-24g of notopterygium root, 12-18g of radix clematidis, 12-17g of bighead atractylodes rhizome, 10-20g of salvia miltiorrhiza, 8-15g of cassia twig, 6-12g of dragon's blood and 4-8g of honey-fried licorice root;
the required equipment is as follows:
500ml container, strainer, glass stirring rod, electric stirrer, electronic balance, electric boiler, crushing grinder, vibration filter, oil-water separator, steam distillation extraction apparatus, carbon dioxide critical extraction apparatus and molecular distillation apparatus;
the preparation method comprises the following steps:
A. weighing materials: firstly, putting the raw materials of astragalus, suberect spatholobus stem, safflower, zaocys dhumnade, notopterygium root, clematis root, largehead atractylodes rhizome, salvia miltiorrhiza, cassia twig, dragon's blood and honey-fried licorice root on an electronic balance one by one, and weighing 28g of astragalus, 30g of suberect spatholobus stem, 35g of safflower, 22g of zaocys dhumnade, 20g of notopterygium root, 16g of clematis root, 14g of bighead atractylodes rhizome, 16g of salvia miltiorrhiza, 12g of cassia twig, 8g of dragon's blood and 6g of honey-fried licorice root for later use by a worker;
B. material pretreatment: then putting 28g of astragalus membranaceus, 30g of caulis spatholobi, 35g of safflower, 22g of zaocys dhumnade, 20g of notopterygium root, 16g of radix clematidis, 14g of bighead atractylodes rhizome, 16g of salvia miltiorrhiza, 12g of cassia twig, 8g of dragon's blood and 6g of honey-fried licorice root into a 500ml container, then injecting deionized purified water into the 500ml container, soaking, and after the soaking of the raw materials is finished, manually cleaning the raw materials by a worker;
C. boiling and crushing: then, putting the pretreated raw materials into an electric boiler by a worker, adding deionized water for high-temperature sterilization at 100 ℃ and boiling treatment, then flatly spreading the boiled raw materials in a room by the worker, physically cooling the raw materials to a room temperature state, putting the compatible raw materials into a grinding machine for grinding and crushing until the ground and crushed raw materials are in small-diameter particles, and waiting for standby;
D. removing slag and filtering: then, putting the small-diameter granular compatible raw materials into a cleaned 500ml container again by a worker, injecting deionized purified water to cover the upper end of the compatible raw materials, fishing out floating dregs by the worker by using a strainer, and putting the compatible granular raw materials with the dregs removed into a vibration filter by the worker to obtain the compatible granular raw materials with the same volume and size;
E. leaching and enzymolysis: then, putting the filtered compatible granular raw materials into a dilute hydrochloric acid solution by a worker to obtain a leaching solution, and adding TapDNA polymerase and horseradish peroxidase into the obtained compatible raw material mixed solution by the worker to perform enzymolysis reaction to obtain a compatible raw material enzymolysis solution;
F. coarse extraction: putting the enzymolysis solution of the compatible raw materials after enzymolysis into a steam distillation extraction instrument for primary extraction and collection of an essential oil mixture by a worker, putting the extracted essential oil mixture into an oil-water separator for oil-water separation, and obtaining crude essential oil after oil-water separation;
G. fine extraction: and then, putting the prepared coarse essential oil into a carbon dioxide critical extraction instrument for secondary extraction by a worker, collecting fine essential oil, putting the collected fine essential oil into a molecular distillation instrument for final molecular distillation refining treatment by the worker, collecting the fine essential oil generated in the distillation process of the molecular distillation instrument, thus obtaining fine dehumidifying and nourishing essential oil, then putting the fine dehumidifying and nourishing essential oil into a glass packaging bottle by the worker, and sealing.
Preferably, in the material pretreatment process, the added deionized water needs to cover 28g of astragalus membranaceus, 30g of caulis spatholobi, 35g of safflower, 22g of zaocys dhumnade, 20g of notopterygium root, 16g of radix clematidis, 14g of bighead atractylodes rhizome, 16g of salvia miltiorrhiza, 12g of cassia twig, 8g of dragon's blood and 6g of honey-fried licorice root, and a glass stirring rod is used for stirring the raw materials, so that the raw materials and the deionized water are fully sunk and soaked, and the soaking time of the raw materials is between 1h and 3 h.
