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CN113940443A - Production method of electronic atomized liquid - Google Patents

Production method of electronic atomized liquid Download PDF

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Publication number
CN113940443A
CN113940443A CN202111233497.8A CN202111233497A CN113940443A CN 113940443 A CN113940443 A CN 113940443A CN 202111233497 A CN202111233497 A CN 202111233497A CN 113940443 A CN113940443 A CN 113940443A
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China
Prior art keywords
atomized liquid
fermentation
parts
fresh
component
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CN202111233497.8A
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Chinese (zh)
Inventor
邹阳
邹军
刘梅森
唐忠月
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Shenzhen Zinwi Biotech Co Ltd
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Shenzhen Zinwi Biotech Co Ltd
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Priority to CN202111233497.8A priority Critical patent/CN113940443A/en
Publication of CN113940443A publication Critical patent/CN113940443A/en
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    • A—HUMAN NECESSITIES
    • A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
    • A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
    • A24B15/10—Chemical features of tobacco products or tobacco substitutes
    • A24B15/16—Chemical features of tobacco products or tobacco substitutes of tobacco substitutes
    • A24B15/167—Chemical features of tobacco products or tobacco substitutes of tobacco substitutes in liquid or vaporisable form, e.g. liquid compositions for electronic cigarettes
    • A—HUMAN NECESSITIES
    • A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
    • A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
    • A24B15/18—Treatment of tobacco products or tobacco substitutes
    • A—HUMAN NECESSITIES
    • A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
    • A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
    • A24B15/18—Treatment of tobacco products or tobacco substitutes
    • A24B15/24—Treatment of tobacco products or tobacco substitutes by extraction; Tobacco extracts

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  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Medicines Containing Plant Substances (AREA)

Abstract

The invention discloses a method for producing electronic atomized liquid, in particular to the technical field of electronic atomized liquid, the invention adds Chinese medicinal fermentation liquor prepared by fermenting Chinese herbal medicines, fruits, vegetables, marine products and medicinal and edible medicinal materials by strains in the preparation process of the electronic atomized liquid, can relieve the problems of dry throat, throat itching, irritable cough, chronic pharyngitis, dry mouth and nose, thirst and dry cough, little phlegm or difficult cough caused by sticky sputum in smoking to a certain extent, has the curative effects of clearing away heat and toxic materials and resisting bacteria and diminishing inflammation, and the addition of astragalus root, tuckahoe, coix seed, schisandra fruit, fresh yam, dried kelp, agaric, tremella, fresh oyster, pearl, grape, pomegranate, tomato, celery, fresh edible cactus, mannitol, sodium benzoate, aspartame, sodium citrate, honey, xanthan gum and sodium carboxymethylcellulose enables the finally obtained finished product of the electronic atomized liquid to have certain addiction effect, thereby reducing the dependence of smokers on cigarettes.

Description

Production method of electronic atomized liquid
Technical Field
The invention relates to the technical field of electronic atomized liquid, in particular to a production method of electronic atomized liquid.
Background
It is known that smoking can not only induce various respiratory diseases, harm health and pollute environment, but also mixed smoke released by the burning end of tobacco products and formed by tobacco smoke exhaled by smokers is the most widely and seriously harmful indoor air pollution, is a serious death cause in the world, and according to incomplete statistics, the number of people dying the world due to diseases caused by smoking exceeds one million, so that smoking cessation is urgent, but many smokers rely on cigarettes to a certain extent due to the action of nicotine, the nicotine destroys the normal blood sugar and acid-base balance of human bodies, stimulates excitement nerves and generates transient excitation, and once smoking is stopped, the nicotine in the bodies cannot be supplemented, anxiety, dysphoria, unconcentration, insomnia and depression are generated, smoking is strongly needed to supplement the nicotine in the bodies, and is the root cause of so-called smoking addiction, in addition, people who smoke for a long time can form a smoking habit and are difficult to change in a short time.
