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CN1138302A - Shrinking method - Google Patents

Shrinking method Download PDF

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Publication number
CN1138302A
CN1138302A CN95191134A CN95191134A CN1138302A CN 1138302 A CN1138302 A CN 1138302A CN 95191134 A CN95191134 A CN 95191134A CN 95191134 A CN95191134 A CN 95191134A CN 1138302 A CN1138302 A CN 1138302A
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CN
China
Prior art keywords
die
forging
annulus
section
flexible pipe
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
CN95191134A
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Chinese (zh)
Other versions
CN1067303C (en
Inventor
理查德·谢纳
帕斯卡尔·德塔布勒
米歇尔·安德烈
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Caillau SAS
Original Assignee
Etablissements Caillau SAS
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Publication date
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Publication of CN1138302A publication Critical patent/CN1138302A/en
Application granted granted Critical
Publication of CN1067303C publication Critical patent/CN1067303C/en
Anticipated expiration legal-status Critical
Expired - Fee Related legal-status Critical Current

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    • BPERFORMING OPERATIONS; TRANSPORTING
    • B21MECHANICAL METAL-WORKING WITHOUT ESSENTIALLY REMOVING MATERIAL; PUNCHING METAL
    • B21DWORKING OR PROCESSING OF SHEET METAL OR METAL TUBES, RODS OR PROFILES WITHOUT ESSENTIALLY REMOVING MATERIAL; PUNCHING METAL
    • B21D39/00Application of procedures in order to connect objects or parts, e.g. coating with sheet metal otherwise than by plating; Tube expanders
    • B21D39/04Application of procedures in order to connect objects or parts, e.g. coating with sheet metal otherwise than by plating; Tube expanders of tubes with tubes; of tubes with rods
    • B21D39/046Connecting tubes to tube-like fittings
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B21MECHANICAL METAL-WORKING WITHOUT ESSENTIALLY REMOVING MATERIAL; PUNCHING METAL
    • B21DWORKING OR PROCESSING OF SHEET METAL OR METAL TUBES, RODS OR PROFILES WITHOUT ESSENTIALLY REMOVING MATERIAL; PUNCHING METAL
    • B21D39/00Application of procedures in order to connect objects or parts, e.g. coating with sheet metal otherwise than by plating; Tube expanders
    • B21D39/04Application of procedures in order to connect objects or parts, e.g. coating with sheet metal otherwise than by plating; Tube expanders of tubes with tubes; of tubes with rods

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  • Engineering & Computer Science (AREA)
  • Mechanical Engineering (AREA)
  • Shaping Of Tube Ends By Bending Or Straightening (AREA)
  • Forging (AREA)
  • Joints That Cut Off Fluids, And Hose Joints (AREA)
  • Medicinal Preparation (AREA)
  • Feeding, Discharge, Calcimining, Fusing, And Gas-Generation Devices (AREA)
  • Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
  • Medicines Containing Material From Animals Or Micro-Organisms (AREA)
  • Lining Or Joining Of Plastics Or The Like (AREA)
  • Absorbent Articles And Supports Therefor (AREA)
  • Transition And Organic Metals Composition Catalysts For Addition Polymerization (AREA)
  • Shaping By String And By Release Of Stress In Plastics And The Like (AREA)
  • Rigid Pipes And Flexible Pipes (AREA)
  • Pipe Accessories (AREA)

Abstract

A method for shrinking a ring (14) is disclosed. The free end (10a) of a flexible tube (10) linking between the ring (14) and a rigid tubular member (12). The method uses a shrinking die (16) with an axial cavity (18) including a splayed section (18a) with a broad open end (20) whereat the diameter of the cavity is substantially the same as the greatest diameter (d) of said section. The shrinking die (16) is positioned so that at least the broad end of the cavity is located around the portion (14) to be shrunk while its narrow end is in front of the tube, and, while axially supporting one of the ring (14) and the shrinking die (16), both are mutually axially moved in a direction extending from the free end (10a) of the tube (10) towards the other end thereof.

