CN113149764A - Lande goose manure organic fertilizer and preparation process thereof - Google Patents
Lande goose manure organic fertilizer and preparation process thereof Download PDFInfo
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- 239000003895 organic fertilizer Substances 0.000 title claims abstract description 40
- 241000272814 Anser sp. Species 0.000 title claims abstract description 28
- 210000003608 fece Anatomy 0.000 title claims abstract description 28
- 239000010871 livestock manure Substances 0.000 title claims abstract description 28
- 238000002360 preparation method Methods 0.000 title claims abstract description 24
- 239000004005 microsphere Substances 0.000 claims abstract description 75
- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 claims abstract description 72
- 230000000844 anti-bacterial effect Effects 0.000 claims abstract description 63
- 230000012010 growth Effects 0.000 claims abstract description 53
- 229920001661 Chitosan Polymers 0.000 claims abstract description 27
- 239000008139 complexing agent Substances 0.000 claims abstract description 25
- IXPNQXFRVYWDDI-UHFFFAOYSA-N 1-methyl-2,4-dioxo-1,3-diazinane-5-carboximidamide Chemical compound CN1CC(C(N)=N)C(=O)NC1=O IXPNQXFRVYWDDI-UHFFFAOYSA-N 0.000 claims abstract description 22
- 235000010413 sodium alginate Nutrition 0.000 claims abstract description 22
- 239000000661 sodium alginate Substances 0.000 claims abstract description 22
- 229940005550 sodium alginate Drugs 0.000 claims abstract description 22
- 239000010902 straw Substances 0.000 claims abstract description 10
- 239000002994 raw material Substances 0.000 claims abstract description 8
- 239000000843 powder Substances 0.000 claims abstract description 7
- 238000011534 incubation Methods 0.000 claims abstract 5
- 239000003242 anti bacterial agent Substances 0.000 claims description 23
- 239000003814 drug Substances 0.000 claims description 21
- 239000003630 growth substance Substances 0.000 claims description 20
- 229940010698 activated attapulgite Drugs 0.000 claims description 14
- 238000002156 mixing Methods 0.000 claims description 13
- 238000001816 cooling Methods 0.000 claims description 10
- 229960000892 attapulgite Drugs 0.000 claims description 8
- 229910052625 palygorskite Inorganic materials 0.000 claims description 8
- 239000000463 material Substances 0.000 claims description 7
- 238000000855 fermentation Methods 0.000 claims description 6
- 230000004151 fermentation Effects 0.000 claims description 6
- 239000005979 Forchlorfenuron Substances 0.000 claims description 5
- 238000001354 calcination Methods 0.000 claims description 5
- -1 compound sodium nitrophenolate Chemical class 0.000 claims description 5
- GPXLRLUVLMHHIK-UHFFFAOYSA-N forchlorfenuron Chemical compound C1=NC(Cl)=CC(NC(=O)NC=2C=CC=CC=2)=C1 GPXLRLUVLMHHIK-UHFFFAOYSA-N 0.000 claims description 5
- 238000003756 stirring Methods 0.000 claims description 5
- 239000000203 mixture Substances 0.000 claims description 4
- 238000005469 granulation Methods 0.000 claims description 3
- 230000003179 granulation Effects 0.000 claims description 3
- 238000012216 screening Methods 0.000 claims description 3
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 abstract description 4
- 241000238631 Hexapoda Species 0.000 abstract description 3
- 230000001954 sterilising effect Effects 0.000 abstract description 3
- 229910052757 nitrogen Inorganic materials 0.000 abstract description 2
- 230000001737 promoting effect Effects 0.000 abstract description 2
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 9
- 238000001035 drying Methods 0.000 description 9
- 239000003337 fertilizer Substances 0.000 description 6
- 239000007952 growth promoter Substances 0.000 description 5
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 5
- 241000628997 Flos Species 0.000 description 4
- 239000009636 Huang Qi Substances 0.000 description 4
- 241001673966 Magnolia officinalis Species 0.000 description 4
- 241001619461 Poria <basidiomycete fungus> Species 0.000 description 4
- 230000000052 comparative effect Effects 0.000 description 4
- 238000001914 filtration Methods 0.000 description 4
