CN112402314B - A kind of traditional Chinese medicine nourishing lipstick containing danshen diterpene quinone and preparation method thereof - Google Patents

Abstract

The invention discloses a traditional Chinese medicine nourishing lipstick containing danshen diterpene quinone and a preparation method thereof, and the traditional Chinese medicine nourishing lipstick comprises the following raw materials: the coloring and medicinal system is Saviae Miltiorrhizae radix diterpene quinone and titanium dioxide; a fragrance system for enhancing fragrance; the matrix is natural cacao butter, white vaseline, lanolin, beeswax, and ceresin. The method comprises the following steps: a. preparing diterpenoid tanshinone of salvia miltiorrhiza; b. coloring, maintaining, brightening and aromatic system preparation; c. preparing a matrix system; d. preparing traditional Chinese medicine nourishing lipstick. The colorant of the traditional Chinese medicine nourishing lipstick is a fat-soluble component of the red sage diterpene quinone extracted from traditional Chinese medicine red sage root, and the extracted and purified red sage root fat-soluble component of the red sage diterpene quinone coagulates the effects of red sage root in enriching blood, activating blood and cooling blood. The traditional Chinese medicine nourishing lipstick has a good improvement effect on phenomena of fading lip color, deepening lip lines and the like of women. The diterpenoid tanshinone has good coloring ability and coloring effect, and has special fragrance of Chinese medicinal materials.

Description

A kind of traditional Chinese medicine nourishing lipstick containing danshen diterpene quinone and preparation method thereof

technical field

The invention belongs to the technical field of cosmetics, and in particular relates to a traditional Chinese medicine nourishing lipstick containing salvia diterpene quinone and a preparation method thereof.

Background technique

Lipstick is a general term for all lip make-up, the main function is to give the lips a tone, emphasize or change the contour of the lips, showing more vitality and vitality.

Traditional Chinese medicine lipstick is a kind of lipstick, which has the effect of lipstick and the effect of traditional Chinese medicine ingredients. For example, the Chinese patent disclosed an invention patent named Zigui traditional Chinese medicine lipstick and its preparation method (application number: CN201711139793.5) on 2017.11.16, which can maintain good moisture and durability, and is also a kind of green , Natural and healthy products, suitable for people of different ages, the comfrey and angelica extracts in the raw materials have a good blood-activating effect, no unfriendly reagents are used, while showing the beauty of femininity, it is also suitable for mild cheilitis. Consumers also have a certain role. While effectively solving the color and odor problems of traditional Chinese medicine lipsticks, it also provides blood-activating, detoxifying and anti-inflammatory effects.

Another example is the Chinese patent on 2020.05.18 discloses an invention patent named as a kind of traditional Chinese medicine lipstick and its preparation method (application number: CN202010419897.7), which can overcome the drawbacks of the traditional Chinese medicine lipstick being too strong, and also has a certain spleen and stomach , Antibacterial and anti-ulcer effect.

In the prior art, all lipsticks with traditional Chinese medicine ingredients can play the role of traditional Chinese medicine ingredients, but the coloring ability of traditional Chinese medicine lipsticks is poor.

SUMMARY OF THE INVENTION

The purpose of the present invention is to solve the above-mentioned technical problems existing in the prior art, and to provide a traditional Chinese medicine nourishing lipstick containing danshen diterpene quinone and a preparation method thereof. The traditional Chinese medicine nourishing lipstick has better coloring ability and coloring effect, and has special The aroma of traditional Chinese medicine, and the triple effect of salvia miltiorrhiza invigorating blood, promoting blood circulation and cooling blood, has a good improvement effect on women's lip color lightening and lip wrinkles deepening.

In the preparation method, the salvia diterpene quinone is difficult to dissolve in the matrix, so ethanol is added to dissolve it. Since Salvia diterpene quinone is an anthraquinone chemical, it is easily decomposed when exposed to light and heat, so it is operated by an ultrasonic heating oscillator. The traditional Chinese medicine salvia miltiorrhiza decoction pieces are placed in a pulverizer and pulverized, and it is easy to be fully dissolved with 95% medical ethanol to obtain a higher content of salvia diterpene quinone. Since the lipstick solution is easy to generate bubbles in the lipstick mold, a rotary assembly device is used to rotate the lipstick mold. Through centrifugal action, the air bubbles in the lipstick mold are discharged, and at the same time, the lipstick solution in the lipstick mold is filled with the entire lipstick mold. The pattern ensures that the texture of the obtained traditional Chinese medicine nourishing lipstick is clear and distinct, and improves the overall aesthetics.

In order to solve the above-mentioned technical problems, the present invention adopts the following technical solutions:

A traditional Chinese medicine nourishing lipstick containing salvia diterpene quinone, the preparation raw materials of the traditional Chinese medicine nourishing lipstick include:

Coloring and medicinal systems: salvia diterpene quinone, titanium dioxide, titanium dioxide has the effect of covering and whitening.

Fragrance system used to enhance aroma.

Matrix system: natural cocoa butter, white petrolatum, lanolin, beeswax, ozokerite, which is convenient for the lipstick to be molded in the lipstick mold in the later stage.

Wherein, the coloring agent of the traditional Chinese medicine nourishing lipstick of the present invention is the fat-soluble component salvia diterpene quinone extracted from the traditional Chinese medicine Salvia miltiorrhiza. There is a saying in the traditional Chinese medicine books: "Blindly Danshen Drink, Gongtong Siwu Decoction", the extracted and purified Salvia miltiorrhiza fat-soluble The ingredient Salvia diterpene quinone condenses the triple effect of Salvia miltiorrhiza to nourish blood, activate blood and cool blood. Traditional Chinese medicine nourishing lipstick has a good improvement effect on women's lip color lightening and lip lines deepening. Salvia diterpene quinone itself has good coloring ability and coloring effect, and it also has a special aroma of traditional Chinese medicine. It is a rare lipstick (lip balm) coloring material with the characteristics of traditional Chinese medicine.

