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CN113318094A - Silicone gel patch containing plant herbal components and manufacturing method thereof - Google Patents

Silicone gel patch containing plant herbal components and manufacturing method thereof Download PDF

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Publication number
CN113318094A
CN113318094A CN202110499704.8A CN202110499704A CN113318094A CN 113318094 A CN113318094 A CN 113318094A CN 202110499704 A CN202110499704 A CN 202110499704A CN 113318094 A CN113318094 A CN 113318094A
Authority
CN
China
Prior art keywords
silicone gel
herbal
components
plant
gel patch
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN202110499704.8A
Other languages
Chinese (zh)
Inventor
李国明
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Guangzhou Beihao Medical Technology Co ltd
Original Assignee
Guangzhou Beihao Medical Technology Co ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Guangzhou Beihao Medical Technology Co ltd filed Critical Guangzhou Beihao Medical Technology Co ltd
Priority to CN202110499704.8A priority Critical patent/CN113318094A/en
Publication of CN113318094A publication Critical patent/CN113318094A/en
Pending legal-status Critical Current

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    • A61K9/00—Medicinal preparations characterised by special physical form
    • A61K9/70—Web, sheet or filament bases ; Films; Fibres of the matrix type containing drug
    • A61K9/7023—Transdermal patches and similar drug-containing composite devices, e.g. cataplasms
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K31/00—Medicinal preparations containing organic active ingredients
    • A61K31/045—Hydroxy compounds, e.g. alcohols; Salts thereof, e.g. alcoholates
    • A—HUMAN NECESSITIES
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    • A61K31/74—Synthetic polymeric materials
    • A61K31/80—Polymers containing hetero atoms not provided for in groups A61K31/755 - A61K31/795
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Abstract

The invention discloses a silicone gel patch containing plant herbal components and a manufacturing method thereof, belonging to the technical field of medical supplies. The components of the composition comprise vinyl polysiloxane, a cross-linking agent, a catalyst, a tackifier and a plant herbal component. The method is coating and forming. The silicone gel patch prepared by the invention can bear various different plant herbaceous components, can be prepared into silicone gel patches with different effects according to different requirements, and has a wide application range; meanwhile, due to the good sealing property and antibacterial property of the silicone gel patch, the silicone gel patch can be reused, generally, the silicone gel patch can be reused for 2-8 times, and the slow release effect of each use is not attenuated basically. The preparation method provided by the invention is mild in condition, simple in steps and suitable for large-scale production.