- 238000010992 reflux Methods 0.000 description 4
- 238000002791 soaking Methods 0.000 description 4
- 238000010025 steaming Methods 0.000 description 4
- 238000001291 vacuum drying Methods 0.000 description 4
- 241000196324 Embryophyta Species 0.000 description 3
- 239000000575 pesticide Substances 0.000 description 3
- 239000000126 substance Substances 0.000 description 3
- 240000008042 Zea mays Species 0.000 description 2
- 235000005824 Zea mays ssp. parviglumis Nutrition 0.000 description 2
- 235000002017 Zea mays subsp mays Nutrition 0.000 description 2
- 238000010521 absorption reaction Methods 0.000 description 2
- 230000003115 biocidal effect Effects 0.000 description 2
- 239000002131 composite material Substances 0.000 description 2
- 235000005822 corn Nutrition 0.000 description 2
- 238000005516 engineering process Methods 0.000 description 2
- 230000002708 enhancing effect Effects 0.000 description 2
- 230000035558 fertility Effects 0.000 description 2
- 150000004676 glycans Chemical class 0.000 description 2
- 238000004519 manufacturing process Methods 0.000 description 2
- 235000015097 nutrients Nutrition 0.000 description 2
- 230000008635 plant growth Effects 0.000 description 2
- 229920001282 polysaccharide Polymers 0.000 description 2
- 239000005017 polysaccharide Substances 0.000 description 2
- 230000004083 survival effect Effects 0.000 description 2
- 241000894006 Bacteria Species 0.000 description 1
- 240000003183 Manihot esculenta Species 0.000 description 1
- 235000016735 Manihot esculenta subsp esculenta Nutrition 0.000 description 1
- 241000607626 Vibrio cholerae Species 0.000 description 1
- 239000013543 active substance Substances 0.000 description 1
- 238000010564 aerobic fermentation Methods 0.000 description 1
- 229910000323 aluminium silicate Inorganic materials 0.000 description 1
- SNAAJJQQZSMGQD-UHFFFAOYSA-N aluminum magnesium Chemical compound [Mg].[Al] SNAAJJQQZSMGQD-UHFFFAOYSA-N 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 238000005341 cation exchange Methods 0.000 description 1
- 239000002734 clay mineral Substances 0.000 description 1
- 230000000536 complexating effect Effects 0.000 description 1
- 239000011162 core material Substances 0.000 description 1
- 238000001514 detection method Methods 0.000 description 1
- 238000011161 development Methods 0.000 description 1
- 235000019621 digestibility Nutrition 0.000 description 1
- HNPSIPDUKPIQMN-UHFFFAOYSA-N dioxosilane;oxo(oxoalumanyloxy)alumane Chemical compound O=[Si]=O.O=[Al]O[Al]=O HNPSIPDUKPIQMN-UHFFFAOYSA-N 0.000 description 1
- 235000019441 ethanol Nutrition 0.000 description 1
- 230000002045 lasting effect Effects 0.000 description 1
- 230000007774 longterm Effects 0.000 description 1
- 230000004060 metabolic process Effects 0.000 description 1
- 230000000813 microbial effect Effects 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 231100000956 nontoxicity Toxicity 0.000 description 1
- 239000005416 organic matter Substances 0.000 description 1
- 238000011056 performance test Methods 0.000 description 1
- 230000002035 prolonged effect Effects 0.000 description 1
- 150000003839 salts Chemical class 0.000 description 1
- 239000002689 soil Substances 0.000 description 1
- 238000004659 sterilization and disinfection Methods 0.000 description 1
- 229940118696 vibrio cholerae Drugs 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05G—MIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
- C05G3/00—Mixtures of one or more fertilisers with additives not having a specially fertilising activity
-
- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05D—INORGANIC FERTILISERS NOT COVERED BY SUBCLASSES C05B, C05C; FERTILISERS PRODUCING CARBON DIOXIDE
- C05D5/00—Fertilisers containing magnesium
-
- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05G—MIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
- C05G3/00—Mixtures of one or more fertilisers with additives not having a specially fertilising activity
- C05G3/60—Biocides or preservatives, e.g. disinfectants, pesticides or herbicides; Pest repellants or attractants
Landscapes
- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Pest Control & Pesticides (AREA)
- Organic Chemistry (AREA)
- Plant Pathology (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Inorganic Chemistry (AREA)
- Fertilizers (AREA)
Abstract
The invention discloses a landes goose manure organic fertilizer which is prepared from the following raw materials: lande goose manure, straw powder, biological strains and a growth antibacterial complexing agent; the preparation process of the growth antibacterial complexing agent comprises the following steps: adding the growth antibacterial microspheres into an acetic acid solution of chitosan for incubation, taking out, and airing to remove the solution on the surfaces of the growth antibacterial microspheres to obtain first coated microspheres; adding the first coated microspheres into a sodium alginate solution for incubation, taking out, and airing to remove the solution on the surfaces of the first coated microspheres to obtain second coated microspheres; adding the second coated microspheres into an acetic acid solution of chitosan again for incubation, taking out, and airing to remove the solution on the surfaces of the growing antibacterial microspheres to obtain third coated microspheres; the organic fertilizer prepared by taking the Langder goose manure as the main raw material has high nitrogen content, the efficiency of the organic fertilizer is improved, and the growth antibacterial complexing agent has good growth promoting and insect-resistant and sterilizing effects on crops.
Description
Technical Field
The invention belongs to the technical field of organic fertilizers, relates to an organic fertilizer and a preparation process thereof, and particularly relates to a lander goose manure organic fertilizer and a preparation process thereof.
Background
The invention patent CN105330375A discloses a high-efficiency biological organic fertilizer and a preparation method thereof. By utilizing an aerobic fermentation technology, mechanically dehydrating cassava alcohol biogas residues, adding auxiliary materials, inoculating aerobic microbial flora, drying, crushing, granulating and adding composite functional bacteria, wherein the organic fertilizer obtained after fermentation comprises the following components in percentage by weight: 40-60% of organic matter (calculated by dry basis), 6-7% of total nutrient (calculated by dry basis) and 0.5-2 hundred million/g of effective viable count. Solves the problems that the prior organic fertilizer production technology has long fermentation period, the fertilizer efficiency of the fermented product is low, secondary pollution is caused to the environment, and the soil hardening caused by long-term application of the fertilizer restricts large-scale application. The obtained organic fertilizer meets the organic fertilizer detection standard of Ministry of agriculture, has high fertilizer efficiency and short fermentation period, does not cause secondary pollution to the environment, and is very suitable for industrial mass production.
In the market, most organic fertilizers only have the functions of increasing fertility and enhancing efficiency, but are poor in the aspects of antibiosis and disinsection, and the survival rate of crops during growth is influenced; in addition, the growth promoter is not effectively combined with the organic fertilizer; when the pesticide and the growth promoter are used independently, the pesticide and the growth promoter have the problems of too fast release and difficult absorption by plants.
Disclosure of Invention
The invention aims to solve the problems that most organic fertilizers only play a role in increasing fertility and enhancing efficiency in the market, but are poor in the aspects of antibiosis and disinsection and influence the survival rate of crops during growth; in addition, the growth promoter is not effectively combined with the organic fertilizer; when the pesticide and the growth promoter are used independently, the problems of too fast release and difficult plant absorption exist, and the Lander goose manure organic fertilizer and the preparation process thereof are provided.
