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CN113155252B - A weighing system with deoxygenation function and cyclic dehumidification - Google Patents

A weighing system with deoxygenation function and cyclic dehumidification Download PDF

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CN113155252B
CN113155252B CN202110449031.5A CN202110449031A CN113155252B CN 113155252 B CN113155252 B CN 113155252B CN 202110449031 A CN202110449031 A CN 202110449031A CN 113155252 B CN113155252 B CN 113155252B
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dehumidification
weighing
gas
operation box
chamber
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CN113155252A (en
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张峰
赵惠忠
孙有改
张斌斌
高娅洁
张真真
张晶
侯宏伟
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Shanghai Maritime University
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    • GPHYSICS
    • G01MEASURING; TESTING
    • G01GWEIGHING
    • G01G17/00Apparatus for or methods of weighing material of special form or property
    • G01G17/04Apparatus for or methods of weighing material of special form or property for weighing fluids, e.g. gases, pastes
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D53/00Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
    • B01D53/02Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols by adsorption, e.g. preparative gas chromatography
    • B01D53/04Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols by adsorption, e.g. preparative gas chromatography with stationary adsorbents
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D53/00Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
    • B01D53/22Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols by diffusion
    • B01D53/229Integrated processes (Diffusion and at least one other process, e.g. adsorption, absorption)
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D53/00Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
    • B01D53/26Drying gases or vapours
    • B01D53/261Drying gases or vapours by adsorption
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D53/00Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
    • B01D53/34Chemical or biological purification of waste gases
    • B01D53/46Removing components of defined structure
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D53/00Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
    • B01D53/34Chemical or biological purification of waste gases
    • B01D53/74General processes for purification of waste gases; Apparatus or devices specially adapted therefor
    • B01D53/81Solid phase processes
    • B01D53/82Solid phase processes with stationary reactants
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01GWEIGHING
    • G01G23/00Auxiliary devices for weighing apparatus
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01GWEIGHING
    • G01G23/00Auxiliary devices for weighing apparatus
    • G01G23/06Means for damping oscillations, e.g. of weigh beams
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D2253/00Adsorbents used in seperation treatment of gases and vapours
    • B01D2253/10Inorganic adsorbents
    • B01D2253/102Carbon
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D2257/00Components to be removed
    • B01D2257/10Single element gases other than halogens
    • B01D2257/104Oxygen

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Abstract

本发明公开了一种带有除氧功能同时可循环除湿的称重系统,包括:称量装置、湿度控制处理系统、除氧系统;称量装置包括:用于进行称量操作的操作箱,操作箱内设有若干个匀流减速装置;操作箱中的气体由湿度控制处理系统和除氧系统处理后,经匀流减速装置回输至操作箱内;湿度控制处理系统包括:多个交替循环使用的除湿室,除湿室包括:除湿吸附剂、气体输送开关、用于对除湿吸附剂加热的加热同心管、用于检测除湿室出口处气体湿度的除湿室湿度检测器;湿度控制处理系统处理气体时,其中一个除湿室的气体输送开关打开,当除湿室湿度检测器的检测值达到设定值后,加热同心管开始加热,气体输送开关关闭,待处理的气体进入另一个除湿室内。

Figure 202110449031

The invention discloses a weighing system with deoxidizing function and cyclic dehumidification, comprising: a weighing device, a humidity control processing system, and a deoxidizing system; the weighing device comprises: an operation box for performing weighing operations, There are several uniform flow deceleration devices in the operation box; after the gas in the operation box is processed by the humidity control processing system and the deaerator system, it is returned to the operation box through the uniform flow deceleration device; the humidity control processing system includes: a plurality of alternating A dehumidification chamber used for recycling, the dehumidification chamber includes: a dehumidification adsorbent, a gas delivery switch, a heating concentric tube for heating the dehumidification adsorbent, a dehumidification chamber humidity detector for detecting the gas humidity at the outlet of the dehumidification chamber; a humidity control processing system When processing gas, the gas delivery switch of one of the dehumidification chambers is turned on. When the detection value of the humidity detector in the dehumidification chamber reaches the set value, the heating concentric tube starts to heat, the gas delivery switch is turned off, and the gas to be treated enters the other dehumidification chamber.

Figure 202110449031

Description

一种带有除氧功能同时可循环除湿的称重系统A weighing system with deoxygenation function and cyclic dehumidification

技术领域technical field

本发明涉及称重技术邻域,具体涉及一种带有除氧功能同时可循环除湿的称重系统。The invention relates to the field of weighing technology, in particular to a weighing system with deoxygenation function and cyclic dehumidification.

背景技术Background technique

淡水资源短缺依然是当今世界亟待解决的问题之一,太阳能空气取水是一种通过利用吸附剂吸附空气中的水蒸气,并利用太阳能进行脱附以获得淡水的方法。在太阳能空气取水研究当中,开式吸附条件下吸附剂的性能研究有着至关重要的影响,在吸附剂性实验与性能检测中,由于空气取水装置所用的吸附剂有极高的吸水吸湿能力,所以在吸附剂取样和称量实验,以及测试其吸附性能时候,对环境的湿度有着较高的要求。在取样和样本称重时候我们希望环境尽可能湿度低且能保持恒定。The shortage of fresh water resources is still one of the problems that need to be solved urgently in the world today. Solar air water extraction is a method to obtain fresh water by using adsorbents to absorb water vapor in the air and desorption by solar energy. In the research of solar air water intake, the performance of the adsorbent under the open adsorption condition has a crucial impact. In the adsorption experiment and performance test, the adsorbent used in the air water intake device Therefore, when the adsorbent is sampled and weighed, and its adsorption performance is tested, there is a high requirement for the humidity of the environment. We want the humidity to be as low and constant as possible when sampling and weighing samples.

