CN112811559A - Low-deuterium hydrogen water and preparation method and application thereof - Google Patents
Low-deuterium hydrogen water and preparation method and application thereof Download PDFInfo
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- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F1/00—Treatment of water, waste water, or sewage
- C02F1/68—Treatment of water, waste water, or sewage by addition of specified substances, e.g. trace elements, for ameliorating potable water
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- A—HUMAN NECESSITIES
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- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F2103/00—Nature of the water, waste water, sewage or sludge to be treated
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- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F2103/00—Nature of the water, waste water, sewage or sludge to be treated
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Abstract
The invention discloses low deuterium hydrogen water and a preparation method and application thereof, and the preparation method comprises the following steps: 1) preparation of deuterium-depleted hydrogen gas: using deuterium-depleted water as a raw material to generate deuterium-depleted hydrogen; 2) hydrogen gas into deuterium-depleted water: filling the deuterium-depleted hydrogen obtained in the step 1) into deuterium-depleted water and uniformly mixing to obtain deuterium-depleted hydrogen water; 3) and (6) filling. The deuterium-depleted hydrogen water prepared by using the deuterium-depleted water as the raw material has low deuterium content, can be used as high-quality drinking water, has obvious effects in the fields of tumor treatment, oxidation resistance and the like, has simple preparation method, few process parameters and loose preparation conditions, is suitable for industrial popularization and use, can further increase the hydrogen content by adopting a better gas-liquid mixing measure on the basis of the invention, provides better product varieties, and provides a new idea for the preparation and research and development of deuterium-depleted hydrogen water products.
Description
Technical Field
The invention belongs to the technical field of low deuterium hydrogen water preparation, and particularly relates to low deuterium hydrogen water and a preparation method and application thereof.
Background
Deuterium-depleted water is water with deuterium content lower than that of natural water (natural deuterium content is generally 150-155ppm), especially water with deuterium content less than 135 ppm. In the area with higher altitude in nature, the deuterium content is slightly reduced, but the deuterium content is generally reduced little.
At present, many researches show that the deuterium-depleted water has obvious effects in the fields of tumor adjuvant therapy, nervous system disease improvement, immunity improvement and the like, and is one of the hot spots of the current researches. However, hydrogen contained in water has been studied in the fields of radical scavenging and adjuvant therapy of tumor.
From the perspective of relevant mechanisms, no matter low deuterium is adopted, or hydrogen is added into the low deuterium, the low deuterium and hydrogen have similar effects on the fields of radical scavenging, oxidation resistance and the like, and the two components can be superposed to produce more remarkable effects. However, no related product exists in the current market, and in order to make up for the blank, the invention prepares the deuterium-depleted hydrogen for the first time, and the deuterium-depleted hydrogen is used as a raw material and mixed with the deuterium-depleted water to prepare the deuterium-depleted hydrogen water, so that the effect of the product is expected to be further enhanced.
Disclosure of Invention
In order to solve the problems in the prior art, the invention aims to provide low deuterium hydrogen water and a preparation method and application thereof.
In order to achieve the purpose and achieve the technical effect, the invention adopts the technical scheme that:
a deuterium-depleted hydrogen water is prepared by filling deuterium-depleted hydrogen prepared from deuterium-depleted water with optionally added auxiliary agent.
The invention discloses a preparation method of low deuterium hydrogen water, which comprises the following steps:
1) preparation of deuterium-depleted hydrogen
Using deuterium-depleted water as a raw material to generate hydrogen and oxygen, wherein the generated hydrogen is deuterium-depleted hydrogen;
2) filling hydrogen into deuterium-depleted water
Filling the deuterium-depleted hydrogen obtained in the step 1) into deuterium-depleted water and uniformly mixing to obtain deuterium-depleted hydrogen water;
3) and (6) filling.
Further, in the step 1), the deuterium content in the deuterium-depleted water is 1-140ppm, an auxiliary agent is selectively added into the deuterium-depleted water, and the deuterium-depleted water generates deuterium-depleted hydrogen and oxygen through electrolysis or chemical reaction.