The purpose of the invention can be realized by the following technical scheme:
the organic fertilizer is prepared from the following raw materials in parts by weight: 60-70 parts of Langde goose manure, 20-30 parts of straw powder, 1-2 parts of biological strain and 10-18 parts of growth antibacterial complexing agent;
the preparation process of the growth antibacterial complexing agent comprises the following steps:
the first step is as follows: adding the growth antibacterial microspheres into an acetic acid solution of chitosan with the mass fraction of 1%, incubating for 10min, taking out, and airing to remove the solution on the surfaces of the growth antibacterial microspheres to obtain first coated microspheres;
the second step is that: adding the first coated microspheres into a sodium alginate solution with the mass fraction of 1%, incubating for 10min, taking out, and drying in the air to remove the solution on the surfaces of the first coated microspheres to obtain second coated microspheres;
the third step: adding the second coated microspheres into an acetic acid solution of chitosan with the mass fraction of 1% again, incubating for 10min, taking out, and airing to remove the solution on the surfaces of the growing antibacterial microspheres to obtain third coated microspheres; placing the third coated microspheres in an oven and drying to constant weight to obtain a growth antibacterial complexing agent;
the acetic acid solution of chitosan with the mass fraction of 1% is prepared by 10g of chitosan and 100g of acetic acid solution with the mass fraction of 2%; controlling the mass ratio of growth antibacterial microspheres, 1% of chitosan acetic acid solution and 1% of sodium alginate solution to be 5: 20-30:20-30.
A preparation process of a landes goose manure organic fertilizer comprises the following steps:
the first step is as follows: placing the activated biological strains, crop straws and Langde goose manure into a turning and throwing machine for uniform mixing, and performing stack fermentation to obtain an organic fertilizer primary material;
the second step is that: mixing the organic fertilizer primary material with the growth antibacterial complexing agent, adding the mixture into a granulator for granulation and screening to obtain the landes goose manure organic fertilizer.
Preferably, the preparation process of the growing antibacterial microspheres comprises the following steps:
the first step is as follows: calcining the attapulgite in a muffle furnace at the temperature of 300 ℃ for 3h, and cooling to room temperature to obtain activated attapulgite;
the second step is that: mixing the traditional Chinese medicine antibacterial agent, the growth regulator, sodium alginate and activated attapulgite, stirring for 3h at the temperature of 100 ℃, and cooling to room temperature to obtain growth antibacterial microspheres;
controlling the mass ratio of the activated attapulgite to the traditional Chinese medicine antibacterial agent to the growth regulator to the sodium alginate to be 5-10: 1: 1: 1.2-1.5.
Preferably, the preparation process of the traditional Chinese medicine antibacterial agent comprises the following steps:
soaking the Chinese medicinal decoction pieces in anhydrous ethanol for 30min, extracting under reflux in water bath for 3 hr, filtering, rotary steaming, and vacuum drying to obtain Chinese medicinal antibacterial agent; the mass ratio of the traditional Chinese medicine decoction pieces to the absolute ethyl alcohol is controlled to be 20-30: 100-150.
Preferably, the Chinese medicinal decoction pieces comprise one or more of radix astragali, Poria, flos Lonicerae, radix Angelicae sinensis and cortex Magnolia officinalis;
preferably, the growth regulator comprises one or more of forchlorfenuron and compound sodium nitrophenolate.
Compared with the prior art, the invention has the beneficial effects that:
the physiological active substances in the traditional Chinese medicine not only have the functions of sterilization and insect resistance, but also can improve the digestibility and the utilization rate of nutrient substances, enhance the metabolism and promote the growth of plants; the growth regulator can effectively regulate and control the growth and development of plants; the attapulgite is a chain layered water-containing magnesium-aluminum-rich aluminosilicate clay mineral and has good physical and chemical properties such as adsorptivity, cation exchange property, thermal stability, salt resistance and the like; mixing the attapulgite with the traditional Chinese medicine antibacterial agent and the growth regulator to ensure that the traditional Chinese medicine antibacterial agent and the growth regulator are well attached to the attapulgite;
according to the invention, sodium alginate is a natural polyanionic polysaccharide, chitosan is a polycationic polysaccharide, and sodium alginate and chitosan have the advantages of good degradability, biocompatibility and nontoxicity, so that the growing antibacterial microspheres are taken as core materials by utilizing the electrostatic acting force between substances with opposite charges of sodium alginate and chitosan, and the surface of the growing antibacterial microspheres is subjected to layer-by-layer complexing alternation to form a composite film, thus obtaining the growing antibacterial complexing agent;
then, mixing the growth antibacterial complexing agent with the Langder goose manure and straw powder to prepare the Langder goose manure organic fertilizer, so that the growth antibacterial complexing agent in the organic fertilizer can control the release rate and the release period of the traditional Chinese medicine antibacterial agent and the growth regulator, the lasting period of the antibacterial agent and the growth regulator is prolonged, the growth regulator can be efficiently absorbed by crops, and the antibacterial agent can be efficiently sterilized;
the organic fertilizer prepared by taking the Langder goose manure as the main raw material contains high nitrogen content, the efficiency of the organic fertilizer is improved, and the growth antibacterial complexing agent has good growth promoting and insect-resistant and sterilizing effects on crops.