Further, the aroma system includes saccharin and compound essential oil, among which the compound essential oil can use DOTTERA light compound essential oil, and saccharin and DOTTERA light compound essential oil for fragrance are added, so that the lipstick has the characteristics of "sweetness", which improves the user's experience.

Further, the ratio of natural cocoa butter, white petrolatum, lanolin, beeswax and ozokerite by weight is 6:6:10:4:4.

A method for preparing a traditional Chinese medicine nourishing lipstick containing danshen diterpene quinone is characterized in that: the preparation of the above-mentioned traditional Chinese medicinal nourishing lipstick is used for preparation.

Specifically include the following steps:

a. Preparation of salvia diterpene quinone.

b. Preparation of coloring, curing, brightening and aroma system:

1) Weigh salvia diterpene quinone, titanium dioxide and saccharin, put them in a beaker, add 75% ethanol, and then carry out the ultrasonic step in an ultrasonic heating oscillator until the solution is bright orange-red, place it in a cool and ventilated place to volatilize the remaining Ethanol to obtain a coloring and curing solution, so that the salvia diterpene quinone is dissolved in 75% ethanol.

2) Add lanolin to the coloring and curing solution, stir, and continue to perform the ultrasonic step in the ultrasonic heating oscillator until the solution is bright orange-red semi-fluid.

3) The solution is heated in an ultrasonic heating oscillator, and then the compound essential oil is added dropwise to the solution to obtain a coloring and curing fragrance solution.

c. Preparation of matrix system: Weigh natural cocoa butter, white petrolatum, lanolin, beeswax and ozokerite, place in a beaker, heat and stir in a constant temperature water bath until the solution is light yellow and transparent, adjust the temperature of the constant temperature water bath low to maintain the liquid properties of the matrix system, and obtain a liquid matrix solution. Lanolin is used for skin care, calming, moisturizing and other properties. In clinical practice, the role of lanolin is mainly reflected in the application of lanolin together with vaseline, which can increase the permeability of vaseline. At the same time, because lanolin can also be used for skin care, especially for dry skin, it can effectively replenish moisture and prevent moisture loss. , can resist oxidation, and can remove harmful acidic substances.

d. Preparation of traditional Chinese medicine nourishing lipstick containing salvia diterpene quinone:

1) Take the coloring and curing aroma solution obtained in step b and the liquid matrix solution obtained in step c and mix them in a constant temperature water bath, and stir them so that the solution is opaque and bright orange, and the solution is Lipstick solution.

2) Select a lipstick mold for preparation, and preheat the plastic lipstick mold.

3) pouring the lipstick solution into a lipstick mold, and then cooling at room temperature to obtain a traditional Chinese medicine nourishing lipstick containing salvia miltiorrhiza quinone.

Further, step a includes:

1) Put the Chinese medicine Danshen decoction pieces in a pulverizer to pulverize, then sieve the Danshen powder, and then store the sieved Danshen powder in a cool and dry place for later use.

2) Mix the salvia miltiorrhiza powder and 95% medical ethanol in an equal volume in a spherical bottle, and carry out the ultrasonic step in an ultrasonic oscillator until the ethanol solution in the bottle turns dark red, filter out the drug residues, and remove the dark red containing salvia miltiorrhiza dissolved substances. 95% ethanol was placed in a beaker, sealed and protected from light for later use, and then the previous ultrasonic extraction step was continued, 95% ethanol eluate was collected repeatedly, and all 95% ethanol eluates were combined.

3) The combined 95% ethanol eluates were concentrated in a rotary evaporator.

4) Take a pear-shaped separatory funnel, mix the 95% ethanol concentrate with an equal volume of petroleum ether solution and leave it to stand, carry out the extraction step, until the solution is layered, collect the lower solution part, then continue the previous extraction step, repeat the operation .

5) Continue to concentrate the extracted ethanol solution until it is a dark red semi-fluid, collect the semi-fluid Salvia miltiorrhiza extract, cool and store in a desiccator to obtain a dark red solid substance Salvia diterpene quinone.

The traditional Chinese medicine salvia miltiorrhiza decoction pieces are pulverized in a pulverizer, and it is easy to be fully dissolved with 95% medical ethanol. After extraction and purification, the fat-soluble component of salvia miltiorrhiza diterpene quinone can be obtained, which can extract and retain more salvia diterpene quinone, and then obtain a higher content of danshen diterpene quinone. Salvia diterpene quinone, and the extraction and purification has strong operability, shortens the preparation period of salvia diterpene quinone, reduces cost, and gives full play to the performance of salvia diterpene quinone in traditional Chinese medicine nourishing lipstick.

Further, test the content of the obtained dark red solid substance salvia diterpene quinone, specifically extract the dark red solid substance salvia diterpene quinone, weigh it, place it in a conical flask, add methanol, seal it, and weigh it, Ultrasonic treatment for 30min, let cool, weighed again, then used methanol to make up the lost weight, shake well, filter, take the continuous filtrate, filter with 0.45um filter membrane, and analyze by HPLC to obtain the content of danshen diterpene quinone, according to The content of salvia diterpene quinone improves the extraction and purification operation in the preparation of the above salvia diterpene quinone.

Further, in step b, the ratio of salvia diterpene quinone, titanium dioxide and saccharin by weight is 5:5:3.