At present, a lot of cigarette substitutes appear in the market, wherein electronic cigarettes are the most common, the electronic liquid electronic atomization liquid for electronic cigarettes is used for atomization and smoke generation, although the harm of second-hand cigarettes to nearby people can be reduced, the liquid electronic atomization liquid for electronic cigarettes usually contains three types of non-nitrogen-containing compounds, nitrogen-containing compounds and inorganic salts, the main components of the liquid electronic atomization liquid comprise monosaccharide, disaccharide, starch, pinosylvin, pectin, resin, protein, amino acid, nicotine, aromatic oil, polyphenols and the like, wherein 40 types of substances such as tar, phenols, alcohols, acids, aldehydes and the like are not good for human health, and are easy to cause the problems of dry throat, itching throat, irritable cough, chronic pharyngitis, dry mouth and nose, thirst and dry cough, little phlegm or difficult cough due to sticky sputum and the like, and the frequent use of electronic cigarettes by some smokers can cause difficult harm to make up to smokers, therefore, it is important to research a new method for producing an electronically atomized liquid to solve the above problems.
Disclosure of Invention
In order to overcome the defects in the prior art, the invention provides an electronic atomized liquid production method, and the technical problems to be solved by the invention are as follows: although the electronic cigarette can reduce the harm of second-hand smoke to nearby people, the cigarette liquid usually contains some non-nitrogen-containing compounds, nitrogen-containing compounds and inorganic salts, the main components of the cigarette liquid comprise monosaccharide, disaccharide, starch, pirn vitamins, pectin, resin, protein, amino acid, nicotine, aromatic oil, polyphenol and the like, wherein 40 substances such as tar, phenols, alcohols, acids, aldehydes and the like are not beneficial to the health of people, and the problems of dry throat, throat itching, irritable cough, chronic pharyngitis, dry mouth and nose, thirst and dry cough, little phlegm or difficult phlegm adhesion and the like are easily caused, and the dependence of some smokers on the cigarette is serious, and the frequent use of the electronic cigarette can also cause the problem of difficult-to-compensate harm to the smokers.
In order to achieve the purpose, the invention provides the following technical scheme: an electronic atomized liquid production method, which comprises the following steps:
s1, preparing the following materials in parts by mass: 3-5 parts of tobacco leaf extract, 25-40 parts of propylene glycol, 25-40 parts of glycerol, 6-8 parts of fruit juice, 0.2-0.5 part of stabilizer, 0.1-0.3 part of tobacco flavoring agent, 5-8 parts of traditional Chinese medicine mixture, 15-24 parts of pure water, 3-5 parts of plant extract and 0.5-0.8 part of tea tree essential oil.
S2, mixing a traditional Chinese medicine mixture with a predetermined weight with pure water with a predetermined weight, carrying out ultrasonic treatment for 30 minutes after mixing, heating until boiling after treatment, standing and cooling the boiled mixed solution for 20-23 hours at room temperature, pouring into an axe type fermentation tank, adding 500 g of brown sugar and bean powder mixed according to the mass ratio of 3:2 to meet the carbon source and nitrogen source required by early growth of a fermentation strain, then inoculating the strain for fermentation treatment to obtain fermentation liquor, filtering and centrifuging the obtained fermentation liquor to obtain filtrate, adding 1% of powdered activated carbon into the filtrate at the temperature of 40 ℃, stirring for 40 minutes, carrying out vacuum pumping to remove the powdered activated carbon and residual impurities to obtain decolorized solution, and concentrating the decolorized solution at 80-90.6KPa to obtain the traditional Chinese medicine fermentation liquor.
S3, heating the traditional Chinese medicine fermentation liquor obtained in the above steps, pouring tobacco leaf extract with a set weight when the temperature rises to 65-75 ℃, uniformly mixing, pouring the mixture of propylene glycol and glycerol with a set weight, uniformly stirring, pouring plant extract with a set weight and tea tree essential oil with a set weight after 10min, uniformly mixing, pouring fruit juice and tobacco flavoring agent which are mixed in advance, finally adding stabilizing agent with a set weight, and uniformly stirring to obtain the finished product of the electronic atomization liquid.
