CN113548867A - Red feather Jianzhan and preparation process thereof - Google Patents
Red feather Jianzhan and preparation process thereof Download PDFInfo
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- CN113548867A CN113548867A CN202110914159.4A CN202110914159A CN113548867A CN 113548867 A CN113548867 A CN 113548867A CN 202110914159 A CN202110914159 A CN 202110914159A CN 113548867 A CN113548867 A CN 113548867A
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- 210000003746 feather Anatomy 0.000 title claims abstract description 49
- 238000002360 preparation method Methods 0.000 title claims abstract description 15
- 238000000034 method Methods 0.000 claims abstract description 10
- 235000005881 Calendula officinalis Nutrition 0.000 claims abstract description 6
- UQSXHKLRYXJYBZ-UHFFFAOYSA-N Iron oxide Chemical compound [Fe]=O UQSXHKLRYXJYBZ-UHFFFAOYSA-N 0.000 claims description 24
- 239000002283 diesel fuel Substances 0.000 claims description 24
- 241000196324 Embryophyta Species 0.000 claims description 23
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 23
- 230000032683 aging Effects 0.000 claims description 22
- 238000010438 heat treatment Methods 0.000 claims description 22
- 238000007873 sieving Methods 0.000 claims description 22
- 239000002002 slurry Substances 0.000 claims description 21
- 238000002156 mixing Methods 0.000 claims description 20
- 239000004575 stone Substances 0.000 claims description 15
- 238000001816 cooling Methods 0.000 claims description 14
- 238000000227 grinding Methods 0.000 claims description 14
- 235000019738 Limestone Nutrition 0.000 claims description 13
- 235000008331 Pinus X rigitaeda Nutrition 0.000 claims description 13
- 235000011613 Pinus brutia Nutrition 0.000 claims description 13
- 241000018646 Pinus brutia Species 0.000 claims description 13
- 239000006028 limestone Substances 0.000 claims description 13
- 239000005995 Aluminium silicate Substances 0.000 claims description 12
- 244000302661 Phyllostachys pubescens Species 0.000 claims description 12
- 235000003570 Phyllostachys pubescens Nutrition 0.000 claims description 12
- 235000012211 aluminium silicate Nutrition 0.000 claims description 12
- NLYAJNPCOHFWQQ-UHFFFAOYSA-N kaolin Chemical compound O.O.O=[Al]O[Si](=O)O[Si](=O)O[Al]=O NLYAJNPCOHFWQQ-UHFFFAOYSA-N 0.000 claims description 12
- 229910001710 laterite Inorganic materials 0.000 claims description 11
- 239000011504 laterite Substances 0.000 claims description 11
- 238000003825 pressing Methods 0.000 claims description 10
- 238000007670 refining Methods 0.000 claims description 10
- 238000009966 trimming Methods 0.000 claims description 10
- KWYUFKZDYYNOTN-UHFFFAOYSA-M Potassium hydroxide Chemical compound [OH-].[K+] KWYUFKZDYYNOTN-UHFFFAOYSA-M 0.000 claims description 9
- 239000010433 feldspar Substances 0.000 claims description 9
- 229940072033 potash Drugs 0.000 claims description 9
- BWHMMNNQKKPAPP-UHFFFAOYSA-L potassium carbonate Substances [K+].[K+].[O-]C([O-])=O BWHMMNNQKKPAPP-UHFFFAOYSA-L 0.000 claims description 9
- 235000015320 potassium carbonate Nutrition 0.000 claims description 9
- 238000005520 cutting process Methods 0.000 claims description 5
- 238000010304 firing Methods 0.000 claims description 5
- DLHONNLASJQAHX-UHFFFAOYSA-N aluminum;potassium;oxygen(2-);silicon(4+) Chemical compound [O-2].[O-2].[O-2].[O-2].[O-2].[O-2].[O-2].[O-2].[Al+3].[Si+4].[Si+4].[Si+4].[K+] DLHONNLASJQAHX-UHFFFAOYSA-N 0.000 claims description 3
- 235000015895 biscuits Nutrition 0.000 claims description 3
- 238000000465 moulding Methods 0.000 claims description 3
- 240000000254 Agrostemma githago Species 0.000 claims description 2
- 235000009899 Agrostemma githago Nutrition 0.000 claims description 2
- 240000000785 Tagetes erecta Species 0.000 claims 1
- 244000269722 Thea sinensis Species 0.000 claims 1
- 240000001432 Calendula officinalis Species 0.000 abstract description 7
- BQCADISMDOOEFD-UHFFFAOYSA-N Silver Chemical compound [Ag] BQCADISMDOOEFD-UHFFFAOYSA-N 0.000 abstract description 4
- 229910052709 silver Inorganic materials 0.000 abstract description 4
- 239000004332 silver Substances 0.000 abstract description 4
- 239000003205 fragrance Substances 0.000 abstract description 2
- 239000011148 porous material Substances 0.000 abstract description 2
- 239000000758 substrate Substances 0.000 abstract description 2
- 239000002956 ash Substances 0.000 description 24
- 230000000052 comparative effect Effects 0.000 description 16
- 210000004209 hair Anatomy 0.000 description 11
- 238000004519 manufacturing process Methods 0.000 description 7
- 229910052573 porcelain Inorganic materials 0.000 description 3
- AJBZENLMTKDAEK-UHFFFAOYSA-N 3a,5a,5b,8,8,11a-hexamethyl-1-prop-1-en-2-yl-1,2,3,4,5,6,7,7a,9,10,11,11b,12,13,13a,13b-hexadecahydrocyclopenta[a]chrysene-4,9-diol Chemical compound CC12CCC(O)C(C)(C)C1CCC(C1(C)CC3O)(C)C2CCC1C1C3(C)CCC1C(=C)C AJBZENLMTKDAEK-UHFFFAOYSA-N 0.000 description 2
- 235000003880 Calendula Nutrition 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- RSWGJHLUYNHPMX-UHFFFAOYSA-N Abietic-Saeure Natural products C12CCC(C(C)C)=CC2=CCC2C1(C)CCCC2(C)C(O)=O RSWGJHLUYNHPMX-UHFFFAOYSA-N 0.000 description 1
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- KHPCPRHQVVSZAH-HUOMCSJISA-N Rosin Natural products O(C/C=C/c1ccccc1)[C@H]1[C@H](O)[C@@H](O)[C@@H](O)[C@@H](CO)O1 KHPCPRHQVVSZAH-HUOMCSJISA-N 0.000 description 1
- 230000003796 beauty Effects 0.000 description 1
- 239000000919 ceramic Substances 0.000 description 1
