CN113718530B - A deodorant for down jackets containing marine biological components - Google Patents
A deodorant for down jackets containing marine biological components Download PDFInfo
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- 239000002781 deodorant agent Substances 0.000 title claims description 32
- 239000013543 active substance Substances 0.000 claims description 43
- ZYGHJZDHTFUPRJ-UHFFFAOYSA-N coumarin Chemical compound C1=CC=C2OC(=O)C=CC2=C1 ZYGHJZDHTFUPRJ-UHFFFAOYSA-N 0.000 claims description 28
- 239000003795 chemical substances by application Substances 0.000 claims description 19
- 229920001661 Chitosan Polymers 0.000 claims description 16
- 241000196324 Embryophyta Species 0.000 claims description 16
- 239000003960 organic solvent Substances 0.000 claims description 16
- 150000004676 glycans Chemical class 0.000 claims description 15
- 229920001282 polysaccharide Polymers 0.000 claims description 15
- 239000005017 polysaccharide Substances 0.000 claims description 15
- 238000002360 preparation method Methods 0.000 claims description 15
- 239000000341 volatile oil Substances 0.000 claims description 15
- 229960000956 coumarin Drugs 0.000 claims description 14
- 235000001671 coumarin Nutrition 0.000 claims description 14
- 229930013686 lignan Natural products 0.000 claims description 14
- 150000005692 lignans Chemical class 0.000 claims description 14
- 235000009408 lignans Nutrition 0.000 claims description 14
- 125000003118 aryl group Chemical group 0.000 claims description 10
- 239000000706 filtrate Substances 0.000 claims description 10
- 239000002994 raw material Substances 0.000 claims description 10
- 238000003756 stirring Methods 0.000 claims description 10
- XEKOWRVHYACXOJ-UHFFFAOYSA-N Ethyl acetate Chemical group CCOC(C)=O XEKOWRVHYACXOJ-UHFFFAOYSA-N 0.000 claims description 9
- LYCAIKOWRPUZTN-UHFFFAOYSA-N Ethylene glycol Chemical group OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 claims description 9
- 230000003750 conditioning effect Effects 0.000 claims description 8
- 230000005415 magnetization Effects 0.000 claims description 6
- 244000246386 Mentha pulegium Species 0.000 claims description 3
- 235000016257 Mentha pulegium Nutrition 0.000 claims description 3
- 235000004357 Mentha x piperita Nutrition 0.000 claims description 3
- 235000001050 hortel pimenta Nutrition 0.000 claims description 3
- 238000001914 filtration Methods 0.000 claims 1
- 238000002156 mixing Methods 0.000 claims 1
- 241001474374 Blennius Species 0.000 description 13
- 230000000052 comparative effect Effects 0.000 description 9
- 230000000694 effects Effects 0.000 description 7
- 241000894006 Bacteria Species 0.000 description 6
- 230000001877 deodorizing effect Effects 0.000 description 6
- 239000003205 fragrance Substances 0.000 description 6
- 230000000844 anti-bacterial effect Effects 0.000 description 5
- 230000007423 decrease Effects 0.000 description 5
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 4
- 239000000203 mixture Substances 0.000 description 4
- UHOVQNZJYSORNB-UHFFFAOYSA-N Benzene Chemical compound C1=CC=CC=C1 UHOVQNZJYSORNB-UHFFFAOYSA-N 0.000 description 3
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 description 3
- 238000004332 deodorization Methods 0.000 description 3
- 239000000835 fiber Substances 0.000 description 3
- CSCPPACGZOOCGX-UHFFFAOYSA-N Acetone Chemical compound CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 description 2
- 241000272525 Anas platyrhynchos Species 0.000 description 2
- 241000272814 Anser sp. Species 0.000 description 2
- HEDRZPFGACZZDS-UHFFFAOYSA-N Chloroform Chemical compound ClC(Cl)Cl HEDRZPFGACZZDS-UHFFFAOYSA-N 0.000 description 2
- 244000178870 Lavandula angustifolia Species 0.000 description 2
- 235000010663 Lavandula angustifolia Nutrition 0.000 description 2
- 241000234435 Lilium Species 0.000 description 2