Description

A kind of die forging method
As everyone knows, for example, the flexible hose free end can be tightened with an annulus and a rigid tubular member for making coupling arrangement have the rigid tubular end piece, arranged coaxial, annulus is in the flexible pipe outside, and rigid tubular member is in its inside.
For reaching this purpose, just must implement the die forging operation, to dwindle circle diameter.
Put it briefly, the present invention relates to a kind of die forging annulus method, this annulus is engaged on the flexible hose free end, and this flexible pipe is engaged on the rigid tubular member, described annulus to have at least can die forging section, its diameter is greater than hose diameter originally.
The method is to use the forging die of a tape spool to die cavity, it comprises an oared segrne pii, open from first end to second end, this die cavity has a uncovered big end, the diameter of die cavity described herein in fact with the equal diameters of the described oared segrne pii at the second end place.
Axially die forging generally is used to do the scattered work of rigidity pipe fitting.
United States Patent (USP) 2314002 has been recorded and narrated a kind of method, attempts to utilize axial die forging, and die forging is engaged in the annulus on the flexible hose free end.
In the method, forging die is to be enclosed within on this mould originally, and after annulus move to hose free end.
Because will be enclosed within forging die on the flexible pipe, so axial die cavity minimum diameter is not less than the overall diameter of flexible pipe.Because annulus itself is enclosed within on the flexible pipe, so its interior diameter also is not less than this flexible pipe overall diameter.Therefore, when die forging, the actual reduction volume of diameter must not be greater than the thickness of annulus.
Therefore, diameter reduction is emitted a little risks always, does not promptly have fully to hold and guarantees to be fitted together securely by the device that flexible pipe, annulus and tubular element constitute.
Improve the die forging degree, even also the unique method that further dwindles of diameter improves annulus thickness exactly, the raising that this just must bring fee of material makes the energy requirement raising of die forging institute.
Everybody knows that also radially die forging can be carried out with a kind of swaging tools.This instrument has many angled fan sections (angular sectors), can move mutually, and this method is not too satisfactory, damage occurs because of it can make the die forging appearance.Vertical fold appears because the radial fissure between the angle fan section, this damage may seriously arrive.This damage can increase the crush injury that flexible pipe occurs, and destroys sealing.
The present invention attempts to overcome these shortcomings.
This purpose is by following true the realization, promptly placing the forging die method is, at least be that the big end of die cavity will encase the die forging section, the first end of described die cavity oared segrne pii will exceed the flexible pipe scope in the front of hose free end, when axially blocking one of these two parts of annulus and forging die, between described two members, move to axial to doing towards the rear, promptly move to the other end that is considered as flexible pipe " back " end from the free end that is considered as flexible pipe " preceding " end.
By these configurations, die forging also not only is confined to the thickness of annulus.In addition, by moving backward,, just may obviously improve the mechanical strength of the device of forming by flexible pipe, annulus and tubular element owing to the reason of hose material (generally comprising rubber) shown characteristics when the die forging operation.
Some hose material is just pushed ahead when die forging, that is material is forced to wriggling, and is to be benchmark with the flexible pipe, advances along the forging die direction of displacement.If this displacement is moving to hose free end, the material of pushing ahead so just tends to assemble to described free end.When not having vacant lot in the annulus, surfacing just is easy to wriggle round about, and consequently whole wriggling all is to wriggle backward, that is wriggling is to be benchmark with the annulus, towards carrying out with forging die displacement rightabout.
By chance, the thickness of the flexible hose that rubber type of material is made obviously becomes with the function of manufacturing parameter, so that the size of the margin of tolerance may be about 1 millimeter, because thickness generation localized variation, the volume of excess stock, that is, the volume of the material that wriggling will be pushed open in the part, too can significant change, consequently, great changes will take place local for the pressure of the hose material in the annulus, for making annulus can bear these variations, and don't as for distortion, the tension intensity that connects between assurance flexible pipe, annulus and the tubular element, the thickness of annulus just must be quite big so.
In addition, when displacement when hose free end is moving, the flexible pipe constituent material also will bear huge pressure and change when being forced to wriggle, this will have influence on mechanical performance.