The auxiliary agents comprise auxiliary agents for improving mouthfeel and taste or various auxiliary agents for realizing the effects of improving nutrient components and the like, and comprise mineral substances, sugar, citric acid, phosphoric acid, fruit juice, tea and the like, and can be flexibly added according to actual requirements.
Furthermore, the deuterium-depleted water is added into pure water or electrolyte for electrolysis to generate deuterium-depleted hydrogen and oxygen, and the electrolysis speed is 0.01-1000000L/min.
Further, the electrolyte is strong base or salt solution, the strong base is one or a combination of several of sodium hydroxide, potassium hydroxide and calcium hydroxide, and the salt solution is one or a combination of several of sodium chloride, potassium sulfate and sodium sulfate.
Further, deuterium-depleted water is mixed with the metal or the metal hydride and generates deuterium-depleted hydrogen and oxygen through a chemical reaction, wherein the molar ratio of the deuterium-depleted water to the metal hydride is 1: 1000000-1: 10.
further, the metal is one or a combination of several of lithium, sodium, potassium, calcium and magnesium, and the metal hydride is one or a combination of several of lithium hydride, sodium hydride, potassium hydride and calcium hydride.
Further, in the step 2), the deuterium-depleted water is introduced into a gas-liquid mixer, and the temperature of the deuterium-depleted water is stabilized at 0-35 ℃; filling the deuterium-depleted hydrogen obtained in the step 1) into deuterium-depleted water, dispersing the deuterium-depleted hydrogen into bubbles with the size of 0.01nm-10mm through a gas-liquid mixer, wherein the molar flow ratio of the deuterium-depleted hydrogen to the deuterium-depleted water is 1: 1000000-1: 10, the temperature in the gas-liquid mixer is 0-35 ℃, and the pressure is 0-10 MPa.
Further, in the step 2), the deuterium content in the deuterium-depleted hydrogen water is 1-140ppm, and the hydrogen content in the deuterium-depleted hydrogen water is 0.0001-100 ppm.
The invention discloses application of low deuterium hydrogen water in the fields of high-quality drinking water, tumor treatment and oxidation resistance.
Compared with the prior art, the invention has the beneficial effects that:
the invention discloses low deuterium hydrogen water and a preparation method and application thereof, and the preparation method comprises the following steps: 1) preparation of deuterium-depleted hydrogen gas: using deuterium-depleted water as a raw material to generate hydrogen and oxygen, wherein the generated hydrogen is deuterium-depleted hydrogen; 2) hydrogen gas into deuterium-depleted water: filling the deuterium-depleted hydrogen obtained in the step 1) into deuterium-depleted water and uniformly mixing to obtain deuterium-depleted hydrogen water; 3) and (6) filling. The invention provides deuterium-depleted hydrogen water and a preparation method and application thereof.A deuterium-depleted hydrogen gas is prepared for the first time by using deuterium-depleted water or deuterium-depleted water containing an auxiliary agent, the deuterium-depleted hydrogen gas is prepared by taking the deuterium-depleted water as a raw material and mixing the raw material with the deuterium-depleted water, the deuterium content in the deuterium-depleted hydrogen water prepared by taking the deuterium-depleted water as the raw material is low, the deuterium-depleted hydrogen water can be used as high-quality drinking water, and the deuterium-depleted hydrogen water has obvious effects in the fields of tumor treatment, oxidation resistance and the like.
Drawings
FIG. 1 is a process flow diagram of the present invention.
Detailed Description
The following detailed description of the embodiments of the present invention is provided to enable those skilled in the art to more easily understand the advantages and features of the present invention, and to clearly and clearly define the scope of the present invention.
A deuterium-depleted hydrogen water is prepared through filling deuterium-depleted hydrogen prepared from deuterium-depleted water at low temp (0-35 deg.C) to deuterium-depleted water, and selectively adding assistants including the assistants for improving taste and taste or the assistants for increasing nutrients, including minerals, sugar, citric acid, phosphoric acid, fruit juice, tea, etc.