As a further scheme of the invention: the preparation method of the traditional Chinese medicine mixture comprises the following steps: decocting equivalent parts by mass of sauropus spatulifolius, tea leaves and common andrographis herb in water for three times, filtering, merging filtrate and concentrating, then extracting with ethanol twice, filtering to obtain ethanol extractive solution, mixing, recovering ethanol under reduced pressure, concentrating to obtain component A, decocting radix astragali, Poria, Coicis semen, fructus Schisandrae chinensis, fresh rhizoma Dioscoreae, dried herba Zosterae Marinae, Auricularia and Tremella with water to obtain concentrated decoction as component B, hydrolyzing fresh oysters and pearls with sulfuric acid, adding calcium hydroxide for neutralization, filtering, washing medicine residues with purified water, merging, concentrating into a component C, respectively juicing grapes, pomegranates, tomatoes, celery, fresh edible cactus, mannitol, sodium benzoate, aspartame, sodium citrate, honey, xanthan gum and sodium carboxymethylcellulose, uniformly mixing to obtain a component D, and uniformly mixing the component A, the component B, the component C and the component D according to the mass ratio of 1:1:1:1 to form a traditional Chinese medicine mixture.
As a further scheme of the invention: the weight ratio of the astragalus membranaceus, the poria cocos, the coix seed, the schisandra chinensis, the fresh Chinese yam, the dried kelp to the agaric, the tremella fuciformis, the fresh oyster to the pearl to the grape, the pomegranate to the tomato to the celery to the fresh edible cactus to the mannitol to the sodium benzoate to the aspartame to the sodium citrate to the honey to the xanthan gum to the sodium carboxymethylcellulose is 6:6:6:8:3: 4:2:16:0.5:30:6:30: 15:5:2:0.3:1:4:2: 1.
As a further scheme of the invention: the fermentation treatment in the S2 comprises the following specific steps: anaerobic fermentation is carried out for 15-20 days at the temperature of 26-32 ℃, the growth condition of colonies is checked every 3 days, and the fermentation is stopped when the average bacteria content in each milliliter of fermentation liquor reaches 2.5 multiplied by 108 CFU/mL.
As a further scheme of the invention: the ultrasonic treatment frequency in the S2 is 40KHz, the fermentation strain is EM composite strain, and the EM composite strain comprises bacillus, Aerobacter, lactobacillus, photosynthetic bacteria, Aspergillus niger and yeast.
As a further scheme of the invention: the glycerol is vegetable glycerol, the stabilizer is formed by uniformly mixing dextrin, pectin and xanthan gum according to the mass ratio of 1:1:1, and the tobacco flavoring agent is ethyl acetate or ethyl butyrate.
As a further scheme of the invention: the preparation method of the plant extract comprises the following steps: mixing flos Lonicerae and herba Houttuyniae at a weight ratio of 1:6, cleaning, crushing, and steam distilling to obtain the plant extractive solution.
As a further scheme of the invention: the fruit juice is one or more of vanilla, apple, cherry, chocolate, coffee, mango, strawberry, watermelon, peach, grape, pineapple, bubble gum, Hami melon, lemon, banana, spearmint, kiwi fruit, coconut and blueberry.
The invention has the beneficial effects that: the Chinese medicinal fermentation liquor prepared by fermenting Chinese herbal medicines, fruits, vegetables, marine products and medicinal and edible medicinal materials by strains is added in the preparation process of the electronic atomized liquid, wherein the honeysuckle and the houttuynia cordata can relieve the problems of dry throat, throat itch, irritable cough, chronic pharyngitis, dry mouth and nose, dry cough with thirst, little phlegm or difficult cough with sticky sputum and the like caused by smoking to a certain extent, has the curative effects of clearing away heat and toxic materials, resisting bacteria and diminishing inflammation, has no toxic or side effect and no pollution to the environment, and the finished product of the electronic atomized liquid finally obtained has a certain addiction stopping effect due to the addition of the astragalus mongholicus, the poria cocos, the coix seeds, the schisandra chinensis, the fresh Chinese yam, the dried kelp, the agaric, the tremella, the fresh oyster, the pearl, the grape, the pomegranate, the tomatoes, the celery, the fresh cactus, the mannitol, the sodium benzoate, the aspartame, the sodium citrate, the honey, the xanthan gum and the sodium carboxymethylcellulose, thereby reducing the dependence of smokers on cigarettes.