Preferably, in the material pretreatment process, after soaking of the raw materials is completed, the worker uses the strainer to take out the floating powder floating on the surface layer of the 500ml container, the strainer is wrapped by the fine filter screen, the mesh density of the fine filter screen is between 200 meshes and 400 meshes, and the cleaning standard is as follows: the surface of each raw material has no impurity particles attached, each raw material is taken out and is not taken into a medicine section, and the surface of each raw material is not damaged.
Preferably, in the boiling and crushing process, the electric boiler is used for cooking the raw materials for 10min by firstly adjusting the temperature to 80 ℃, then the electric boiler is used for cooking the raw materials for 30min by adjusting the temperature to 100 ℃, and finally the electric boiler is used for cooking the raw materials for 15min by adjusting the temperature to 80 ℃.
Preferably, in the boiling and pulverizing process, the pulverizing and pulverizing machine grinds and pulverizes the compatible materials in a manner of pulverizing and pulverizing while drying, wherein the drying temperature range is between 60 ℃ and 80 ℃, and the pulverizing and pulverizing rotation speed range of the pulverizing and pulverizing machine is between 600 and 1000 r/min.
Preferably, in the deslagging and filtering process, the vibration frequency of the vibration filter is 50HZ, the vibration filter adopts a three-layer filter screen frame structure to uniformly vibrate and screen compatible granular raw materials, and the mesh densities of the upper, middle and lower filter screens of the three-layer filter screen frame are respectively between 400-mesh 600 meshes, 600-mesh 800 meshes and 800-mesh 1000 meshes.
Preferably, in the leaching enzymolysis process, the mass of the dilute hydrochloric acid solution is 4-8 times of that of the compatible granular raw materials, the pH value of the dilute hydrochloric acid solution is 6, and the mass ratio of the TapDNA polymerase to the horseradish peroxidase to the compatible raw material mixed solution is as follows: 1: 1.5: 80, the purity of the horseradish peroxidase HRP is expressed by RZ (the ratio of absorbance of the HRP at 403nm to that at 275nm respectively), the RZ value of the horseradish peroxidase is more than 3.0, the enzymolysis temperature is between 30 and 40 ℃, and the enzymolysis time is between 2 and 4 hours.
Preferably, in the crude extraction process, the extraction temperature of the steam distillation extraction instrument is between 120-160 ℃, the extraction is carried out for 3-5h, the oil-water separator firstly carries out standing precipitation on the enzymolysis solution of the compatible raw materials for 30-45min, after the oil-water separation of the essential oil mixture is finished, the water is firstly filtered and discharged, and then, the sewage sodium sulfate is added to carry out drying separation on the oil layer left by the essential oil mixture.
Preferably, in the fine extraction process, the extraction temperature of a carbon dioxide critical extraction instrument is between 40 ℃ and 50 ℃, the pressure is between 12MPa and 20MPa, the fine extraction time is 1 to 2min, the flow rate of carbon dioxide in the carbon dioxide critical extraction instrument is 20kg/h to 40kg/h, and a molecular distillation instrument carries out two-section distillation treatment on the fine essential oil, wherein the first-section evaporation temperature is 120 ℃ to 130 ℃, and the second-section evaporation temperature is 50 ℃ to 70 ℃.
Compared with the prior art, the invention has the beneficial effects that:
according to the invention, through the matching of the raw materials of astragalus, caulis spatholobi, safflower, zaocys dhumnade, notopterygium root, radix clematidis, bighead atractylodes rhizome, salvia miltiorrhiza, cassia twig, dragon's blood and honey-fried licorice root, raw materials for treating rheumatism are selected from compatibility, so that the raw materials are reasonably matched, and the physical conflict among the raw materials is prevented, so that the essential oil prepared from the raw materials has strong damp-clearing property, and then the raw materials are subjected to three key steps of raw material pretreatment, crude extraction and fine extraction through the matching of preparation processes of material weighing, material pretreatment, boiling and crushing, residue removal and filtration, leaching and enzymolysis, crude extraction and fine extraction, so that the refined dehumidifying and nourishing essential oil with a dehumidifying function is obtained.