Description

Silicone gel patch containing plant herbal components and manufacturing method thereof
Technical Field
The invention relates to the technical field of medical and daily chemical products, in particular to a silicone gel patch containing plant herbal components and a manufacturing method thereof.
Background
At present, the nation pays great attention to the development and application of traditional Chinese medicines and is dedicated to developing various medical and health care purposes of the traditional Chinese medicines and plant herbs.
The silicone gel is medical and daily chemical health dressing mainly made of polysiloxane. Because of the good slow release property and biocompatibility of the polysiloxane, the polysiloxane has been applied to treat, improve or soften scars caused by burns, scalds and wound hyperplasia in an external application mode in the 80 s in the world. Since the silicone gel can maintain certain temperature, pressure, oxygen content and water content in a target area, besides being used for lightening scars, the silicone gel can also be used for preventing postoperative wound infection, moisturizing and other purposes, but related researches on the combination of the silicone gel and plant herbal ingredients are in a blank stage at present.
Disclosure of Invention
The first purpose of the invention is to provide a silicone gel patch containing plant herbaceous components, which is combined with the plant herbaceous components, and can stably and directly reach the focus for a long time by utilizing the slow release effect of the silicone gel to achieve the required treatment purpose.
The second purpose of the invention is to provide a method for preparing the silicone gel patch containing the herbal components.
The first purpose of the invention is realized by the following technical scheme:
the second purpose of the invention is to provide a method for preparing the silicone gel patch containing the herbal components.
The first purpose of the invention is realized by the following technical scheme:
a silicone gel patch containing plant herbal components comprises the following components in parts by mass:
Figure BDA0003055873230000021
further, the plant herbal component comprises at least one of the following components:
radix sophorae flavescentis, garden burnet root, weeping forsythia, wild chrysanthemum flower, mugwort, asiatic pennywort herb, lavender, bletilla striata, liquorice, ginger, ginseng, mangnolia officinalis, Chinese angelica, pseudo-ginseng, musk, bezoar, pearl powder, calamine, borax, borneol, chaulmoogra, rehmannia root, cochinchina momordica seed, belvedere fruit, red sage root, dandelion, glabrous greenbrier rhizome, medicinal cyathula root, drynaria rhizome, clematis root, common cnidium fruit, raw common monkshood mother root, doubleteeth pubescent angelica root, oriental waterplantain rhizome, dried orange peel, tuber fleeceflower root, grassleaf sweelflag rhizome, rhizoma atractylodis, perilla leaf, honeysuckle flower, adenophora tetraphylla, rose essential oil, lavender oil, rose hip oil, lemon oil, wormwood oil, olive oil, lithospermum oil, phellodendron bark oil and ligusticum chuanxiong oil.
Further, the feed additive also comprises animal components and mineral components; the animal component and mineral component comprise at least one of periostracum Cicadae, Margarita powder, and Calamina; the total content of the animal component, the mineral component and the plant herbal component is 0.1-10 parts.
Further, the cross-linking agent is hydrogen-containing silicone oil, the catalyst is chloroplatinic acid, and the tackifier is MQ silicone resin.
Further, the physical form of the plant herbal ingredients is liquid or powder; the particle size of the powder of the plant herbal components is within 10-3-10-9m。
Further, the particle size of the silica is in the range of 10-3-10-9m。
Further, the molecular weight of the vinyl polysiloxane is in the range of 10k-200 kDal.
The second purpose of the invention is realized by the following technical scheme:
a method of making a silicone gel patch containing herbal plant ingredients added to a silicone gel base by at least one of the following methods:
pulverizing the powder of the plant herbaceous components, and adding the pulverized powder into the silicone gel base material;
the liquid of the plant herbaceous components is directly added into the silicone gel base material or is added into the silicone gel base material by taking silicon dioxide as a carrier;
decocting the plant herbaceous components, and adding the decocted components into the silicone gel base material by using silicon dioxide as a carrier;
then coating and forming.
The solvent is at least one of ethanol, petroleum ether and dimethyl sulfoxide;
the pressure range of the reduced pressure is less than 101.325 kPa;
the low temperature range is-10 to 80 ℃.
Further, when the plant herbaceous components are added into the silicone gel base material through silicon dioxide serving as a carrier, the plant herbaceous components are dissolved by water, then the dissolved plant herbaceous components are added into the silicon dioxide to be extracted by a solvent, and then the solvent is removed through a low-temperature drying method or a low-temperature reduced pressure suction filtration method to obtain the silicon dioxide absorbed with the plant herbaceous components; the solvent is at least one of ethanol, petroleum ether and dimethyl sulfoxide.
Further, the reduced pressure is in the pressure range < 101.325kPa, and the low temperature is in the temperature range of-10 to 80 ℃.
Further, the temperature of the coating is-10 ℃ to 100 ℃.
In the invention, the MQ silicone resin is a silicone resin consisting of a monofunctional Si-O unit and a tetrafunctional Si-O unit).
The invention has the following beneficial effects:
1. the silicone gel patch prepared by the invention can bear various different plant herbaceous components, can be prepared into silicone gel patches with different effects according to different requirements, and has a wide application range; meanwhile, due to the good slow release property and antibacterial property of the silicone gel patch, the silicone gel patch can be reused, and the slow release effect of each use is attenuated stably.
2. The silicone gel patch prepared by the invention can release the plant herbal components in the silicone gel patch in a sustained-release manner to directly reach the focus and deeply permeate into the bottom layer of the skin on the premise of exerting self moisture retention, sealing and good biocompatibility of the silicone gel.
3. The preparation method provided by the invention is mild in condition, simple in steps and suitable for large-scale production.
Detailed Description