Detailed Description
The technical solutions of the present invention will be described clearly and completely with reference to the following embodiments, and it should be understood that the described embodiments are only a part of the embodiments of the present invention, and not all of the embodiments. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention.
Example 1
The organic fertilizer is prepared from the following raw materials in parts by weight: 60 parts of Langde goose manure, 20 parts of straw powder, 1 part of biological strain and 10 parts of growth antibacterial complexing agent;
the preparation process of the growth antibacterial complexing agent comprises the following steps:
the first step is as follows: adding the growth antibacterial microspheres into an acetic acid solution of chitosan with the mass fraction of 1%, incubating for 10min, taking out, and airing to remove the solution on the surfaces of the growth antibacterial microspheres to obtain first coated microspheres;
the second step is that: adding the first coated microspheres into a sodium alginate solution with the mass fraction of 1%, incubating for 10min, taking out, and drying in the air to remove the solution on the surfaces of the first coated microspheres to obtain second coated microspheres;
the third step: adding the second coated microspheres into an acetic acid solution of chitosan with the mass fraction of 1% again, incubating for 10min, taking out, and airing to remove the solution on the surfaces of the growing antibacterial microspheres to obtain third coated microspheres; placing the third coated microspheres in an oven and drying to constant weight to obtain a growth antibacterial complexing agent;
the acetic acid solution of chitosan with the mass fraction of 1% is prepared by 10g of chitosan and 100g of acetic acid solution with the mass fraction of 2%; controlling the mass ratio of growth antibacterial microspheres, 1% of chitosan acetic acid solution and 1% of sodium alginate solution to be 5: 20:20.
Example 2
The organic fertilizer is prepared from the following raw materials in parts by weight: 65 parts of Langde goose manure, 25 parts of straw powder, 1.5 parts of biological strains and 14 parts of growth antibacterial complexing agent;
the preparation process of the growth antibacterial complexing agent comprises the following steps:
the first step is as follows: adding the growth antibacterial microspheres into an acetic acid solution of chitosan with the mass fraction of 1%, incubating for 10min, taking out, and airing to remove the solution on the surfaces of the growth antibacterial microspheres to obtain first coated microspheres;
the second step is that: adding the first coated microspheres into a sodium alginate solution with the mass fraction of 1%, incubating for 10min, taking out, and drying in the air to remove the solution on the surfaces of the first coated microspheres to obtain second coated microspheres;
the third step: adding the second coated microspheres into an acetic acid solution of chitosan with the mass fraction of 1% again, incubating for 10min, taking out, and airing to remove the solution on the surfaces of the growing antibacterial microspheres to obtain third coated microspheres; placing the third coated microspheres in an oven and drying to constant weight to obtain a growth antibacterial complexing agent;
the acetic acid solution of chitosan with the mass fraction of 1% is prepared by 10g of chitosan and 100g of acetic acid solution with the mass fraction of 2%; controlling the mass ratio of growth antibacterial microspheres, 1% of chitosan acetic acid solution and 1% of sodium alginate solution to be 5: 25:25.