By this invention, when die forging was carried out in the position backward, the pressure that acts on hose free end was uniformly distributed in its whole periphery, so that any position of flexible pipe can not crushed suddenly or squeeze bad.
In addition, because die forging begins to carry out gradually from hose free end in the axial direction, the flexible pipe constituent material will be wriggled gradually so, and this can not damage flexible pipe, and helps to keep the airtight quality of this matching requirements especially.
Die forging is equably, little by little carry out, so just can be annulus and flexible pipe safety, be assembled together reliably, material aggregation appears in the pipe end that does not cause flexible pipe crush injury to occur or block mutually between annulus and rigid tubular member, especially the weak spot district can not appear at the petiolarea away from the free-ended annulus of pipe, even use quite thin annulus, also can guarantee reliable connection.
Favourable a kind of situation is, the moving to axial of annulus and forging die stopped before the first terminal end that arrives away from section hose free end, will die forging of oared segrne pii.
Like this, the horn mouth at annulus rear portion opens a little, thereby has avoided the danger of damage flexible pipe.Reliability and durability for guaranteeing hookup, will carry out the long duration test that intensity improves constantly to it.One of test is exactly to make the relative annulus vibration of flexible pipe.The annulus rear portion is this fact of horn mouth formula, is cut off even flexible pipe is impaired when making it avoid doing experiment.
As long as have a look the following detailed description of non-limiting example, just can good understanding be arranged to the present invention, its advantage also will be more apparent.Illustrate to relate to accompanying drawing, wherein:
Fig. 1 is a sectional side elevation, the annulus that is engaged on the flexible hose free end is shown, and flexible pipe itself is engaged on the rigid tubular member, it also shows a forging die, and first kind of embodiment of method therefor of the present invention just will be implemented with this mould.
Fig. 2 and Fig. 3 express the beginning and the ending of the inventive method respectively.
Fig. 4 is a view similar to Fig. 1, and visible another embodiment of the invention will be used among the figure.
Fig. 5 represents the performance of this method
Fig. 1 illustrates flexible hose 10, and its free end 10a is bonded on the rigid tubular member 12, and cylindrical shape annulus 14 then is bonded on the free end 10a.
For simplifying following explanation, suppose that end 10a is the front end of flexible hose 10, because these figure are brachymemma figure, an end of the back in other words that it is far away is then not shown.
Annulus 14 shown in Fig. 1 is the situations before the die forging.Its diameter D is greater than the diameter of flexible pipe 10.
Fig. 1 also illustrates the forging die 16 that has axial die cavity 18.This die cavity has an oared segrne pii 18a, this oared segrne pii 18a is the former first end 19a of d ' to diameter from diameter is that the second end 19b of d opens, diameter d is greater than diameter D, and diameter D itself is greater than diameter d ', the die cavity that joins with loudspeaker section first end 19a comprises that diameter is the cylindrical sections 18b of d ', and this section external-open is gone into narrow open end 17.At the other end, die cavity has a very big openend, and in the example shown, the second end 19b of it and conical butt loudspeaker section coincides.
Various different components before Fig. 1 illustrates the die forging operation and is about to begin, its position are, the longitudinal axis of die cavity axis and flexible hose is in alignment, and openend 20 opens backward greatly.
Fig. 1 also illustrates the instrument 22 that blocks annulus 14 vertically.And the rear end 14b of annulus abuts against with it.Fig. 1 this instrument that only schematically draws.This instrument can have two catch jackets on flexible pipe, matches with the free end 14b of annulus 14, so that be fixed in due position during die forging.
Wanting to place so earlier forging die, promptly is that the big end 20 of die cavity is enclosed within around the annulus of wanting die forging at least, and before the first end 19a will be placed on annulus, the front end above flexible pipe just began the die forging operation then.In other words, be exactly that forging die will be aimed at the die forging annulus by arrow F direction and configure, that is 10a moves to its rear end from the flexible pipe front end, or the end 20 that will move die cavity at least reach the front end 14a of annulus.
When the die cavity wall began to match with the annulus neighboring, formal die forging promptly began.
When carrying out die forging, as shown in Figures 2 and 3, forging die 16 is pressed arrow F direction, that is backward, move axially on the annulus 14.
Certainly, implementing thisly when mobile, because annulus is by chucking instrument 22 fix in position, its overall diameter is narrowed down to the minor diameter d ' of die cavity 18 gradually.When carrying out this operation, creep just takes place in flexible hose end 10a gradually.
