CN112972307A - Waterproof sweat-proof lasting eyebrow pencil and preparation method thereof - Google Patents
Waterproof sweat-proof lasting eyebrow pencil and preparation method thereof Download PDFInfo
- Publication number
- CN112972307A CN112972307A CN202110206819.3A CN202110206819A CN112972307A CN 112972307 A CN112972307 A CN 112972307A CN 202110206819 A CN202110206819 A CN 202110206819A CN 112972307 A CN112972307 A CN 112972307A
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- wax
- eyebrow pencil
- polyethylene glycol
- waterproof
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- 210000004709 eyebrow Anatomy 0.000 title claims abstract description 36
- 238000002360 preparation method Methods 0.000 title abstract description 6
- 230000002045 lasting effect Effects 0.000 title abstract description 5
- 239000001993 wax Substances 0.000 claims abstract description 40
- 239000002202 Polyethylene glycol Substances 0.000 claims abstract description 25
- 229920001223 polyethylene glycol Polymers 0.000 claims abstract description 25
- 239000003086 colorant Substances 0.000 claims abstract description 20
- 239000012182 japan wax Substances 0.000 claims abstract description 19
- 239000000945 filler Substances 0.000 claims abstract description 16
- UYXTWWCETRIEDR-UHFFFAOYSA-N Tributyrin Chemical compound CCCC(=O)OCC(OC(=O)CCC)COC(=O)CCC UYXTWWCETRIEDR-UHFFFAOYSA-N 0.000 claims abstract description 9
- 239000004359 castor oil Substances 0.000 claims abstract description 9
- 235000019438 castor oil Nutrition 0.000 claims abstract description 9
- ZEMPKEQAKRGZGQ-XOQCFJPHSA-N glycerol triricinoleate Natural products CCCCCC[C@@H](O)CC=CCCCCCCCC(=O)OC[C@@H](COC(=O)CCCCCCCC=CC[C@@H](O)CCCCCC)OC(=O)CCCCCCCC=CC[C@H](O)CCCCCC ZEMPKEQAKRGZGQ-XOQCFJPHSA-N 0.000 claims abstract description 9
- 210000004243 sweat Anatomy 0.000 claims abstract description 8
- 229920001800 Shellac Polymers 0.000 claims description 20
- 239000004208 shellac Substances 0.000 claims description 20
- 235000013874 shellac Nutrition 0.000 claims description 20
- ZLGIYFNHBLSMPS-ATJNOEHPSA-N shellac Chemical compound OCCCCCC(O)C(O)CCCCCCCC(O)=O.C1C23[C@H](C(O)=O)CCC2[C@](C)(CO)[C@@H]1C(C(O)=O)=C[C@@H]3O ZLGIYFNHBLSMPS-ATJNOEHPSA-N 0.000 claims description 20
- 229940113147 shellac Drugs 0.000 claims description 20
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims description 6
- 238000002844 melting Methods 0.000 claims description 6
- 230000008018 melting Effects 0.000 claims description 6
- 238000000034 method Methods 0.000 claims description 6
- 238000003756 stirring Methods 0.000 claims description 6
- 238000000227 grinding Methods 0.000 claims description 4
- 239000000463 material Substances 0.000 claims description 4
- 239000010445 mica Substances 0.000 claims description 4
- 229910052618 mica group Inorganic materials 0.000 claims description 4
- 238000001816 cooling Methods 0.000 claims description 3
- 238000010438 heat treatment Methods 0.000 claims description 3
- 238000010299 mechanically pulverizing process Methods 0.000 claims description 3
- 238000002156 mixing Methods 0.000 claims description 3
- 239000000377 silicon dioxide Substances 0.000 claims description 3
- 238000000465 moulding Methods 0.000 claims description 2
- 230000001166 anti-perspirative effect Effects 0.000 claims 2
- 239000003213 antiperspirant Substances 0.000 claims 2
- 239000002537 cosmetic Substances 0.000 abstract description 7
- 230000000694 effects Effects 0.000 abstract description 7
- 238000000926 separation method Methods 0.000 abstract description 5
- 239000000203 mixture Substances 0.000 abstract description 3
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 abstract description 2
- 230000000052 comparative effect Effects 0.000 description 10
- 238000012360 testing method Methods 0.000 description 10