在实验室的物品称量操作中,有两类性质的物品最常见,一类是遇空气极易潮解的物品,如无水氯化钙、氯化镁和固体氢氧化钠等无机盐在空气中很容易潮解。第二类是极易氧化的物品,常温下一些不稳定的烷烃类似物可以和氧气发生剧烈的反应,如硼烷、硅烷等,还有其他常见的极易氧化的物品如亚硫酸钠、硫酸亚铁、硫代硫酸钠等等。这些易潮解的物品会在称量时严重影响到称量的精度和准确性,易氧化的物品在称量时氧化从而影响物品的化学性能和称量的精度及准确性。In the weighing operation of items in the laboratory, there are two types of items that are the most common. One is items that are easily deliquescent in the air, such as inorganic salts such as anhydrous calcium chloride, magnesium chloride and solid sodium hydroxide, which are very Deliquescence easily. The second category is the items that are easily oxidized. Some unstable alkane analogs at room temperature can react violently with oxygen, such as borane, silane, etc., as well as other common items that are easily oxidized such as sodium sulfite, ferrous sulfate , sodium thiosulfate, etc. These deliquescent items will seriously affect the weighing accuracy and accuracy during weighing, and the oxidizable items will oxidize during weighing, which will affect the chemical properties of the items and the precision and accuracy of weighing.

被公开的关于除湿无氧的称重系统的专利有:中国专利申请公布号CN208872401U提出了一种带有除湿装置的恒温恒湿称重系统,通过风扇的转动形成空气流,经过除湿装置将空气中的湿度进行冷凝达到除湿的效果,但存在除湿效果差的问题,且没有考虑风扇转动对称重精度的影响。The published patents on dehumidification and oxygen-free weighing systems are: Chinese Patent Application Publication No. CN208872401U proposes a constant temperature and humidity weighing system with a dehumidification device, which forms an air flow through the rotation of the fan, and passes the air through the dehumidification device. The dehumidification effect is achieved by condensing the humidity in the medium, but there is a problem that the dehumidification effect is poor, and the influence of the rotation of the fan on the weighing accuracy is not considered.

发明内容SUMMARY OF THE INVENTION

本发明的目的是提供一种具有干燥低氧环境、环境气流影响较低的称重系统,解决上述太阳能取水研究中吸附剂取样称重存在的问题;在提供低湿环境保护易潮解物品化学性质不变的同时,提高了易潮解物品称量的准确性。The purpose of the present invention is to provide a weighing system with a dry and low oxygen environment and a low impact of environmental airflow, so as to solve the problems existing in the above-mentioned solar water extraction research of adsorbent sampling and weighing; At the same time, the accuracy of weighing items that are prone to deliquescence is improved.

为了达到上述目的,本发明提供了一种带有除氧功能同时可循环除湿的称重系统,包括:称量装置、湿度控制处理系统、除氧系统;所述称量装置包括:用于进行称量操作的操作箱,所述操作箱内设有若干个匀流减速装置;操作箱中的气体由所述湿度控制处理系统和所述除氧系统处理后,经所述匀流减速装置回输至所述操作箱内;所述除氧系统包括:与所述操作箱连接的除氧管和氮气置换装置;所述湿度控制处理系统包括:多个交替循环使用的除湿室,所述除湿室包括:加热使水分脱附后能够循环利用的除湿吸附剂、用于对所述除湿吸附剂加热的加热同心管、用于检测所述除湿室出口处气体湿度的除湿室湿度检测器、气体输送开关;In order to achieve the above purpose, the present invention provides a weighing system with deoxidizing function and cyclic dehumidification, including: a weighing device, a humidity control processing system, and a deoxidizing system; the weighing device includes: The operation box for weighing operation is provided with several uniform flow deceleration devices; the gas in the operation box is processed by the humidity control processing system and the deaeration system, and then returned to the uniform flow deceleration device through the uniform flow deceleration device. into the operation box; the deaeration system includes: a deaeration pipe connected to the operation box and a nitrogen replacement device; the humidity control treatment system includes: a plurality of dehumidification chambers used alternately, the dehumidification The chamber includes: a dehumidification adsorbent that can be recycled after desorption of moisture, a heating concentric tube for heating the dehumidification adsorbent, a dehumidification chamber humidity detector for detecting the gas humidity at the outlet of the dehumidification chamber, and a gas delivery switch;

可选的,所述湿度控制处理系统处理气体时,其中一个除湿室的气体输送开关打开,当所述湿度检测器的检测值达到设定值后,加热同心管开始加热,气体输送开关关闭,除湿室内未达标的气体、以及称量装置内待处理的气体进入另一个除湿室内。Optionally, when the humidity control processing system processes gas, the gas delivery switch of one of the dehumidification chambers is turned on, when the detection value of the humidity detector reaches the set value, the heating concentric tube starts to heat, and the gas delivery switch is turned off, The gas that does not meet the standard in the dehumidification chamber and the gas to be processed in the weighing device enter another dehumidification chamber.

可选的,所述同心加热圆管内管为网状,除湿室下方装有吹风装置;当加热同心管加热蒸发吸附剂中的水分时,底部吹风装置向上吹风,加热蒸发的水分由排气管道排出除湿室,吹风装置同时加快了除湿吸附剂的干燥。Optionally, the inner tube of the concentric heating circular tube is in the shape of a mesh, and a blowing device is installed under the dehumidification chamber; when the heating concentric tube heats and evaporates the moisture in the adsorbent, the bottom blowing device blows upward, and the heated and evaporated water is discharged by the exhaust pipe. Out of the dehumidification chamber, the blower also speeds up the drying of the dehumidifying adsorbent.

可选的,所述匀流减速装置包括:两段孔径不同的蜂窝状气流通道。Optionally, the uniform flow deceleration device includes: two sections of honeycomb airflow passages with different apertures.