- 241000607142 Salmonella Species 0.000 description 2
- 229920013822 aminosilicone Polymers 0.000 description 2
- 230000009286 beneficial effect Effects 0.000 description 2
- 230000004071 biological effect Effects 0.000 description 2
- 239000001102 lavandula vera Substances 0.000 description 2
- 235000018219 lavender Nutrition 0.000 description 2
- 238000000034 method Methods 0.000 description 2
- 235000019645 odor Nutrition 0.000 description 2
- 239000003921 oil Substances 0.000 description 2
- 102000004169 proteins and genes Human genes 0.000 description 2
- 108090000623 proteins and genes Proteins 0.000 description 2
- 230000001954 sterilising effect Effects 0.000 description 2
- 238000004659 sterilization and disinfection Methods 0.000 description 2
- 238000012360 testing method Methods 0.000 description 2
- 238000005406 washing Methods 0.000 description 2
- OYHQOLUKZRVURQ-NTGFUMLPSA-N (9Z,12Z)-9,10,12,13-tetratritiooctadeca-9,12-dienoic acid Chemical compound C(CCCCCCC\C(=C(/C\C(=C(/CCCCC)\[3H])\[3H])\[3H])\[3H])(=O)O OYHQOLUKZRVURQ-NTGFUMLPSA-N 0.000 description 1
- 239000002028 Biomass Substances 0.000 description 1
- 244000223760 Cinnamomum zeylanicum Species 0.000 description 1
- 229920000832 Cutin Polymers 0.000 description 1
- 241000194032 Enterococcus faecalis Species 0.000 description 1
- 235000010254 Jasminum officinale Nutrition 0.000 description 1
- 240000005385 Jasminum sambac Species 0.000 description 1
- 102000011782 Keratins Human genes 0.000 description 1
- 108010076876 Keratins Proteins 0.000 description 1
- 240000007817 Olea europaea Species 0.000 description 1
- 241000220317 Rosa Species 0.000 description 1
- 241000194017 Streptococcus Species 0.000 description 1
- 241000700605 Viruses Species 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 239000004480 active ingredient Substances 0.000 description 1
- 239000003513 alkali Substances 0.000 description 1
- 235000017803 cinnamon Nutrition 0.000 description 1
- 230000007547 defect Effects 0.000 description 1
- 125000004177 diethyl group Chemical group [H]C([H])([H])C([H])([H])* 0.000 description 1
- 125000001033 ether group Chemical group 0.000 description 1
- 235000019197 fats Nutrition 0.000 description 1
- 230000002550 fecal effect Effects 0.000 description 1
- 239000010643 fennel seed oil Substances 0.000 description 1
- 239000004615 ingredient Substances 0.000 description 1
- OYHQOLUKZRVURQ-IXWMQOLASA-N linoleic acid Natural products CCCCC\C=C/C\C=C\CCCCCCCC(O)=O OYHQOLUKZRVURQ-IXWMQOLASA-N 0.000 description 1
- 235000020778 linoleic acid Nutrition 0.000 description 1
- OYHQOLUKZRVURQ-HZJYTTRNSA-N linoleic acid group Chemical group C(CCCCCCC\C=C/C\C=C/CCCCC)(=O)O OYHQOLUKZRVURQ-HZJYTTRNSA-N 0.000 description 1
- 230000002503 metabolic effect Effects 0.000 description 1
- 230000004060 metabolic process Effects 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 235000015097 nutrients Nutrition 0.000 description 1
- 230000035699 permeability Effects 0.000 description 1
- 239000000843 powder Substances 0.000 description 1
- 239000000047 product Substances 0.000 description 1
- 210000002374 sebum Anatomy 0.000 description 1
- 230000003248 secreting effect Effects 0.000 description 1
- 230000001953 sensory effect Effects 0.000 description 1
- 238000002791 soaking Methods 0.000 description 1
- 239000000344 soap Substances 0.000 description 1
- FQENQNTWSFEDLI-UHFFFAOYSA-J sodium diphosphate Chemical compound [Na+].[Na+].[Na+].[Na+].[O-]P([O-])(=O)OP([O-])([O-])=O FQENQNTWSFEDLI-UHFFFAOYSA-J 0.000 description 1
- RYYKJJJTJZKILX-UHFFFAOYSA-M sodium octadecanoate Chemical compound [Na+].CCCCCCCCCCCCCCCCCC([O-])=O RYYKJJJTJZKILX-UHFFFAOYSA-M 0.000 description 1
- 229940048086 sodium pyrophosphate Drugs 0.000 description 1
- 235000013599 spices Nutrition 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 210000004243 sweat Anatomy 0.000 description 1
