CN114480036A - Preparation method of quartz sand abrasive cleaner - Google Patents
Preparation method of quartz sand abrasive cleaner Download PDFInfo
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- CN114480036A CN114480036A CN202210112054.1A CN202210112054A CN114480036A CN 114480036 A CN114480036 A CN 114480036A CN 202210112054 A CN202210112054 A CN 202210112054A CN 114480036 A CN114480036 A CN 114480036A
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- sodium
- na2sio3
- quartz sand
- sodium metasilicate
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D7/00—Compositions of detergents based essentially on non-surface-active compounds
- C11D7/02—Inorganic compounds
- C11D7/04—Water-soluble compounds
- C11D7/10—Salts
- C11D7/14—Silicates
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D7/00—Compositions of detergents based essentially on non-surface-active compounds
- C11D7/22—Organic compounds
- C11D7/26—Organic compounds containing oxygen
- C11D7/265—Carboxylic acids or salts thereof
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- Chemical Kinetics & Catalysis (AREA)
- Oil, Petroleum & Natural Gas (AREA)
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- Health & Medical Sciences (AREA)
- Emergency Medicine (AREA)
- Inorganic Chemistry (AREA)
- Detergent Compositions (AREA)
Abstract
The invention relates to a preparation method of a quartz sand abrasive cleaner, which comprises the following materials: sodium metasilicate (Na2SiO 3); sodium gluconate (C6H11NaO 7); sodium citrate (C6H5Na3O 7). Comprises the following steps; s1: firstly, taking a sodium metasilicate (Na2SiO3) sample out of a container filled with the sodium metasilicate (Na2SiO3), detecting the chemical property of the sodium metasilicate (Na2SiO3) by a chemical experiment detecting instrument, and accurately weighing and taking out a quantitative sodium metasilicate (Na2SiO3) by using a special chemical weighing device after the sodium metasilicate (Na2SiO3) sample is detected to be qualified. According to the preparation method of the quartz sand abrasive cleaner, sodium metasilicate has stronger functions of wetting, emulsifying and saponifying grease, and has excellent performance in the aspects of removing, dispersing and suspending dirt, sodium gluconate can perform corrosion inhibition on impurities such as cementing materials, metal impregnated bodies, humus, mica and the like on the surface of quartz sand and ferric oxide, and sodium citrate can perform complexation on iron, calcium, magnesium and ferric oxide on the surface of quartz sand.
Description
Technical Field
The invention relates to the technical field of abrasive cleaner preparation, in particular to a preparation method of a quartz sand abrasive cleaner.
Background
The quartz sand is quartz particles formed by crushing quartz stones. Quartz is a non-metallic mineral, a silicate mineral that is hard, wear resistant, and chemically stable. The quartz sand is milky white or colorless and semitransparent, and has a Mohs hardness of 7. Quartz sand is an important industrial mineral raw material and a non-chemical hazardous article, and is widely used in the industries of glass, casting, ceramics and fireproof materials, ferrosilicon smelting, metallurgical flux, metallurgy, building, chemical engineering, plastics, rubber, grinding materials, filter materials and the like. The surface of the quartz sand contains a certain amount of clastic impurity minerals, and the existence of the minerals can influence the utilization of the quartz sand, so that purification and impurity removal are needed when the quartz sand is utilized, the existing scrubbing method for purifying the quartz sand basically adopts pure deionized water scrubbing and single sodium metasilicate (Na2SiO3) scrubbing, and the existing preparation method of the quartz sand scrubbing agent has certain defects in use, such as,
1. the removal of ferric oxide is not ideal after the sodium metasilicate is singly added and scrubbed, and because the sodium metasilicate only has wetting, emulsifying, dispersing and suspending effects and has no corrosion inhibition and complexing effects on the cement, the metal dye, humus, mica, ferric oxide and other impurities on the surface of the quartz sand, the purification and impurity removal effects of the quartz sand are not ideal;
there is a need for improvement in view of the above problems.
Disclosure of Invention
The invention aims to provide a preparation method of a quartz sand scrubbing agent, which aims to solve the problem that the removal of ferric oxide is not ideal after the scrubbing by singly adding sodium metasilicate, and the purification and impurity removal effects of quartz sand are not ideal because sodium metasilicate only has wetting, emulsifying, dispersing and suspending effects and has no corrosion inhibition and complexing effects on impurities such as cement, metal impregnated body, humus, mica, ferric oxide and the like on the surface of the quartz sand.
In order to achieve the purpose, the invention provides the following technical scheme: a preparation method of a quartz sand abrasive cleaner comprises the following materials:
sodium metasilicate (Na2SiO 3);
sodium gluconate (C6H11NaO 7);
sodium citrate (C6H5Na3O 7).