可选的,所述匀流减速装置中两段孔径不同的蜂窝状气流通道分为一级通道和二级通道,一级通道和二级通道的横截面均呈正六边形;每个一级通道在靠近操作箱内侧的区段都被分为了19个二级通道,所述二级通道截面六边形的边长为1.5mm-2.3mm。Optionally, the two sections of honeycomb airflow channels with different apertures in the uniform flow deceleration device are divided into a primary channel and a secondary channel, and the cross sections of the primary channel and the secondary channel are both regular hexagons; The passages are divided into 19 secondary passages in the section near the inner side of the operation box, and the side lengths of the hexagonal cross-sections of the secondary passages are 1.5mm-2.3mm.

可选的,所述除湿吸附剂为吸湿性盐与多孔基质的复合吸附材料。Optionally, the dehumidifying adsorbent is a composite adsorbent material of a hygroscopic salt and a porous matrix.

可选的,所述称重系统还包括:若干个空气净化装置,操作箱中的气体由所述空气净化装置处理后,输入所述除氧管和所述湿度控制处理系统中;所述空气净化装置的内部填充有活性炭,所述空气净化装置的出口设有过滤膜。Optionally, the weighing system further includes: a plurality of air purification devices, and after the gas in the operation box is processed by the air purification devices, it is input into the deaerator pipe and the humidity control processing system; the air The interior of the purification device is filled with activated carbon, and the outlet of the air purification device is provided with a filter membrane.

可选的,所述过滤膜为合成纤维滤纸或聚四氟乙烯微孔膜;所述过滤膜安装在活性炭的后面,空气先进行活性炭的初步净化再经过过滤膜的过滤,提高了净化的效果的同时增加了过滤膜的使用寿命。Optionally, the filter membrane is a synthetic fiber filter paper or a polytetrafluoroethylene microporous membrane; the filter membrane is installed behind the activated carbon, and the air is initially purified by the activated carbon and then filtered through the filter membrane, which improves the purification effect. At the same time increase the service life of the filter membrane.

可选的,所述称重系统还包括:减震装置,所述减震装置设于所述称量装置的下方。Optionally, the weighing system further includes: a shock absorbing device, and the shock absorbing device is arranged below the weighing device.

可选的,所述除氧管为多个,并且除氧管之间为并列设置。Optionally, there are multiple deaeration pipes, and the deaeration pipes are arranged in parallel.

可选的,所述除氧管内填充脱氧剂,所述脱氧剂以分子筛为载体,分子筛表面负载金属。Optionally, the deoxidizing tube is filled with a deoxidizing agent, the deoxidizing agent uses a molecular sieve as a carrier, and the surface of the molecular sieve is loaded with metal.

可选的,所述气体输送开关为电磁阀。Optionally, the gas delivery switch is a solenoid valve.

可选的,所述称量装置还包括:物品放置箱,所述物品放置箱设于所述操作箱的旁侧;所述物品放置箱的外侧、所述操作箱与所述物品放置箱之间设有密封门。Optionally, the weighing device further includes: an article placing box, the article placing box is arranged on the side of the operation box; the outer side of the article placing box, the operation box and the article placing box; The room has a sealed door.

相比于现有技术,本发明的有益效果是:Compared with the prior art, the beneficial effects of the present invention are:

(1)本发明的操作箱内设有匀流减速装置,使湿度控制处理系统及除氧系统均匀缓慢地向操作箱内输送气体,有效减少了气体流动对物品称量的影响;(1) The operation box of the present invention is provided with a uniform flow deceleration device, so that the humidity control processing system and the deoxygenation system evenly and slowly transport gas into the operation box, effectively reducing the influence of gas flow on the weighing of items;

(2)本发明的称量装置与湿度控制处理系统、以及除氧系统相互独立,且称量装置的底部设有减震装置,能有效减少湿度控制处理系统、以及除氧系统的机器震动对称量装置的影响;(2) The weighing device of the present invention is independent of the humidity control processing system and the deoxidizing system, and the bottom of the weighing device is provided with a shock absorbing device, which can effectively reduce the machine vibration symmetry of the humidity control processing system and the deoxidizing system. the effect of the measuring device;

(3)本发明通过三个互相连通的除湿室对操作箱进行交替除湿,满足物品称量时干燥低湿的环境需求。(3) The present invention dehumidifies the operation box alternately through three interconnected dehumidification chambers, so as to meet the environmental requirements of dryness and low humidity when weighing items.

附图说明Description of drawings

图1为本发明带有除氧功能同时可循环除湿的称重系统的结构示意图;Fig. 1 is the structural representation of the weighing system with deoxygenation function and cyclic dehumidification simultaneously;

图2为本发明一级通道及二级通道的截面示意图;2 is a schematic cross-sectional view of a primary channel and a secondary channel of the present invention;

图3本发明湿度控制处理系统的路线原理流程图;3 is a flow chart of the route principle of the humidity control processing system of the present invention;

图4为本发明除湿室的纵截面示意图;Fig. 4 is the longitudinal sectional schematic diagram of the dehumidification chamber of the present invention;

图5为本发明除湿室的横截面示意图;5 is a schematic cross-sectional view of a dehumidification chamber of the present invention;

图6为本发明除氧系统的路线原理流程图;Fig. 6 is the route principle flow chart of the deaeration system of the present invention;

图7为本发明图1中A处放大结构示意图。FIG. 7 is an enlarged schematic view of the structure at A in FIG. 1 of the present invention.