Detailed Description
The technical solutions in the embodiments of the present invention will be clearly and completely described below, and it is obvious that the described embodiments are only a part of the embodiments of the present invention, and not all embodiments. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention.
Example 1:
a production method of electronic atomized liquid comprises the following steps:
s1, preparing the following materials in parts by mass: 3-5 parts of tobacco leaf extract, 25-40 parts of propylene glycol, 25-40 parts of glycerol, 6-8 parts of fruit juice, 0.2-0.5 part of stabilizer, 0.1-0.3 part of tobacco flavoring agent, 5-8 parts of traditional Chinese medicine mixture, 15-24 parts of pure water, 3-5 parts of plant extract and 0.5-0.8 part of tea tree essential oil.
S2, mixing a traditional Chinese medicine mixture with a predetermined weight with pure water with a predetermined weight, carrying out ultrasonic treatment for 30 minutes after mixing, heating until boiling after treatment, standing and cooling the boiled mixed solution for 20-23 hours at room temperature, pouring into an axe type fermentation tank, adding 500 g of brown sugar and bean powder mixed according to the mass ratio of 3:2 to meet the carbon source and nitrogen source required by early growth of a fermentation strain, then inoculating the strain for fermentation treatment to obtain fermentation liquor, filtering and centrifuging the obtained fermentation liquor to obtain filtrate, adding 1% of powdered activated carbon into the filtrate at the temperature of 40 ℃, stirring for 40 minutes, carrying out vacuum pumping to remove the powdered activated carbon and residual impurities to obtain decolorized solution, and concentrating the decolorized solution at 80-90.6KPa to obtain the traditional Chinese medicine fermentation liquor.
S3, heating the traditional Chinese medicine fermentation liquor obtained in the above steps, pouring tobacco leaf extract with a set weight when the temperature rises to 65-75 ℃, uniformly mixing, pouring the mixture of propylene glycol and glycerol with a set weight, uniformly stirring, pouring plant extract with a set weight and tea tree essential oil with a set weight after 10min, uniformly mixing, pouring fruit juice and tobacco flavoring agent which are mixed in advance, finally adding stabilizing agent with a set weight, and uniformly stirring to obtain the finished product of the electronic atomization liquid.
The preparation method of the traditional Chinese medicine mixture comprises the following steps: decocting equivalent parts by mass of sauropus spatulifolius, tea leaves and common andrographis herb in water for three times, filtering, merging filtrate, concentrating, adding ethanol, extracting for two times, filtering to obtain ethanol extract, merging, recovering ethanol under reduced pressure, and concentrating to obtain a traditional Chinese medicine mixture.
The fermentation treatment in S2 comprises the following specific steps: anaerobic fermentation is carried out for 15-20 days at the temperature of 26-32 ℃, the growth condition of colonies is checked every 3 days, and the fermentation is stopped when the average bacteria content in each milliliter of fermentation liquor reaches 2.5 multiplied by 108 CFU/mL.
The ultrasonic treatment frequency in S2 is 40KHz, the fermentation strain is EM composite strain, and the EM composite strain comprises bacillus, Aerobacter, lactobacillus, photosynthetic bacteria, Aspergillus niger and yeast.
The glycerol is vegetable glycerol, the stabilizer is formed by uniformly mixing dextrin, pectin and xanthan gum according to the mass ratio of 1:1:1, and the tobacco flavoring agent is ethyl acetate or ethyl butyrate.
The preparation method of the plant extract comprises the following steps: mixing flos Lonicerae and herba Houttuyniae at a weight ratio of 1:6, cleaning, crushing, and steam distilling to obtain plant extractive solution.
The fruit juice is one or more of vanilla, apple, cherry, chocolate, coffee, mango, strawberry, watermelon, peach, grape, pineapple, bubble gum, Hami melon, lemon, banana, spearmint, kiwi fruit, coconut and blueberry.