When die forging finishes, structural form shown in Figure 3 occurs, wherein annulus 14 is crimped on the hose end 10a, and flexible pipe then is clamped between rigid tubular member 12 and the annulus 14.
As what seen on this figure, the situation after this illustrates die forging and finishes preferably before the minor diameter of the oared segrne pii 18a of die cavity moves on to rear end 14b away from the flexible pipe 14 of the free end 10a of flexible pipe 10, stops to move axially of forging die 16 relative annulus 14.Therefore, just a bit open as horn-like the rear section of annulus, and this has not just had the danger of damage flexible pipe.
In addition, can see on these figure that tubular element 12 is radially expanded portion 13 near himself rear end.Preferably before the complete die forging of annulus is to the bulge, just finish die forging.This has just guaranteed the reliable connection between the hookup member, and has avoided flexible pipe to be damaged by pressure by the part at bulge simultaneously, otherwise can damage the mechanical performance of flexible pipe.
As long as die forging one is finished, just, annulus is removed from forging die, and it is just passable to remove chucking instrument 22 by moving forging die to arrow F rightabout.
On Fig. 1 to Fig. 3, cylindrical shape annulus 14 total lengths in some cases, as shown in Figure 4 and Figure 5, it would be desirable the only part of die forging annulus basically all by die forging.On these figure, all be marked with same numeral with the similar member of Fig. 1 to Fig. 3 and add 100.
Annulus 114 has the first section 115a of a not die forging, shown in legend, this section 115a stretches forward, the front end 110a that surpasses flexible hose 110, and can be used as the shell of sealing ring 117, it has the fixedly member used of rigid tubular end piece in other words, and also we are desirable just above the end piece and flexible pipe 110 is connected to this.
Therefore, have only the rear end 115b of annulus 114 to need die forging section 115a to constitute an axial obstacle, it makes it possible to use single-piece forging die 16 under the described condition referring to figs. 1 to Fig. 3.Therefore, just used the forging die of forming by two housing 116a and 116b 116.
For this forging die is enclosed within on the annulus, shell 116a and 116b are left mutually, so that reserve a passage, its size will be enough to annulus is passed through, and or rather, is that its front section 115a is passed through.When two shells are incorporated into together, encase annulus, to remove after the described passage, forging die moves by F arrow direction, at this moment just formally begins axial die forging.
In case two shells according to said method are assembled together, and just form die cavity 118, it has an oared segrne pii 118a and the cylindrical section 118b that diameter is less.
Small end 121 away from the big end 120 of die cavity is openings.Seen as Fig. 5, this just can make forging die 116 that section 115b is impaled, and implements die forging, and the first section 115a that reserves annulus 114 simultaneously stretches out forging die forward.
The die forging of section 115b is by moving by arrow F direction, that is makes it to begin to move to from the die forging that dots that the die forging end that represents with solid line finishes.In the whole process that the forging groove moves, annulus is axially blocked by chucking instrument 122.In Fig. 4 and example shown in Figure 5, instrument 122 has claw, can match with the front end of annulus 114, or rather, the claw of instrument 122 just is trapped among around the annulus that is right after first section, 115 back, and engages with shoulder 114 ', so that block annulus, move backward when preventing its die forging.
On Fig. 4, can see, the arbitrary diameter of the second section 115b of the first section 115a back that is positioned at annulus before die forging all greater than the diameter of annulus after dwindling through die forging.This point is particularly suited for the front end region 115c near the 115b section of the first section 115a back.Therefore, close mutually around annulus 114 when shell, before moving axially forging die, distinguish 115c at this, implement the preliminary step of radially die forging, its size accounts for a very little part of wanting the die forging span access location length.
Preferably as shown in Figure 4 and Figure 5, implement radially that the regional 115c of die forging preliminary step stretches forward, surpass the front end 110a of flexible hose, the shortcoming relevant with die forging radially is unlikely to exert an influence to flexible pipe so that make.
The diameter of centre portion 115c also might just be less than or equal to the die forging diameter originally, in this case, just needn't implement radially die forging step in advance.
Though annulus is axially blocked, forging die moves by the direction shown in the arrow F as the example shown in scheming to go up, and it should be understood that equally and might move annulus by arrow F rightabout by axially blocking forging die, implements die forging.The important point is that two members that are made of annulus and forging die produce displacement each other, make forging die press arrow F direction, that is move along die forging backward.