Further, in the second) operation of step b, the bright orange-red semi-fluid solution is placed in a 4° C. refrigerator for future use, to prevent the semi-fluid solution from breeding bacteria, and the retention time is longer.

Further, in step d, a pattern is arranged on the outer layer of the lipstick mold, when the lipstick solution is poured into the lipstick mold, the lipstick mold is rotated, and the lipstick solution is added, and then cooled at room temperature to obtain a traditional Chinese medicine containing salvia diterpene quinone. Nourishing lipstick. The lipstick mold is rotated, and the air bubbles in the lipstick mold are discharged through centrifugal action, and at the same time, the lipstick solution in the lipstick mold is filled with the pattern set by the entire lipstick mold, so as to ensure that the texture of the obtained traditional Chinese medicine nourishing lipstick is clear and distinct, and the overall appearance is improved. sex.

Further, a rotary assembly device is used to rotate the lipstick mold, and the lipstick solution is added. The rotary assembly device includes a rotary table and an assembly device. The top of the rotary table is provided with a fixed frame, and the top of the fixed frame is provided with a first motor. A motor can rotate the entire rotary table, thereby making the lipstick mold on the rotary table rotate.

The assembling device includes a fixed plate, a first clamping plate, a second clamping plate, a movable limit plate and a positioning plate, the first clamping plate and the second clamping plate are both L-shaped, and the first clamping plate and the Both the two clamping plates are provided with oblong holes, the two oblong holes are correspondingly arranged up and down, a first screw is arranged between the two oblong holes, the first screw is fixed on the fixing plate, and the first screw connects the first clamping plate and the second clamping plate. The second clamping plate is pressed against the fixing plate, and through the tightening action of the first screw, the distance between the first clamping plate and the second clamping plate can be adjusted according to the length of the lipstick mold, so that the lipstick mold can just be snapped in between the first clamping plate and the second clamping plate, so that the first clamping plate and the second clamping plate limit the length direction of the lipstick mold. The bottoms of the first clamping plate and the second clamping plate are both provided with limit posts, the fixing plate is provided with two through holes, the limit posts pass through the through holes, and the limit posts are in the through holes along the length direction of the oblong hole When moving, the limit post acts as a limit, which makes the first clamping plate and the second clamping plate move directionally, improves the stability of the movement of the first clamping plate and the second clamping plate, and is convenient for the length of the lipstick mold according to the length of the lipstick mold. , quickly adjust the distance between the first clamping plate and the second clamping plate.

The movable limit plate is provided with two first openings, the first clamping plate and the second clamping plate respectively pass through the first openings, the front side of the movable limit plate is provided with a force-bearing rod, and the movable limit plate The rear side is provided with a guide rod, the positioning plate is fixed on the first clamping plate and the second clamping plate by nuts, the positioning plate is provided with a second opening, and the first clamping plate and the second clamping plate pass through the first clamping plate and the second clamping plate respectively. Two openings, the guide rod passes through the positioning plate, the guide rod is sleeved with a spring, and the spring is arranged between the movable limit plate and the positioning plate. By exerting force on the force-receiving rod, the guide rod moves directionally on the movable limit plate, while the movable limit plate moves directionally on the first clamping plate and the second clamping plate. The first clamping plate, the second clamping plate and the movable limiting plate can clamp the width direction of the lipstick mold. Through the reciprocating motion of the movable limiting plate, it can be quickly installed or removed up and down. Lipstick stencils. Moreover, the movable limit plate is provided with a rectangular first opening, and the positioning plate is provided with a rectangular second opening, so that the arrangement of the movable limit plate and the positioning plate does not hinder the first clamping plate and the second clamping plate. The distance between them can be adjusted to adapt to the clamping effect of lipstick molds of different specifications.

The number of assembling devices is at least four. The assembling devices are evenly installed on the rotary table in the circumferential direction. The rotary table is provided with an embedded groove with an opening facing downward. On the rotary table, it is convenient to quickly install or remove the entire assembly unit. By arranging a plurality of assembling devices, the rotary table can rotate the plurality of lipstick molds at the same time, and the plurality of assembling devices are evenly installed on the rotary table in the circumferential direction, so that the force-receiving rods on the assembling devices can be rotationally exerted force.

The central position of the rotary table is provided with a central hole, the central hole is provided with a rotary shaft, the bottom of the rotary shaft is provided with a second motor, the second motor drives the rotary shaft to rotate in the central hole, and the side of the rotary shaft is provided with a circular outer surface. Arc-shaped bumps, the bumps squeeze the force-bearing rod, so that the force-bearing rod on the assembly device can be rotated to apply force. This method makes the assembly device open and close at the same time interval, which is convenient for batches of lipstick molds. Perform a rotation operation.

The steps of rotating the lipstick mold by using the rotating assembly device are as follows:

a. Loosen the first screw and the second screw, adjust the distance between the first clamping plate and the second clamping plate according to the length of the lipstick mold, when the inner side of the first clamping plate and the second clamping plate When the distance between the inner sides of the lipstick mold is the length of the lipstick mold, tighten the first screw, and then tighten the second screw.

b. Install the lipstick mold:

1) Turn on the second motor, the second motor drives the rotating shaft to rotate in the center hole, when the bump on the side of the rotating shaft squeezes the force rod of the first rotating assembly device, the movable limit plate moves away from the center of the rotating table. Move in the direction, the spring is compressed. At this time, the L-shaped moving rod is used to pass through the ear plate on the top of the lipstick mold, and then the L-shaped moving rod is moved down to embed the lipstick mold into the first clamping plate and the second clamping plate. When the bump on the side of the rotating shaft leaves the force-bearing rod of the first rotating assembly device, under the deformation recovery action of the spring, the movable limit plate moves towards the center of the rotary table, and the movable limit The position plate presses the lipstick mold, and then moves out the L-shaped moving rod to complete the loading of the first lipstick mold into the rotary assembly device.