- 238000011156 evaluation Methods 0.000 description 1
- 239000002932 luster Substances 0.000 description 1
- 239000002689 soil Substances 0.000 description 1
- KHPCPRHQVVSZAH-UHFFFAOYSA-N trans-cinnamyl beta-D-glucopyranoside Natural products OC1C(O)C(O)C(CO)OC1OCC=CC1=CC=CC=C1 KHPCPRHQVVSZAH-UHFFFAOYSA-N 0.000 description 1
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B33/00—Clay-wares
- C04B33/02—Preparing or treating the raw materials individually or as batches
- C04B33/04—Clay; Kaolin
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C8/00—Enamels; Glazes; Fusion seal compositions being frit compositions having non-frit additions
- C03C8/14—Glass frit mixtures having non-frit additions, e.g. opacifiers, colorants, mill-additions
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
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- C04B33/00—Clay-wares
- C04B33/32—Burning methods
- C04B33/34—Burning methods combined with glazing
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- C04B41/00—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone
- C04B41/45—Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements
- C04B41/50—Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements with inorganic materials
- C04B41/5022—Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements with inorganic materials with vitreous materials
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- C04B41/00—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone
- C04B41/80—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone of only ceramics
- C04B41/81—Coating or impregnation
- C04B41/85—Coating or impregnation with inorganic materials
- C04B41/86—Glazes; Cold glazes
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- C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
- C04B2235/65—Aspects relating to heat treatments of ceramic bodies such as green ceramics or pre-sintered ceramics, e.g. burning, sintering or melting processes
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- C04B2235/65—Aspects relating to heat treatments of ceramic bodies such as green ceramics or pre-sintered ceramics, e.g. burning, sintering or melting processes
- C04B2235/656—Aspects relating to heat treatments of ceramic bodies such as green ceramics or pre-sintered ceramics, e.g. burning, sintering or melting processes characterised by specific heating conditions during heat treatment
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- C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
- C04B2235/65—Aspects relating to heat treatments of ceramic bodies such as green ceramics or pre-sintered ceramics, e.g. burning, sintering or melting processes
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Abstract
The invention relates to a red feather Jianzhan and a preparation process thereof. Specifically, the invention provides a preparation process of red feather Jianzhan, which comprises the following steps: preparing a blank body and glaze slip, applying the glaze slip to the blank body, and roasting the glazed blank body to obtain the red feather pot-marigold. The red feather cup-building prepared by the process has orange yellow mouth edge, red main body, thin and clear nano-filaments, compactness, uniformity, strong layering sense, and the nano-filaments at the joint with the main body edge are mostly silver gray, and the nano-filaments at the joint with the mouth edge are yellow, so that the red feather cup-building glaze is moist, fresh and alive in mimicry and unique in brilliant fragrance, and has rich and elegant glaze color and deep artistic background and charm as the substrate with moist and generous texture is hidden, and in addition, the red feather cup-building glaze has no spots, no pores and good quality, so that the red feather cup-building has elegant art and collection values.
Description
Technical Field
The invention relates to the technical field of porcelain, in particular to a red feather Jianzhan and a preparation process thereof.
Background
The cup is deeply loved by people, the cup is ancient in shape, the glaze color is changeable and measured, the cup is bright and colorful, the cup is famous due to the excellent artistic level, the cup is a bright pearl in the ceramic history, and compared with other porcelain, the cup has unique beauty and is still fashionable after thousands of years.
However, the firing difficulty of the built cup is high, the selection of a formula, a firing atmosphere and a temperature is difficult to master, the improper selection of a preparation process causes a plurality of problems of the prepared built cup, such as glaze bubbles and plaques, and the fired built cup is dull and dim in color, fuzzy in hair, poor in texture and the like, so that the preparation of the built cup fails.
With the continuous improvement of appreciation and artistic level, the demand for the cup building with beautiful appearance is higher and higher, and how to fire a cup building with beautiful appearance to improve the artistic and collection values of the cup building becomes a hot spot of the current porcelain world research.
Therefore, there is a need in the art to develop a cup that has an elegant appearance, artistic and collectable value.
Disclosure of Invention
The invention aims to provide a red feather Jian calendula with excellent appearance and a preparation process thereof, so that the artistic and collection values of the Jian calendula are improved.