Example 3
The organic fertilizer is prepared from the following raw materials in parts by weight: 70 parts of Langde goose manure, 30 parts of straw powder, 2 parts of biological strains and 18 parts of growth antibacterial complexing agent;
the preparation process of the growth antibacterial complexing agent comprises the following steps:
the first step is as follows: adding the growth antibacterial microspheres into an acetic acid solution of chitosan with the mass fraction of 1%, incubating for 10min, taking out, and airing to remove the solution on the surfaces of the growth antibacterial microspheres to obtain first coated microspheres;
the second step is that: adding the first coated microspheres into a sodium alginate solution with the mass fraction of 1%, incubating for 10min, taking out, and drying in the air to remove the solution on the surfaces of the first coated microspheres to obtain second coated microspheres;
the third step: adding the second coated microspheres into an acetic acid solution of chitosan with the mass fraction of 1% again, incubating for 10min, taking out, and airing to remove the solution on the surfaces of the growing antibacterial microspheres to obtain third coated microspheres; placing the third coated microspheres in an oven and drying to constant weight to obtain a growth antibacterial complexing agent;
the acetic acid solution of chitosan with the mass fraction of 1% is prepared by 10g of chitosan and 100g of acetic acid solution with the mass fraction of 2%; controlling the mass ratio of growth antibacterial microspheres, 1% of chitosan acetic acid solution and 1% of sodium alginate solution to be 5: 30:30.
Example 4
The preparation process of the growing antibacterial microspheres comprises the following steps:
the first step is as follows: calcining the attapulgite in a muffle furnace at the temperature of 300 ℃ for 3h, and cooling to room temperature to obtain activated attapulgite;
the second step is that: mixing the traditional Chinese medicine antibacterial agent, the growth regulator, sodium alginate and activated attapulgite, stirring for 3h at the temperature of 100 ℃, and cooling to room temperature to obtain growth antibacterial microspheres;
controlling the mass ratio of the activated attapulgite to the traditional Chinese medicine antibacterial agent to the growth regulator to the sodium alginate to be 5: 1: 1: 1.2.
the preparation process of the traditional Chinese medicine antibacterial agent comprises the following steps:
soaking the Chinese medicinal decoction pieces in anhydrous ethanol for 30min, extracting under reflux in water bath for 3 hr, filtering, rotary steaming, and vacuum drying to obtain Chinese medicinal antibacterial agent; the mass ratio of the traditional Chinese medicine decoction pieces to the absolute ethyl alcohol is controlled to be 20: 100.
The Chinese medicinal decoction pieces comprise one or more of radix astragali, Poria, flos Lonicerae, radix Angelicae sinensis and cortex Magnolia officinalis;
the growth regulator comprises one or more of forchlorfenuron and compound sodium nitrophenolate.
Example 5
The preparation process of the growing antibacterial microspheres comprises the following steps:
the first step is as follows: calcining the attapulgite in a muffle furnace at the temperature of 300 ℃ for 3h, and cooling to room temperature to obtain activated attapulgite;
the second step is that: mixing the traditional Chinese medicine antibacterial agent, the growth regulator, sodium alginate and activated attapulgite, stirring for 3h at the temperature of 100 ℃, and cooling to room temperature to obtain growth antibacterial microspheres;
controlling the mass ratio of the activated attapulgite to the traditional Chinese medicine antibacterial agent to the growth regulator to the sodium alginate to be 8: 1: 1: 1.3.
the preparation process of the traditional Chinese medicine antibacterial agent comprises the following steps:
soaking the Chinese medicinal decoction pieces in anhydrous ethanol for 30min, extracting under reflux in water bath for 3 hr, filtering, rotary steaming, and vacuum drying to obtain Chinese medicinal antibacterial agent; the mass ratio of the traditional Chinese medicine decoction pieces to the absolute ethyl alcohol is controlled to be 25: 125.
The Chinese medicinal decoction pieces comprise one or more of radix astragali, Poria, flos Lonicerae, radix Angelicae sinensis and cortex Magnolia officinalis;
the growth regulator comprises one or more of forchlorfenuron and compound sodium nitrophenolate.