As shown in fig. 1, a method for preparing deuterium-depleted hydrogen water comprises the following steps:
1) preparation of deuterium-depleted hydrogen
Using deuterium-depleted water as a raw material, generating hydrogen and oxygen by methods of electrolysis, chemical reaction and the like, wherein the generated hydrogen is deuterium-depleted hydrogen, and the deuterium content in the deuterium-depleted water raw material is 1-140ppm, preferably 25-100 ppm; the chemical equation is as follows:
2H2O→2H2+O2
when deuterium-depleted water is added into pure water or electrolyte for electrolysis to generate deuterium-depleted hydrogen and oxygen, the electrolysis process can be realized by pure water electrolysis or electrolyte addition for electrolysis, and the electrolyte can be in the form of strong base or other salt solution; the strong base can be sodium hydroxide, potassium hydroxide, calcium hydroxide, etc., and the salt solution can be sodium chloride, potassium sulfate, sodium sulfate, etc.; the electrolysis speed is 0.01-1000000L/min, preferably 0.1-100L/min.
The invention can generate deuterium-depleted hydrogen by the reaction of metal and deuterium-depleted water; the chemical equation is as follows:
2R+2H2O→2ROH+H2
the invention can also generate deuterium-depleted hydrogen by the reaction of metal hydride and deuterium-depleted water, wherein the molar ratio of the metal hydride to the deuterium-depleted water is 1: 1000000-1: 10, preferably 1: 100000-1: 1000, parts by weight; the chemical equation is as follows:
RH+H2O→ROH+H2
r, RH is metal or metal hydride respectively; the metal is one or a combination of more of lithium, sodium, potassium, calcium and magnesium; the metal hydride RH is one of lithium hydride, sodium hydride, potassium hydride, calcium hydride, and the like.
The deuterium-depleted water can be pure deuterium-depleted water, a certain amount of water for improving the taste or flavor or adding some auxiliary agents such as nutrient substances and the like can be added into the deuterium-depleted water, the auxiliary agents comprise minerals, sugar, citric acid, phosphoric acid, fruit juice, tea and the like, and other auxiliary agents can be added according to actual requirements.
2) Preparation of low deuterium hydrogen water
Filling the deuterium-depleted hydrogen obtained in the step 1) into deuterium-depleted water, wherein the molar flow ratio of the deuterium-depleted hydrogen to the deuterium-depleted water is 1: 1000000-1: 10, preferably 1: 100000-1: 1000, specifically: the low deuterium hydrogen and the low deuterium water are respectively led into a gas-liquid mixer, and the low deuterium hydrogen is dispersed by the gas-liquid mixer to generate smaller bubbles, so that the low deuterium hydrogen is more favorably dissolved in the low deuterium water to prepare the low deuterium hydrogen water, wherein the low deuterium content in the low deuterium hydrogen is 1-140ppm, preferably 25-100ppm, and the low deuterium content in the low deuterium hydrogen is 0.0001-100ppm, preferably 0.01-10 ppm.
In the step 2), in the gas-liquid mixer, the diameter size of the hydrogen bubbles is 0.01nm-10mm, preferably 0.1nm-10 μm, and the mixing pressure is 0-10MPa (gauge pressure), preferably 0.1-0.5MPa (gauge pressure), and the pressure can be directly used by the high-pressure hydrogen generated by electrolysis, or can be further pressurized to generate the high-pressure hydrogen.
In the step 2), the process of filling the deuterium depleted hydrogen gas obtained in the step 1) into deuterium depleted water is generally a low temperature process, and the temperature is 0-35 ℃, preferably 2-25 ℃.
3) And (6) filling.
In the step 3), the filling temperature is 0-35 ℃, and preferably 2-25 ℃; the bottle for filling can be a glass bottle, an aluminum bottle or a plastic bottle, and the plastic bottle is generally made of PP, PE, PET and other materials; the bottle cap for filling can be a plastic cap or a metal cap, the plastic cap is generally made of PP, PE and the like, and the metal cap is an aluminum cap, a stainless steel cap and the like.
The invention discloses application of low deuterium hydrogen water in the fields of high-quality drinking water, tumor treatment and oxidation resistance.