Detailed Description
The technical solutions in the embodiments of the present invention will be clearly and completely described below with reference to the embodiments of the present invention, and it is obvious that the described embodiments are only a part of the embodiments of the present invention, and not all of the embodiments. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention.
Example 1
The invention provides a technical scheme that: a conditioning essential oil with dehumidifying function comprises the following raw materials;
astragalus root, spatholobus stem, safflower, zaocys dhumnade, notopterygium root, clematis root, bighead atractylodes rhizome, salvia miltiorrhiza, cassia twig, dragon's blood and honey-fried licorice root;
and the mass ranges of the raw material components are as follows:
25-35g of astragalus membranaceus, 20-40g of caulis spatholobi, 25-40g of safflower, 15-25g of zaocys dhumnade, 18-24g of notopterygium root, 12-18g of radix clematidis, 12-17g of bighead atractylodes rhizome, 10-20g of salvia miltiorrhiza, 8-15g of cassia twig, 6-12g of dragon's blood and 4-8g of honey-fried licorice root;
the required equipment is as follows:
500ml container, strainer, glass stirring rod, electric stirrer, electronic balance, electric boiler, crushing grinder, vibration filter, oil-water separator, steam distillation extraction apparatus, carbon dioxide critical extraction apparatus and molecular distillation apparatus;
the preparation method comprises the following steps:
A. weighing materials: firstly, putting the raw materials of astragalus, suberect spatholobus stem, safflower, zaocys dhumnade, notopterygium root, clematis root, largehead atractylodes rhizome, salvia miltiorrhiza, cassia twig, dragon's blood and honey-fried licorice root on an electronic balance one by one, and weighing 28g of astragalus, 30g of suberect spatholobus stem, 35g of safflower, 22g of zaocys dhumnade, 20g of notopterygium root, 16g of clematis root, 14g of bighead atractylodes rhizome, 16g of salvia miltiorrhiza, 12g of cassia twig, 8g of dragon's blood and 6g of honey-fried licorice root for later use by a worker;
B. material pretreatment: then putting 28g of astragalus membranaceus, 30g of caulis spatholobi, 35g of safflower, 22g of zaocys dhumnade, 20g of notopterygium root, 16g of radix clematidis, 14g of bighead atractylodes rhizome, 16g of salvia miltiorrhiza, 12g of cassia twig, 8g of dragon's blood and 6g of honey-fried licorice root into a 500ml container, then injecting deionized purified water into the 500ml container, soaking, and after the soaking of the raw materials is finished, manually cleaning the raw materials by a worker;
C. boiling and crushing: then, putting the pretreated raw materials into an electric boiler by a worker, adding deionized purified water to perform high-temperature sterilization and boiling treatment at 100 ℃, then, spreading the steamed and boiled raw materials in a room by the worker, physically cooling the raw materials to a room temperature state, putting the compatible raw materials into a grinding grinder to perform grinding and crushing treatment until the ground and crushed raw materials are in small-diameter particles, and waiting for standby;
D. removing slag and filtering: then, putting the small-diameter granular compatible raw materials into a cleaned 500ml container again by a worker, injecting deionized purified water to cover the upper end of the compatible raw materials, fishing out floating dregs by the worker by using a strainer, and putting the compatible granular raw materials with the dregs removed into a vibration filter by the worker to obtain the compatible granular raw materials with the same volume and size;
E. leaching and enzymolysis: then, putting the filtered compatible granular raw materials into a dilute hydrochloric acid solution by a worker to obtain a leaching solution, and adding TapDNA polymerase and horseradish peroxidase into the obtained compatible raw material mixed solution by the worker to perform enzymolysis reaction to obtain a compatible raw material enzymolysis solution;
F. coarse extraction: putting the enzymolysis solution of the compatible raw materials after enzymolysis into a steam distillation extraction instrument for primary extraction and collection of essential oil mixture by workers, putting the extracted essential oil mixture into an oil-water separator for oil-water separation, and obtaining coarse-grade essential oil after oil-water separation;