2) The second motor drives the rotating shaft to rotate continuously in the center hole, and the remaining lipstick molds are loaded into the rotary assembly device in the same way as the first lipstick mold loading work.

3) When the second motor drives the rotating shaft to rotate in the center hole for one turn, turn off the second motor.

c. Turn on the first motor, the first motor drives the entire rotary table to rotate at a constant speed, and rotates the lipstick mold. Through centrifugal action, the air bubbles in the lipstick mold are discharged, and at the same time, the lipstick solution in the lipstick mold is filled with the entire lipstick mold. pattern.

d. When the first motor drives the entire rotary table to rotate at a constant speed for 5 minutes, turn off the first motor. When the rotary table stops rotating, let the lipstick mold stand for 2-3 minutes, then add lipstick solution to the lipstick mold, and then cool at room temperature.

e. Take out the lipstick mold:

1) Turn on the second motor, the second motor drives the rotating shaft to rotate in the center hole, when the bump on the side of the rotating shaft squeezes the force rod of the first rotating assembly device, the movable limit plate moves away from the center of the rotating table. Moving in the direction, the spring is compressed. At this time, the L-shaped moving rod is used to pass through the ear plate on the top of the lipstick mold, and then the L-shaped moving rod is moved upward to move the lipstick mold from the first clamping plate and the second clamping plate. The area is taken out. When the bump on the side of the rotating shaft leaves the force-bearing rod of the first rotating assembly device, under the deformation recovery action of the spring, the movable limit plate moves towards the center of the rotating table and returns to the starting position. , remove the first lipstick mold from the rotary assembly unit.

2) The second motor drives the rotating shaft to rotate continuously in the center hole, and takes out the remaining lipstick molds from the rotating assembly device in the same way as the first lipstick mold is taken out.

3) When the second motor drives the rotating shaft to rotate in the center hole for one turn, turn off the second motor.

f. Open the lipstick mold to obtain a traditional Chinese medicine nourishing lipstick containing salvia diterpene quinone.

The present invention has the following beneficial effects due to the adoption of the above-mentioned technical solutions:

1. The coloring agent of traditional Chinese medicine nourishing lipstick of the present invention is the fat-soluble component salvia diterpene quinone extracted from Chinese medicine Salvia miltiorrhiza, and there is a word in the traditional Chinese medicine books: "blindly drinking Salvia miltiorrhiza, Gong Tong Siwu Decoction", the Salvia miltiorrhiza fat-soluble through extraction and purification The ingredient Salvia diterpene quinone condenses the triple effect of Salvia miltiorrhiza to nourish blood, activate blood and cool blood. Traditional Chinese medicine nourishing lipstick has a good improvement effect on women's lip color lightening and lip lines deepening. Salvia diterpene quinone itself has good coloring ability and coloring effect, and it also has a special aroma of traditional Chinese medicine. It is a rare lipstick (lip balm) coloring material with the characteristics of traditional Chinese medicine.

2. The aroma system includes saccharin and compound essential oil. The compound essential oil can use DOTTERA light compound essential oil, and saccharin and DOTTERA light compound essential oil for fragrance are added, so that the lipstick has the characteristics of "sweetness", which improves the user's experience.

3. In this preparation method, it is difficult to dissolve salvia miltiorrhiza quinone in the matrix, so ethanol is added to dissolve it. Since Salvia diterpene quinone is an anthraquinone chemical, it is easily decomposed when exposed to light and heat, so it is operated by an ultrasonic heating oscillator.

4. Put the traditional Chinese medicine salvia miltiorrhiza decoction pieces in a pulverizer, and it is easy to be fully dissolved with 95% medical ethanol. After extraction and purification, the fat-soluble salvia miltiorrhiza diterpene quinone can be obtained, which can extract and retain more salvia diterpene quinone, thereby obtaining higher Salvia diterpene quinone content, and the extraction and purification has strong operability, shortens the preparation period of salvia diterpene quinone, reduces cost, and gives full play to the performance of salvia diterpene quinone in traditional Chinese medicine nourishing lipstick.

5. Rotate the lipstick mold, and through centrifugal action, the air bubbles in the lipstick mold are discharged, and at the same time, the lipstick solution in the lipstick mold is filled with the pattern set by the entire lipstick mold, so as to ensure that the texture of the obtained traditional Chinese medicine nourishing lipstick is clear and distinct, improving the overall of aesthetics.

6. Through the tightening effect of the first screw, the distance between the first clamping plate and the second clamping plate can be adjusted according to the length of the lipstick mold, so that the lipstick mold can just be inserted into the first clamping plate and the second clamping plate. between the clamping plates, so that the first clamping plate and the second clamping plate limit the length direction of the lipstick mold. By exerting force on the force-receiving rod, the guide rod moves directionally on the movable limit plate, while the movable limit plate moves directionally on the first clamping plate and the second clamping plate. The first clamping plate, the second clamping plate and the movable limiting plate can clamp the width direction of the lipstick mold. Through the reciprocating motion of the movable limiting plate, it can be quickly installed or removed up and down. Lipstick stencils. Moreover, the movable limit plate is provided with a rectangular first opening, and the positioning plate is provided with a rectangular second opening, so that the arrangement of the movable limit plate and the positioning plate does not hinder the first clamping plate and the second clamping plate. The distance between them can be adjusted to adapt to the clamping effect of lipstick molds of different specifications.

7. The rotary table is provided with an embedded groove with an opening facing downward, and the fixed plate is embedded in the embedded groove, so that the connection operation of the rotary table and the fixed plate is carried out under the rotary table, so as to avoid the structural damage of the fixed frame due to the connection operation.