In order to achieve the purpose, the invention adopts the following technical scheme:
the first aspect of the invention provides a preparation process of red feather Jianzhan, which comprises the following steps:
(1) mixing 5-7 parts by weight of laterite and 3-5 parts by weight of kaolin, crushing, adding water for elutriation, sieving by a sieve of 60-100 meshes, performing filter pressing, refining mud and ageing to obtain blank mud; performing blank drawing and forming on the blank mud, trimming, biscuiting at 780-820 ℃ for 14-18h, and taking out to obtain a blank body;
(2) mixing 3-5 parts by weight of moso bamboo and 1.5-2.5 parts by weight of pine, burning, and collecting ash to obtain plant ash;
(3) grinding 3-5 parts by weight of glaze stone, 0.6-1.0 part by weight of potassium feldspar, 0.2-0.6 part by weight of limestone, 0.1-0.2 part by weight of iron oxide red, 0.06-0.14 part by weight of plant ash prepared in the step (2) and 4-5 parts by weight of water, sieving by a 80-120-mesh sieve, and ageing for 1.5-2.5 days to obtain glaze slurry;
(4) applying the glaze slurry prepared in the step (3) to the blank prepared in the step (1) to obtain a glazed blank with the glazing thickness of 0.4-0.8 mm;
(5) and (3) roasting the glazed green body obtained in the step (4) in an electric kiln, wherein the roasting comprises the following steps:
raising the temperature of the furnace from normal temperature to 980-minus 1020 ℃ at the rate of 230-minus one DEG C/h, raising the temperature from 980-minus one DEG C to 1160-minus one DEG C at the rate of 50-70 ℃/h, raising the temperature from 1160-minus one DEG C to 1280-minus one DEG C at the rate of 30-50 ℃/h, keeping the temperature at 1280-minus one DEG C for 2.5-3.5h, then throwing the diesel into the electric furnace once every 10-14min for 6 times, throwing the amount of 640-minus one DEG G for every cubic meter of electric furnace space into the diesel each time, after the diesel is thrown, lowering the temperature from 1280-minus one DEG C to 980-minus one DEG C at the rate of 100-minus one DEG C/h, then throwing the amount of 360-minus one G for 1 time into the electric furnace space into the electric furnace, after the diesel is thrown, opening the furnace door, cutting off the power of the electric furnace, when the furnace temperature is reduced to 720 ℃ plus 680 ℃., the furnace door is closed, the electric kiln furnace is electrified, the furnace temperature is increased from 720 ℃ plus 680 ℃ to 1070 ℃ plus 1030 ℃ at the rate of 300 ℃/h plus 260 ℃., then the furnace door is opened, the electric kiln furnace is powered off, the furnace temperature is reduced to the normal temperature, and the red feather building cup is obtained.
In a preferred embodiment of the present invention, the process comprises the following steps:
(1) mixing 5.5-6.5 parts by weight of laterite and 3.5-4.5 parts by weight of kaolin, crushing, adding water for elutriation, sieving by a 80-mesh sieve, performing filter pressing, refining mud and ageing to obtain blank mud; performing blank drawing and molding on the blank mud, trimming, biscuiting for 15-17h at 790-810 ℃, and taking out to obtain a blank body;
(2) mixing 3.8-4.2 parts by weight of moso bamboo and 1.8-2.2 parts by weight of pine, burning, and collecting ash to obtain plant ash;
(3) grinding 3.8-4.2 parts by weight of glaze stone, 0.7-0.9 part by weight of potash feldspar, 0.3-0.5 part by weight of limestone, 0.13-0.17 part by weight of iron oxide red, 0.08-0.12 part by weight of plant ash prepared in the step (2) and 4.2-4.8 parts by weight of water, sieving by a 100-mesh sieve, and ageing for 1.8-2.2 days to obtain glaze slurry;
(4) applying the glaze slurry prepared in the step (3) to the blank prepared in the step (1) to obtain a glazed blank with the glazing thickness of 0.5-0.7 mm;
(5) and (3) roasting the glazed green body obtained in the step (4) in an electric kiln, wherein the roasting comprises the following steps:
raising the temperature of the furnace from normal temperature to 990-, when the furnace temperature is reduced to 690-plus-710 ℃, the furnace door is closed, the electric furnace is electrified, the furnace temperature is increased from 690-plus-710 ℃ to 1040-plus-1060 ℃ at the rate of 270-plus-290 ℃/h, then the furnace door is opened, the electric furnace is powered off, the furnace temperature is reduced to the normal temperature, and the red feather building cup is obtained.
In a preferred embodiment of the present invention, the process comprises the following steps:
(1) mixing 6 parts by weight of laterite and 4 parts by weight of kaolin, crushing, adding water for elutriation, sieving by a 80-mesh sieve, performing filter pressing, refining mud and ageing to obtain blank mud; the blank mud is subjected to blank drawing, forming and trimming, biscuit firing is carried out for 16h at 800 ℃, and a blank body is obtained after the blank mud is taken out;
(2) mixing 4 parts by weight of moso bamboo and 2 parts by weight of pine, burning, and collecting ash to obtain plant ash;
(3) grinding 4 parts by weight of glaze stone, 0.8 part by weight of potash feldspar, 0.4 part by weight of limestone, 0.15 part by weight of iron oxide red, 0.1 part by weight of plant ash prepared in the step (2) and 4.5 parts by weight of water, sieving by a 100-mesh sieve, and ageing for 2 days to obtain glaze slurry;
(4) applying the glaze slurry prepared in the step (3) to the blank prepared in the step (1) to obtain a glazed blank with the glazing thickness of 0.6 mm;
(5) and (3) roasting the glazed green body obtained in the step (4) in an electric kiln, wherein the roasting comprises the following steps:
heating the furnace temperature from normal temperature to 1000 ℃ at the rate of 250 ℃/h, heating from 1000 ℃ to 1180 ℃ at the rate of 60 ℃/h, heating from 1180 ℃ to 1300 ℃ at the rate of 40 ℃/h, continuously keeping the temperature of 1300 ℃ for 3h, then adding the diesel oil into the electric kiln, adding the diesel oil once every 12min for 6 times, adding 660g of the diesel oil into each cubic meter of electric kiln space, after the diesel oil is completely added, cooling the furnace temperature from 1300 ℃ to 1005 ℃ at the rate of 120 ℃/h, then adding 1g of the diesel oil into each cubic meter of electric kiln space, after the diesel oil is completely added, opening the furnace door, powering off the electric kiln, when the furnace temperature is cooled to 700 ℃, closing the furnace door, powering on the electric kiln, heating the furnace temperature from 700 ℃ to 1050 ℃ at the rate of 280 ℃/h, then opening the furnace door, powering off the electric kiln, cooling the furnace temperature to normal temperature, to obtain the red feather Jianzhan.