G. fine extraction: then, the worker puts the prepared coarse-grade essential oil into a carbon dioxide critical extraction instrument for secondary extraction, and collects fine-grade essential oil, the worker puts the collected fine-grade essential oil into a molecular distillation instrument for final molecular distillation refining treatment, and collects the fine-grade essential oil generated in the distillation process of the molecular distillation instrument, so as to obtain refined dehumidifying and nourishing essential oil, then the worker puts the refined dehumidifying and nourishing essential oil into a glass packaging bottle and performs sealing treatment, raw materials for treating rheumatism are selected from compatibility through the matching of the raw materials of astragalus, caulis spatholobi, safflower, zaocys dhumnade, notopterygium root, clematis root, bighead atractylodes rhizome, salvia miltiorrhiza, cassia twig, dragon's blood and honey-fried licorice root, so that the raw materials are reasonably matched, the raw materials are prevented from generating physical impact among the raw materials, the essential oil prepared from the raw materials has strong damp-clearing medicine property, and the essential oil prepared from the raw materials is weighed by the materials, The preparation processes of material pretreatment, boiling and crushing, slag removal and filtration, leaching and enzymolysis, crude extraction and fine extraction are matched, the raw materials are subjected to three key steps of raw material pretreatment, crude extraction and fine extraction, the refined dehumidifying and recuperating essential oil with the dehumidifying function is obtained, after people apply the refined dehumidifying and recuperating essential oil, moisture in the human body or at the joint position can be effectively removed, and the recuperation effect of the refined dehumidifying and recuperating essential oil on the human body is enhanced.
Example 2
The invention provides a technical scheme that: a conditioning essential oil with dehumidifying function comprises the following raw materials;
astragalus root, spatholobus stem, safflower, zaocys dhumnade, notopterygium root, clematis root, bighead atractylodes rhizome, salvia miltiorrhiza, cassia twig, dragon's blood and honey-fried licorice root;
and the mass ranges of the raw material components are as follows:
25-35g of astragalus membranaceus, 20-40g of caulis spatholobi, 25-40g of safflower, 15-25g of zaocys dhumnade, 18-24g of notopterygium root, 12-18g of radix clematidis, 12-17g of bighead atractylodes rhizome, 10-20g of salvia miltiorrhiza, 8-15g of cassia twig, 6-12g of dragon's blood and 4-8g of honey-fried licorice root;
the required equipment is as follows:
500ml container, strainer, glass stirring rod, electric stirrer, electronic balance, electric boiler, crushing grinder, vibration filter, oil-water separator, steam distillation extraction apparatus, carbon dioxide critical extraction apparatus and molecular distillation apparatus;
the preparation method comprises the following steps:
A. weighing materials: firstly, putting the raw materials of astragalus, suberect spatholobus stem, safflower, zaocys dhumnade, notopterygium root, clematis root, largehead atractylodes rhizome, salvia miltiorrhiza, cassia twig, dragon's blood and honey-fried licorice root on an electronic balance one by one, and weighing 28g of astragalus, 30g of suberect spatholobus stem, 35g of safflower, 22g of zaocys dhumnade, 20g of notopterygium root, 16g of clematis root, 14g of bighead atractylodes rhizome, 16g of salvia miltiorrhiza, 12g of cassia twig, 8g of dragon's blood and 6g of honey-fried licorice root for later use by a worker;
B. material pretreatment: then putting 28g of astragalus mongholicus, 30g of caulis spatholobi, 35g of safflower carthamus, 22g of zaocys dhumnade, 20g of notopterygium root, 16g of radix clematidis, 14g of bighead atractylodes rhizome, 16g of salvia miltiorrhiza, 12g of cassia twig, 8g of dragon blood and 6g of honey-fried licorice root into a 500ml container, then injecting deionized purified water into the 500ml container, soaking, wherein the added deionized purified water needs to be higher than the three fingers to five fingers of the astragalus mongholicus, 30g of caulis spatholobi, 35g of safflower carthamus, 22g of zaocys dhumnade, 20g of notopterygium root, 16g of radix clematidis, 14g of bighead atractylodes rhizome, 16g of salvia miltiorrhiza, 12g of cassia twig, 8g of dragon blood and 6g of honey-fried licorice root, stirring the raw materials by using a glass stirring rod, fully sinking and soaking the raw materials with the deionized purified water, the soaking time of the raw materials is between 1h and 3h, after the soaking of the raw materials is finished, fishing out the floating powder floating on the surface layer of the 500ml container by using a spoon, the strainer is wrapped by a fine filter screen, the mesh density of the fine filter screen is between 200 and 400 meshes, and the cleaning standard is as follows: the surfaces of the raw materials are free from attachment of impurity particles, the raw materials are taken out and are not fed into a medicine section, the surfaces of the raw materials are not damaged, and after the raw materials are soaked, workers manually clean the raw materials;