- 230000032798 delamination Effects 0.000 description 6
- 230000001953 sensory effect Effects 0.000 description 4
- 235000013871 bee wax Nutrition 0.000 description 3
- 239000012166 beeswax Substances 0.000 description 3
- 239000004519 grease Substances 0.000 description 3
- 239000000843 powder Substances 0.000 description 3
- 125000003178 carboxy group Chemical group [H]OC(*)=O 0.000 description 2
- 239000003153 chemical reaction reagent Substances 0.000 description 2
- 125000000524 functional group Chemical group 0.000 description 2
- 239000008266 hair spray Substances 0.000 description 2
- 230000006872 improvement Effects 0.000 description 2
- 230000007774 longterm Effects 0.000 description 2
- 238000012986 modification Methods 0.000 description 2
- 230000004048 modification Effects 0.000 description 2
- 230000008569 process Effects 0.000 description 2
- 238000007493 shaping process Methods 0.000 description 2
- 238000003860 storage Methods 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- 238000006467 substitution reaction Methods 0.000 description 2
- DSEKYWAQQVUQTP-XEWMWGOFSA-N (2r,4r,4as,6as,6as,6br,8ar,12ar,14as,14bs)-2-hydroxy-4,4a,6a,6b,8a,11,11,14a-octamethyl-2,4,5,6,6a,7,8,9,10,12,12a,13,14,14b-tetradecahydro-1h-picen-3-one Chemical compound C([C@H]1[C@]2(C)CC[C@@]34C)C(C)(C)CC[C@]1(C)CC[C@]2(C)[C@H]4CC[C@@]1(C)[C@H]3C[C@@H](O)C(=O)[C@@H]1C DSEKYWAQQVUQTP-XEWMWGOFSA-N 0.000 description 1
- 239000004166 Lanolin Substances 0.000 description 1
- 229920000469 amphiphilic block copolymer Polymers 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 235000013869 carnauba wax Nutrition 0.000 description 1
- 239000004203 carnauba wax Substances 0.000 description 1
- 229940082483 carnauba wax Drugs 0.000 description 1
- 230000008859 change Effects 0.000 description 1
- 235000019868 cocoa butter Nutrition 0.000 description 1
- 229940110456 cocoa butter Drugs 0.000 description 1
- 230000003750 conditioning effect Effects 0.000 description 1
- 230000007547 defect Effects 0.000 description 1
- 239000006185 dispersion Substances 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 238000002474 experimental method Methods 0.000 description 1
- 238000009472 formulation Methods 0.000 description 1
- 230000002209 hydrophobic effect Effects 0.000 description 1
- 125000002887 hydroxy group Chemical group [H]O* 0.000 description 1
- 235000019388 lanolin Nutrition 0.000 description 1
- 229940039717 lanolin Drugs 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 238000004806 packaging method and process Methods 0.000 description 1
- 239000012188 paraffin wax Substances 0.000 description 1
- 239000000049 pigment Substances 0.000 description 1
- 229920000867 polyelectrolyte Polymers 0.000 description 1
- 238000010298 pulverizing process Methods 0.000 description 1
- 239000011347 resin Substances 0.000 description 1
- 229920005989 resin Polymers 0.000 description 1
- 238000007711 solidification Methods 0.000 description 1
- 230000008023 solidification Effects 0.000 description 1
- 230000006641 stabilisation Effects 0.000 description 1
- 238000013112 stability test Methods 0.000 description 1
- 238000011105 stabilization Methods 0.000 description 1
- 230000000087 stabilizing effect Effects 0.000 description 1
- 238000010998 test method Methods 0.000 description 1
- 230000008719 thickening Effects 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/84—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
- A61K8/86—Polyethers
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q1/00—Make-up preparations; Body powders; Preparations for removing make-up
- A61Q1/02—Preparations containing skin colorants, e.g. pigments
- A61Q1/10—Preparations containing skin colorants, e.g. pigments for eyes, e.g. eyeliner, mascara
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/52—Stabilizers