The following specific examples are provided to further illustrate the present invention so that those skilled in the art may better understand the invention and practice it, but the examples are not intended to limit the invention. Other various modifications, substitutions and alterations of the above-described structures of the present invention will occur to those skilled in the art without departing from the basic technical spirit of the invention as described herein.
The preparation method comprises the following steps:
the first step is as follows:
the method comprises the following steps: weighing the components, dissolving and extracting the plant herbaceous components by using water and a solvent, then adding silicon dioxide powder, and removing the solvent through low-temperature drying or low-temperature reduced pressure suction filtration to obtain the silicon dioxide powder containing the plant herbaceous components.
The solvent is at least one of ethanol, petroleum ether and dimethyl sulfoxide.
The pressure range of the reduced pressure is less than 101.325kPa, and the temperature range of the low temperature is-10 to 80 ℃.
The second method comprises the following steps: weighing the components, pulverizing the powdery plant herbaceous components into powder of 0.1mm-10nm, adding into silicone gel base material, and directly adding the liquid plant herbaceous components into the silicone gel base material.
The third method comprises the following steps: weighing the components, decocting powdery plant herbal components, dissolving and extracting with water and a solvent, adding silicon dioxide powder, and removing the solvent through low-temperature drying or low-temperature reduced-pressure suction filtration to obtain silicon dioxide powder containing the plant herbal components; silicon dioxide powder containing plant herbaceous components is added into the silicone gel base material, and liquid plant herbaceous components are directly added into the silicone gel base material.
The second step is that: uniformly mixing vinyl polysiloxane, a cross-linking agent, a catalyst and a tackifier to prepare a silicone gel base material; the silicone gel base material and the plant herbaceous component, and the silicon dioxide powder containing the plant herbaceous component are mixed, coated and molded.
The raw materials for the silicone gel system were weighed as in table 1 below, and the raw materials for the plant herbal component, the animal component, and the mineral component were weighed as in table 2 below.
TABLE 1
Serial number Vinyl polysiloxane Hydrogen-containing silicone oil Chloroplatinic acid MQ silicone resin Silicon dioxide
Example 1 100 0.01 0.0001 0.0001 0.01
Example 2 100 0.08 0.0005 0.001 5
Example 3 100 0.08 0.001 0.1 5
Example 4 100 0.08 0.005 1 10
Example 5 100 0.16 0.01 5 10
Example 6 100 0.16 0.05 20 20
Example 7 100 0.16 0.1 20 20
Example 8 100 0.16 0.3 20 20
Example 9 100 0.16 0.6 20 20
Example 10 100 0.20 1 30 20
Example 11 100 0.20 1 30 20
Example 12 100 0.20 1 30 20
In Table 1, the molecular weight of the vinyl polysiloxane of examples 1-3 was 10Kdal, the molecular weight of the vinyl polysiloxane of examples 4-6 was 50Kdal, and the molecular weight of the vinyl polysiloxane of examples 7-10 was 200 Kdal.
TABLE 2
Figure BDA0003055873230000061
Example 11 the added herbal, animal and mineral ingredients included: 1.25 parts of chaulmoogra, 1.25 parts of rehmannia, 1.25 parts of momordica cochinchinensis, 0.25 parts of fructus kochiae, 0.25 parts of salvia miltiorrhiza, 0.25 parts of dandelion, 0.25 parts of glabrous greenbrier rhizome, 0.25 parts of medicinal cyathula root, 0.25 parts of rhizoma drynariae, 0.25 parts of radix clematidis, 0.25 parts of fructus cnidii, 0.25 parts of unprocessed radix aconiti, 0.25 parts of radix angelicae pubescentis, 0.25 parts of periostracum cicadae, 0.25 parts of rhizoma alismatis, 0.25 parts of dried orange peel, 0.25 parts of polygonum multiflorum, 0.25 parts of rhizoma acori graminei, 0.25 parts of rhizoma atractylodis, 0.25 parts of perilla leaf, 0.25 parts of honeysuckle and 0.25 parts of adenophora ladybell root, and is used for preparing the silicone gel plaster for treating rheumatism pain.
Example 12 added herbal ingredients of plants include: 2 parts of rose essential oil, 1 part of lavender oil, 1 part of rose hip oil, 1 part of lemon oil, 1 part of wormwood oil, 1 part of olive oil, 1 part of lithospermum oil, 1.5 parts of phellodendron amurense oil and 0.5 part of ligusticum chuanxiong hort oil, and the antibacterial and moisturizing silicone gel patch is prepared. .
The coating temperature, the preparation method of the silica powder containing the herbal ingredients, and other process parameters are shown in table 3.
TABLE 3
Figure BDA0003055873230000071
Example 1 moxibustion silicone gel patch with heating function can be prepared for nursing physiotherapy of knee rheumatism, spondylitis and scapulohumeral periarthritis,
examples 2 and 8 can be used to prepare an antibacterial silicone gel patch for treating inflammatory skin diseases such as pox, cyst, and mosquito bite,
example 3 an antibacterial silicone gel patch with whitening function can be prepared for skin whitening care treatment.
Example 4 a silicone gel patch with scar treatment functionality can be prepared for preventive care treatment of hypertrophic scars.
Examples 5 and 6 can prepare silicone gel patches with skin care and treatment functions for skin nutrition restoration and protection physiotherapy.
Example 7 a silicone gel patch with antibacterial whitening effect can be prepared for skin nutrition, whitening, repair, and protective physical therapy.
Examples 9 and 10 can be used for preparing antibacterial moxibustion silicone gel patch for treating inflammatory skin diseases such as pox, cyst, and mosquito bite.
Example 11 a silicone gel patch for the treatment of rheumatic pain can be prepared.
Example 12 a silicone gel patch with skin care and treatment functions of pure natural essential oils can be prepared for skin nourishment, repair, protection and physical therapy.
And (3) slow release test: examples 2, 6, 7, 8 and 9, which contain sanguisorba officinalis as an indicator, were tested for sustained release properties. The silicone gel patch was immersed in purified water, and the water was changed every 3 hours, and the sanguisorba officinalis content in the solution was measured for the corresponding time, with the results shown in table 5.
TABLE 4
Figure BDA0003055873230000081
According to the analysis of sanguisorba officinalis in the solution in table 4, the silicone gel patch has the effect of slowly releasing the herbal ingredients of the plants, and the slow release effect is stable. The silicone gel patch can continuously and slowly release the active ingredients of the plants by contacting with the skin for a long time, and the active ingredients act on the skin and permeate into the bottom layer of the skin to achieve the expected beautifying and treating effects.