C. boiling and crushing: then the working personnel puts the pretreated raw materials into an electric boiler, then deionized purified water is added for high-temperature sterilization and boiling treatment at 100 ℃, the electric boiler is firstly adjusted to 80 ℃ for boiling the raw materials for 10min, then the electric boiler is adjusted to 100 ℃ for boiling the raw materials for 30min, finally the electric boiler is adjusted to 80 ℃ for boiling the raw materials for 15min, then the working personnel spread the boiled raw materials in a room to ensure that the raw materials are physically cooled to the room temperature, then the working personnel put the compatible raw materials into a grinding grinder for grinding and crushing treatment, the grinding grinder grinds and grinds the compatible raw materials in a grinding and crushing way while drying, the drying temperature range is between 60 ℃ and 80 ℃, the grinding and grinding speed range of the grinding grinder is between 600 r/min and 1000r/min, until all the ground and crushed raw materials are in small-diameter particles, waiting for standby;
D. removing slag and filtering: then, the worker puts the small-diameter granular compatible raw materials into a cleaned 500ml container again, injects deionized purified water and sinks the upper end of the compatible raw materials, then uses a strainer to fish out the floating dregs, then places the compatible granular raw materials with dregs removed into a vibration filter, the vibration frequency of the vibration filter is 50HZ, the vibration filter adopts a three-layer filter screen frame structure to uniformly vibrate and screen the compatible granular raw materials, and the mesh densities of the upper, middle and lower filter screens of the three-layer filter screen frame are respectively between 400-mesh and 600-mesh, between 600-mesh and 800-mesh and 1000-mesh, so as to obtain the compatible granular raw materials with the same volume and size;
E. leaching and enzymolysis: then, the staff puts the filtered compatible granular raw materials into a dilute hydrochloric acid solution for leaching the solution, the mass of the dilute hydrochloric acid solution is 4-8 times of that of the compatible granular raw materials, the pH value of the dilute hydrochloric acid solution is 6, compatible raw material mixed solution is obtained, then, the staff adds TapDNA polymerase and horseradish peroxidase into the obtained compatible raw material mixed solution for enzymolysis reaction treatment, and the mass ratio of the TapDNA polymerase to the horseradish peroxidase to the compatible raw material mixed solution is as follows: 1: 1.5: 80, the purity of the horseradish peroxidase HRP is expressed by RZ (the absorbance ratio of the HRP at 403nm and 275nm respectively), the RZ value of the horseradish peroxidase is more than 3.0, the enzymolysis temperature is between 30 and 40 ℃, the enzymolysis time is between 2 and 4 hours, and a compatible raw material enzymolysis solution is obtained;
F. coarse extraction: the working personnel put the enzymolysis solution of the compatible raw materials after the enzymolysis into a steam distillation extraction instrument for extracting and collecting the primary essential oil mixture, the extraction temperature of the steam distillation extraction instrument is between 120 ℃ and 160 ℃, the extraction is carried out for 3-5h, then the extracted essential oil mixture is put into an oil-water separator for oil-water separation, the oil-water separator firstly carries out standing and precipitation on the enzymolysis solution of the compatible raw materials for 30-45min, after the oil-water separation of the essential oil mixture is finished, water is firstly filtered and discharged, then sewage sodium sulfate is added to carry out drying separation on the oil layer left by the essential oil mixture, and after the oil-water separation, the crude essential oil is obtained;