图中:1-物品放置箱;2-操作箱隔热密封门;3-放置箱隔热密封门;4-减震装置;5-除氧湿度控制处理系统壳体;6-底座;7-伸缩滑轮;8-匀流减速装置;9-操作箱;10-操作手孔;11-一级通道;12-高精度称量天平;13-操作箱温湿度测量器;14-空气净化装置;15-固体活性炭;16-过滤膜;17-二级通道;18-除湿装置壳体;19-排气管道;20-除湿室湿度检测器;21-加热同心管;22-除湿吸附剂;23-吹风装置;24-气体压力表;25-氮气瓶固定夹;26-氮气瓶;27-氮气瓶支架;28-气体流量流速调节记录仪;29-除氧管;30-含氧量检测器;31-第一除湿室;32-第二除湿室;33-第三除湿室;34-轴滑动孔位。In the figure: 1-Item placement box; 2-Insulation sealing door of operation box; 3-Insulation sealing door of placing box; 4-Shock absorption device; Telescopic pulley; 8- Uniform flow deceleration device; 9- Operation box; 10- Operating hand hole; 11- Primary channel; 12- High precision weighing balance; 13- Operation box temperature and humidity measuring device; 14- Air purification device; 15-solid activated carbon; 16-filter membrane; 17-secondary channel; 18-dehumidification device shell; 19-exhaust pipe; 20-dehumidification chamber humidity detector; 21-heating concentric pipe; 22-dehumidification adsorbent; 23 -Blowing device; 24-Gas pressure gauge; 25-Nitrogen cylinder clamp; 26-Nitrogen cylinder; 27-Nitrogen cylinder bracket; 28-Gas flow rate adjustment recorder; 29-Deoxygenation tube; 30-Oxygen content detector ; 31- the first dehumidification chamber; 32- the second dehumidification chamber; 33- the third dehumidification chamber; 34- shaft sliding hole.

具体实施方式Detailed ways

以下结合附图和实施例对本发明的技术方案做进一步的说明。The technical solutions of the present invention will be further described below with reference to the accompanying drawings and embodiments.

如图1-图6所示,本发明提供了一种带有除氧功能同时可循环除湿的称重系统,包括:称量装置、湿度控制处理系统、除氧系统;称量装置包括:用于进行称量操作的操作箱9,操作箱9内设有若干个匀流减速装置8;操作箱9中的气体由湿度控制处理系统和除氧系统处理后,经匀流减速装置8回输至操作箱9内;除氧系统包括:与操作箱9连接的除氧管29和氮气置换装置;湿度控制处理系统包括:多个除湿室,所述除湿室包括:加热使水分脱附后能够循环利用的除湿吸附剂22、用于对除湿吸附剂22加热的加热同心管21、用于检测除湿室出口处气体湿度的除湿室湿度检测器20、气体输送开关;湿度控制处理系统处理气体时,其中一个除湿室的气体输送开关打开,当湿度检测器的检测值达到设定值后,加热同心管21开始加热,气体输送开关关闭,待处理的气体进入另一个除湿室内。As shown in FIG. 1-FIG. 6, the present invention provides a weighing system with deoxidizing function and cyclic dehumidification, including: weighing device, humidity control processing system, and deoxidizing system; weighing device includes: In the operation box 9 for weighing operation, several uniform flow deceleration devices 8 are arranged in the operation box 9; after the gas in the operation box 9 is processed by the humidity control processing system and the deoxidation system, it is returned to the uniform flow deceleration device 8. into the operation box 9; the deaeration system includes: a deaeration pipe 29 connected to the operation box 9 and a nitrogen replacement device; the humidity control treatment system includes: a plurality of dehumidification chambers, the dehumidification chambers Recycled dehumidification adsorbent 22, heating concentric tube 21 for heating dehumidification adsorbent 22, dehumidification chamber humidity detector 20 for detecting gas humidity at the outlet of the dehumidification chamber, gas delivery switch; when the humidity control processing system processes gas , the gas delivery switch of one of the dehumidification chambers is turned on, when the detection value of the humidity detector reaches the set value, the heating concentric tube 21 starts to heat, the gas delivery switch is turned off, and the gas to be treated enters the other dehumidification chamber.

图1的实施例中,匀流减速装置8为两个,分别设于操作箱9的侧边和顶部;其中,侧边的匀流减速装置8通过气体软管与湿度控制处理系统及除氧管连通,顶部的匀流减速装置8与氮气置换装置连通。如图2所示,所述匀流减速装置8包括:两段孔径不同的蜂窝状气流通道,靠近操作箱9外侧的气流通道具有若干个一级通道11,靠近操作箱9内侧的气流通道具有若干个二级通道17;一级通道11、二级通道17的横截面均呈正六边形;每个一级通道11在靠近操作箱9内侧的区段都被分为了19个二级通道17,所述二级通道17截面六边形的边长为1.5mm-2.3mm,使得经过匀流减速装置8输出的气体缓慢而均匀,减少了气体流动对称重结果的影响。In the embodiment of FIG. 1, there are two uniform flow deceleration devices 8, which are respectively arranged on the side and the top of the operation box 9; wherein, the uniform flow deceleration device 8 on the side is controlled by a gas hose and a humidity control processing system and a deoxidizer. The pipes are communicated, and the uniform flow deceleration device 8 at the top is communicated with the nitrogen replacement device. As shown in FIG. 2 , the uniform flow deceleration device 8 includes: two honeycomb airflow passages with different apertures, the airflow passage near the outside of the operation box 9 has several primary passages 11 , and the airflow passage close to the inside of the operation box 9 has a plurality of primary passages 11 . Several secondary channels 17; the cross-sections of the primary channels 11 and the secondary channels 17 are all regular hexagons; each primary channel 11 is divided into 19 secondary channels 17 in the section close to the inner side of the operation box 9 , the side length of the hexagonal cross-section of the secondary channel 17 is 1.5mm-2.3mm, so that the gas output through the uniform flow deceleration device 8 is slow and uniform, and the influence of the gas flow on the weighing result is reduced.

如图1及图3所示,本发明操作箱9的内部设有操作箱温湿度测量器13、含氧量检测器、高精度称量天平12,以监控操作箱9称量时的温湿度及氧气含量;本发明操作箱9上设有操作手孔10,所述操作手孔10上套有操作手套,以方便工作人员操作称量天平,操作手套与操作手孔10之间用密封环密封,防止外界空气的进入。As shown in FIG. 1 and FIG. 3 , the operation box 9 of the present invention is provided with an operation box temperature and humidity measuring device 13, an oxygen content detector, and a high-precision weighing balance 12 to monitor the temperature and humidity of the operation box 9 during weighing. and oxygen content; the operating box 9 of the present invention is provided with an operating hand hole 10, and the operating hand hole 10 is covered with operating gloves to facilitate the staff to operate the weighing balance, and a sealing ring is used between the operating gloves and the operating hand hole 10 Sealed to prevent the entry of outside air.