Example 2:
a production method of electronic atomized liquid comprises the following steps:
s1, preparing the following materials in parts by mass: 3-5 parts of tobacco leaf extract, 25-40 parts of propylene glycol, 25-40 parts of glycerol, 6-8 parts of fruit juice, 0.2-0.5 part of stabilizer, 0.1-0.3 part of tobacco flavoring agent, 5-8 parts of traditional Chinese medicine mixture, 15-24 parts of pure water and 0.5-0.8 part of tea tree essential oil.
S2, mixing a traditional Chinese medicine mixture with a predetermined weight with pure water with a predetermined weight, carrying out ultrasonic treatment for 30 minutes after mixing, heating until boiling after treatment, standing and cooling the boiled mixed solution for 20-23 hours at room temperature, pouring into an axe type fermentation tank, adding 500 g of brown sugar and bean powder mixed according to the mass ratio of 3:2 to meet the carbon source and nitrogen source required by early growth of a fermentation strain, then inoculating the strain for fermentation treatment to obtain fermentation liquor, filtering and centrifuging the obtained fermentation liquor to obtain filtrate, adding 1% of powdered activated carbon into the filtrate at the temperature of 40 ℃, stirring for 40 minutes, carrying out vacuum pumping to remove the powdered activated carbon and residual impurities to obtain decolorized solution, and concentrating the decolorized solution at 80-90.6KPa to obtain the traditional Chinese medicine fermentation liquor.
S3, heating the traditional Chinese medicine fermentation liquor obtained in the above steps, pouring tobacco leaf extract with a set weight when the temperature rises to 65-75 ℃, uniformly mixing, pouring the mixture of propylene glycol and glycerol with a set weight, uniformly stirring, pouring tea tree essential oil with a set weight after 10min, uniformly mixing, pouring fruit juice and a tobacco flavoring agent which are mixed in advance, finally adding a stabilizing agent with a set weight, and uniformly stirring to obtain the finished product of the electronic atomization liquid.
The preparation method of the traditional Chinese medicine mixture comprises the following steps: decocting equivalent parts by mass of sauropus spatulifolius, tea leaves and common andrographis herb in water for three times, filtering, merging filtrate and concentrating, then extracting with ethanol twice, filtering to obtain ethanol extractive solution, mixing, recovering ethanol under reduced pressure, concentrating to obtain component A, decocting radix astragali, Poria, Coicis semen, fructus Schisandrae chinensis, fresh rhizoma Dioscoreae, dried herba Zosterae Marinae, Auricularia and Tremella with water to obtain concentrated decoction as component B, hydrolyzing fresh oysters and pearls with sulfuric acid, adding calcium hydroxide for neutralization, filtering, washing medicine residues with purified water, merging, concentrating into a component C, respectively juicing grapes, pomegranates, tomatoes, celery, fresh edible cactus, mannitol, sodium benzoate, aspartame, sodium citrate, honey, xanthan gum and sodium carboxymethylcellulose, uniformly mixing to obtain a component D, and uniformly mixing the component A, the component B, the component C and the component D according to the mass ratio of 1:1:1:1 to form a traditional Chinese medicine mixture.
The weight ratio of astragalus membranaceus, poria cocos, coix seeds, schisandra chinensis, fresh Chinese yam, dried kelp, agaric, tremella, fresh oyster, pearl, grape, pomegranate, tomato, celery, fresh edible cactus, mannitol, sodium benzoate, aspartame, sodium citrate, honey, xanthan gum and sodium carboxymethylcellulose is 6:6:6:8:3: 4:2:16:0.5:30:6:30: 15:5:2:0.3:1:4:2: 1.
The fermentation treatment in S2 comprises the following specific steps: anaerobic fermentation is carried out for 15-20 days at the temperature of 26-32 ℃, the growth condition of colonies is checked every 3 days, and the fermentation is stopped when the average bacteria content in each milliliter of fermentation liquor reaches 2.5 multiplied by 108 CFU/mL.
The ultrasonic treatment frequency in S2 is 40KHz, the fermentation strain is EM composite strain, and the EM composite strain comprises bacillus, Aerobacter, lactobacillus, photosynthetic bacteria, Aspergillus niger and yeast.