Preferably, the method comprises the following steps;
s1: firstly, taking a sodium metasilicate (Na2SiO3) sample out of a container filled with the sodium metasilicate (Na2SiO3), detecting the chemical property of the sodium metasilicate (Na2SiO3) by using a chemical experiment detection instrument, and accurately weighing and taking out a quantitative sodium metasilicate (Na2SiO3) by using a special chemical weighing device after the sodium metasilicate (Na2SiO3) sample is detected to be qualified;
s2: sodium metasilicate (Na2SiO3) weighed quantitatively was put into a mixing cylinder of a chemical substance mixing exclusive device.
Preferably, the sodium metasilicate (Na2SiO3) is a white granular chemical substance, and the weighed amount of the sodium metasilicate (Na2SiO3) is 0.25-0.35 percent of the mass of the sand of the quartz sand to be treated.
Preferably, S3: taking a sodium gluconate (C6H11NaO7) sample out of a container filled with the sodium gluconate (C6H11NaO7), detecting the chemical property of the sodium gluconate (C6H11NaO7) sample by using a chemical experimental instrument, quantitatively weighing the sodium gluconate (C6H11NaO7) after the detection result of the sodium gluconate (C6H11NaO7) sample is normal, and putting the sodium gluconate (C6H11NaO7) into a charging barrel of a mixing device;
s4: a sample of sodium citrate (C6H5Na3O7) was taken out from the container containing the sodium citrate (C6H5Na3O7), a chemical property test was performed on the sample of sodium citrate (C6H5Na3O7) using a chemical laboratory instrument, and after the test result was normal, the sodium citrate (C6H5Na3O7) was quantitatively weighed, and sodium citrate (C6H5Na3O7) was put into a cylinder of a mixing device.
Preferably, the sodium gluconate (C6H11NaO7) and the sodium citrate (C6H5Na3O7) are both white granular chemical substances, and the weighed amount of the sodium gluconate (C6H11NaO7) is 0.25 to 0.35 percent of the mass of the quartz sand to be treated, and the weighed amount of the sodium citrate (C6H5Na3O7) is 0.08 to 0.12 percent of the mass of the quartz sand to be treated.
Preferably, the method comprises the following steps;
s5: after the sodium metasilicate (Na2SiO3), the sodium gluconate (C6H11NaO7) and the sodium citrate (C6H5Na3O7) are put into the charging barrel, the mixing device can be operated until the three chemical substances are uniformly mixed;
s6: and taking out the three uniformly mixed chemical substances, filling the three chemical substances into a container, and preparing the quartz sand abrasive cleaner.
Compared with the prior art, the invention has the beneficial effects that: the sodium metasilicate has stronger functions of wetting, emulsifying and saponifying oil, has excellent performance in the aspects of removing, dispersing and suspending dirt, and can prevent the dirt from being redeposited, the sodium gluconate has excellent corrosion and scale inhibition effects, and has excellent coordination capacity on iron, calcium, copper and other ions in an aqueous solution, so that the corrosion inhibition can be performed on the cement, metal impregnant, humus, mica and other impurities on the surface of quartz sand and ferric oxide, the sodium citrate is used as an iron-calcium-magnesium ion complexing agent and can be used for complexing the iron-calcium-magnesium impurities and the ferric oxide on the surface of the quartz sand, the scrubbing agent is mainly weakly alkaline, and can neutralize humic acid rich in humus in sea sand, so that the scrubbing agent has excellent effects on purifying and removing the dirt of the quartz sand.
Drawings
FIG. 1 is a schematic view of the flow structure of the present invention;
fig. 2 is a schematic structural diagram of the principle of the present invention.
Detailed Description
The technical solutions in the embodiments of the present invention will be clearly and completely described below with reference to the drawings in the embodiments of the present invention, and it is obvious that the described embodiments are only a part of the embodiments of the present invention, and not all of the embodiments. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention.
Referring to fig. 1-2, the present invention provides a technical solution: a preparation method of a quartz sand abrasive cleaner comprises the following materials:
sodium metasilicate (Na2SiO 3);
sodium gluconate (C6H11NaO 7);
sodium citrate (C6H5Na3O 7).