本发明的称量装置还包括:置于所述操作箱9旁侧的物品放置箱1,所述物品放置箱1用于放置物品,物品放置箱1的外侧设有放置箱隔热密封门3、操作箱9与物品放置箱1之间设有操作箱隔热密封门2,以层层阻挡称重系统外部的气体进入操作箱9中。The weighing device of the present invention further comprises: an article placing box 1 placed beside the operation box 9, the article placing box 1 is used for placing articles, and the outer side of the article placing box 1 is provided with a placing box heat insulation sealing door 3 . Between the operation box 9 and the article placing box 1, there is an operation box heat-insulating and sealing door 2 to block the gas from the outside of the weighing system from entering the operation box 9 layer by layer.

在操作人员使用称量装置对物品进行称量之前,湿度控制处理系统内的除湿室对操作箱9进行除湿。如图3所示,所述除湿室内部设有除湿装置,除湿吸附剂22填充于除湿装置内部,一些实施例中,除湿吸附剂22为吸湿性盐与多孔基质的复合吸附材料,多孔基质可以是硅胶、沸石、石墨烯,吸湿性盐可以是氯化镁、氯化钙,氯化锂等盐类。Before the operator uses the weighing device to weigh the items, the dehumidification chamber in the humidity control processing system dehumidifies the operation box 9 . As shown in FIG. 3 , a dehumidification device is provided inside the dehumidification chamber, and the dehumidification adsorbent 22 is filled in the dehumidification device. In some embodiments, the dehumidification adsorbent 22 is a composite adsorbent material of hygroscopic salt and a porous matrix. The porous matrix can be It is silica gel, zeolite, graphene, and the hygroscopic salt can be magnesium chloride, calcium chloride, lithium chloride and other salts.

如图4及图5所示,一些实施例中,除湿室以及除湿装置均呈横向设置的圆筒状,加热同心管21设于除湿装置的内部且与除湿装置壳体18同心,使除湿装置内的除湿吸附剂22干燥程度相同,不至于局部干燥过快损伤吸附剂。优选的,所述加热同心管21呈网状,进一步均衡了除湿吸附剂22整体的干燥程度。As shown in FIG. 4 and FIG. 5 , in some embodiments, the dehumidification chamber and the dehumidification device are horizontally arranged cylindrical shapes, and the heating concentric pipe 21 is arranged inside the dehumidification device and is concentric with the dehumidification device housing 18 , so that the dehumidification device The drying degree of the dehumidifying adsorbent 22 inside is the same, and the adsorbent will not be damaged by local drying too fast. Preferably, the heating concentric tubes 21 are in the shape of a mesh, which further balances the drying degree of the dehumidifying adsorbent 22 as a whole.

本发明的除湿装置还包括:设于除湿吸附剂22下方的吹风装置23、与除湿室外部连通的排气管道19;所述吹风装置23用于加快吸附剂中水分蒸发的速度,所述排气管道19用于将蒸发的水分排出除湿室。The dehumidifying device of the present invention further includes: a blowing device 23 arranged below the dehumidifying adsorbent 22, and an exhaust duct 19 communicating with the outside of the dehumidifying chamber; the blowing device 23 is used to speed up the evaporation of water in the adsorbent, and the exhausting device 23 The air duct 19 is used to discharge the evaporated moisture out of the dehumidification chamber.

其中,可选的,本发明除湿室内部的加热同心管21及除湿室湿度检测器20、除湿室外部的电磁阀及抽气泵能够与计算机连接,使用者可以在计算机中设置湿度检测器的阈值,在湿度检测器的数值高于阈值时,计算机控制电磁阀使气体不再通入除湿室中,开启加热同心管21对吸附剂进行加热。Wherein, optionally, the heating concentric tube 21 inside the dehumidification chamber and the humidity detector 20 of the dehumidification chamber, the solenoid valve and the air pump outside the dehumidification chamber of the present invention can be connected to the computer, and the user can set the threshold value of the humidity detector in the computer , when the value of the humidity detector is higher than the threshold value, the computer controls the electromagnetic valve so that the gas will no longer pass into the dehumidification chamber, and the heating concentric pipe 21 is opened to heat the adsorbent.

图3的实施例中,湿度控制处理系统包括:三个除湿室,分别为第一除湿室31、第二除湿室32、以及第三除湿室33;第一除湿室31、第二除湿室32、以及第三除湿室33彼此连通且均与称量装置连通,三个除湿室的外部设有抽气泵(图中未示出)及电磁阀,湿度控制处理系统的工作流程如下:In the embodiment of FIG. 3 , the humidity control processing system includes: three dehumidification chambers, respectively a first dehumidification chamber 31 , a second dehumidification chamber 32 , and a third dehumidification chamber 33 ; the first dehumidification chamber 31 and the second dehumidification chamber 32 , and the third dehumidification chamber 33 is communicated with each other and is all communicated with the weighing device, the outside of the three dehumidification chambers is provided with an air pump (not shown in the figure) and a solenoid valve, and the workflow of the humidity control processing system is as follows:

(1)打开电磁阀V1、V2、V10,其余电磁阀处于关闭状态,抽气泵使称量装置中的气体进入第一除湿室31中;(1) Open the solenoid valves V1, V2, V10, the other solenoid valves are in a closed state, and the air pump makes the gas in the weighing device enter the first dehumidification chamber 31;