The glycerol is vegetable glycerol, the stabilizer is formed by uniformly mixing dextrin, pectin and xanthan gum according to the mass ratio of 1:1:1, and the tobacco flavoring agent is ethyl acetate or ethyl butyrate.
The fruit juice is one or more of vanilla, apple, cherry, chocolate, coffee, mango, strawberry, watermelon, peach, grape, pineapple, bubble gum, Hami melon, lemon, banana, spearmint, kiwi fruit, coconut and blueberry.
Example 3:
a production method of electronic atomized liquid comprises the following steps:
s1, preparing the following materials in parts by mass: 3-5 parts of tobacco leaf extract, 25-40 parts of propylene glycol, 25-40 parts of glycerol, 0.2-0.5 part of stabilizer, 0.1-0.3 part of tobacco flavoring agent, 5-8 parts of traditional Chinese medicine mixture, 15-24 parts of pure water and 3-5 parts of plant extract.
S2, mixing a traditional Chinese medicine mixture with a predetermined weight with pure water with a predetermined weight, carrying out ultrasonic treatment for 30 minutes after mixing, heating until boiling after treatment, standing and cooling the boiled mixed solution for 20-23 hours at room temperature, pouring into an axe type fermentation tank, adding 500 g of brown sugar and bean powder mixed according to the mass ratio of 3:2 to meet the carbon source and nitrogen source required by early growth of a fermentation strain, then inoculating the strain for fermentation treatment to obtain fermentation liquor, filtering and centrifuging the obtained fermentation liquor to obtain filtrate, adding 1% of powdered activated carbon into the filtrate at the temperature of 40 ℃, stirring for 40 minutes, carrying out vacuum pumping to remove the powdered activated carbon and residual impurities to obtain decolorized solution, and concentrating the decolorized solution at 80-90.6KPa to obtain the traditional Chinese medicine fermentation liquor.
S3, heating the traditional Chinese medicine fermentation liquor obtained in the above steps, pouring the tobacco leaf extract with a set weight when the temperature rises to 65-75 ℃, uniformly mixing, pouring the mixture of propylene glycol and glycerol with a set weight, uniformly stirring, pouring the plant extracting solution with a set weight after 10min, uniformly mixing, pouring the tobacco flavoring agent which is mixed in advance, finally adding the stabilizing agent with a set weight, and uniformly stirring to obtain the finished product of the electronic atomization liquid.
The preparation method of the traditional Chinese medicine mixture comprises the following steps: decocting equivalent parts by mass of sauropus spatulifolius, tea leaves and common andrographis herb in water for three times, filtering, merging filtrate and concentrating, then extracting with ethanol twice, filtering to obtain ethanol extractive solution, mixing, recovering ethanol under reduced pressure, concentrating to obtain component A, decocting radix astragali, Poria, Coicis semen, fructus Schisandrae chinensis, fresh rhizoma Dioscoreae, dried herba Zosterae Marinae, Auricularia and Tremella with water to obtain concentrated decoction as component B, hydrolyzing fresh oysters and pearls with sulfuric acid, adding calcium hydroxide for neutralization, filtering, washing medicine residues with purified water, merging, concentrating into a component C, respectively juicing grapes, pomegranates, tomatoes, celery, fresh edible cactus, mannitol, sodium benzoate, aspartame, sodium citrate, honey, xanthan gum and sodium carboxymethylcellulose, uniformly mixing to obtain a component D, and uniformly mixing the component A, the component B, the component C and the component D according to the mass ratio of 1:1:1:1 to form a traditional Chinese medicine mixture.
The weight ratio of astragalus membranaceus, poria cocos, coix seeds, schisandra chinensis, fresh Chinese yam, dried kelp, agaric, tremella, fresh oyster, pearl, grape, pomegranate, tomato, celery, fresh edible cactus, mannitol, sodium benzoate, aspartame, sodium citrate, honey, xanthan gum and sodium carboxymethylcellulose is 6:6:6:8:3: 4:2:16:0.5:30:6:30: 15:5:2:0.3:1:4:2: 1.
The fermentation treatment in S2 comprises the following specific steps: anaerobic fermentation is carried out for 15-20 days at the temperature of 26-32 ℃, the growth condition of colonies is checked every 3 days, and the fermentation is stopped when the average bacteria content in each milliliter of fermentation liquor reaches 2.5 multiplied by 108 CFU/mL.