In a preferred embodiment of the present invention, in the step (2), the moso bamboo is sun-dried moso bamboo.
In a preferred embodiment of the present invention, in the step (2), the pine is sun-dried pine.
In a preferred embodiment of the present invention, in the step (3), the grinding is performed in a ball mill.
In a preferred embodiment of the present invention, in the step (3), the glaze stone, potash feldspar, limestone, iron oxide red, plant ash and water are put into a ball mill for grinding.
In a preferred embodiment of the present invention, the normal temperature is 18-22 ℃, preferably 20 ℃.
In a preferred embodiment of the present invention, in the step (5), the temperature reduction after opening the oven door is a natural temperature reduction.
In a preferred embodiment of the invention, the glaze stone is from southern Lincun of Jianyang area of Nanping city of Fujian province.
In a preferred embodiment of the invention, the red soil is from the Shuizhiji town of Jianyang city of south Ping city, Fujian province.
In a preferred embodiment of the present invention, the kaolin is from Jianyang district Shuijing of Nanping city, Fujian province.
In a second aspect, the invention provides a red feather cockle prepared by the process of the first aspect of the invention.
In a preferred embodiment of the invention, the red feather marigold is shown in the attached figures 1, 2 and 3 in the specification.
Within the scope of the present invention, the above-mentioned technical features of the present invention and those specifically described hereinafter may be combined with each other to constitute new or preferred technical solutions.
Drawings
FIG. 1 shows Red feather Jianzhan prepared in example 1 of the present invention.
FIG. 2 shows Red feather Jianzhan prepared in example 1 of the present invention.
FIG. 3 shows the red feather Jianzhan prepared in example 1 of the present invention.
Detailed Description
The red feather cup has orange yellow color at the edge, red main body, fine and clear, dense, clear and uniform hairs, strong layering, and the hairs at the joint with the main body edge are mostly silver gray, and the hairs at the joint with the edge are yellow, so that the glaze of the red feather cup is moist, fresh and vivid in mimicry, and unique and gorgeous in character, like a substrate with moist everything in the house, and has rich and elegant glaze color and deep artistic background and charm.
Term(s) for
As used herein, the terms "comprising," "including," and "containing" are used interchangeably and include not only open-ended definitions, but also semi-closed and closed-ended definitions. In other words, the term includes "consisting of … …", "consisting essentially of … …".
In the invention, the firewood is pine root rich in rosin and can be vigorously combusted.
As used herein, the term "part by weight" can be any fixed weight expressed in milligrams, grams, or kilograms (e.g., 1mg, 1g, or 1kg, etc.). For example, in a combination of 1 part by weight of component a and 9 parts by weight of component b, 1g of component a +9 g of component b, or 10 g of component a +90 g of component b, etc. may be used. In the combinations described, the percentage content of a certain component is (weight part of this component/sum of weight parts of all components) × 100%, so that in a composition consisting of 1 part by weight of component a and 9 parts by weight of component b, the content of component a is 10% and the content of component b is 90%.
Red feather Jianzhan and preparation process thereof
The invention provides a red feather Jianzhan and a preparation process thereof, and the red feather Jianzhan prepared by the process has attractive appearance and collection value. Preferably, the red feather marigold of the invention is shown in fig. 1, fig. 2 and fig. 3.
In a preferred embodiment of the present invention, a process for preparing red feather Jianzhan is provided, which comprises the following steps:
(1) mixing 5-7 parts by weight of laterite and 3-5 parts by weight of kaolin, crushing, adding water for elutriation, sieving by a sieve of 60-100 meshes, performing filter pressing, refining mud and ageing to obtain blank mud; performing blank drawing and forming on the blank mud, trimming, biscuiting at 780-820 ℃ for 14-18h, and taking out to obtain a blank body;
(2) mixing 3-5 parts by weight of moso bamboo and 1.5-2.5 parts by weight of pine, burning, and collecting ash to obtain plant ash;
(3) grinding 3-5 parts by weight of glaze stone, 0.6-1.0 part by weight of potassium feldspar, 0.2-0.6 part by weight of limestone, 0.1-0.2 part by weight of iron oxide red, 0.06-0.14 part by weight of plant ash prepared in the step (2) and 4-5 parts by weight of water, sieving by a 80-120-mesh sieve, and ageing for 1.5-2.5 days to obtain glaze slurry;
(4) applying the glaze slurry prepared in the step (3) to the blank prepared in the step (1) to obtain a glazed blank with the glazing thickness of 0.4-0.8 mm;
(5) and (3) roasting the glazed green body obtained in the step (4) in an electric kiln, wherein the roasting comprises the following steps:
raising the temperature of the furnace from normal temperature to 980-minus 1020 ℃ at the rate of 230-minus one DEG C/h, raising the temperature from 980-minus one DEG C to 1160-minus one DEG C at the rate of 50-70 ℃/h, raising the temperature from 1160-minus one DEG C to 1280-minus one DEG C at the rate of 30-50 ℃/h, keeping the temperature at 1280-minus one DEG C for 2.5-3.5h, then throwing the diesel into the electric furnace once every 10-14min for 6 times, throwing the amount of 640-minus one DEG G for every cubic meter of electric furnace space into the diesel each time, after the diesel is thrown, lowering the temperature from 1280-minus one DEG C to 980-minus one DEG C at the rate of 100-minus one DEG C/h, then throwing the amount of 360-minus one G for 1 time into the electric furnace space into the electric furnace, after the diesel is thrown, opening the furnace door, cutting off the power of the electric furnace, when the furnace temperature is reduced to 720 ℃ plus 680 ℃., the furnace door is closed, the electric kiln furnace is electrified, the furnace temperature is increased from 720 ℃ plus 680 ℃ to 1070 ℃ plus 1030 ℃ at the rate of 300 ℃/h plus 260 ℃., then the furnace door is opened, the electric kiln furnace is powered off, the furnace temperature is reduced to the normal temperature, and the red feather building cup is obtained.