Landscapes
- Life Sciences & Earth Sciences (AREA)
- Health & Medical Sciences (AREA)
- Animal Behavior & Ethology (AREA)
- General Health & Medical Sciences (AREA)
- Public Health (AREA)
- Veterinary Medicine (AREA)
- Birds (AREA)
- Epidemiology (AREA)
- Chemical & Material Sciences (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Cosmetics (AREA)
Abstract
The invention belongs to the technical field of cosmetics, and particularly relates to a waterproof sweat-proof lasting eyebrow pencil and a preparation method thereof, wherein the waterproof sweat-proof lasting eyebrow pencil comprises the following components in parts by weight: 10-25 parts of a filler, 20-32 parts of a colorant, 5-15 parts of Japan wax, 3-10 parts of polyethylene glycol wax, 1-5 parts of hydrogenated castor oil and 2-5 parts of glycerol tri (ethyl acetate). The eyebrow pencil provided by the invention solves the problem of separation of wax and colorant by adjusting the formula composition, and the obtained product has good appearance and stability, has the functions of water resistance and sweat resistance, can effectively keep makeup, is smooth in use, is easy to develop color and has a good use effect.
Description
Technical Field
The invention belongs to the technical field of cosmetics. More particularly, it relates to a waterproof sweat-proof durable eyebrow pencil and a preparation method thereof.
Background
The eyebrow pencil lead is made from materials including grease, wax and pigment, wherein the wax is paraffin, Japan wax, beeswax, ozokerite, lanolin, carnauba wax, cocoa butter and the like, the wax mainly has thickening, solidifying and shaping effects in a formula, the melting point of the wax is generally between 45 and 110 ℃, and the wax is required to be melted firstly and then changed into flowing liquid through temperature rise to be mixed with coloring agent, filler and the like when the eyebrow pencil is prepared. But in the subsequent preparation process, the temperature is inevitably reduced for 2 to 3 times, and in the process, the separation of grease and coloring agent is easily caused, and the delamination of the product is caused.
Shellac, also known as shellac, shellac and the like, is a fatty resin, is currently used as a component of legal cosmetics in the countries of the united states, japan and the like, which are leading in cosmetic science and technology, is commonly used in hair-setting products such as hair spray, conditioning hair spray and the like, and is also used in eyeliner cosmetics. But it is not seen to be applied to eyebrow pencils to prevent wax from separating from toner.
In addition, after the eyebrow pencil is made up, the skin of a human body can secrete grease and sweat, and the eyebrow pencil without the waterproof and oil-proof functions can be made up, so that the eyebrow pencil with the waterproof and sweat-proof functions is needed.
Disclosure of Invention
The invention aims to solve the technical problem of overcoming the defects of the existing eyebrow pencil and providing the eyebrow pencil with the waterproof and sweat-proof functions.
The above purpose of the invention is realized by the following technical scheme: a waterproof sweat-proof lasting eyebrow pencil comprises the following components in parts by weight: 10-25 parts of a filler, 20-32 parts of a colorant, 5-15 parts of Japan wax, 3-10 parts of polyethylene glycol wax, 1-5 parts of hydrogenated castor oil and 2-5 parts of glycerol tri (ethyl acetate).
Preferably, the eyebrow pencil comprises the following components in parts by weight: 15-25 parts of a filler, 25-32 parts of a colorant, 10-15 parts of Japan wax, 6-10 parts of polyethylene glycol wax, 2-4 parts of hydrogenated castor oil and 2-4 parts of glycerol tri (ethyl acetate).