The method comprises the following steps:
s1: firstly, taking a sodium metasilicate (Na2SiO3) sample from a container filled with sodium metasilicate (Na2SiO3), wherein the sodium metasilicate (Na2SiO3) is a white granular chemical substance, detecting the chemical property of the sodium metasilicate (Na2SiO3) by using a chemical experiment detecting instrument, accurately weighing and taking out a quantitative sodium metasilicate (Na2SiO3) by using a special chemical weighing device after the sodium metasilicate (Na2SiO3) sample is detected to be qualified, weighing the sodium metasilicate (Na2SiO3) in an amount of 0.25-0.35% of the mass of the quartz sand to be treated, and S2: sodium metasilicate (Na2SiO3) weighed quantitatively was put into a mixing cylinder of a chemical substance mixing exclusive device.
The method comprises the following steps:
s3: taking a sodium gluconate (C6H11NaO7) sample from a container filled with sodium gluconate (C6H11NaO7), wherein the sodium gluconate (C6H11NaO7) is a white granular chemical substance, performing chemical property detection on the sodium gluconate (C6H11NaO7) sample by using a chemical experimental instrument, quantitatively weighing the sodium gluconate (C6H11NaO7) after the detection result of the sodium gluconate (C6H11NaO7) sample is normal, weighing the sodium gluconate (C6H11NaO7) in an amount of 0.25-0.35% of the mass of the quartz sand to be treated, putting the sodium gluconate (C6H11NaO7) into a charging barrel of a mixing device, and S4: taking a sodium citrate (C6H5Na3O7) sample from a container filled with sodium citrate (C6H5Na3O7), wherein the sodium citrate (C6H5Na3O7) is a white granular chemical substance, carrying out chemical property detection on the sodium citrate (C6H5Na3O7) sample by using a chemical laboratory instrument, quantitatively weighing the sodium citrate (C6H5Na3O7) after the detection result is normal, weighing the sodium citrate (C6H5Na3O7) in an amount of 0.08-0.12 percent of the mass of the quartz sand to be treated, and putting the sodium citrate (C6H5Na3O7) into a barrel of a mixing device.
Comprises the following steps;
s5: after sodium metasilicate (Na2SiO3), sodium gluconate (C6H11NaO7) and sodium citrate (C6H5Na3O7) are put into the charging barrel, the mixing device may be operated, the mixing device is operated until the three chemical substances are uniformly mixed, S6: and taking out the three uniformly mixed chemical substances, filling the three chemical substances into a container, and preparing the quartz sand abrasive cleaner.
The working principle is as follows: the preparation method of the quartz sand scouring agent is needed to be simply known, the quartz sand scouring agent is adjusted to the concentration of 1:1 of volume solid-liquid ratio, the quartz sand pulp is added into a horizontal or vertical scouring machine, the scouring agent is prepared according to the quality of quartz sand, the prepared scouring agent is put into the quartz sand pulp, the pulp is scrubbed for 30-60 minutes to realize the suspension complexing removal of quartz sand inclusion impurities, the scrubbed pulp rapidly enters a solid-liquid separation device, the scouring agent separated by the solid-liquid separation device is precipitated in a sedimentation tank and can be repeatedly added into the scouring machine for use, so that the sodium metasilicate has strong functions of wetting, emulsifying and saponifying grease, has excellent performances in the aspects of removing, dispersing and suspending dirt, can prevent the dirt from redepositing, and has excellent scale inhibition effect, the scrubbing agent has excellent coordination capacity to iron, calcium, copper and other ions in an aqueous solution, so that the corrosion inhibition can be performed on the cementing material, metal dye-dipping body, humus, mica and other impurities on the surface of quartz sand and ferric oxide, sodium citrate is used as an iron-calcium-magnesium ion complexing agent and can complex the iron-calcium-magnesium impurities and the ferric oxide on the surface of the quartz sand, and the scrubbing agent mainly has weak alkalinity and can neutralize humic acid rich in humus in sea sand, so that the scrubbing agent has excellent effect on purification and impurity removal of the quartz sand, which is the characteristic of the preparation method of the scrubbing agent for the quartz sand, and the content which is not described in detail in the description belongs to the prior art known by professional technicians in the field.
Although the present invention has been described in detail with reference to the foregoing embodiments, it will be apparent to those skilled in the art that various changes in the embodiments and/or modifications of the invention can be made, and equivalents and modifications of some features of the invention can be made without departing from the spirit and scope of the invention.
Claims (6)
1. The preparation method of the quartz sand abrasive cleaner is characterized by comprising the following materials:
sodium metasilicate (Na2SiO 3);
sodium gluconate (C6H11NaO 7);
sodium citrate (C6H5Na3O 7).