- 239000010677 tea tree oil Substances 0.000 description 1
- 229940111630 tea tree oil Drugs 0.000 description 1
- 235000019818 tetrasodium diphosphate Nutrition 0.000 description 1
- 239000001577 tetrasodium phosphonato phosphate Substances 0.000 description 1
- 239000004753 textile Substances 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
Classifications
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M19/00—Treatment of feathers
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/10—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing oxygen
- D06M13/11—Compounds containing epoxy groups or precursors thereof
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/10—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing oxygen
- D06M13/224—Esters of carboxylic acids; Esters of carbonic acid
- D06M13/228—Cyclic esters, e.g. lactones
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
- D06M15/01—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with natural macromolecular compounds or derivatives thereof
- D06M15/03—Polysaccharides or derivatives thereof
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
- D06M15/01—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with natural macromolecular compounds or derivatives thereof
- D06M15/03—Polysaccharides or derivatives thereof
- D06M15/13—Alginic acid or derivatives thereof
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M16/00—Biochemical treatment of fibres, threads, yarns, fabrics, or fibrous goods made from such materials, e.g. enzymatic
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02A—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
- Y02A50/00—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE in human health protection, e.g. against extreme weather
- Y02A50/20—Air quality improvement or preservation, e.g. vehicle emission control or emission reduction by using catalytic converters
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- Engineering & Computer Science (AREA)
- Textile Engineering (AREA)
- Life Sciences & Earth Sciences (AREA)
- Chemical & Material Sciences (AREA)
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- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Microbiology (AREA)
- Disinfection, Sterilisation Or Deodorisation Of Air (AREA)
Abstract
本发明涉及羽绒除味技术领域,具体公开了一种含有海洋生物成分的羽绒服除味剂,所述羽绒服除味剂的制备原料包括:海洋活性剂、植物活性剂、有机溶剂、芳香剂和调理剂,其中,所述海洋活性剂为海藻多糖和甲壳胺,所述植物活性剂由香豆素和木酚素按5:1‑2的质量比混合而成。本发明除味剂加入有由海藻多糖和甲壳胺组成的海洋生物成分,可有效去除羽绒服表面滋生的细菌、病毒,另外甲壳胺的加入还可增加除味剂的流动分散性,促进生物活性稳定释放;本发明采用香豆素和木酚素作为植物活性剂,能起到了良好的除味作用,尤其是针对羽绒角蛋白纤维的腥味,同时还能配合海藻多糖,起到良好的抗菌作用,从源头上避免腥味的产生。The invention relates to the technical field of down deodorization, and specifically discloses a down jacket deodorant containing marine biological components. agent, wherein the marine active agent is seaweed polysaccharide and chitosan, and the plant active agent is formed by mixing coumarin and lignan in a mass ratio of 5:1-2. The deodorant of the present invention is added with marine biological components composed of seaweed polysaccharides and chitosan, which can effectively remove bacteria and viruses that grow on the surface of down jackets. In addition, the addition of chitosan can also increase the flow dispersibility of the deodorant, and promote the stability of biological activity. release; the present invention uses coumarin and lignan as plant active agents, which can play a good deodorizing effect, especially for the fishy smell of down keratin fibers, and can also cooperate with seaweed polysaccharides to play a good antibacterial effect , to avoid the generation of fishy smell from the source.
Description
技术领域technical field
本发明涉及羽绒除味技术领域,具体涉及一种含有海洋生物成分的羽绒服除味剂。The invention relates to the technical field of down deodorization, in particular to a deodorant for down clothing containing marine biological components.