G. fine extraction: then, the worker puts the prepared crude essential oil into a carbon dioxide critical extraction instrument for secondary extraction, the temperature of extraction of the carbon dioxide critical extraction instrument is 40-50 ℃, the pressure is 12MPa-20MPa, the fine extraction time is 1-2min, the flow rate of carbon dioxide in the carbon dioxide critical extraction instrument is 20kg/h-40kg/h, the fine essential oil is collected, the worker puts the collected fine essential oil into a molecular distillation instrument for final molecular distillation refining treatment, the molecular distillation instrument carries out two-section distillation treatment on the fine essential oil, the first-section evaporation temperature is 120-130 ℃, the second-section evaporation temperature is 50-70 ℃, and the fine essential oil generated in the second-section distillation process of the molecular distillation instrument is collected, so that the fine dehumidifying and nourishing essential oil can be obtained, then the worker puts the fine dehumidifying and nourishing essential oil into a glass packaging bottle, sealing, selecting raw materials for treating rheumatism from compatibility through matching of the raw materials of astragalus, caulis spatholobi, safflower, zaocys dhumnade, notopterygium root, radix clematidis, bighead atractylodes rhizome, salvia miltiorrhiza, cassia twig, dragon's blood and honey-fried licorice root, reasonably matching the raw materials, preventing physical conflict among the raw materials, enabling essential oil prepared from the raw materials to have strong damp-clearing medicine property, then performing material weighing, material pretreatment, boiling and crushing, deslagging and filtering, leaching and enzymolysis, crude extraction and fine extraction on the raw materials through matching of preparation processes of raw material pretreatment, crude extraction and fine extraction to obtain fine dehumidifying and conditioning essential oil with a dehumidifying function, and coating the fine dehumidifying and conditioning essential oil by people, can effectively remove moisture in the body or at the joint position and enhance the recuperation effect of the refined dehumidifying and recuperating essential oil on the human body.
Although embodiments of the present invention have been shown and described, it will be appreciated by those skilled in the art that changes, modifications, substitutions and alterations can be made in these embodiments without departing from the principles and spirit of the invention, the scope of which is defined in the appended claims and their equivalents.

Claims (9)

1. The conditioning essential oil with the dehumidifying function is characterized in that: comprises the following raw materials;
astragalus root, spatholobus stem, safflower, zaocys dhumnade, notopterygium root, clematis root, bighead atractylodes rhizome, salvia miltiorrhiza, cassia twig, dragon's blood and honey-fried licorice root;
and the mass ranges of the raw material components are as follows:
25-35g of astragalus membranaceus, 20-40g of caulis spatholobi, 25-40g of safflower, 15-25g of zaocys dhumnade, 18-24g of notopterygium root, 12-18g of radix clematidis, 12-17g of bighead atractylodes rhizome, 10-20g of salvia miltiorrhiza, 8-15g of cassia twig, 6-12g of dragon's blood and 4-8g of honey-fried licorice root;
the required equipment is as follows:
500ml container, strainer, glass stirring rod, electric stirrer, electronic balance, electric boiler, crushing grinder, vibration filter, oil-water separator, steam distillation extraction apparatus, carbon dioxide critical extraction apparatus and molecular distillation apparatus;
the preparation method comprises the following steps:
A. weighing materials: the method comprises the following steps that firstly, workers respectively place the raw materials of astragalus, suberect spatholobus stem, safflower, zaocys dhumnade, notopterygium root, clematis root, bighead atractylodes rhizome, salvia miltiorrhiza, cassia twig, dragon's blood and honey-fried licorice root on an electronic balance to be weighed one by one, and the raw materials are weighed to obtain 28g of astragalus, 30g of suberect spatholobus stem, 35g of safflower, 22g of zaocys dhumnade, 20g of notopterygium root, 16g of clematis root, 14g of bighead atractylodes rhizome, 16g of salvia miltiorrhiza, 12g of cassia twig, 8g of dragon's blood and 6g of honey-fried licorice root for later use;