8. The second motor drives the rotating shaft to rotate in the center hole, and the side of the rotating shaft is provided with a convex block whose outer surface is in the shape of an arc, so that the circumferentially rotating convex block exerts a force on the force-receiving rod, and the assembly device can be rotated around it. The directions are distributed on the rotary table, so that the assembly device can be installed reasonably, without wasting the use space, and it is also convenient for the processing and manufacture of the rotary table. The arc-shaped bumps are used to rotate into or out of the load-bearing rod very smoothly, ensuring that the bumps continuously exert force on multiple load-bearing rods.

9. Pass the L-shaped moving rod through the ear plate on the top of the lipstick mold, which is convenient for loading and taking out the lipstick mold, and avoids the staff directly touching the lipstick mold and causing the lipstick solution to get on the hands.

10. In the present invention, the fixed plate, the first clamping plate, the second clamping plate, the movable limit plate and the positioning plate are all detachable connection, which is convenient for cleaning after dismantling and removing lipstick solution, which is convenient for repeated use later .

Description of drawings

The present invention will be further described below in conjunction with the accompanying drawings:

Fig. 1 is the structural representation of the rotary assembly device in the present invention;

Fig. 2 is the bottom structure schematic diagram of Fig. 1;

Fig. 3 is the structural representation of the rotary table in the present invention;

Fig. 4 is the structural representation of the rotating shaft in the present invention;

5 is a schematic structural diagram of an assembling device in the present invention;

6 is a schematic structural diagram of a movable limit plate in the present invention;

7 is a schematic structural diagram of the connection between the first clamping plate and the second clamping plate in the present invention;

8 is a schematic structural diagram of a fixed plate in the present invention;

9 is a schematic structural diagram of the present invention when the lipstick mold is embedded in the region between the first clamping plate and the second clamping plate;

10 is a schematic structural diagram of the present invention when the first lipstick mold is loaded into the rotary assembly device;

11 is a schematic structural diagram of the present invention when all the lipstick molds are loaded into the rotary assembly device;

12 is a schematic structural diagram of the present invention when the first lipstick mold is taken out from the rotary assembly device.

In the figure, 1-rotating table; 2-assembling device; 3-fixing frame; 4-first motor; 5-fixing plate; 6-first clamping plate; 7-second clamping plate; 8-first screw ;9-limiting column;10-through hole;11-movable limiter plate;12-first opening;13-forced rod;14-guide rod;15-spring;16-nut; 17-positioning plate; 18-Second opening; 19-Inlay slot; 20-Second screw; 21-Center hole; 22-Rotating shaft; 23-Bump; 24-Second motor; ; 27- ear plate; 28- lipstick mold.

Detailed ways

As shown in Figure 1 to Figure 12, it is a kind of traditional Chinese medicine nourishing lipstick containing salvia miltiorrhiza quinone of the present invention, and the preparation raw materials of the traditional Chinese medicine nourishing lipstick include:

Coloring and medicinal systems: salvia diterpene quinone, titanium dioxide, titanium dioxide has the effect of covering and whitening.

Fragrance system used to enhance aroma. The aroma system includes saccharin and compound essential oil, among which the compound essential oil can use DOTTERA light compound essential oil, and add saccharin and DOTTERA light compound essential oil for fragrance, so that the lipstick has the characteristics of "sweetness", which improves the user's experience.

Matrix system: natural cocoa butter, white petrolatum, lanolin, beeswax, ozokerite, which is convenient for the lipstick to be molded in the lipstick mold in the later stage. Natural cocoa butter, white petrolatum, lanolin, beeswax and ozokerite are in a weight ratio of 6:6:10:4:4.

Wherein, the coloring agent of the traditional Chinese medicine nourishing lipstick of the present invention is the fat-soluble component salvia diterpene quinone extracted from the traditional Chinese medicine Salvia miltiorrhiza. There is a saying in the traditional Chinese medicine books: "Blindly Danshen Drink, Gongtong Siwu Decoction", the extracted and purified Salvia miltiorrhiza fat-soluble The ingredient Salvia diterpene quinone condenses the triple effect of Salvia miltiorrhiza to nourish blood, activate blood and cool blood. Traditional Chinese medicine nourishing lipstick has a good improvement effect on women's lip color lightening and lip lines deepening. Salvia diterpene quinone itself has good coloring ability and coloring effect, and it also has a special aroma of traditional Chinese medicine. It is a rare lipstick (lip balm) coloring material with the characteristics of traditional Chinese medicine.

A preparation method of a traditional Chinese medicine nourishing lipstick containing salvia diterpene quinone is prepared by using the above-mentioned preparation raw materials of the traditional Chinese medicine nourishing lipstick.

Specifically include the following steps:

a, preparation of salvia diterpene quinone:

1) Put the traditional Chinese medicine salvia miltiorrhiza decoction pieces in a pulverizer, and then sieve the salvia miltiorrhiza powder, pass through a 1000-mesh sieve, and then store the sieved salvia miltiorrhiza powder in a cool and dry place for later use.

2) Mix the powder of Salvia miltiorrhiza with 95% medical ethanol in an equal volume in a spherical bottle, and perform ultrasonic waves in an ultrasonic oscillator for 30 minutes until the ethanol solution in the bottle turns dark red, filter out the medicinal residues, and remove the salvia milt. The red 95% ethanol was placed in a beaker and sealed in a dark place for future use. Then, the last ultrasonic extraction step was continued, and the 95% ethanol eluate was collected repeatedly for 5 times, and all the 95% ethanol eluate was combined.