Preferably, the eyebrow pencil further comprises shellac.
Preferably, in the eyebrow pencil, the weight ratio of the Japan wax, the polyethylene glycol wax and the shellac is 3: 1-2: 0.1 to 1.5.
Preferably, in the eyebrow pencil, the weight ratio of the Japan wax, the polyethylene glycol wax and the shellac is 3: 1.2: 0.8.
preferably, the colorant is selected from at least one of CI77499, CI77492, CI77491 and CI 77891.
Preferably, the filler is selected from one or both of mica and silica.
Preferably, the filler is silica.
Another object of the present invention is to provide a method for preparing the eyebrow pencil, which comprises the following steps:
s1, mechanically pulverizing Japan wax, polyethylene glycol wax, colorant and filler respectively;
s2, adding the Japan wax and the polyethylene glycol wax into a melting material pot, heating to melt, adding the hydrogenated castor oil and the glycerol tri (ethyl acetate), and stirring and mixing uniformly;
s3, cooling to 60-80 ℃, adding the filler and the colorant, and uniformly stirring; grinding; and (5) molding to obtain the product.
Preferably, the step S1 further includes a step of adding shellac during the mechanical pulverization; the step S2 further includes a step of putting the crushed shellac together with the japan wax and the polyethylene glycol wax into a melting pot.
The invention adopts the Japan wax as the main wax to play the roles of solidification and shaping, but the repeated temperature change in the subsequent process causes the wax to be separated from the colorant, and the product has more heterochromatic spots. It has been unexpectedly found that the addition of shellac can overcome the separation between the wax and the colorant, and the inventors speculate that this may be due to the specific amphiphilic block copolymer nature of shellac. The lac has hydrophilic and hydrophobic parts simultaneously, has a large amount of functional groups such as hydroxyl, carboxyl and the like simultaneously, can serve as a bridging effect between toner and wax, has ionizable carboxyl, has certain polyelectrolyte polymer properties, can provide double-electron-layer stabilization and steric hindrance effects simultaneously, has strong dispersion in a system, and thus plays a role in preventing wax from being separated from a coloring agent.
But the lac is very unstable due to a large number of functional groups, and the product is layered in long-term storage tests. In this regard, the inventors further found through experiments that the addition of the polyethylene glycol wax on the basis of the above results in the improvement of the overall stability of the product, and the effect of the polyethylene glycol wax is considered by the inventors to be mainly due to the stabilizing effect of the polyethylene glycol wax on the shellac.
The invention has the following beneficial effects:
the eyebrow pencil provided by the invention solves the problem of separation of wax and colorant by adjusting the formula composition, and the obtained product has good appearance and stability, has the functions of water resistance and sweat resistance, can effectively keep makeup, is smooth in use, is easy to develop color and has a good use effect.
Detailed Description
The present invention is further illustrated by the following specific examples, which are not intended to limit the invention in any way. Reagents, methods and apparatus used in the present invention are conventional in the art unless otherwise indicated.
Unless otherwise indicated, reagents and materials used in the following examples are commercially available.
Examples 1 to 3 waterproof and sweat-proof eyebrow pencil and its formulation (parts by weight)
| Components | Example 1 | Example 2 | Example 3 | Example 4 |
| Mica | 10 | 16 | 20 | 23 |
| Japanese wax | 9 | 6 | 12 | 15 |
| Polyethylene glycol wax | 3.6 | 4 | 4 | 5 |
| Lac | 2.4 | 3 | 2 | 1.5 |
| Hydrogenated castor oil | 1.5 | 2.5 | 3 | 5 |
| Glycerol tri (ethyl acetate) | 2 | 3 | 4 | 5 |
| CI77499 | 5 | 6 | 7 | 8 |
| CI77492 | 5 | 6 | 7 | 8 |
| CI77491 | 5 | 6 | 7 | 8 |
| CI77891 | 5 | 6 | 7 | 8 |
The preparation method comprises the following steps:
s1, mechanically pulverizing Japan wax, polyethylene glycol wax, colorant, filler and lac respectively;
s2, adding Japan wax, polyethylene glycol wax and shellac into the melting pot, heating to melt, adding hydrogenated castor oil and glycerol tri (ethyl acetate), stirring and mixing uniformly;
s3, cooling to 60 ℃, adding the filler and the colorant, and uniformly stirring; grinding until the powder is uniformly dispersed;
s4, placing the powder at a constant temperature of 25 ℃ for 12h, pouring the powder into a plodder, extruding a pen core, placing the pen core until the hardness is recovered, and packaging after the color matching is qualified.