The ultrasonic treatment frequency in S2 is 40KHz, the fermentation strain is EM composite strain, and the EM composite strain comprises bacillus, Aerobacter, lactobacillus, photosynthetic bacteria, Aspergillus niger and yeast.
The glycerol is vegetable glycerol, the stabilizer is formed by uniformly mixing dextrin, pectin and xanthan gum according to the mass ratio of 1:1:1, and the tobacco flavoring agent is ethyl acetate or ethyl butyrate.
The preparation method of the plant extract comprises the following steps: mixing flos Lonicerae and herba Houttuyniae at a weight ratio of 1:6, cleaning, crushing, and steam distilling to obtain plant extractive solution.
The invention adds Chinese herbal medicine fermentation liquor prepared by fermenting Chinese herbal medicine, fruit, vegetable, marine product and medicinal and edible medicinal material by strains in the preparation process of the electronic atomized liquid, wherein the honeysuckle and the heartleaf houttuynia herb can relieve the problems of dry throat, throat itch, irritable cough, chronic pharyngitis, dry mouth and nose, dry thirst, little phlegm or difficult phlegm adhesion cough and the like caused by smoking to a certain extent, has the curative effects of clearing away heat and toxic materials and resisting bacteria and diminishing inflammation, has no toxic or side effect and no pollution to the environment, and the addition of the astragalus, the tuckahoe, the coix seed, the schisandra, the fresh yam, the dried kelp, the agaric, the tremella, the fresh oyster, the pearl, the grape, the pomegranate, the tomato, the celery, the fresh cactus, the mannitol, the sodium benzoate, the aspartame, the sodium citrate, the honey, the xanthan gum and the sodium carboxymethyl cellulose ensures that the finally obtained finished product of the electronic atomized liquid has a certain addiction stopping effect, thereby reducing the dependence of smokers on cigarettes.
The points to be finally explained are: although the present invention has been described in detail with reference to the general description and the specific embodiments, on the basis of the present invention, the above embodiments are only used for illustrating the technical solutions of the present invention, and not for limiting the same; while the invention has been described in detail and with reference to the foregoing embodiments, it will be understood by those skilled in the art that: the technical solutions described in the foregoing embodiments may still be modified, or some or all of the technical features may be equivalently replaced; and the modifications or the substitutions do not make the essence of the corresponding technical solutions depart from the scope of the technical solutions of the embodiments of the present invention.

Claims (8)

1. An electronic atomized liquid production method, which is characterized by comprising the following steps:
s1, preparing the following materials in parts by mass: 3-5 parts of tobacco leaf extract, 25-40 parts of propylene glycol, 25-40 parts of glycerol, 6-8 parts of fruit juice, 0.2-0.5 part of stabilizer, 0.1-0.3 part of tobacco flavoring agent, 5-8 parts of traditional Chinese medicine mixture, 15-24 parts of pure water, 3-5 parts of plant extract and 0.5-0.8 part of tea tree essential oil;
S2, mixing a traditional Chinese medicine mixture with a predetermined weight with pure water with a predetermined weight, carrying out ultrasonic treatment for 30 minutes after mixing, heating until boiling after treatment, standing and cooling the boiled mixed solution for 20-23 hours at room temperature, pouring into an axe type fermentation tank, adding 500 g of brown sugar and bean powder mixed according to the mass ratio of 3:2 to meet the carbon source and nitrogen source required by early growth of a fermentation strain, then inoculating the strain for fermentation treatment to obtain fermentation liquor, filtering and centrifuging the obtained fermentation liquor to obtain filtrate, adding 1% of powdered activated carbon into the filtrate at the temperature of 40 ℃, stirring for 40 minutes, carrying out vacuum pumping to remove the powdered activated carbon and residual impurities to obtain decolorized solution, and concentrating the decolorized solution at 80-90.6KPa to obtain the traditional Chinese medicine fermentation liquor;
s3, heating the traditional Chinese medicine fermentation liquor obtained in the above steps, pouring tobacco leaf extract with a set weight when the temperature rises to 65-75 ℃, uniformly mixing, pouring the mixture of propylene glycol and glycerol with a set weight, uniformly stirring, pouring plant extract with a set weight and tea tree essential oil with a set weight after 10min, uniformly mixing, pouring fruit juice and tobacco flavoring agent which are mixed in advance, finally adding stabilizing agent with a set weight, and uniformly stirring to obtain the finished product of the electronic atomization liquid.