B. material pretreatment: then putting 28g of astragalus membranaceus, 30g of caulis spatholobi, 35g of safflower, 22g of zaocys dhumnade, 20g of notopterygium root, 16g of radix clematidis, 14g of bighead atractylodes rhizome, 16g of salvia miltiorrhiza, 12g of cassia twig, 8g of dragon's blood and 6g of honey-fried licorice root into a 500ml container, then injecting deionized purified water into the 500ml container, soaking, and after the soaking of the raw materials is finished, manually cleaning the raw materials by a worker;
C. boiling and crushing: then, putting the pretreated raw materials into an electric boiler by a worker, adding deionized purified water to perform high-temperature sterilization and boiling treatment at 100 ℃, then, spreading the steamed and boiled raw materials in a room by the worker, physically cooling the raw materials to a room temperature state, putting the compatible raw materials into a grinding grinder to perform grinding and crushing treatment until the ground and crushed raw materials are in small-diameter particles, and waiting for standby;
D. removing slag and filtering: then, putting the small-diameter granular compatible raw materials into a cleaned 500ml container again by a worker, injecting deionized purified water to cover the upper end of the compatible raw materials, fishing out floating dregs by the worker by using a strainer, and putting the compatible granular raw materials with the dregs removed into a vibration filter by the worker to obtain the compatible granular raw materials with the same volume and size;
E. leaching and enzymolysis: then, putting the filtered compatible granular raw materials into a dilute hydrochloric acid solution by a worker to obtain a leaching solution, and adding TapDNA polymerase and horseradish peroxidase into the obtained compatible raw material mixed solution by the worker to perform enzymolysis reaction to obtain a compatible raw material enzymolysis solution;
F. coarse extraction: putting the enzymolysis solution of the compatible raw materials after enzymolysis into a steam distillation extraction instrument for primary extraction and collection of essential oil mixture by workers, putting the extracted essential oil mixture into an oil-water separator for oil-water separation, and obtaining coarse-grade essential oil after oil-water separation;
G. fine extraction: and then, putting the prepared coarse essential oil into a carbon dioxide critical extraction instrument for secondary extraction by a worker, collecting fine essential oil, putting the collected fine essential oil into a molecular distillation instrument for final molecular distillation refining treatment by the worker, collecting the fine essential oil generated in the distillation process of the molecular distillation instrument, thus obtaining fine dehumidifying and nourishing essential oil, then putting the fine dehumidifying and nourishing essential oil into a glass packaging bottle by the worker, and sealing.
2. The essential oil for recuperation with dehumidification function according to claim 1, wherein: in the material pretreatment process, the added deionized purified water needs to be higher than three fingers to five fingers of 28g of astragalus, 30g of caulis spatholobi, 35g of safflower, 22g of zaocys dhumnade, 20g of notopterygium root, 16g of radix clematidis, 14g of bighead atractylodes rhizome, 16g of salvia miltiorrhiza, 12g of cassia twig, 8g of dragon's blood and 6g of honey-fried licorice root, and the raw materials are stirred by a glass stirring rod to fully sink and soak the raw materials and the deionized purified water, wherein the soaking time of the raw materials is between 1h and 3 h.
3. The essential oil for recuperation with dehumidification function according to claim 1, wherein: in the material pretreatment process, after soaking of the raw materials is completed, the worker uses the strainer to take out the floating powder floating on the surface layer of the 500ml container, the strainer is wrapped by the fine filter screen, the mesh density of the fine filter screen is between 200 and 400 meshes, and the cleaning standard is as follows: the surface of each raw material has no impurity particles attached, each raw material is taken out and is not taken into a medicine section, and the surface of each raw material is not damaged.
4. The essential oil for recuperation with dehumidification function according to claim 1, wherein: in the boiling and crushing process, the temperature of the electric boiler is firstly adjusted to 80 ℃ to cook each raw material for 10min, then the temperature of the electric boiler is adjusted to 100 ℃ to cook each raw material for 30min, and finally the temperature of the electric boiler is adjusted to 80 ℃ to cook each raw material for 15 min.