Example 1
A deuterium-depleted hydrogen water is prepared by charging deuterium-depleted hydrogen gas prepared from deuterium-depleted water into deuterium-depleted water at 0-35 deg.C.
As shown in fig. 1, a method for preparing deuterium depleted aqueous hydrogen by electrolysis comprises the following steps:
1) preparation of deuterium-depleted hydrogen
Adding deuterium-depleted water with 25ppm of deuterium content into an electrolytic cell containing pure water, and generating deuterium-depleted hydrogen at the electrolytic rate of 500ml/min and the pressure of 0.3 MPa;
2) preparation of low deuterium hydrogen water
2.1) cooling the deuterium-depleted water, and controlling the temperature to be about 2 ℃;
2.2) mixing the deuterium-depleted hydrogen generated in the step 1) with the deuterium-depleted water cooled in the step 2.1) at the flow rate of 0.1mol/h and the flow rate of 100mol/h in a gas-liquid mixer, dispersing the deuterium-depleted hydrogen by using the gas-liquid mixer to generate smaller bubbles, wherein the diameter size of the hydrogen bubbles is 0.01nm-10mm, and the deuterium-depleted hydrogen is more favorably dissolved in the deuterium-depleted water;
3) the produced deuterium-depleted water is filled in an aluminum bottle, and the bottle cap is an aluminum cap.
Example 2
A preparation method of deuterium-depleted hydrogen water, which produces deuterium-depleted hydrogen water by an electrolysis method, comprises the following steps:
1) preparation of deuterium-depleted hydrogen
Adding deuterium-depleted water with 25ppm of deuterium content into an electrolytic cell containing sodium hydroxide to generate deuterium-depleted hydrogen at an electrolysis rate of 500 ml/min; the pressure in the steam-water mixer is 0.3 MPa;
2) preparation of low deuterium hydrogen water
2.1) cooling the deuterium-depleted water, and controlling the temperature to be about 10 ℃;
2.2) mixing the deuterium-depleted hydrogen generated in the step 1) with the deuterium-depleted water cooled in the step 2.1) at the flow rate of 0.1mol/h and the flow rate of 100mol/h in a gas-liquid mixer, wherein the diameter size of hydrogen bubbles is 0.01nm-10 mm;
3) the produced deuterium-depleted water is filled in a glass bottle, and the bottle cap is an aluminum cap.
Example 3
A method for preparing low deuterium hydrogen water by metal hydride, comprising the following steps:
1) preparation of deuterium-depleted hydrogen
Slowly adding sodium hydride NaH into deuterium-depleted water with 100ppm of deuterium content to perform chemical reaction, pressurizing the generated deuterium-depleted hydrogen, then feeding the hydrogen into a gas-liquid mixer, and dispersing the hydrogen into fine bubbles, wherein the pressure in the gas-liquid mixer is 0.5 MPa;
2) preparation of low deuterium hydrogen water
2.1) cooling the deuterium-depleted water, and controlling the temperature to be about 25 ℃;
2.2) mixing the deuterium-depleted hydrogen generated in the step 1) with the deuterium-depleted water cooled in the step 2.1) at the flow rate of 0.001mol/h in a gas-liquid mixer, wherein the diameter size of hydrogen bubbles is 0.01nm-10 mm;
3) the produced deuterium-depleted water is filled in a PET bottle, and the bottle cap is a PP plastic cap.
Example 4
A preparation method of deuterium-depleted hydrogen water, which produces deuterium-depleted hydrogen water through metal preparation, comprises the following steps:
1) preparation of deuterium-depleted hydrogen
Slowly adding sodium metal into deuterium-depleted water with deuterium content of 100ppm, pressurizing the generated deuterium-depleted hydrogen, and then feeding the hydrogen into a gas-liquid mixer, wherein the pressure in the gas-liquid mixer is 0.1 MPa;
2) preparation of low deuterium hydrogen water
2.1) cooling the deuterium-depleted water, and controlling the temperature to be about 25 ℃;
2.2) mixing the deuterium-depleted hydrogen generated in the step 1) with the deuterium-depleted water cooled in the step 2.1) at the flow rate of 0.001mol/h and the flow rate of 100mol/h in a steam-water mixer, wherein the diameter size of hydrogen bubbles is 0.01nm-10 mm;
3) the produced deuterium-depleted water is filled in a PET bottle, and the bottle cap is a PE plastic cap.