Claims (5)

1. die forging annulus (14,114) method, this annulus is engaged in flexible hose (10,110) free end (10a, 110a), and flexible pipe itself is engaged in rigid tubular member (12,112) on, described annulus has a section (14 of wanting die forging at least, 115b), its diameter D is greater than hose diameter, this method adopts a forging die (16,116), this forging die has axial die cavity (18,118), this die cavity comprises an oared segrne pii (18a, 118a), open to the second end (19b) from first end (19a), this die cavity has a big open end (20 at its second end, 120), the as many as described oared segrne pii diameter of described die cavity diameter (d) herein
It is characterized in that: forging die (16,116) be in this way place, be the big end (20,120) of die cavity (18, the 118) section that will contain die forging (14,115b) at least, and described die cavity oared segrne pii (18a, first end 118a) will be at hose free end (10a, front 110a) exceeds flexible pipe (10,110), and
Axially tightening annulus (14,114) and during one of two members formed of forging die (16,116), backward directions (F) are done and are moved to axial between described two members, that is, from being considered as flexible pipe (10, (10a 110a) moves to the other end that is considered as " back " end the free end of " preceding " end 110).
2. the method for claim 1, it is characterized in that: at oared segrne pii (18a, first end 118a) (19a) arrives the section (14 of wanting die forging, 115b), away from flexible pipe (10,110) free end (10a, end (14b 110a), 114b) before, stop to move to axial of annulus (14,114) and forging die (16,116).
3. method as claimed in claim 1 or 2 is characterized in that: annulus (14,114) axial restraint, forging die (16,116) want the section of die forging (14, move axially on 115b).
4. as each described method of claim 1 to 3, it is characterized in that: used forging die (116) comprises two housing (116a, 116b), for forging die (116) is installed on the annulus, and housing (116a, 116b) separated from each other, form a passage, its size is enough to make annulus (114) to pass through, and described housing moves to around the described annulus in opposite directions, eliminates until passage.
5. method as claimed in claim 4, it is characterized in that: when housing (116a, 116b) moves in opposite directions and surrounds when annulus (114), end regions (115c) at section (115b) that will die forging is implemented radially die forging step in advance earlier, this zone is a short section of described section (115b) near the free end (110a) of flexible pipe (110).
CN95191134A 1994-11-02 1995-11-02 Shrinking method Expired - Fee Related CN1067303C (en)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
FR94/13063 1994-11-02
FR9413063A FR2726208B1 (en) 1994-11-02 1994-11-02 SHRINKING PROCESS

Publications (2)

Publication Number Publication Date
CN1138302A true CN1138302A (en) 1996-12-18
CN1067303C CN1067303C (en) 2001-06-20

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ID=9468416

Family Applications (1)

Application Number Title Priority Date Filing Date
CN95191134A Expired - Fee Related CN1067303C (en) 1994-11-02 1995-11-02 Shrinking method

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EP (1) EP0737114B1 (en)
JP (1) JP3179499B2 (en)
KR (1) KR100264241B1 (en)
CN (1) CN1067303C (en)
AT (1) ATE214983T1 (en)
BR (1) BR9506434A (en)
CA (1) CA2178740C (en)
CZ (1) CZ292243B6 (en)
DE (1) DE69526065T2 (en)
ES (1) ES2173984T3 (en)
FR (1) FR2726208B1 (en)
HU (1) HU214856B (en)
MX (1) MX9602541A (en)
PL (1) PL178959B1 (en)
RU (1) RU2113929C1 (en)
TW (1) TW305783B (en)
WO (1) WO1996014177A1 (en)

Cited By (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101856695A (en) * 2010-05-21 2010-10-13 柳州市金元机械制造有限公司 Method and equipment thereof for buckling-riveting outer sleeve of push-pull flexible shaft
CN103143661A (en) * 2013-03-21 2013-06-12 陕西飞机工业(集团)有限公司 Tolerance optimization method for die forging
CN104139145A (en) * 2014-08-11 2014-11-12 贵州航天新力铸锻有限责任公司 Method for forging guide horn mouth forge pieces applied to internal components of nuclear reactor
CN105537488A (en) * 2016-02-04 2016-05-04 柳州龙润汽车零部件制造有限公司 Single-process air-conditioning pipe and bolt upsetting molding die
CN109215932A (en) * 2017-07-03 2019-01-15 大陆汽车系统公司 Fuel pump solenoid component and method
CN111093853A (en) * 2017-09-18 2020-05-01 伯斯有限公司 Method of forming a loudspeaker enclosure and associated tool