5. The essential oil for recuperation with dehumidification function according to claim 1, wherein: in the boiling and crushing process, the crushing and grinding machine grinds and crushes the compatible raw materials in a mode of crushing and grinding while drying, the drying temperature range is between 60 and 80 ℃, and the crushing and grinding rotating speed range of the crushing and grinding machine is between 600 and 1000 r/min.
6. The essential oil for recuperation with dehumidification function according to claim 1, wherein: in the deslagging and filtering process, the vibration frequency of the vibration filter is 50HZ, the vibration filter adopts a three-layer filter screen frame structure to uniformly vibrate and screen compatible granular raw materials, and the mesh densities of the upper filter screen layer, the middle filter screen layer and the lower filter screen layer of the three-layer filter screen frame are respectively between 400-mesh and 600-mesh screens, between 600-mesh and 800-mesh screens and between 800-mesh and 1000-mesh screens.
7. The essential oil for recuperation with dehumidification function according to claim 1, characterized in that: in the leaching enzymolysis process, the mass of the dilute hydrochloric acid solution is 4-8 times of that of the compatible granular raw materials, the pH value of the dilute hydrochloric acid solution is 6, and the mass ratio of the TapDNA polymerase to the horseradish peroxidase to the mixed solution of the compatible raw materials is as follows: 1: 1.5: the purity of the horseradish peroxidase HRP is expressed by RZ (absorbance ratio of the HRP at 403nm and 275nm respectively), the RZ value of the horseradish peroxidase is more than 3.0, the enzymolysis temperature is between 30 and 40 ℃, and the enzymolysis time is between 2 and 4 hours.
8. The essential oil for recuperation with dehumidification function according to claim 1, wherein: in the crude extraction process, the extraction temperature of a steam distillation extraction instrument is between 120-160 ℃, extraction is carried out for 3-5h, an oil-water separator firstly carries out standing precipitation on the compatible raw material enzymolysis solution for 30-45min, after the oil-water separation of the essential oil mixture is finished, water is firstly filtered and discharged, and then, sewage sodium sulfate is added to carry out drying separation on the oil layer left by the essential oil mixture.
9. The essential oil for recuperation with dehumidification function according to claim 1, wherein: in the fine extraction process, the extraction temperature of a carbon dioxide critical extraction instrument is between 40 ℃ and 50 ℃, the pressure is between 12MPa and 20MPa, the fine extraction time is 1 to 2min, the flow rate of carbon dioxide in the carbon dioxide critical extraction instrument is between 20kg/h and 40kg/h, and a molecular distillation instrument carries out two-section distillation treatment on fine essential oil, wherein the first-section evaporation temperature is between 120 ℃ and 130 ℃, and the second-section evaporation temperature is between 50 ℃ and 70 ℃.
CN202210310460.9A 2022-03-28 2022-03-28 Essential oil with dehumidifying function Pending CN114558073A (en)

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Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1422644A (en) * 2001-12-06 2003-06-11 高大海 Skin-beauty capsule
CN105125658A (en) * 2015-07-22 2015-12-09 江西中医药大学附属医院 Granules with effects of eliminating obstruction to activate collaterals and preparation method thereof
CN109420037A (en) * 2017-08-22 2019-03-05 张忠远 A kind of Chinese medicine composition for treating cervical spondylosis
CN109820997A (en) * 2019-03-22 2019-05-31 四川郡益康健康管理有限公司 One kind pulling out cold oil
CN111588832A (en) * 2020-07-09 2020-08-28 文秋方 Herbal purification liquid

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1422644A (en) * 2001-12-06 2003-06-11 高大海 Skin-beauty capsule
CN105125658A (en) * 2015-07-22 2015-12-09 江西中医药大学附属医院 Granules with effects of eliminating obstruction to activate collaterals and preparation method thereof
CN109420037A (en) * 2017-08-22 2019-03-05 张忠远 A kind of Chinese medicine composition for treating cervical spondylosis
CN109820997A (en) * 2019-03-22 2019-05-31 四川郡益康健康管理有限公司 One kind pulling out cold oil
CN111588832A (en) * 2020-07-09 2020-08-28 文秋方 Herbal purification liquid

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Application publication date: 20220531