In a preferred embodiment of the present invention, a process for preparing red feather Jianzhan is provided, which comprises the following steps:
(1) mixing 5.5-6.5 parts by weight of laterite and 3.5-4.5 parts by weight of kaolin, crushing, adding water for elutriation, sieving by a 80-mesh sieve, performing filter pressing, refining mud and ageing to obtain blank mud; performing blank drawing and molding on the blank mud, trimming, biscuiting for 15-17h at 790-810 ℃, and taking out to obtain a blank body;
(2) mixing 3.8-4.2 parts by weight of moso bamboo and 1.8-2.2 parts by weight of pine, burning, and collecting ash to obtain plant ash;
(3) grinding 3.8-4.2 parts by weight of glaze stone, 0.7-0.9 part by weight of potash feldspar, 0.3-0.5 part by weight of limestone, 0.13-0.17 part by weight of iron oxide red, 0.08-0.12 part by weight of plant ash prepared in the step (2) and 4.2-4.8 parts by weight of water, sieving by a 100-mesh sieve, and ageing for 1.8-2.2 days to obtain glaze slurry;
(4) applying the glaze slurry prepared in the step (3) to the blank prepared in the step (1) to obtain a glazed blank with the glazing thickness of 0.5-0.7 mm;
(5) and (3) roasting the glazed green body obtained in the step (4) in an electric kiln, wherein the roasting comprises the following steps:
raising the temperature of the furnace from normal temperature to 990-, when the furnace temperature is reduced to 690-plus-710 ℃, the furnace door is closed, the electric furnace is electrified, the furnace temperature is increased from 690-plus-710 ℃ to 1040-plus-1060 ℃ at the rate of 270-plus-290 ℃/h, then the furnace door is opened, the electric furnace is powered off, the furnace temperature is reduced to the normal temperature, and the red feather building cup is obtained.
In a preferred embodiment of the present invention, the preparation process of the red feather Jianzhan comprises the following steps:
(1) mixing 6 parts by weight of laterite and 4 parts by weight of kaolin, crushing, adding water for elutriation, sieving by a 80-mesh sieve, performing filter pressing, refining mud and ageing to obtain blank mud; the blank mud is subjected to blank drawing, forming and trimming, biscuit firing is carried out for 16h at 800 ℃, and a blank body is obtained after the blank mud is taken out;
(2) mixing 4 parts by weight of moso bamboo and 2 parts by weight of pine, burning, and collecting ash to obtain plant ash;
(3) grinding 4 parts by weight of glaze stone, 0.8 part by weight of potash feldspar, 0.4 part by weight of limestone, 0.15 part by weight of iron oxide red, 0.1 part by weight of plant ash prepared in the step (2) and 4.5 parts by weight of water, sieving by a 100-mesh sieve, and ageing for 2 days to obtain glaze slurry;
(4) applying the glaze slurry prepared in the step (3) to the blank prepared in the step (1) to obtain a glazed blank with the glazing thickness of 0.6 mm;
(5) and (3) roasting the glazed green body obtained in the step (4) in an electric kiln, wherein the roasting comprises the following steps:
heating the furnace temperature from normal temperature to 1000 ℃ at the rate of 250 ℃/h, heating from 1000 ℃ to 1180 ℃ at the rate of 60 ℃/h, heating from 1180 ℃ to 1300 ℃ at the rate of 40 ℃/h, continuously keeping the temperature of 1300 ℃ for 3h, then adding the diesel oil into the electric kiln, adding the diesel oil once every 12min for 6 times, adding 660g of the diesel oil into each cubic meter of electric kiln space, after the diesel oil is completely added, cooling the furnace temperature from 1300 ℃ to 1005 ℃ at the rate of 120 ℃/h, then adding 1g of the diesel oil into each cubic meter of electric kiln space, after the diesel oil is completely added, opening the furnace door, powering off the electric kiln, when the furnace temperature is cooled to 700 ℃, closing the furnace door, powering on the electric kiln, heating the furnace temperature from 700 ℃ to 1050 ℃ at the rate of 280 ℃/h, then opening the furnace door, powering off the electric kiln, cooling the furnace temperature to normal temperature, to obtain the red feather Jianzhan.
In a preferred embodiment of the present invention, the preparation process of the red feather marigold is the same as that described in embodiment 1 of the present invention.