2. The method for producing an electronically atomized liquid as set forth in claim 1, wherein: the preparation method of the traditional Chinese medicine mixture comprises the following steps: decocting equivalent parts by mass of sauropus spatulifolius, tea leaves and common andrographis herb in water for three times, filtering, merging filtrate and concentrating, then extracting with ethanol twice, filtering to obtain ethanol extractive solution, mixing, recovering ethanol under reduced pressure, concentrating to obtain component A, decocting radix astragali, Poria, Coicis semen, fructus Schisandrae chinensis, fresh rhizoma Dioscoreae, dried herba Zosterae Marinae, Auricularia and Tremella with water to obtain concentrated decoction as component B, hydrolyzing fresh oysters and pearls with sulfuric acid, adding calcium hydroxide for neutralization, filtering, washing medicine residues with purified water, merging, concentrating into a component C, respectively juicing grapes, pomegranates, tomatoes, celery, fresh edible cactus, mannitol, sodium benzoate, aspartame, sodium citrate, honey, xanthan gum and sodium carboxymethylcellulose, uniformly mixing to obtain a component D, and uniformly mixing the component A, the component B, the component C and the component D according to the mass ratio of 1:1:1:1 to form a traditional Chinese medicine mixture.
3. The method for producing an electronically atomized liquid as set forth in claim 2, wherein: the weight ratio of the astragalus membranaceus, the poria cocos, the coix seed, the schisandra chinensis, the fresh Chinese yam, the dried kelp to the agaric, the tremella fuciformis, the fresh oyster to the pearl to the grape, the pomegranate to the tomato to the celery to the fresh edible cactus to the mannitol to the sodium benzoate to the aspartame to the sodium citrate to the honey to the xanthan gum to the sodium carboxymethylcellulose is 6:6:6:8:3: 4:2:16:0.5:30:6:30: 15:5:2:0.3:1:4:2: 1.
4. The method for producing an electronically atomized liquid as set forth in claim 1, wherein: the fermentation treatment in the S2 comprises the following specific steps: anaerobic fermentation is carried out for 15-20 days at the temperature of 26-32 ℃, the growth condition of colonies is checked every 3 days, and the fermentation is stopped when the average bacteria content in each milliliter of fermentation liquor reaches 2.5 multiplied by 108 CFU/mL.
5. The method for producing an electronically atomized liquid as set forth in claim 4, wherein: the ultrasonic treatment frequency in the S2 is 40KHz, the fermentation strain is EM composite strain, and the EM composite strain comprises bacillus, Aerobacter, lactobacillus, photosynthetic bacteria, Aspergillus niger and yeast.
6. The method for producing an electronically atomized liquid as set forth in claim 1, wherein: the glycerol is vegetable glycerol, the stabilizer is formed by uniformly mixing dextrin, pectin and xanthan gum according to the mass ratio of 1:1:1, and the tobacco flavoring agent is ethyl acetate or ethyl butyrate.
7. The method for producing an electronically atomized liquid as set forth in claim 1, wherein: the preparation method of the plant extract comprises the following steps: mixing flos Lonicerae and herba Houttuyniae at a weight ratio of 1:6, cleaning, crushing, and steam distilling to obtain the plant extractive solution.
8. The method for producing an electronically atomized liquid as set forth in claim 1, wherein: the fruit juice is one or more of vanilla, apple, cherry, chocolate, coffee, mango, strawberry, watermelon, peach, grape, pineapple, bubble gum, Hami melon, lemon, banana, spearmint, kiwi fruit, coconut and blueberry.
CN202111233497.8A 2021-10-22 2021-10-22 Production method of electronic atomized liquid Pending CN113940443A (en)

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