背景技术Background technique
羽绒是一种绿色天然蛋白质纤维,也是宝贵的生物质资源,其具有轻盈、柔软,保暖性能好、资源丰富,性价比极高等特性。随着人们生活水平的提高,对羽绒的品质要求也越来越高。Down is a green natural protein fiber and a valuable biomass resource. It has the characteristics of lightness, softness, good thermal performance, rich resources, and high cost performance. With the improvement of people's living standards, the quality requirements for down are also getting higher and higher.
但是羽绒属于一种角蛋白纤维,其耐碱性较差,在人们日常使用中用肥皂或一般洗衣粉清洗,较强的碱性会破坏其表面的脂肪膜,加上存放不当,极易滋生细菌,并产生腥味。人的皮肤每时每。刻都在新陈代谢,分泌皮脂、汗液、角质、废气等代谢废物,成为了细菌生长的养分,同时影响和皮肤接触的纺织品,使其发臭、发腥,尤其在我国南方湿气重的环境下更容易这样。那么无论是保护人体不受环境中有害细菌和气味的侵害,还是防止细菌在羽绒制品上的生长和散发腥味,对其进行抗菌除腥味处理都是有必要的。However, down belongs to a kind of keratin fiber, and its alkali resistance is poor. In people's daily use, it is washed with soap or general washing powder. Strong alkalinity will destroy the fat film on its surface. Bacteria and produce a fishy smell. People's skin all the time. Metabolism is always in progress, secreting sebum, sweat, cutin, exhaust gas and other metabolic wastes, which become nutrients for the growth of bacteria, and at the same time affect the textiles in contact with the skin, making them smelly and fishy, especially in the humid environment in southern my country Easier this way. So whether it is to protect the human body from harmful bacteria and odors in the environment, or to prevent the growth of bacteria and fishy smell on down products, it is necessary to carry out antibacterial and deodorizing treatment.
目前,市面上的羽绒的腥味去除剂效果一般,更为重要的是,其制剂中的化学成份容易对羽绒造成损伤,影响保暖性能。At present, the fishy smell removers on the market are generally effective, and more importantly, the chemical components in the preparations are likely to cause damage to the down and affect the thermal performance.
发明内容Contents of the invention
本发明的目的在于提供一种含有海洋生物成分的羽绒服除味剂,其解决了现有的羽绒腥味处理剂存在的效果不理想,且易对羽绒造成损伤的缺陷。The purpose of the present invention is to provide a down jacket deodorant containing marine biological components, which solves the defects that the existing down odor treatment agents have unsatisfactory effects and are easy to cause damage to down.
本发明通过以下技术方案来实现上述目的:The present invention achieves the above object through the following technical solutions:
一种含有海洋生物成分的羽绒服除味剂,所述羽绒服除味剂的制备原料包括:海洋活性剂、植物活性剂、有机溶剂、芳香剂和调理剂,其中,所述海洋活性剂为海藻多糖和甲壳胺,所述植物活性剂由香豆素和木酚素按5:1-2的质量比混合而成;A down jacket deodorant containing marine biological components, the preparation raw materials of the down jacket deodorant include: marine active agent, plant active agent, organic solvent, fragrance and conditioning agent, wherein the marine active agent is seaweed polysaccharide and chitosan, the phytoactive agent is mixed by coumarin and lignans in a mass ratio of 5:1-2;
所述羽绒服除味剂的制备方法为:The preparation method of described down jacket deodorant is:
(1)取香豆素和木酚素按比例混合后加入到有机溶剂中,在温度为35-55℃、以300-500r/min的转速搅拌提取5-7h,过滤得活性滤液备用;(1) Mix coumarin and lignans in proportion and add them into an organic solvent, stir and extract at a temperature of 35-55° C. at a speed of 300-500 r/min for 5-7 hours, and filter to obtain an active filtrate for later use;
(2)分别提取海藻多糖和甲壳胺作为海洋活性剂,将海洋活性剂加入到活性滤液中,再加入芳香剂和调理剂,搅拌均匀,即得羽绒服除味剂。(2) extract seaweed polysaccharide and chitosan respectively as marine active agents, add the marine active agents to the active filtrate, add fragrance and conditioner, stir evenly, and obtain the down jacket deodorant.