In a preferred embodiment of the invention, the red feather marigold is shown in the attached figures 1, 2 and 3 in the specification.
The main excellent effects of the invention include:
the red feather cup with beautiful appearance and artistic value has orange yellow edge, red main body, fine and clear hairs, dense and clear hairs and strong layering, and the hairs in the joint with the main body edge are silver grey while the hairs in the joint with the main body edge are yellow.
The invention will be further illustrated with reference to the following specific examples. It should be understood that the following specific examples are provided to illustrate the detailed embodiments and specific procedures, but the scope of the present invention is not limited to these examples.
Examples and comparative examples
The glaze stone is from Nanlincun of Jianyang region of Nanping city of Fujian province; the laterite is from Jianyang district Jizhen in Nanping City of Fujian province; kaolin is from Jianyang district Jizhen in Nanping city, Fujian province.
Example 1 Red feather Jianzhan
The preparation method of the red feather Jianzhan comprises the following steps:
(1) mixing 6 parts by weight of laterite and 4 parts by weight of kaolin, crushing, adding water for elutriation, sieving by a 80-mesh sieve, performing filter pressing, refining mud and ageing to obtain blank mud; and (3) performing blank drawing and forming on the blank mud, trimming, biscuiting for 16h at 800 ℃, and taking out to obtain a blank body.
(2) Mixing 4 parts by weight of dried moso bamboo with 2 parts by weight of dried pine, burning, and collecting ashes to obtain plant ash.
(3) Putting 4 parts by weight of glaze stone, 0.8 part by weight of potash feldspar, 0.4 part by weight of limestone, 0.15 part by weight of iron oxide red, 0.1 part by weight of plant ash prepared in the step (2) and 4.5 parts by weight of water into a ball mill for grinding, sieving with a 100-mesh sieve, and ageing for 2 days to obtain the glaze slurry.
(4) And (4) applying the glaze slip prepared in the step (3) to the blank prepared in the step (1) to obtain a glazed blank with the glazing thickness of 0.6 mm.
(5) And (3) roasting the glazed green body obtained in the step (4) in an electric kiln, wherein the roasting comprises the following steps:
heating the furnace temperature from 20 ℃ to 1000 ℃ at the rate of 250 ℃/h, heating from 1000 ℃ to 1180 ℃ at the rate of 60 ℃/h, heating from 1180 ℃ to 1300 ℃ at the rate of 40 ℃/h, continuously keeping the temperature of 1300 ℃ for 3h, then adding diesel oil into the electric kiln, adding the diesel oil once every 12min for 6 times, adding 660g of diesel oil into each cubic meter of electric kiln space, cooling the furnace temperature from 1300 ℃ to 1005 ℃ at the rate of 120 ℃/h after the diesel oil is added, then adding 1g of diesel oil into the electric kiln according to each cubic meter of electric kiln space, opening the furnace door after the diesel oil is added, powering off the electric kiln, naturally cooling the furnace temperature to 700 ℃, closing the furnace door, powering on the electric kiln, heating the furnace temperature from 700 ℃ to 1050 ℃ at the rate of 280 ℃/h, opening the furnace door, powering off the electric kiln, naturally cooling the furnace temperature to 20 ℃, to obtain the red feather Jianzhan.
Evaluation of the effects:
the cup prepared in the embodiment 1 is a red feather cup, as shown in fig. 1, fig. 2 and fig. 3, the edge of the red feather cup is orange yellow, the main body is red, the hairs are thin and clear, dense, clear and uniform, the layering is strong, the hairs at the joint of the edge of the main body are mostly silver gray, and the hairs at the joint of the edge of the mouth are yellow, so that the luster, the mimicry, fresh and lively, and magnificent characteristics and unique and brilliant fragrance of the red feather cup are shown, and the red feather cup has rich and elegant glaze color and deep artistic background and charm, and in addition, the red feather cup has the advantages of no spots, no air holes and good texture, so that the red feather cup has elegant art and collection values.
Comparative example 1
The process for preparing the cup of the comparative example 1 is the same as that of the example 1, except that: and (3):
putting 4 parts by weight of glaze stone, 0.8 part by weight of potash feldspar, 0.4 part by weight of limestone, 0.1 part by weight of plant ash prepared in the step (2) and 4.5 parts by weight of water into a ball mill for grinding, sieving by a 100-mesh sieve, and ageing for 2 days to obtain the glaze slurry.
The glaze of the cup built prepared in the comparative example 1 is lack of red and yellow background, and is dull, lusterless and poor in texture.
Comparative example 2
The process for preparing the cup of the comparative example 2 is the same as that of the example 1, except that: and (3):
putting 4 parts by weight of glaze stone, 0.4 part by weight of limestone, 0.15 part by weight of iron oxide red, 0.1 part by weight of plant ash prepared in the step (2) and 4.5 parts by weight of water into a ball mill for grinding, sieving by a 100-mesh sieve, and ageing for 2 days to obtain the glaze slurry.
The glaze of the cup prepared in the comparative example 2 is dull, lusterless and fuzzy, and has patches and poor texture.
Comparative example 3
The process for preparing the cup of the comparative example 3 is the same as that of the example 1, except that: and (5) roasting the glazed green body obtained in the step (4) in an electric kiln, wherein the roasting comprises the following steps:
heating the furnace temperature from 20 ℃ to 1000 ℃ at the rate of 250 ℃/h, heating from 1000 ℃ to 1180 ℃ at the rate of 60 ℃/h, heating from 1180 ℃ to 1300 ℃ at the rate of 40 ℃/h, continuously preserving heat at 1300 ℃ for 3h, then adding firewood into the electric kiln, adding the firewood once every 12min for 6 times, adding 660g of firewood into each cubic meter of space of the electric kiln, opening a furnace door after the firewood is added, and naturally cooling the furnace temperature to 20 ℃ and normal temperature to obtain the building cup.