3) The combined 95% ethanol eluates were concentrated in a rotary evaporator until the volume was 100 ml.

4) Take a pear-shaped separatory funnel, mix 100ml of 95% ethanol concentrate with an equal volume of petroleum ether solution (boiling range is 35-65° C.) and leave it to stand for extraction, until the solution is layered, and the lower layer (ethanol) is collected. solution part, and then continue with the previous extraction step, repeating the operation 5 times.

5) Continue to concentrate the extracted 100ml ethanol solution until it is a dark red semi-fluid (paste), collect the semi-fluid salvia miltiorrhiza extract, cool it and store it in a desiccator for 3 days to obtain a deep red with special fragrance. Red solid substance Salvia diterpene quinone.

The traditional Chinese medicine salvia miltiorrhiza decoction pieces are pulverized in a pulverizer, and it is easy to be fully dissolved with 95% medical ethanol. After extraction and purification, the fat-soluble component of salvia miltiorrhiza diterpene quinone can be obtained, which can extract and retain more salvia diterpene quinone, and then obtain a higher content of danshen diterpene quinone. Salvia diterpene quinone, and the extraction and purification has strong operability, shortens the preparation period of salvia diterpene quinone, reduces cost, and gives full play to the performance of salvia diterpene quinone in traditional Chinese medicine nourishing lipstick.

The content of the obtained dark red solid substance salvia diterpene quinone is tested, specifically, extracting a small amount of dark red solid substance salvia diterpene quinone, weighing it, placing it in a conical flask, adding methanol, sealing it, weighing it, ultrasonicating. Treat for 30min, let it cool, re-weigh the weight, then use methanol to make up the lost weight, shake well, filter, take the subsequent filtrate, filter it with a 0.45um filter membrane, and analyze it by HPLC to obtain the content of Salvia miltiorrhiza diterpene quinone, according to Salvia miltiorrhiza The content of diterpene quinone improves the extraction and purification operation in the preparation of salvia miltiorrhiza diterpene quinone.

b. Preparation of coloring, curing, brightening and aroma system:

1) Precisely weigh 0.5 g of salvia diterpene quinone, 0.5 g of titanium dioxide and 0.3 g of saccharin, and place them in a clean beaker. Then add 15ml of 75% ethanol, and then sonicate in an ultrasonic heating shaker for 1 hour until the solution is bright orange-red, place it in a cool and ventilated place to volatilize the remaining ethanol, and obtain a coloring and curing solution of about 12ml.

2) Add 3 g of lanolin to the coloring and curing solution, stir with a glass rod for 3 minutes, and continue to sonicate in an ultrasonic heating oscillator for 1 hour until the solution is bright orange-red and semi-fluid, and the solution is basically free of alcohol odor. The solution was stored in a 4°C refrigerator for later use, to prevent the semi-fluid solution from breeding bacteria and to keep it for a longer time.

3) The solution is heated to 60°C in an ultrasonic heating oscillator, and then 5-10 drops of compound essential oil are added dropwise to the solution. The compound essential oil can be made of DOTTERA light compound essential oil to obtain a coloring and maintenance fragrance solution.

c. Preparation of matrix system: Weigh 60g of natural cocoa butter, 60g of white petrolatum, 100g of lanolin, 40g of beeswax and 40g of ozokerite, placed in a clean beaker, heated and stirred in a constant temperature water bath at 70°C, until the solution is pale yellow Transparent, the temperature of the constant temperature water bath was adjusted to 60°C to maintain the liquid properties of the matrix system to obtain a liquid matrix solution. Lanolin is used for skin care, calming, moisturizing and other properties. In clinical practice, the role of lanolin is mainly reflected in the application of lanolin together with vaseline, which can increase the permeability of vaseline. At the same time, because lanolin can also be used for skin care, especially for dry skin, it can effectively replenish moisture and prevent moisture loss. , can resist oxidation, and can remove harmful acidic substances.

d. Preparation of traditional Chinese medicine nourishing lipstick containing salvia diterpene quinone:

1) Take 3.5 ml of the coloring and curing aroma solution prepared in step b and 10 ml of the liquid matrix solution prepared in step c, mix them in a constant temperature water bath at 60°C, and stir for 30 seconds, so that the solution is opaque and bright. Orange red, the solution is the lipstick solution.

2) Select a lipstick mold for preparation, and preheat the plastic lipstick mold.

3) pouring the lipstick solution into a lipstick mold, and then cooling at room temperature to obtain a traditional Chinese medicine nourishing lipstick containing salvia miltiorrhiza quinone.

A pattern is arranged on the outer layer of the lipstick mold, and when the lipstick solution is poured into the lipstick mold, the lipstick mold is rotated, the lipstick solution is added, and then cooled at room temperature to obtain a traditional Chinese medicine nourishing lipstick containing salvia diterpene quinone. The lipstick mold is rotated, and the air bubbles in the lipstick mold are discharged through centrifugal action, and at the same time, the lipstick solution in the lipstick mold is filled with the pattern set by the entire lipstick mold, so as to ensure that the texture of the obtained traditional Chinese medicine nourishing lipstick is clear and distinct, and the overall appearance is improved. sex.

The lipstick mold 28 is rotated by a rotary assembly device, and the lipstick solution is added. The rotary assembly device includes a rotary table 1 and an assembly device 2. The top of the rotary table 1 is provided with a fixed frame 3, and the top of the fixed frame 3 is provided with a first The motor 4, through the first motor 4, can make the entire rotating table 1 rotate, thereby making the lipstick mold 28 on the rotating table 1 rotate.