进一步改进在于,所述羽绒服除味剂的制备原料按重量份数包括:1-5份海洋活性剂、4-10份植物活性剂、20-50份有机溶剂、0.1-1份芳香剂和0.5-3份调理剂。A further improvement is that the raw materials for the preparation of the down jacket deodorant include, in parts by weight: 1-5 parts of marine active agents, 4-10 parts of plant active agents, 20-50 parts of organic solvents, 0.1-1 parts of aromatic agents and 0.5 parts of -3 parts conditioner.
进一步改进在于,所述海洋活性剂中海藻多糖和甲壳胺的质量比为10:1-5。A further improvement is that the mass ratio of seaweed polysaccharide to chitosan in the marine active agent is 10:1-5.
进一步改进在于,所述有机溶剂选自乙醇、乙醚、丙酮、苯、氯仿、乙酸乙酯中的一种或多种。A further improvement is that the organic solvent is selected from one or more of ethanol, ether, acetone, benzene, chloroform, and ethyl acetate.
进一步改进在于,所述芳香剂为经过高磁化处理的天然精油,在磁场作用下使精油分子团变小,实现微米化,且活性和渗透性提升,而粘性降低,从而有利于精油效果的发挥。A further improvement is that the aromatic agent is a natural essential oil that has undergone a high magnetization treatment. Under the action of a magnetic field, the molecular clusters of the essential oil are reduced to achieve micronization, and the activity and permeability are improved, while the viscosity is reduced, which is beneficial to the effect of the essential oil. .
进一步改进在于,所述天然精油选自薰衣草精油、茉莉精油、茶树油、橄榄精油、薄荷精油、肉桂精油、茴香油、百合精油、玫瑰精油中的一种或多种。A further improvement is that the natural essential oil is selected from one or more of lavender essential oil, jasmine essential oil, tea tree oil, olive essential oil, peppermint essential oil, cinnamon essential oil, fennel oil, lily essential oil, and rose essential oil.
进一步改进在于,所述高磁化处理的磁场强度为8000-20000GS,处理时间为20-80min。A further improvement is that the magnetic field strength of the high magnetization treatment is 8000-20000GS, and the treatment time is 20-80min.
进一步改进在于,所述调理剂选自亚油酸、硬脂酸钠、焦磷酸钠、乙二醇、氨基硅油、酸二乙酯中的一种或多种。A further improvement is that the conditioner is selected from one or more of linoleic acid, sodium stearate, sodium pyrophosphate, ethylene glycol, amino silicone oil, and diethyl acid.
本发明的有益效果在于:The beneficial effects of the present invention are:
(1)本发明除味剂加入有由海藻多糖和甲壳胺组成的海洋生物成分,可有效去除羽绒服表面滋生的细菌、病毒,另外甲壳胺的加入还可增加除味剂的流动分散性,促进生物活性稳定释放;(1) The deodorant of the present invention is added with marine biological components composed of seaweed polysaccharide and chitosan, which can effectively remove bacteria and viruses growing on the surface of down jackets, and the addition of chitosan can also increase the flow dispersibility of the deodorant and promote Stable release of biological activity;
(2)本发明采用香豆素和木酚素作为植物活性剂,其中香豆素自身属于天然的香料,在与木酚素配合使用时能起到了良好的除味作用,尤其是针对羽绒角蛋白纤维的腥味,同时还能配合海藻多糖,起到良好的抗菌作用,从源头上避免腥味的产生;本发明所采用的成分不会对羽绒造成任何损伤,且有助于增加羽绒的蓬松柔顺度、芳香度。(2) The present invention adopts coumarin and lignan as plant active agents, wherein coumarin itself belongs to natural spices, and can play a good deodorizing effect when used in conjunction with lignan, especially for down horn The fishy smell of protein fiber can also cooperate with seaweed polysaccharide to play a good antibacterial effect and avoid the generation of fishy smell from the source; the ingredients used in the present invention will not cause any damage to down and down, and help to increase the quality of down. Fluffy softness, aroma.