The glaze of the cup prepared in the comparative example 3 has patches, pores, dull and rough color and poor texture.
Comparative example 4
The process for preparing the cup of the comparative example 4 is the same as that of the example 1, except that: and (5) roasting the glazed green body obtained in the step (4) in an electric kiln, wherein the roasting comprises the following steps:
heating the furnace temperature from 20 ℃ to 1000 ℃ at the rate of 250 ℃/h, heating from 1000 ℃ to 1180 ℃ at the rate of 60 ℃/h, heating from 1180 ℃ to 1300 ℃ at the rate of 40 ℃/h, continuously keeping the temperature at 1300 ℃ for 3h, then adding firewood into the electric kiln, adding the firewood once every 12min for 6 times, adding 660g of firewood into each cubic meter of electric kiln space, after the firewood is completely added, cooling the furnace temperature from 1300 ℃ to 1005 ℃ at the rate of 120 ℃/h, then adding 1g of firewood into each cubic meter of electric kiln space, opening a furnace door after the firewood is completely added, and naturally cooling the furnace temperature to 20 ℃ and normal temperature to obtain the building block.
The glaze of the cup prepared in the comparative example 4 is dull and lackluster, fuzzy in texture, rough and poor in texture.
Comparative example 5
The process for preparing the cup of the comparative example 5 is the same as that of the example 1, except that: and (5) roasting the glazed green body obtained in the step (4) in an electric kiln, wherein the roasting comprises the following steps:
the furnace temperature is increased from 20 ℃ to 1000 ℃ at the rate of 250 ℃/h, then is increased from 1000 ℃ to 1180 ℃ at the rate of 60 ℃/h, and is increased from 1180 ℃ to 1300 ℃ at the rate of 40 ℃/h, then throwing the firewood into the electric kiln once every 12min for 6 times, throwing 660g of the firewood into each cubic meter of space of the electric kiln every time, after the firewood is thrown, the furnace temperature is reduced from 1300 ℃ to 1005 ℃ at the speed of 120 ℃/h, then adding the firewood oil for 1 time according to the amount of 380g per cubic meter of the electric kiln space into the electric kiln, opening the furnace door after the firewood oil is added, cutting off the power of the electric kiln, naturally cooling the furnace temperature to 700 ℃, closing the furnace door, electrifying the electric furnace, raising the furnace temperature from 700 ℃ to 1050 ℃ at the speed of 280 ℃/h, and then opening the furnace door, cutting off the power of the electric kiln, and naturally cooling the furnace temperature to 20 ℃ and normal temperature to obtain the building cup.
The glaze of the cup prepared in the comparative example 5 has patches, dull glaze, fuzzy texture and poor texture.
While the invention has been described in terms of a preferred embodiment, it will be understood by those skilled in the art that various changes in form and detail may be made without departing from the spirit and scope of the invention.
Claims (5)
1. A preparation process of Jianzhuijian tea is characterized by comprising the following steps:
(1) mixing 5-7 parts by weight of laterite and 3-5 parts by weight of kaolin, crushing, adding water for elutriation, sieving by a sieve of 60-100 meshes, performing filter pressing, refining mud and ageing to obtain blank mud; performing blank drawing and forming on the blank mud, trimming, biscuiting at 780-820 ℃ for 14-18h, and taking out to obtain a blank body;
(2) mixing 3-5 parts by weight of moso bamboo and 1.5-2.5 parts by weight of pine, burning, and collecting ash to obtain plant ash;
(3) grinding 3-5 parts by weight of glaze stone, 0.6-1.0 part by weight of potassium feldspar, 0.2-0.6 part by weight of limestone, 0.1-0.2 part by weight of iron oxide red, 0.06-0.14 part by weight of plant ash prepared in the step (2) and 4-5 parts by weight of water, sieving by a 80-120-mesh sieve, and ageing for 1.5-2.5 days to obtain glaze slurry;
(4) applying the glaze slurry prepared in the step (3) to the blank prepared in the step (1) to obtain a glazed blank with the glazing thickness of 0.4-0.8 mm;
(5) and (3) roasting the glazed green body obtained in the step (4) in an electric kiln, wherein the roasting comprises the following steps:
raising the temperature of the furnace from normal temperature to 980-minus 1020 ℃ at the rate of 230-minus one DEG C/h, raising the temperature from 980-minus one DEG C to 1160-minus one DEG C at the rate of 50-70 ℃/h, raising the temperature from 1160-minus one DEG C to 1280-minus one DEG C at the rate of 30-50 ℃/h, keeping the temperature at 1280-minus one DEG C for 2.5-3.5h, then throwing the diesel into the electric furnace once every 10-14min for 6 times, throwing the amount of 640-minus one DEG G for every cubic meter of electric furnace space into the diesel each time, after the diesel is thrown, lowering the temperature from 1280-minus one DEG C to 980-minus one DEG C at the rate of 100-minus one DEG C/h, then throwing the amount of 360-minus one G for 1 time into the electric furnace space into the electric furnace, after the diesel is thrown, opening the furnace door, cutting off the power of the electric furnace, when the furnace temperature is reduced to 720 ℃ plus 680 ℃., the furnace door is closed, the electric kiln furnace is electrified, the furnace temperature is increased from 720 ℃ plus 680 ℃ to 1070 ℃ plus 1030 ℃ at the rate of 300 ℃/h plus 260 ℃., then the furnace door is opened, the electric kiln furnace is powered off, the furnace temperature is reduced to the normal temperature, and the red feather building cup is obtained.