The assembly device 2 includes a fixed plate 5, a first clamping plate 6, a second clamping plate 7, a movable limit plate 11 and a positioning plate 17, and the first clamping plate 6 and the second clamping plate 7 are both L-shaped , both the first clamping plate 6 and the second clamping plate 7 are provided with an oblong hole 25, the two oblong holes 25 are arranged correspondingly up and down, and a first screw 8 is arranged between the two oblong holes 25, and the first screw 8 is fixed in On the fixing plate 5, the first screw 8 presses the first clamping plate 6 and the second clamping plate 7 on the fixing plate 5, and through the tightening action of the first screw 8, the length of the lipstick mold 28 can be adjusted. The distance between the first clamping plate 6 and the second clamping plate 7 is such that the lipstick mold 28 can just be clamped between the first clamping plate 6 and the second clamping plate 7, so that the first clamping plate 6 and the The second clamping plate 7 limits the lengthwise direction of the lipstick mold 28 . The bottoms of the first clamping plate 6 and the second clamping plate 7 are provided with limit posts 9, the fixing plate 5 is provided with two through holes 10, the limit posts 9 pass through the through holes 10, and the limit posts 9 are located in the through holes. 10 moves along the length direction of the oblong hole 25, and the limit post 9 acts as a limit, so that the first clamping plate 6 and the second clamping plate 7 move directionally, raising the first clamping plate 6 and the second clamping plate 7. The stability of the movement of the clamping plate 7 facilitates quick adjustment of the distance between the first clamping plate 6 and the second clamping plate 7 according to the length of the lipstick mold 28 .

The movable limiting plate 11 is provided with two rectangular first openings 12 , and the first clamping plate 6 and the second clamping plate 7 pass through the first openings 12 respectively. The front side of the movable limit plate 11 (the direction close to the rotary table 1) is provided with a force rod 13, the rear side of the movable limit plate 11 (in the direction away from the rotary table 1) is provided with a guide rod 14, and the positioning plate 17 is provided with a nut. 16 is fixed on the raised portion of the first clamping plate 6 and the raised portion of the second clamping plate 7 . The positioning plate 17 is provided with a rectangular second opening 18, the first clamping plate 6 and the second clamping plate 7 respectively pass through the second opening 18, the guide rod 14 passes through the positioning plate 17, and the guide rod 14 is sleeved with a spring 15. The spring 15 is arranged between the movable limit plate 11 and the positioning plate 17. In the present invention, one end of the spring 15 is welded on the movable limit plate 11, and the positioning plate 17 is pressed against the other end of the spring 15, which is convenient for movement. The connection between the type limit plate 11 and the positioning plate 17. By exerting a force on the force receiving rod 13, the guide rod 14 moves directionally on the movable limit plate 11, and at the same time, the movable limit plate 11 moves directionally on the first clamping plate 6 and the second clamping plate 7, By setting the spring 15, the movable limiting plate 11 reciprocates, so that the first clamping plate 6, the second clamping plate 7 and the movable limiting plate 11 clamp the width direction of the lipstick mold 28. The limit plate 11 reciprocates, and the lipstick mold 28 can be quickly installed up and down or removed. In addition, the movable limit plate 11 is provided with a rectangular first opening 12, and the positioning plate 17 is provided with a rectangular second opening 18, so that the movable limit plate 11 and the positioning plate 17 are provided without hindering the first clamping plate. The distance between 6 and the second clamping plate 7 is adjusted to adapt to the clamping action of lipstick molds 28 of different specifications.

The number of assembling devices 2 is at least four. The assembling devices 2 are evenly installed on the rotary table 1 in the circumferential direction. The rotary table 1 is provided with an embedded groove 19 with an opening facing downward. The plate 5 is fixedly connected to the rotary table 1 through the second screw 20 , which is convenient and quick to install or remove the entire assembly device 2 . By arranging a plurality of assembling devices 2, the rotary table 1 can rotate the plurality of lipstick molds 28 at the same time, and the plurality of assembling devices 2 are evenly installed on the rotary table 1 in the circumferential direction, which is convenient for the force-bearing rod 13 on the assembling device 2. Perform rotary application of force.

The central position of the rotary table 1 is provided with a central hole 21, a rotary shaft 22 is provided in the central hole 21, a second motor 24 is provided at the bottom of the rotary shaft 22, and the second motor 24 drives the rotary shaft 22 to rotate in the central hole 21, and rotates The side surface of the shaft 22 is provided with a convex block 23 whose outer surface is in the shape of an arc, and the convex block 23 squeezes the force-bearing rod 13 to achieve a rotary application of force to the force-bearing rod 13 on the assembly device 2. This method makes the assembly device 2. The opening and closing are performed at the same time interval, which is convenient for rotating the lipstick mold 28 in batches.

The steps of rotating the lipstick mold 28 by using the rotating assembly device 2 are as follows:

a. Loosen the first screw 8 and the second screw 20, adjust the distance between the first clamping plate 6 and the second clamping plate 7 according to the length of the lipstick mold 28, when the inner side of the first clamping plate 6 When the distance from the inner side of the second clamping plate 7 is the length of the lipstick mold 28 , the first screw 8 is tightened, and then the second screw 20 is tightened.

b. Install the lipstick mold 28:

1) Turn on the second motor 24, the second motor 24 drives the rotating shaft 22 to rotate in the central hole 21, when the bump 23 on the side of the rotating shaft 22 squeezes the force-bearing rod 13 of the first rotating assembly device 2, the movable The limit plate 11 moves away from the center of the rotary table 1, and the spring 15 is compressed. At this time, the L-shaped moving rod 26 is used to pass through the ear plate 27 on the top of the lipstick mold 28, and then the L-shaped moving rod 26 is moved downward to remove the lipstick. The mold 28 is embedded in the area between the first clamping plate 6 and the second clamping plate 7, and the lipstick mold 28 has been filled with lipstick solution at this time. When the projection 23 on the side of the rotating shaft 22 leaves the force-receiving rod 13 of the first rotating assembly device 2, under the action of the deformation recovery of the spring 15, the movable limit plate 11 moves toward the center of the rotating table 1. At this time, The movable limit plate 11 presses the lipstick mold 28 , and then moves out the L-shaped moving rod 26 to complete the loading of the first lipstick mold 28 into the rotary assembly device 2 .