Comparative example 1 differs from example 1 in that no shellac was added and the remaining parameters were the same as in example 1.
Comparative example 2 differs from example 1 in that no polyethylene glycol wax was added and the remaining parameters are the same as in example 1.
Comparative example 3 differs from example 1 in that beeswax is used instead of polyethylene glycol wax, and the remaining parameters are the same as in example 1.
Test I, sensory index and physicochemical index test
The refills prepared in examples 1-4 and comparative examples 1-3 were tested according to the test method for sensory and physical and chemical indexes in GB/T27575 & 2011 cosmetic pencil and cosmetic refill, and the test results are shown in tables 1 and 2 below.
TABLE 1 sensory index test results
TABLE 2 results of physical and chemical index testing
From the above table, the pen core prepared in the embodiments 1 to 4 of the present invention has good sensory and physicochemical indexes, and analysis of test results of other comparative examples shows that the problem of separation of wax and toner in the eyebrow pencil can be solved by adding the shellac, and the addition of the polyethylene glycol wax facilitates improvement of stability of the shellac, so that cold resistance and heat resistance of the eyebrow pencil are improved, but the effect disappears when the beeswax is used to replace the polyethylene glycol wax.
Test example two, Long-term storage test
The eyebrow pencil leads prepared in examples 1 to 4 and comparative examples 1 to 3 were stored at 25. + -.2 ℃ and 60. + -. 5% RH for 36 months, and the appearance of the lead was observed, and the test results are shown in Table 3 below.
| Sample (I) | Stability test results |
| Example 1 | The refill has no fracture and delamination |
| Example 2 | The refill has no fracture and delamination |
| Example 3 | The refill has no breakCracking and delamination phenomena |
| Example 4 | The refill has no fracture and delamination |
| Comparative example 1 | The refill has no fracture and delamination |
| Comparative example 2 | The refill has obvious layering phenomenon |
| Comparative example 3 | The layered phenomenon of the pen core |
The above table shows that the pen cores prepared in the embodiments 1 to 4 of the present invention have excellent stability, the shelf life of the pen cores is as long as 36 months, and the pen cores prepared in the comparative examples 2 to 3 have an obvious layering phenomenon, which indicates that the stability of the pen cores is not good.
The above embodiments are preferred embodiments of the present invention, but the present invention is not limited to the above embodiments, and any other changes, modifications, substitutions, combinations, and simplifications which do not depart from the spirit and principle of the present invention should be construed as equivalents thereof, and all such changes, modifications, substitutions, combinations, and simplifications are intended to be included in the scope of the present invention.
Claims (10)
1. The waterproof sweat-proof durable eyebrow pencil is characterized by comprising the following components in parts by weight: 10-25 parts of a filler, 20-32 parts of a colorant, 5-15 parts of Japan wax, 3-10 parts of polyethylene glycol wax, 1-5 parts of hydrogenated castor oil and 2-5 parts of glycerol tri (ethyl acetate).
2. The waterproof sweat-resistant durable eyebrow pencil of claim 1, comprising the following components in parts by weight: 15-25 parts of a filler, 25-32 parts of a colorant, 10-15 parts of Japan wax, 6-10 parts of polyethylene glycol wax, 2-4 parts of hydrogenated castor oil and 2-4 parts of glycerol tri (ethyl acetate).