2. The process according to claim 1, characterized in that it comprises the following steps:
(1) mixing 5.5-6.5 parts by weight of laterite and 3.5-4.5 parts by weight of kaolin, crushing, adding water for elutriation, sieving by a 80-mesh sieve, performing filter pressing, refining mud and ageing to obtain blank mud; performing blank drawing and molding on the blank mud, trimming, biscuiting for 15-17h at 790-810 ℃, and taking out to obtain a blank body;
(2) mixing 3.8-4.2 parts by weight of moso bamboo and 1.8-2.2 parts by weight of pine, burning, and collecting ash to obtain plant ash;
(3) grinding 3.8-4.2 parts by weight of glaze stone, 0.7-0.9 part by weight of potash feldspar, 0.3-0.5 part by weight of limestone, 0.13-0.17 part by weight of iron oxide red, 0.08-0.12 part by weight of plant ash prepared in the step (2) and 4.2-4.8 parts by weight of water, sieving by a 100-mesh sieve, and ageing for 1.8-2.2 days to obtain glaze slurry;
(4) applying the glaze slurry prepared in the step (3) to the blank prepared in the step (1) to obtain a glazed blank with the glazing thickness of 0.5-0.7 mm;
(5) and (3) roasting the glazed green body obtained in the step (4) in an electric kiln, wherein the roasting comprises the following steps:
raising the temperature of the furnace from normal temperature to 990-, when the furnace temperature is reduced to 690-plus-710 ℃, the furnace door is closed, the electric furnace is electrified, the furnace temperature is increased from 690-plus-710 ℃ to 1040-plus-1060 ℃ at the rate of 270-plus-290 ℃/h, then the furnace door is opened, the electric furnace is powered off, the furnace temperature is reduced to the normal temperature, and the red feather building cup is obtained.
3. The process according to claim 1, characterized in that it comprises the following steps:
(1) mixing 6 parts by weight of laterite and 4 parts by weight of kaolin, crushing, adding water for elutriation, sieving by a 80-mesh sieve, performing filter pressing, refining mud and ageing to obtain blank mud; the blank mud is subjected to blank drawing, forming and trimming, biscuit firing is carried out for 16h at 800 ℃, and a blank body is obtained after the blank mud is taken out;
(2) mixing 4 parts by weight of moso bamboo and 2 parts by weight of pine, burning, and collecting ash to obtain plant ash;
(3) grinding 4 parts by weight of glaze stone, 0.8 part by weight of potash feldspar, 0.4 part by weight of limestone, 0.15 part by weight of iron oxide red, 0.1 part by weight of plant ash prepared in the step (2) and 4.5 parts by weight of water, sieving by a 100-mesh sieve, and ageing for 2 days to obtain glaze slurry;
(4) applying the glaze slurry prepared in the step (3) to the blank prepared in the step (1) to obtain a glazed blank with the glazing thickness of 0.6 mm;
(5) and (3) roasting the glazed green body obtained in the step (4) in an electric kiln, wherein the roasting comprises the following steps:
heating the furnace temperature from normal temperature to 1000 ℃ at the rate of 250 ℃/h, heating from 1000 ℃ to 1180 ℃ at the rate of 60 ℃/h, heating from 1180 ℃ to 1300 ℃ at the rate of 40 ℃/h, continuously keeping the temperature of 1300 ℃ for 3h, then adding the diesel oil into the electric kiln, adding the diesel oil once every 12min for 6 times, adding 660g of the diesel oil into each cubic meter of electric kiln space, after the diesel oil is completely added, cooling the furnace temperature from 1300 ℃ to 1005 ℃ at the rate of 120 ℃/h, then adding 1g of the diesel oil into each cubic meter of electric kiln space, after the diesel oil is completely added, opening the furnace door, powering off the electric kiln, when the furnace temperature is cooled to 700 ℃, closing the furnace door, powering on the electric kiln, heating the furnace temperature from 700 ℃ to 1050 ℃ at the rate of 280 ℃/h, then opening the furnace door, powering off the electric kiln, cooling the furnace temperature to normal temperature, to obtain the red feather Jianzhan.
4. The process of claim 1, wherein the red feather marigold is as shown in the accompanying fig. 1, fig. 2 and fig. 3 of the specification.
5. A red feather cockle, which is prepared by the process as claimed in claim 1.
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| CN202110914159.4A CN113548867A (en) | 2021-08-10 | 2021-08-10 | Red feather Jianzhan and preparation process thereof |
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113800883A (en) * | 2021-11-08 | 2021-12-17 | 许家有 | Blue rabbit hair building cup |
| CN113880549A (en) * | 2021-11-08 | 2022-01-04 | 廖珍琴 | Hu blue cup |
| CN113979721A (en) * | 2021-11-11 | 2022-01-28 | 黄德兴 | Colorful building cup |
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2021
- 2021-08-10 CN CN202110914159.4A patent/CN113548867A/en not_active Withdrawn
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113800883A (en) * | 2021-11-08 | 2021-12-17 | 许家有 | Blue rabbit hair building cup |
| CN113880549A (en) * | 2021-11-08 | 2022-01-04 | 廖珍琴 | Hu blue cup |
| CN113800883B (en) * | 2021-11-08 | 2023-12-19 | 南平市建阳区许家有建盏陶瓷有限公司 | Blue rabbit milli-building cup |
| CN113979721A (en) * | 2021-11-11 | 2022-01-28 | 黄德兴 | Colorful building cup |
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