(2)待第一除湿室31内的除湿吸附剂22吸附饱和后,关闭V10、V2,打开V3、V7、V5、V16,同时第一除湿室31中的加热同心管21开始加热,蒸发吸附剂中的水分,吹风装置23向上吹风,水汽从V16排出,此时抽气泵使称量装置、以及第一除湿室31除湿装置外部湿度未达标的气体进入第二除湿室32中进行除湿;(2) After the dehumidification adsorbent 22 in the first dehumidification chamber 31 is saturated with adsorption, close V10, V2, open V3, V7, V5, V16, and at the same time, the heating concentric tube 21 in the first dehumidification chamber 31 starts to heat, evaporation adsorption The moisture in the agent, the blowing device 23 blows upward, and the water vapor is discharged from V16. At this time, the air pump makes the weighing device and the outside humidity of the first dehumidifying chamber 31 dehumidifying device not up to the standard gas into the second dehumidifying chamber 32 for dehumidification;

(3)同理,当第二除湿室32吸附达到饱和时,关闭V3、V7、V5,打开V4、V8、V6、V15,同时第二除湿室32中的加热同心管21开始加热,蒸发吸附剂中的水分,吹风装置23向上吹风,水汽从V15排出,此时抽气泵使称量装置、以及第二除湿室32除湿装置外部湿度未达标的气体进入第三除湿室33中进行除湿;(3) Similarly, when the adsorption of the second dehumidification chamber 32 reaches saturation, close V3, V7, V5, open V4, V8, V6, V15, and at the same time the heating concentric tube 21 in the second dehumidification chamber 32 starts to heat, evaporation adsorption The moisture in the agent, the blowing device 23 blows upward, and the water vapor is discharged from V15, and the air pump makes the weighing device and the second dehumidifying chamber 32 dehumidifying device external humidity not up to the standard gas into the third dehumidifying chamber 33 for dehumidification;

(4)待第三除湿室33吸附达到饱和时,第一除湿室31中的吸附剂已经被同心加热圆管蒸发干燥,可以再次投入工作,此时关闭V4、V8、V6、V16,打开V10、V2、V14、V9,第三除湿室33中的加热同心管21开始加热,蒸发吸附剂中的水分,吹风装置23向上吹风,水汽从V14排出,抽气泵使称量装置、以及第三除湿室33除湿装置外部湿度未达标的气体进入第一除湿室31中进行除湿。三个除湿室通过上述循环进行湿度的处理。(4) When the adsorption of the third dehumidification chamber 33 reaches saturation, the adsorbent in the first dehumidification chamber 31 has been evaporated and dried by the concentric heating circular tube, and can be put into work again. At this time, close V4, V8, V6, V16, and open V10 , V2, V14, V9, the heating concentric tube 21 in the third dehumidification chamber 33 starts to heat, evaporates the moisture in the adsorbent, the blowing device 23 blows upward, the water vapor is discharged from V14, and the air pump makes the weighing device and the third dehumidifier The gas whose external humidity of the dehumidifying device in the chamber 33 does not meet the standard enters the first dehumidifying chamber 31 for dehumidification. The three dehumidification chambers carry out humidity treatment through the above cycle.

若需三个除湿室同时工作则关闭V2、V5、V7、V8、V9、V14、V15、V16,打开其余电磁阀,称量装置中的气体依次经过三个除湿室除湿再流回称量装置中。If three dehumidification chambers need to work at the same time, close V2, V5, V7, V8, V9, V14, V15, V16, open other solenoid valves, and the gas in the weighing device will pass through the three dehumidification chambers in turn to be dehumidified and then flow back to the weighing device middle.

如图6所示,本发明的除氧管29为多个且除氧管29之间为并列设置,其中一个除氧管29发生问题时,气体可以进入其余除氧管29进行除氧;所述除氧管29为耐压透明玻璃管,除氧管29内部填充脱氧剂,使用者可以观察脱氧剂氧化后颜色的变化判断脱氧剂的消耗情况;所述脱氧剂载体为分子筛,其表面负载活性金属,所述活性金属为铜、钴、铁、镍、锰等。As shown in FIG. 6 , there are multiple deaerator pipes 29 in the present invention, and the deaerator pipes 29 are arranged in parallel. When a problem occurs in one deaerator pipe 29, the gas can enter the other deaerator pipes 29 for deoxygenation; The deoxidizer tube 29 is a pressure-resistant transparent glass tube, and the deoxidizer is filled inside the deoxidizer tube 29. The user can observe the change of the color of the deoxidizer after oxidation to judge the consumption of the deoxidizer; the deoxidizer carrier is a molecular sieve, and its surface load Active metal, the active metal is copper, cobalt, iron, nickel, manganese, etc.

本发明称量装置与湿度控制处理系统之间、称量装置与除氧管29之间均设有空气净化装置14,所述空气净化装置14用于过滤称量装置空气中的大颗粒尘埃;所述空气净化装置14的内部设有固体活性炭15,出口设有过滤膜16,气体经活性炭初步净化后通过过滤膜16过滤排出,保证了净化的效果的同时延长了吸附膜的使用寿命。According to the present invention, an air purification device 14 is provided between the weighing device and the humidity control processing system, and between the weighing device and the deaerator pipe 29, and the air purification device 14 is used to filter large particles of dust in the air of the weighing device; The interior of the air purification device 14 is provided with solid activated carbon 15, and the outlet is provided with a filter membrane 16. After preliminary purification by the activated carbon, the gas is filtered and discharged through the filter membrane 16, which ensures the purification effect and prolongs the service life of the adsorption membrane.

所述过滤膜16为合成纤维滤纸或聚四氟乙烯(PTFE)微孔膜,其具有孔径小、透气量大、化学稳定性高等优点,在过滤空气中大颗粒尘埃的同时,能保持空气正常流通至湿度控制处理系统及除氧管29中。The filter membrane 16 is a synthetic fiber filter paper or a polytetrafluoroethylene (PTFE) microporous membrane, which has the advantages of small pore size, large air permeability, and high chemical stability. While filtering large particles of dust in the air, it can keep the air normal. It flows into the humidity control processing system and the deaeration pipe 29 .