Claims (10)

1. The silicone gel patch containing the herbal components is characterized by comprising the following components in parts by mass:
Figure FDA0003055873220000011
2. the plant herbal component-containing silicone gel patch as claimed in claim 1, wherein the plant herbal component comprises at least one of the following components:
radix sophorae flavescentis, garden burnet root, weeping forsythia, wild chrysanthemum flower, mugwort, asiatic pennywort herb, lavender, bletilla striata, liquorice, ginger, ginseng, mangnolia officinalis, Chinese angelica, pseudo-ginseng, musk, bezoar, pearl powder, calamine, borax, borneol, chaulmoogra, rehmannia root, cochinchina momordica seed, belvedere fruit, red sage root, dandelion, glabrous greenbrier rhizome, medicinal cyathula root, drynaria rhizome, clematis root, common cnidium fruit, raw common monkshood mother root, doubleteeth pubescent angelica root, oriental waterplantain rhizome, dried orange peel, tuber fleeceflower root, grassleaf sweelflag rhizome, rhizoma atractylodis, perilla leaf, honeysuckle flower, adenophora tetraphylla.
3. The herbal silicone gel patch according to claim 1, further comprising an animal component and a mineral component; the animal component and mineral component comprise at least one of periostracum Cicadae, Margarita powder, and Calamina;
the total content of the animal component, the mineral component and the plant herbal component is 0.1-10 parts.
4. The plant herbal component-containing silicone gel patch as claimed in claim 1, wherein the cross-linking agent is hydrogen-containing silicone oil, the catalyst is chloroplatinic acid, and the tackifier is MQ silicone.
5. The herbal plant ingredient-containing silicone gel patch as claimed in claim 1, wherein the herbal plant ingredient is in a physical form of liquid or powder; the particle size of the powder of the plant herbal components is within 10-3-10-9m。
6. The method for preparing a silicone gel patch containing herbal ingredients as claimed in claim 1, wherein the silica has a particle size in the range of 10-3-10-9m。
7. The method for preparing a herbal composition-containing silicone gel patch as claimed in any one of claims 1-5, wherein the herbal composition is added to the silicone gel base by at least one of the following methods:
pulverizing the powder of the herbal components, and adding into the silicone gel base material;
the liquid of the plant herbaceous components is directly added into the silicone gel base material or is added into the silicone gel base material by taking silicon dioxide as a carrier;
decocting the plant herbaceous components, and adding the decocted components into the silicone gel base material by using silicon dioxide as a carrier;
then coating and forming.
The solvent is at least one of ethanol, petroleum ether and dimethyl sulfoxide;
the pressure range of the reduced pressure is less than 101.325 kPa;
the low temperature range is-10 to 80 ℃.
8. The method for preparing a silicone gel patch containing herbal plant components as claimed in claim 7, wherein when the herbal plant components are added to the silicone gel base material via silicon dioxide as a carrier, the herbal plant components are dissolved in water, then added to the silicon dioxide to be extracted by a solvent, and then the solvent is removed by a low-temperature drying or low-temperature reduced-pressure filtration method to obtain the silicon dioxide absorbed with the herbal plant components; the solvent is at least one of ethanol, petroleum ether and dimethyl sulfoxide.
9. The method of preparing a herbal composition containing silicone gel patch as claimed in claim 8, wherein the reduced pressure is in a pressure range of < 101.325kPa and the low temperature is in a temperature range of-10 to 80 ℃.
10. The method for preparing a plant herbal ingredient-containing silicone gel patch as claimed in claim 7, wherein the coating is applied at a cross-linking temperature of-10 ℃ to 100 ℃.
CN202110499704.8A 2021-05-08 2021-05-08 Silicone gel patch containing plant herbal components and manufacturing method thereof Pending CN113318094A (en)

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