3. The waterproof, sweat-resistant and durable eyebrow pencil of claim 1 or 2, further comprising shellac.
4. The waterproof sweat-resistant durable eyebrow pencil of claim 3, wherein the weight ratio of Japan wax, polyethylene glycol wax and shellac in the eyebrow pencil is 3: 1-2: 0.1 to 1.5.
5. The waterproof sweat-resistant durable eyebrow pencil of claim 4, wherein the weight ratio of Japan wax, polyethylene glycol wax and shellac in the eyebrow pencil is 3: 1.2: 0.8.
6. the waterproof, antiperspirant roll-on eyebrow pencil of claim 1 or claim 2, wherein the colorant is at least one selected from the group consisting of CI77499, CI77492, CI77491, and CI 77891.
7. The waterproof sweat-resistant durable eyebrow pencil of claim 1 or 3, wherein said filler is selected from one or both of mica and silica.
8. The waterproof, antiperspirant, and permanent eyebrow pencil of claim 7, wherein said filler is mica.
9. A method for preparing a eyebrow pencil according to any one of claims 1 to 8, comprising the steps of:
s1, mechanically pulverizing Japan wax, polyethylene glycol wax, colorant and filler respectively;
s2, adding the Japan wax and the polyethylene glycol wax into a melting material pot, heating to melt, adding the hydrogenated castor oil and the glycerol tri (ethyl acetate), and stirring and mixing uniformly;
s3, cooling to 60-80 ℃, adding the filler and the colorant, and uniformly stirring; grinding; and (5) molding to obtain the product.
10. The method of claim 9, wherein the step S1 further comprises the step of adding shellac during the mechanical grinding; the step S2 further includes a step of putting the crushed shellac together with the japan wax and the polyethylene glycol wax into a melting pot.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202110206819.3A CN112972307B (en) | 2021-02-24 | 2021-02-24 | Waterproof sweat-proof lasting eyebrow pencil and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202110206819.3A CN112972307B (en) | 2021-02-24 | 2021-02-24 | Waterproof sweat-proof lasting eyebrow pencil and preparation method thereof |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN112972307A true CN112972307A (en) | 2021-06-18 |
| CN112972307B CN112972307B (en) | 2022-12-16 |
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN202110206819.3A Active CN112972307B (en) | 2021-02-24 | 2021-02-24 | Waterproof sweat-proof lasting eyebrow pencil and preparation method thereof |
Country Status (1)
| Country | Link |
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Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1345219A (en) * | 1999-11-25 | 2002-04-17 | 株式会社资生堂 | Method for producing cosmetics |
| CN107669542A (en) * | 2017-10-10 | 2018-02-09 | 浙江中医药大学 | A kind of indigo naturalis eyebrow pencil pen core and its preparation method and application |
| CN110314123A (en) * | 2019-07-01 | 2019-10-11 | 上海欧润化妆品有限公司 | A kind of eyebrow pencil and preparation method thereof |
| CN111727122A (en) * | 2018-02-15 | 2020-09-29 | 施万-斯特比洛化妆品公司 | Method for producing powder refills and products produced by this method |
-
2021
- 2021-02-24 CN CN202110206819.3A patent/CN112972307B/en active Active
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1345219A (en) * | 1999-11-25 | 2002-04-17 | 株式会社资生堂 | Method for producing cosmetics |
| CN107669542A (en) * | 2017-10-10 | 2018-02-09 | 浙江中医药大学 | A kind of indigo naturalis eyebrow pencil pen core and its preparation method and application |
| CN111727122A (en) * | 2018-02-15 | 2020-09-29 | 施万-斯特比洛化妆品公司 | Method for producing powder refills and products produced by this method |
| CN110314123A (en) * | 2019-07-01 | 2019-10-11 | 上海欧润化妆品有限公司 | A kind of eyebrow pencil and preparation method thereof |
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| CN112972307B (en) | 2022-12-16 |
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