本发明的氮气置换装置与称量装置的顶部连接,氮气置换装置通过匀流减速装置8向操作箱9中输送氮气;所述氮气置换装置包括:氮气瓶26、所述氮气瓶26通过氮气瓶固定夹25固定到氮气瓶支架27上,所述氮气瓶26设有电磁阀,气体压力表24及气体流量流速调节记录仪28,以监控氮气瓶26向称量装置输送的氮气量。The nitrogen replacement device of the present invention is connected to the top of the weighing device, and the nitrogen replacement device transports nitrogen into the operation box 9 through the uniform flow deceleration device 8; the nitrogen replacement device includes: a nitrogen cylinder 26, and the nitrogen cylinder 26 passes through the nitrogen cylinder The fixing clip 25 is fixed to the nitrogen cylinder bracket 27, and the nitrogen cylinder 26 is provided with a solenoid valve, a gas pressure gauge 24 and a gas flow rate adjustment recorder 28 to monitor the nitrogen amount delivered by the nitrogen cylinder 26 to the weighing device.

本发明除氧系统、湿度控制处理系统与称量装置之间通过气体软管连通。The deoxygenation system of the present invention, the humidity control processing system and the weighing device are communicated with each other through a gas hose.

请继续参阅图1,除氧管29与所述湿度控制处理系统安装于除氧湿度控制处理系统壳体5内,称量装置与除氧湿度控制处理系统壳体5之间设有减震装置4,所述减震装置4包括:海绵及减震弹簧,所述减震弹簧设于海绵的底部;所述减震装置4减少操作时称量装置外部机器运行的震动,以提高物品称重的精准度。Please continue to refer to FIG. 1 , the deoxidizing tube 29 and the humidity control processing system are installed in the housing 5 of the deoxidizing humidity control processing system, and a shock absorbing device is provided between the weighing device and the housing 5 of the deoxidizing humidity control processing system 4. The shock absorbing device 4 includes: a sponge and a shock absorbing spring, the shock absorbing spring is arranged at the bottom of the sponge; the shock absorbing device 4 reduces the vibration of the external machine of the weighing device during operation, so as to improve the weighing of the item. accuracy.

如图7所示,本发明的带有除氧功能同时可循环除湿的称重系统的下方设有底座6,所述底座6的底部安装有伸缩滑轮7,所述伸缩滑轮7的安装方式如专利CN212757172U所示,使用时使伸缩滑轮7在轴滑动孔位34内直线移动,从而使伸缩滑轮7支出于底座6之外,或收纳于底座6之内,方便了整个称重系统的运输。As shown in FIG. 7 , the weighing system with deoxidizing function and cyclic dehumidification of the present invention is provided with a base 6 below, and a telescopic pulley 7 is installed at the bottom of the base 6. The installation method of the telescopic pulley 7 is as follows As shown in the patent CN212757172U, the telescopic pulley 7 is moved linearly in the shaft sliding hole 34 during use, so that the telescopic pulley 7 is extended outside the base 6 or stored in the base 6, which facilitates the transportation of the entire weighing system.

如图3所示,本发明带有除氧功能同时可循环除湿的称重系统称量易潮解物品的使用方法如下:As shown in Figure 3, the weighing system of the present invention with deoxidizing function and cyclic dehumidification weighing easy deliquescence items is as follows:

(1)在称重开始前,打开放置箱隔热密封门3,将密封着的物品放置到物品放置箱1,然后关闭放置箱隔热密封门3,打开操作箱隔热密封门2;(1) Before starting the weighing, open the heat insulation sealing door 3 of the placing box, place the sealed item in the item placing box 1, then close the heat insulation sealing door 3 of the placing box, and open the heat insulation sealing door 2 of the operation box;

(2)打开电磁阀V1,称量装置内的气体通过空气净化装置14并按照上述湿度控制处理系统的工作流程进行除湿,再经过匀流减速装置8回到称量装置中,待称量装置内的湿度满足物品称量要求时,关闭湿度控制处理系统进行精细称量操作。(2) Open the solenoid valve V1, the gas in the weighing device passes through the air purification device 14 and is dehumidified according to the work flow of the above-mentioned humidity control processing system, and then returns to the weighing device through the uniform flow deceleration device 8, waiting for the weighing device When the humidity inside meets the weighing requirements of the item, close the humidity control processing system for fine weighing operation.

如图6所示,本发明带有除氧功能同时可循环除湿的称重系统称量易氧化物品的使用方法如下:As shown in Figure 6, the weighing system of the present invention with deoxidizing function and cyclic dehumidification is as follows:

(1)与上述称量易潮解物品步骤(1)相同;(1) is identical with the above-mentioned step (1) of weighing easily deliquescent articles;

(2)打开电磁阀V11、V12,关闭电磁阀V13,氮气置换装置向称量装置内充入氮气,称量装置内原有的气体通过V12排出;操作过程中可根据操作箱9内的含氧量检测器30查看操作箱9内的氧气含量,若操作箱9中的氧气含量满足物品的称重要求,则可以通过操作手孔10进行对物品的称量;若氧气含量不能满足物品的称量条件,物品对称量装置的氧气含量要求更为苛刻,则继续下列步骤;(2) Open the solenoid valves V11 and V12, close the solenoid valve V13, the nitrogen replacement device fills the weighing device with nitrogen, and the original gas in the weighing device is discharged through V12; The quantity detector 30 checks the oxygen content in the operation box 9. If the oxygen content in the operation box 9 meets the weighing requirements of the article, the article can be weighed through the operation hand hole 10; if the oxygen content cannot meet the weighing requirement of the article If the item has more stringent requirements on the oxygen content of the weighing device, continue with the following steps;

(3)关闭V12,开启电磁阀V13,称量装置内的气体通过空气净化装置14进入除氧管29,待称量装置内的含氧量满足物品称量要求时,关闭氮气置换装置进行精细称量操作。(3) Close V12, open the solenoid valve V13, the gas in the weighing device enters the deoxidizer 29 through the air purification device 14, and when the oxygen content in the weighing device meets the weighing requirements of the article, close the nitrogen replacement device for fine Weighing operation.