2) The second motor 24 drives the rotating shaft 22 to rotate continuously in the central hole 21, and the remaining lipstick molds 28 are loaded into the rotary assembly device 2 in the same way as the first lipstick mold 28 is loaded.

3) After the second motor 24 drives the rotating shaft 22 to rotate in the central hole 21 for one turn, the second motor 24 is turned off to ensure that all the lipstick molds 28 are loaded.

c. Turn on the first motor 4, the first motor 4 drives the entire rotary table 1 to rotate at a constant speed, and rotates the lipstick mold 28, through centrifugal action, the air bubbles in the lipstick mold 28 are discharged, and the lipstick solution in the lipstick mold 28 is discharged simultaneously. Fill the pattern of the entire lipstick stencil with 28 settings.

d. When the first motor 4 drives the entire rotary table 1 to rotate at a constant speed for 5 minutes, turn off the first motor 4. After the rotary table 1 stops rotating, let the lipstick mold 28 stand for 2-3 minutes, and then fill the lipstick mold 28 with the lipstick solution. , Supplement the missing lipstick solution to ensure the integrity of the traditional Chinese medicine nourishing lipstick obtained later, and then cool it at room temperature, usually for 30 minutes.

e. Take out the lipstick mold 28:

1) Turn on the second motor 24, the second motor 24 drives the rotating shaft 22 to rotate in the central hole 21, when the bump 23 on the side of the rotating shaft 22 squeezes the force-bearing rod 13 of the first rotating assembly device 2, the movable The limit plate 11 moves away from the center of the rotary table 1, and the spring 15 is compressed. At this time, the L-shaped moving rod 26 is used to pass through the lug plate 27 on the top of the lipstick mold 28, and then the L-shaped moving rod 26 is moved upward to move the lipstick mold. 28 is taken out from the area between the first clamping plate 6 and the second clamping plate 7, when the protrusion 23 on the side of the rotating shaft 22 leaves the force-bearing rod 13 of the first rotating assembly device 2, the deformation of the spring 15 Under the recovery action, the movable limit plate 11 moves toward the center of the rotary table 1 and returns to the starting position, and the first lipstick mold 28 is taken out from the rotary assembly device 2 .

2) The second motor 24 drives the rotating shaft 22 to rotate continuously in the central hole 21, and takes out the remaining lipstick molds 28 from the rotary assembly device 2 in the same way as the first lipstick mold 28 is taken out.

3) After the second motor 24 drives the rotating shaft 22 to rotate one turn in the central hole 21, the second motor 24 is turned off.

f. Open the lipstick mold 28 to obtain a traditional Chinese medicine nourishing lipstick containing salvia diterpene quinone.

The above are only specific embodiments of the present invention, but the technical features of the present invention are not limited thereto. Any simple changes, equivalent replacements or modifications made based on the present invention in order to solve basically the same technical problems and achieve basically the same technical effects are all included in the protection scope of the present invention.

Claims (1)

1. The preparation contains rotatory assembly quality of traditional chinese medicine nourishing lipstick of red-rooted salvia diterpenoid quinone, its characterized in that: the lipstick mold is rotated by adopting a rotating assembly device, and lipstick solution is replenished for operation, wherein the rotating assembly device comprises a rotating table and an assembly device, a fixing frame is arranged at the top of the rotating table, and a first motor is arranged at the top of the fixing frame;

the assembling device comprises a fixing plate, a first clamping plate, a second clamping plate, a movable limiting plate and a positioning plate, wherein the first clamping plate and the second clamping plate are both L-shaped, the first clamping plate and the second clamping plate are respectively provided with a long round hole, the two long round holes are arranged in a vertically corresponding mode, a first screw is arranged between the two long round holes and fixed on the fixing plate, the first clamping plate and the second clamping plate are tightly pressed on the fixing plate through the first screw, limiting columns are arranged at the bottoms of the first clamping plate and the second clamping plate, the fixing plate is provided with two through holes, the limiting columns penetrate through the through holes, and the limiting columns move in the through holes along the length direction of the long round holes;

the movable limiting plate is provided with two first openings, the first clamping plate and the second clamping plate respectively penetrate through the first openings, the front side of the movable limiting plate is provided with a stress rod, the rear side of the movable limiting plate is provided with a guide rod, the positioning plate is fixed on the first clamping plate and the second clamping plate through nuts, the positioning plate is provided with a second opening, the first clamping plate and the second clamping plate respectively penetrate through the second opening, the guide rod penetrates through the positioning plate, a spring is sleeved on the guide rod, and the spring is arranged between the movable limiting plate and the positioning plate;

the number of the assembling devices is at least four, the assembling devices are uniformly arranged on the rotating platform in the circumferential direction, the rotating platform is provided with an inner embedded groove with a downward opening, the fixing plate is embedded in the inner embedded groove, and the fixing plate is fixedly connected to the rotating platform through a second screw;

the center position of revolving stage puts and is equipped with the centre bore, be equipped with the rotation axis in the centre bore, the bottom of rotation axis is equipped with the second motor, the second motor drive the rotation axis is in rotatory in the centre bore, the side of rotation axis is equipped with the lug that the surface is convex, the lug extrusion atress pole.

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