Example 6
The preparation process of the growing antibacterial microspheres comprises the following steps:
the first step is as follows: calcining the attapulgite in a muffle furnace at the temperature of 300 ℃ for 3h, and cooling to room temperature to obtain activated attapulgite;
the second step is that: mixing the traditional Chinese medicine antibacterial agent, the growth regulator, sodium alginate and activated attapulgite, stirring for 3h at the temperature of 100 ℃, and cooling to room temperature to obtain growth antibacterial microspheres;
controlling the mass ratio of the activated attapulgite to the traditional Chinese medicine antibacterial agent to the growth regulator to the sodium alginate to be 10: 1: 1: 1.5.
the preparation process of the traditional Chinese medicine antibacterial agent comprises the following steps:
soaking the Chinese medicinal decoction pieces in anhydrous ethanol for 30min, extracting under reflux in water bath for 3 hr, filtering, rotary steaming, and vacuum drying to obtain Chinese medicinal antibacterial agent; the mass ratio of the traditional Chinese medicine decoction pieces to the absolute ethyl alcohol is controlled to be 30: 150.
The Chinese medicinal decoction pieces comprise one or more of radix astragali, Poria, flos Lonicerae, radix Angelicae sinensis and cortex Magnolia officinalis;
the growth regulator comprises one or more of forchlorfenuron and compound sodium nitrophenolate.
Example 7
A preparation process of a landes goose manure organic fertilizer comprises the following steps:
the first step is as follows: placing the activated biological strains, crop straws and Langde goose manure into a turning and throwing machine for uniform mixing, and performing stack fermentation to obtain an organic fertilizer primary material;
the second step is that: mixing the organic fertilizer primary material with the growth antibacterial complexing agent, adding the mixture into a granulator for granulation and screening to obtain the landes goose manure organic fertilizer.
Comparative example 1
Comparative example 1 is the organic fertilizer of examples 1-3 without added growth antibacterial agent;
the antibacterial (the strain is vibrio cholerae) performance tests are carried out on the examples 1-3 and the comparative example 1;
| antibacterial ratio (%) | Corn 60 day height increasing (cm) | |
| Example 1 | 88.3 | 113.9 |
| Example 2 | 88.9 | 118.4 |
| Example 3 | 89.4 | 120.5 |
| Comparative example 1 | 0 | 98.3 |
As can be seen from the table, the organic fertilizer prepared from the Langder goose manure has a good antibacterial effect, and the antibacterial rate is 88.3-89.4%; taking corn as an example, the average growth height of 60 days is 113.9-120.5cm, and the growth of plants can be effectively promoted.
The preferred embodiments of the invention disclosed above are intended to be illustrative only. The preferred embodiments are not intended to be exhaustive or to limit the invention to the precise forms disclosed. Obviously, many modifications and variations are possible in light of the above teaching. The embodiments were chosen and described in order to best explain the principles of the invention and the practical application, to thereby enable others skilled in the art to best utilize the invention. The invention is limited only by the claims and their full scope and equivalents.
Claims (4)
1. A Lande goose manure organic fertilizer is characterized in that: the composition is characterized by comprising the following raw materials in parts by weight: 60-70 parts of Langde goose manure, 20-30 parts of straw powder, 1-2 parts of biological strain and 10-18 parts of growth antibacterial complexing agent;
the preparation process of the growth antibacterial complexing agent comprises the following steps:
the first step is as follows: adding the growth antibacterial microspheres into an acetic acid solution of chitosan for incubation for 10min, taking out, and airing to remove the solution on the surfaces of the growth antibacterial microspheres to obtain first coated microspheres;
the second step is that: adding the first coated microspheres into a sodium alginate solution, incubating for 10min, taking out, and airing to remove the solution on the surfaces of the first coated microspheres to obtain second coated microspheres;
the third step: adding the second coated microspheres into an acetic acid solution of chitosan again for incubation for 10min, taking out, and airing to remove the solution on the surfaces of the growing antibacterial microspheres to obtain third coated microspheres; and (4) placing the third coated microspheres in an oven to dry to constant weight to obtain the growth antibacterial complexing agent.