具体实施方式Detailed ways
下面结合实施例对本申请作进一步详细描述,有必要在此指出的是,以下具体实施方式只用于对本申请进行进一步的说明,不能理解为对本申请保护范围的限制,该领域的技术人员可以根据上述申请内容对本申请作出一些非本质的改进和调整。Below in conjunction with the embodiment the present application is described in further detail, it is necessary to point out here that the following specific embodiments are only used to further illustrate the present application, and cannot be interpreted as limiting the protection scope of the present application. Those skilled in the art can according to The above application content makes some non-essential improvements and adjustments to this application.
实施例1Example 1
一种含有海洋生物成分的羽绒服除味剂,所述羽绒服除味剂的制备原料按重量份数包括:1份海洋活性剂、4份植物活性剂、20份有机溶剂、0.1份芳香剂和0.5份调理剂,其中,所述海洋活性剂为海藻多糖和甲壳胺,且质量比为10:1,所述植物活性剂由香豆素和木酚素按5:1的质量比混合而成;所述有机溶剂为乙醇;所述芳香剂为经过高磁化处理(磁场强度为8000GS,处理时间为80min)的薰衣草精油;所述调理剂为亚油酸。A down jacket deodorant containing marine biological components, the preparation raw materials of the down jacket deodorant include in parts by weight: 1 part of marine active agent, 4 parts of plant active agent, 20 parts of organic solvent, 0.1 part of aromatic agent and 0.5 part of Part conditioning agent, wherein, the marine active agent is seaweed polysaccharide and chitosan, and the mass ratio is 10:1, and the plant active agent is mixed by coumarin and lignan in the mass ratio of 5:1; The organic solvent is ethanol; the aromatic agent is lavender essential oil through high magnetization treatment (the magnetic field strength is 8000GS, and the treatment time is 80min); the conditioning agent is linoleic acid.
所述羽绒服除味剂的制备方法为:The preparation method of described down jacket deodorant is:
(1)取香豆素和木酚素按比例混合后加入到有机溶剂中,在温度为35℃、以300r/min的转速搅拌提取7h,过滤得活性滤液备用;(1) Mix coumarin and lignans in proportion, add them to an organic solvent, stir and extract at a temperature of 35° C. at a speed of 300 r/min for 7 hours, and filter to obtain an active filtrate for later use;
(2)分别提取海藻多糖和甲壳胺作为海洋活性剂,将海洋活性剂加入到活性滤液中,再加入芳香剂和调理剂,搅拌均匀,即得羽绒服除味剂。(2) extract seaweed polysaccharide and chitosan respectively as marine active agents, add the marine active agents to the active filtrate, add fragrance and conditioner, stir evenly, and obtain the down jacket deodorant.
实施例2Example 2
一种含有海洋生物成分的羽绒服除味剂,所述羽绒服除味剂的制备原料按重量份数包括:3份海洋活性剂、7份植物活性剂、35份有机溶剂、0.5份芳香剂和1.5份调理剂,其中,所述海洋活性剂为海藻多糖和甲壳胺,且质量比为10:3,所述植物活性剂由香豆素和木酚素按5:1.5的质量比混合而成;所述有机溶剂为乙酸乙酯;所述芳香剂为经过高磁化处理(磁场强度为15000GS,处理时间为50min)的薄荷精油;所述调理剂为乙二醇。A down jacket deodorant containing marine biological components, the preparation raw materials of the down jacket deodorant include in parts by weight: 3 parts of marine active agents, 7 parts of plant active agents, 35 parts of organic solvents, 0.5 parts of aromatic agents and 1.5 parts of Part conditioning agent, wherein, the marine active agent is seaweed polysaccharide and chitosan, and the mass ratio is 10:3, and the plant active agent is mixed by coumarin and lignan in the mass ratio of 5:1.5; The organic solvent is ethyl acetate; the aromatic agent is peppermint essential oil through high magnetization treatment (the magnetic field strength is 15000GS, and the treatment time is 50min); the conditioning agent is ethylene glycol.