The parts of the invention not specifically described can be realized by adopting the prior art, and the details are not described herein.
The above description is only an embodiment of the present invention, and not intended to limit the scope of the present invention, and all modifications of equivalent structures and equivalent processes performed by the present specification and drawings, or directly or indirectly applied to other related technical fields, are included in the scope of the present invention.
Claims (10)
1. A deuterium-depleted hydrogen water is characterized in that deuterium-depleted hydrogen gas made of deuterium-depleted water is filled into deuterium-depleted water, and an auxiliary agent is selectively added into the deuterium-depleted water.
2. A preparation method of low deuterium hydrogen water is characterized by comprising the following steps:
1) preparation of deuterium-depleted hydrogen
Using deuterium-depleted water as a raw material to generate hydrogen and oxygen, wherein the generated hydrogen is deuterium-depleted hydrogen;
2) filling hydrogen into deuterium-depleted water
Filling the deuterium-depleted hydrogen obtained in the step 1) into deuterium-depleted water and uniformly mixing to obtain deuterium-depleted hydrogen water;
3) and (6) filling.
3. The method of claim 2, wherein in step 1), the deuterium content in the deuterium depleted water is 1-140ppm, optionally adding an auxiliary agent, and the deuterium depleted water is electrolyzed or chemically reacted to produce deuterium depleted hydrogen and oxygen.
4. The method of claim 3, wherein the deuterium depleted water is electrolyzed by adding it to pure water or an electrolyte at an electrolysis rate of 0.01L/min to 1000000L/min to produce deuterium depleted hydrogen and oxygen.
5. The method of claim 4, wherein the electrolyte is a strong base or a salt solution, the strong base is one or a combination of sodium hydroxide, potassium hydroxide and calcium hydroxide, and the salt solution is one or a combination of sodium chloride, potassium sulfate and sodium sulfate.
6. The method of claim 3, wherein the deuterium depleted water is mixed with a metal or metal hydride and chemically reacted to produce deuterium depleted hydrogen and oxygen, and the molar ratio of deuterium depleted water to metal hydride is 1: 1000000-1: 10.
7. the method of claim 6, wherein the metal is one or a combination of lithium, sodium, potassium, calcium, and magnesium, and the metal hydride is one or a combination of lithium hydride, sodium hydride, potassium hydride, and calcium hydride.
8. The method of claim 2, wherein in step 2), the deuterium depleted water is introduced into a gas-liquid mixer, and the temperature of the deuterium depleted water is stabilized at 0-35 ℃; filling the deuterium-depleted hydrogen obtained in the step 1) into deuterium-depleted water, dispersing the deuterium-depleted hydrogen into bubbles with the size of 0.01nm-10mm through a gas-liquid mixer, wherein the molar flow ratio of the deuterium-depleted hydrogen to the deuterium-depleted water is 1: 1000000-1: 10, the temperature in the gas-liquid mixer is 0-35 ℃, and the pressure is 0-10 MPa.
9. The method for preparing deuterium depleted hydrogen water according to claim 3, wherein in step 2), the deuterium content in deuterium depleted hydrogen water is 1-140ppm, and the hydrogen content in deuterium depleted hydrogen water is 0.0001-100 ppm.
10. Use of the deuterium depleted aqueous solution of claim 1 in the fields of high quality drinking water, tumour therapy, anti-oxidation.
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US5855921A (en) * | 1991-10-31 | 1999-01-05 | Somlyai; Gabor | Pharmaceutical products for curing tumorous diseases and process for preparing same |
WO1996033129A1 (en) * | 1995-04-20 | 1996-10-24 | Kotai Laszlo | A chemical procedure to produce water of reduced deuterium content |
CN204550048U (en) * | 2015-01-06 | 2015-08-12 | 朱树勋 | Deuterium-depleted water production equipment |
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Application publication date: 20210518 |