2. The Langdian goose manure organic fertilizer as claimed in claim 1, wherein the preparation process of the growth antibacterial microspheres comprises the following steps:
the first step is as follows: calcining the attapulgite in a muffle furnace at the temperature of 300 ℃ for 3h, and cooling to room temperature to obtain activated attapulgite;
the second step is that: mixing the traditional Chinese medicine antibacterial agent, the growth regulator, sodium alginate and the activated attapulgite, stirring for 3h at the temperature of 100 ℃, and cooling to room temperature to obtain the growth antibacterial microspheres.
3. The Lander goose manure organic fertilizer as claimed in claim 2, wherein the growth regulator comprises one of forchlorfenuron and compound sodium nitrophenolate.
4. A preparation process of a landes goose manure organic fertilizer is characterized by comprising the following steps:
the first step is as follows: placing the activated biological strains, crop straws and Langde goose manure into a turning and throwing machine for uniform mixing, and performing stack fermentation to obtain an organic fertilizer primary material;
the second step is that: mixing the organic fertilizer primary material with the growth antibacterial complexing agent, adding the mixture into a granulator for granulation and screening to obtain the landes goose manure organic fertilizer.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202110495219.3A CN113149764A (en) | 2021-05-07 | 2021-05-07 | Lande goose manure organic fertilizer and preparation process thereof |
Applications Claiming Priority (1)
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Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104311253A (en) * | 2014-09-29 | 2015-01-28 | 成都新柯力化工科技有限公司 | Chitosan controlled release fertilizer microspheres and preparation method thereof |
| CN105565969A (en) * | 2015-12-10 | 2016-05-11 | 深圳市芭田生态工程股份有限公司 | Double-coated slow-release microspherical calcium fertilizer and preparation method and application of same |
| CN106070196A (en) * | 2016-06-29 | 2016-11-09 | 固镇县华丰蔬菜专业合作社 | A kind of Fructus Lycopersici esculenti special plant source pesticide |
| CN108249975A (en) * | 2017-12-29 | 2018-07-06 | 安徽乐农环保科技有限公司 | A kind of preparation method based on concave convex rod modified material complex microorganism organic fertilizer |
| CN112552124A (en) * | 2020-12-01 | 2021-03-26 | 霍邱县荣益喜洋洋有机肥有限公司 | Lande goose manure organic fertilizer and preparation method thereof |
| AU2021101074A4 (en) * | 2021-02-02 | 2021-04-29 | Henan Agricultural University | Method for preparing gel microsphere based on anaerobic fermentation raffinate and application thereof |
-
2021
- 2021-05-07 CN CN202110495219.3A patent/CN113149764A/en active Pending
Patent Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104311253A (en) * | 2014-09-29 | 2015-01-28 | 成都新柯力化工科技有限公司 | Chitosan controlled release fertilizer microspheres and preparation method thereof |
| CN105565969A (en) * | 2015-12-10 | 2016-05-11 | 深圳市芭田生态工程股份有限公司 | Double-coated slow-release microspherical calcium fertilizer and preparation method and application of same |
| CN106070196A (en) * | 2016-06-29 | 2016-11-09 | 固镇县华丰蔬菜专业合作社 | A kind of Fructus Lycopersici esculenti special plant source pesticide |
| CN108249975A (en) * | 2017-12-29 | 2018-07-06 | 安徽乐农环保科技有限公司 | A kind of preparation method based on concave convex rod modified material complex microorganism organic fertilizer |
| CN112552124A (en) * | 2020-12-01 | 2021-03-26 | 霍邱县荣益喜洋洋有机肥有限公司 | Lande goose manure organic fertilizer and preparation method thereof |
| AU2021101074A4 (en) * | 2021-02-02 | 2021-04-29 | Henan Agricultural University | Method for preparing gel microsphere based on anaerobic fermentation raffinate and application thereof |
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Application publication date: 20210723 |