所述羽绒服除味剂的制备方法为:The preparation method of described down jacket deodorant is:
(1)取香豆素和木酚素按比例混合后加入到有机溶剂中,在温度为45℃、以400r/min的转速搅拌提取6h,过滤得活性滤液备用;(1) Mix coumarin and lignans in proportion, add them to an organic solvent, stir and extract at a temperature of 45° C. at a speed of 400 r/min for 6 hours, and filter to obtain an active filtrate for later use;
(2)分别提取海藻多糖和甲壳胺作为海洋活性剂,将海洋活性剂加入到活性滤液中,再加入芳香剂和调理剂,搅拌均匀,即得羽绒服除味剂。(2) extract seaweed polysaccharide and chitosan respectively as marine active agents, add the marine active agents to the active filtrate, add fragrance and conditioner, stir evenly, and obtain the down jacket deodorant.
实施例3Example 3
一种含有海洋生物成分的羽绒服除味剂,所述羽绒服除味剂的制备原料按重量份数包括:5份海洋活性剂、10份植物活性剂、50份有机溶剂、1份芳香剂和3份调理剂,其中,所述海洋活性剂为海藻多糖和甲壳胺,且质量比为10:5,所述植物活性剂由香豆素和木酚素按5:2的质量比混合而成;所述有机溶剂为乙醚;所述芳香剂为经过高磁化处理(磁场强度为20000GS,处理时间为20min)的百合精油;所述调理剂为氨基硅油。A down jacket deodorant containing marine biological components, the preparation raw materials of the down jacket deodorant include in parts by weight: 5 parts of marine active agents, 10 parts of plant active agents, 50 parts of organic solvents, 1 part of fragrance and 3 parts by weight. Part conditioning agent, wherein, the marine active agent is seaweed polysaccharide and chitosan, and the mass ratio is 10:5, and the plant active agent is mixed by coumarin and lignan in the mass ratio of 5:2; The organic solvent is ether; the aromatic agent is lily essential oil that has undergone high magnetization treatment (the magnetic field strength is 20000GS, and the treatment time is 20min); the conditioning agent is amino silicone oil.
所述羽绒服除味剂的制备方法为:The preparation method of described down jacket deodorant is:
(1)取香豆素和木酚素按比例混合后加入到有机溶剂中,在温度为55℃、以500r/min的转速搅拌提取5h,过滤得活性滤液备用;(1) Mix coumarin and lignans in proportion, add them to an organic solvent, stir and extract at a temperature of 55° C. at a speed of 500 r/min for 5 hours, and filter to obtain an active filtrate for later use;
(2)分别提取海藻多糖和甲壳胺作为海洋活性剂,将海洋活性剂加入到活性滤液中,再加入芳香剂和调理剂,搅拌均匀,即得羽绒服除味剂。(2) extract seaweed polysaccharide and chitosan respectively as marine active agents, add the marine active agents to the active filtrate, add fragrance and conditioner, stir evenly, and obtain the down jacket deodorant.
对比例1Comparative example 1
一种羽绒服除味剂,其原料和制备方法与实施例2基本相同,唯一区别在于:植物活性剂为7份香豆素。A deodorant for down jackets, its raw materials and preparation method are basically the same as in Example 2, the only difference is: the plant active agent is 7 parts of coumarin.
对比例2Comparative example 2
一种羽绒服除味剂,其原料和制备方法与实施例2基本相同,唯一区别在于:植物活性剂为7份木酚素。A deodorant for down jackets, its raw materials and preparation method are basically the same as in Example 2, the only difference is that the plant active agent is 7 parts of lignans.
对比例3Comparative example 3
一种羽绒服除味剂,其原料和制备方法与实施例2基本相同,唯一区别在于:去除植物活性剂,替换为7份海洋活性剂。A deodorant for down jackets, its raw materials and preparation method are basically the same as in Example 2, the only difference is: remove the plant active agent and replace it with 7 parts of marine active agent.
对比例4Comparative example 4
一种羽绒服除味剂,其原料和制备方法与实施例2基本相同,唯一区别在于:将海洋活性剂中的甲壳胺去除,替换为等量的海藻多糖。A deodorant for down jackets, its raw materials and preparation method are basically the same as in Example 2, the only difference is that the chitosan in the marine active agent is removed and replaced with an equivalent amount of seaweed polysaccharide.