2. The method for preparing a silica sand abrasive cleaner according to claim 1, wherein: comprises the following steps;
s1: firstly, taking a sodium metasilicate (Na2SiO3) sample out of a container filled with the sodium metasilicate (Na2SiO3), detecting the chemical property of the sodium metasilicate (Na2SiO3) by using a chemical experiment detection instrument, and accurately weighing and taking out a quantitative sodium metasilicate (Na2SiO3) by using a special chemical weighing device after the sodium metasilicate (Na2SiO3) sample is detected to be qualified;
s2: sodium metasilicate (Na2SiO3) weighed quantitatively was put into a mixing cylinder of a chemical substance mixing exclusive device.
3. The method for preparing a silica sand abrasive cleaner according to claim 2, wherein: the sodium metasilicate (Na2SiO3) is a white granular chemical substance, and the weighed amount of the sodium metasilicate (Na2SiO3) is 0.25-0.35 percent of the mass of the quartz sand to be treated.
4. The method for preparing a silica sand abrasive cleaning agent according to claim 1, comprising the steps of;
s3: taking a sodium gluconate (C6H11NaO7) sample out of a container filled with the sodium gluconate (C6H11NaO7), detecting the chemical property of the sodium gluconate (C6H11NaO7) sample by using a chemical experimental instrument, quantitatively weighing the sodium gluconate (C6H11NaO7) after the detection result of the sodium gluconate (C6H11NaO7) sample is normal, and putting the sodium gluconate (C6H11NaO7) into a charging barrel of a mixing device;
s4: taking a sodium citrate (C6H5Na3O7) sample out of a container filled with the sodium citrate (C6H5Na3O7), carrying out chemical property detection on the sodium citrate (C6H5Na3O7) sample by using a chemical laboratory instrument, quantitatively weighing the sodium citrate (C6H5Na3O7) after the detection result is normal, and putting the sodium citrate (C6H5Na3O7) into a cylinder of a mixing device.
5. The method for preparing a silica sand abrasive cleaner according to claim 4, wherein: the sodium gluconate (C6H11NaO7) and the sodium citrate (C6H5Na3O7) are both white granular chemical substances, the weighed amount of the sodium gluconate (C6H11NaO7) is 0.25-0.35% of the mass of the quartz sand to be treated, and the weighed amount of the sodium citrate (C6H5Na3O7) is 0.08-0.12% of the mass of the quartz sand to be treated.
6. The method for preparing a silica sand abrasive cleaning agent according to claim 1, comprising the steps of;
s5: after the sodium metasilicate (Na2SiO3), the sodium gluconate (C6H11NaO7) and the sodium citrate (C6H5Na3O7) are put into the charging barrel, the mixing device can be operated until the three chemical substances are uniformly mixed;
s6: and taking out the three uniformly mixed chemical substances, filling the three chemical substances into a container, and preparing the quartz sand abrasive cleaner.
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Citations (7)
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|---|---|---|---|---|
| GB0204039D0 (en) * | 2002-02-21 | 2002-04-03 | Reckitt Benckiser Inc | Improvements in or relating to organic compositions |
| CN107034038A (en) * | 2017-04-28 | 2017-08-11 | 中昊(大连)化工研究设计院有限公司 | A cleaning agent for cleaning quartz ore |
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| CN109181917A (en) * | 2018-10-17 | 2019-01-11 | 中国地质科学院郑州矿产综合利用研究所 | Quartz sand surface impurity removal cleaning agent and preparation and application thereof |
| CN109338384A (en) * | 2018-12-10 | 2019-02-15 | 徐州特普勒金属科技有限公司 | Water-based metal cleaning agent and preparation method thereof |
| CN113772680A (en) * | 2021-09-13 | 2021-12-10 | 青州统一重工机械有限公司 | Quartz sand acid-free medicament purification process |
| CN114455589A (en) * | 2022-01-28 | 2022-05-10 | 青州统一重工机械有限公司 | Production process for producing high-purity quartz sand by using sea sand |
-
2022
- 2022-01-28 CN CN202210112054.1A patent/CN114480036A/en active Pending
Patent Citations (7)
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| GB0204039D0 (en) * | 2002-02-21 | 2002-04-03 | Reckitt Benckiser Inc | Improvements in or relating to organic compositions |
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| CN109338384A (en) * | 2018-12-10 | 2019-02-15 | 徐州特普勒金属科技有限公司 | Water-based metal cleaning agent and preparation method thereof |
| CN113772680A (en) * | 2021-09-13 | 2021-12-10 | 青州统一重工机械有限公司 | Quartz sand acid-free medicament purification process |
| CN114455589A (en) * | 2022-01-28 | 2022-05-10 | 青州统一重工机械有限公司 | Production process for producing high-purity quartz sand by using sea sand |
Non-Patent Citations (1)
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