尽管本发明的内容已经通过上述优选实施例作了详细介绍,但应当认识到上述的描述不应被认为是对本发明的限制。在本领域技术人员阅读了上述内容后,对于本发明的多种修改和替代都将是显而易见的。因此,本发明的保护范围应由所附的权利要求来限定。While the content of the present invention has been described in detail by way of the above preferred embodiments, it should be appreciated that the above description should not be construed as limiting the present invention. Various modifications and alternatives to the present invention will be apparent to those skilled in the art upon reading the foregoing. Accordingly, the scope of protection of the present invention should be defined by the appended claims.

Claims (10)

1. The utility model provides a weighing system with but deoxidization function circulation dehumidification simultaneously which characterized in that includes: the device comprises a weighing device, a humidity control processing system and a deoxygenation system;
the weighing device includes: the operation box is used for carrying out weighing operation, and a plurality of uniform flow speed reducing devices are arranged in the operation box; after the gas in the operation box is treated by the humidity control treatment system and the oxygen removal system, the gas is returned into the operation box through the uniform flow speed reducing device;
the oxygen scavenging system comprises: the oxygen removal pipe and the nitrogen replacement device are connected with the operation box;
the humidity control processing system includes: a plurality of dehumidification chambers used alternately in cycles, the dehumidification chambers being in communication with each other; the dehumidifying chamber includes: the dehumidification device comprises a dehumidification adsorbent, a gas conveying switch, a heating concentric pipe for heating the dehumidification adsorbent, a dehumidification chamber humidity detector for detecting the humidity of gas at an outlet of a dehumidification chamber, and an exhaust pipeline for exhausting water vapor out of the dehumidification chamber; when the humidity control processing system processes gas, a gas delivery switch of one of the dehumidifying chambers is turned on, the gas to be processed enters the dehumidifying chamber, and the dehumidifying adsorbent adsorbs water vapor in the gas to be processed; when the detection value of the humidity detector reaches a set value, the heating concentric tube starts to heat, the gas conveying switch is closed, the heated and evaporated water vapor is discharged out of the dehumidification chamber through the exhaust pipeline, and the gas with the humidity not reaching the standard in the dehumidification chamber and the gas to be treated in the weighing device enter the other dehumidification chamber.
2. The weighing system with oxygen scavenging while being capable of cyclic dehumidification of claim 1, wherein the dehumidification chamber further comprises: the air blowing device is arranged below the dehumidifying adsorbent; when the heating concentric tube heats and evaporates the moisture in the dehumidifying adsorbent, the blowing device blows air to accelerate the drying of the dehumidifying adsorbent.
3. The weighing system with oxygen removal and simultaneously capable of cyclic dehumidification as claimed in claim 1, wherein said uniform flow deceleration means comprises: two honeycomb airflow channels with different apertures; the two sections of honeycomb airflow channels with different apertures are divided into a primary channel and a secondary channel, and the cross sections of the primary channel and the secondary channel are in regular hexagons; each primary channel is divided into 19 secondary channels at the section close to the inner side of the operation box, and the side length of the section hexagon of the secondary channels is 1.5mm-2.3 mm.
4. The weighing system with oxygen removal and simultaneously capable of cyclically dehumidifying as claimed in claim 1, wherein the dehumidifying adsorbent is a composite adsorbing material of hygroscopic salt and porous matrix.
5. The weighing system with oxygen scavenging while being capable of cyclic dehumidification of claim 1, further comprising: the air in the operation box is treated by the air purification devices and then is input into the oxygen removal pipe and the humidity control treatment system; the inside of air purification device is filled with active carbon, air purification device's export is equipped with filtration membrane.
6. The weighing system with the oxygen removal function and the cyclic dehumidification function as claimed in claim 5, wherein the filtering membrane is a synthetic fiber filter paper or a polytetrafluoroethylene microporous membrane, and the gas in the weighing device is purified by activated carbon and then filtered by the filtering membrane, so that the purifying effect is improved, and the service life of the filtering membrane is prolonged.
7. The weighing system with oxygen scavenging while being capable of cyclic dehumidification of claim 1, further comprising: and the damping device is arranged below the weighing device.
8. The weighing system with the oxygen removing function and the simultaneous cyclic dehumidification function as claimed in claim 1, wherein the number of the oxygen removing pipes is multiple, and the oxygen removing pipes are arranged in parallel; and a deoxidizer is filled in the deoxidizing pipe, the deoxidizer takes a molecular sieve as a carrier, and metal is loaded on the surface of the molecular sieve.
9. The weighing system with oxygen scavenging and simultaneously cyclic dehumidification of claim 1, wherein the gas delivery switch is a solenoid valve.
10. The weighing system with oxygen scavenging while being capable of cyclic dehumidification as claimed in claim 1, wherein said weighing means further comprises: the article placing box is arranged beside the operation box; and sealing doors are arranged on the outer side of the article placing box and between the operating box and the article placing box.
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CN107362661A (en) * 2017-09-14 2017-11-21 中南大学 A kind of gas cleaning plant and its application
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CN208872401U (en) * 2018-09-21 2019-05-17 江苏富奇恒温设备有限公司 A kind of constant temperature and humidity weight box with dehumidification device

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Publication number Priority date Publication date Assignee Title
CN202921152U (en) * 2012-11-21 2013-05-08 深圳清华大学研究院 Environmental testing machine and dehumidifying device thereof
CN104849170A (en) * 2015-06-11 2015-08-19 上海海事大学 System and method for testing open-type adsorption performance of solar energy adsorption water preparation pipe
CN107362661A (en) * 2017-09-14 2017-11-21 中南大学 A kind of gas cleaning plant and its application
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CN208872401U (en) * 2018-09-21 2019-05-17 江苏富奇恒温设备有限公司 A kind of constant temperature and humidity weight box with dehumidification device

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