对上述实施例2以及对比例1-4制得的羽绒服除味剂进行除味效果以及抗菌性能测试,具体测试方式为:取同一批次的鹅绒以及同一批次的鸭绒制成羽绒服,参照《GB/T14272-2011羽绒服装标准》检测其沙门氏菌含量、粪链球菌含量,再取各羽绒服除味剂,对鹅绒以及鸭绒羽绒服分别进行除味处理,处理方式均为浸泡1h,处理完成后取出羽绒服,流水清洗干净后,无菌环境下风干,以同样的方式再次检测羽绒服的沙门氏菌含量、粪链球菌含量,并计算除菌率,同时由专业感官检测人员检测其腥味程度,分为1-5五个等级,等级越高说明腥味越重。所有结果统计得到下表:The deodorants for down jackets obtained in the above-mentioned embodiment 2 and comparative examples 1-4 are tested for their deodorizing effect and antibacterial performance. GB/T14272-2011 Standard for Down Clothing" to detect the content of Salmonella and Streptococcus faecalis, and then take the deodorant of each down jacket to deodorize the goose down and duck down jackets respectively. The treatment methods are soaking for 1 hour, and the down jackets are taken out after the treatment , after washing with running water, air-dry in a sterile environment, test the salmonella content and fecal streptococcus content of the down jacket again in the same way, and calculate the sterilization rate, and at the same time, the degree of fishy smell is detected by professional sensory testing personnel, divided into 1- 5 five grades, the higher the grade, the heavier the fishy smell. All results are summarized in the following table:
从上表可以看出,本发明实施例2制得的羽绒服除味剂的去腥味效果突出,针对鹅绒和鸭绒羽绒服均达到了1级,同时除菌效果突出,达到了99.83%以上;而对比例1因植物活性剂仅采用了香豆素,对比例2仅采用了木酚素,均导致去腥效果明显下降,且除菌率也有所下降,由此说明香豆素和木酚素需要同时使用,才能发挥良好的除菌、除味作用;而对比例3因去除了植物活性剂,腥味严重,同时该实施例中相应增加了等量的海洋活性剂,海洋活性剂具有杀菌、杀病毒作用,然而结果表明其除菌率并没有提升,反而有略微下降,这说明本发明植物活性成分能配合海洋活性剂中的海藻多糖,起到更好的抗菌作用;对比例4因将海洋活性剂中的甲壳胺去除,导致除菌率明显下降,去腥效果也略有下降,说明甲壳胺的加入,一定程度上增加了除味剂的流动分散性,促进生物活性稳定释放。As can be seen from the above table, the deodorizing agent for down jackets prepared in Example 2 of the present invention has an outstanding deodorizing effect, reaching the first grade for goose down and duck down jackets, and the degerming effect is outstanding at the same time, reaching more than 99.83%; In Comparative Example 1, only coumarin was used as a plant active agent, and in Comparative Example 2, only lignans were used, both of which resulted in a significant decrease in the deodorization effect, and a decrease in the rate of bacteria removal, thus indicating that coumarin and lignans Need to use at the same time, just can bring into play good degerming, deodorizing effect; And comparative example 3 is because of removing plant active agent, fishy smell is serious, correspondingly increased the marine active agent of equal amount in this embodiment simultaneously, and marine active agent has bactericidal effect. , virus-killing effect, yet the results show that its degerming rate does not improve, but slightly decreases, which shows that the plant active ingredient of the present invention can cooperate with the seaweed polysaccharide in the marine active agent to play a better antibacterial effect; comparative example 4 is due to Removing the chitosan in the marine active agent resulted in a significant decrease in the sterilization rate and a slight decrease in the deodorization effect, indicating that the addition of chitosan increased the flow dispersibility of the deodorant to a certain extent and promoted the stable release of biological activity.
以上所述实施例仅表达了本发明的几种实施方式,其描述较为具体和详细,但并不能因此而理解为对本发明专利范围的限制。应当指出的是,对于本领域的普通技术人员来说,在不脱离本发明构思的前提下,还可以做出若干变形和改进,这些都属于本发明的保护范围。The above-mentioned embodiments only express several implementation modes of the present invention, and the description thereof is relatively specific and detailed, but should not be construed as limiting the patent scope of the present invention. It should be pointed out that those skilled in the art can make several modifications and improvements without departing from the concept of the present invention, and these all belong to the protection scope of the present invention.
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