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JP4554896B2 (en) * 2003-06-16 2010-09-29 カヤバ工業株式会社 Piston rod manufacturing method
FR2868713B1 (en) * 2004-04-09 2006-07-21 Faurecia Sys Echappement MACHINE FOR RETREATING AN EXHAUST VOLUME
US9857008B2 (en) 2008-11-20 2018-01-02 Gates Corporation Crimpable or swageable fluid power ferrules, couplings, systems and methods employing torque communication
JP5779104B2 (en) * 2009-02-03 2015-09-16 ドナルド ダン,レスリー End hub assembly for conveyors, idlers and rolls
FR2950403B1 (en) 2009-09-24 2011-10-21 Caillau Ets TIGHTENING COLLAR AND METHOD FOR MANUFACTURING THE SAME
CN109590714B (en) * 2018-12-13 2022-07-08 重庆金山医疗技术研究院有限公司 Press mounting mechanism of metal cylinder

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Publication number Priority date Publication date Assignee Title
US2314002A (en) * 1941-12-03 1943-03-16 Scoville Mfg Company Method for manufacturing and assembling high pressure couplings
US3726122A (en) * 1971-03-10 1973-04-10 Mc Donnell Douglas Corp Swaging tool
US5031301A (en) * 1990-01-30 1991-07-16 Hans Oetiker Method for connecting a reinforced hose with a coupling

Cited By (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101856695A (en) * 2010-05-21 2010-10-13 柳州市金元机械制造有限公司 Method and equipment thereof for buckling-riveting outer sleeve of push-pull flexible shaft
CN103143661A (en) * 2013-03-21 2013-06-12 陕西飞机工业(集团)有限公司 Tolerance optimization method for die forging
CN103143661B (en) * 2013-03-21 2015-08-26 陕西飞机工业(集团)有限公司 A kind of forging part tolerance optimization method
CN104139145A (en) * 2014-08-11 2014-11-12 贵州航天新力铸锻有限责任公司 Method for forging guide horn mouth forge pieces applied to internal components of nuclear reactor
CN105537488A (en) * 2016-02-04 2016-05-04 柳州龙润汽车零部件制造有限公司 Single-process air-conditioning pipe and bolt upsetting molding die
CN109215932A (en) * 2017-07-03 2019-01-15 大陆汽车系统公司 Fuel pump solenoid component and method
US10982633B2 (en) 2017-07-03 2021-04-20 Continental Automotive Systems, Inc. Fuel pump solenoid assembly method
CN109215932B (en) * 2017-07-03 2021-08-17 大陆汽车系统公司 Fuel pump solenoid assembly and method
CN111093853A (en) * 2017-09-18 2020-05-01 伯斯有限公司 Method of forming a loudspeaker enclosure and associated tool
CN111093853B (en) * 2017-09-18 2021-09-28 伯斯有限公司 Method of forming a loudspeaker enclosure and associated tool

Also Published As

Publication number Publication date
CZ292243B6 (en) 2003-08-13
CZ189196A3 (en) 1996-09-11
EP0737114A1 (en) 1996-10-16
CA2178740C (en) 2005-09-13
JPH09507795A (en) 1997-08-12
CN1067303C (en) 2001-06-20
PL178959B1 (en) 2000-07-31
CA2178740A1 (en) 1996-05-17
HUT75563A (en) 1997-05-28
FR2726208B1 (en) 1997-01-17
HU9601811D0 (en) 1996-09-30
FR2726208A1 (en) 1996-05-03
DE69526065T2 (en) 2002-11-07
ES2173984T3 (en) 2002-11-01
BR9506434A (en) 1997-09-02
ATE214983T1 (en) 2002-04-15
DE69526065D1 (en) 2002-05-02
JP3179499B2 (en) 2001-06-25
KR960706379A (en) 1996-12-09
KR100264241B1 (en) 2000-08-16
RU2113929C1 (en) 1998-06-27
WO1996014177A1 (en) 1996-05-17
TW305783B (en) 1997-05-21
EP0737114B1 (en) 2002-03-27
MX9602541A (en) 1997-05-31
HU214856B (en) 1998-06-29

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