CN112362391B - Liquid asphalt sampling system and method - Google Patents
Liquid asphalt sampling system and method Download PDFInfo
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- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N1/00—Sampling; Preparing specimens for investigation
- G01N1/02—Devices for withdrawing samples
- G01N1/10—Devices for withdrawing samples in the liquid or fluent state
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- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N1/00—Sampling; Preparing specimens for investigation
- G01N1/02—Devices for withdrawing samples
- G01N1/10—Devices for withdrawing samples in the liquid or fluent state
- G01N1/20—Devices for withdrawing samples in the liquid or fluent state for flowing or falling materials
- G01N1/2035—Devices for withdrawing samples in the liquid or fluent state for flowing or falling materials by deviating part of a fluid stream, e.g. by drawing-off or tapping
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- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N1/00—Sampling; Preparing specimens for investigation
- G01N1/02—Devices for withdrawing samples
- G01N1/10—Devices for withdrawing samples in the liquid or fluent state
- G01N2001/1031—Sampling from special places
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- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N1/00—Sampling; Preparing specimens for investigation
- G01N1/02—Devices for withdrawing samples
- G01N1/10—Devices for withdrawing samples in the liquid or fluent state
- G01N1/20—Devices for withdrawing samples in the liquid or fluent state for flowing or falling materials
- G01N1/2035—Devices for withdrawing samples in the liquid or fluent state for flowing or falling materials by deviating part of a fluid stream, e.g. by drawing-off or tapping
- G01N2001/205—Devices for withdrawing samples in the liquid or fluent state for flowing or falling materials by deviating part of a fluid stream, e.g. by drawing-off or tapping using a valve
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Abstract
本发明涉及一种液体沥青取样系统及方法,所述液体沥青取样系统包括取样管道、冷却单元、取样单元及清洗单元;取样管道的一端连接△P装置上游的液体沥青管道,另一端连接△P装置下游的液体沥青管道;所述冷却单元包括冷却器;所述取样单元包括取样器;所述清洗单元包括高位罐和低位罐;本发明彻底解决了液体沥青在线取样时沥青堵塞管道和阀门的问题,同时解决了取样过程和清洗过程中沥青烟气排放污染环境的问题。
The present invention relates to a liquid asphalt sampling system and method, wherein the liquid asphalt sampling system comprises a sampling pipeline, a cooling unit, a sampling unit and a cleaning unit; one end of the sampling pipeline is connected to the liquid asphalt pipeline upstream of a ΔP device, and the other end is connected to the liquid asphalt pipeline downstream of the ΔP device; the cooling unit comprises a cooler; the sampling unit comprises a sampler; the cleaning unit comprises a high-level tank and a low-level tank; the present invention thoroughly solves the problem of asphalt blocking pipelines and valves during online sampling of liquid asphalt, and simultaneously solves the problem of asphalt fume emissions polluting the environment during the sampling process and the cleaning process.
Description
技术领域Technical Field
本发明涉及焦化技术领域,尤其涉及一种沥青生产及其深加工过程中煤焦油液体沥青取样系统及方法。The invention relates to the field of coking technology, and in particular to a coal tar liquid asphalt sampling system and method in asphalt production and deep processing.
背景技术Background Art
煤焦油加工过程中产生约50%~60%的中温沥青,属于焦油加工的大宗产品,加工规模越大,沥青产量越多。改质沥青是目前沥青的主要下游产品,主要用于电解铝行业生产预焙阳极、制备电池棒或电极粘结剂。此外还有沥青焦、针状焦等,也是中温沥青的下游产品,无论采用何种生产工艺,都需要对生产过程中的液体沥青进行取样检测,从而保证最终产品的质量。During the processing of coal tar, about 50% to 60% of medium-temperature asphalt is produced, which is a major product of tar processing. The larger the processing scale, the more asphalt is produced. Modified asphalt is currently the main downstream product of asphalt, mainly used in the production of pre-baked anodes, preparation of battery rods or electrode binders in the electrolytic aluminum industry. In addition, asphalt coke, needle coke, etc. are also downstream products of medium-temperature asphalt. Regardless of the production process used, it is necessary to sample and test the liquid asphalt in the production process to ensure the quality of the final product.
常规的液体沥青管道的在线取样方法,通常是在需要取样的管道上增设由一个分支短管和一个保温旋塞组成的取样器。沥青常温下为略带臭味的黑色固体,无固定熔点,而沥青的生产过程大多处于130~400℃的高温环境下,此时沥青为黑色流体状态,若在敞开的大气环境中取样,不仅高温沥青本身非常危险,还会散发出大量的沥青烟气,具有强烈的刺激性气味,毒性非常大;操作人员暴露在这样的环境中,会对身体造成伤害,也会对环境造成污染。同时,沥青取样以后,剩余沥青就会凝结在取样管道中,堵塞取样管道及阀门。The conventional online sampling method for liquid asphalt pipelines usually adds a sampler consisting of a branch short pipe and an insulated cock to the pipeline where sampling is required. Asphalt is a slightly smelly black solid at room temperature and has no fixed melting point. The production process of asphalt is mostly in a high temperature environment of 130 to 400°C. At this time, asphalt is in a black fluid state. If sampling is carried out in an open atmospheric environment, not only is the high-temperature asphalt itself very dangerous, but it will also emit a large amount of asphalt fumes with a strong pungent odor and high toxicity. Operators exposed to such an environment will cause harm to their bodies and pollute the environment. At the same time, after the asphalt is sampled, the remaining asphalt will condense in the sampling pipeline, blocking the sampling pipeline and valve.
申请号为CN 202010119181.5的中国专利申请公开了“一种煤焦油沥青沥青取样阀及在线取样系统”,煤焦油沥青在线取样系统包括煤焦油沥青取样阀、沥青冷却器、沥青取样钢瓶、称重电子秤、吹扫单元及排气单元;煤焦油沥青取样阀直接设于煤焦油沥青的主管道上,不仅能够彻底解决采用支管道取样时支管道和取样阀的堵塞问题,并且取得的沥青样本都是现流样,没有管道残留沥青成分的存在。上述技术方案只针对取样过程中的管道堵塞和沥青烟气采取了防治措施,而取样后残留的沥青粘度较大,用氮气吹扫很难吹扫干净,而且吹扫的沥青烟气直接排到大气,同样会造成环境污染,因此其并没有从根本上解决问题。The Chinese patent application with application number CN 202010119181.5 discloses "a coal tar asphalt sampling valve and an online sampling system". The coal tar asphalt online sampling system includes a coal tar asphalt sampling valve, an asphalt cooler, an asphalt sampling cylinder, an electronic weighing scale, a purge unit and an exhaust unit; the coal tar asphalt sampling valve is directly arranged on the main pipeline of the coal tar asphalt, which can not only completely solve the blockage problem of the branch pipeline and the sampling valve when sampling with the branch pipeline, but also the asphalt samples obtained are all live flow samples, and there is no residual asphalt component in the pipeline. The above technical scheme only takes preventive measures for pipeline blockage and asphalt fume during the sampling process, and the residual asphalt after sampling has a large viscosity, and it is difficult to purge it clean with nitrogen, and the purged asphalt fume is directly discharged into the atmosphere, which will also cause environmental pollution. Therefore, it does not fundamentally solve the problem.
目前,还没有一种取样系统能够彻底解决沥青在线取样时残留沥青堵塞管道以及在线取样产生沥青烟气的排放问题。At present, there is no sampling system that can completely solve the problem of residual asphalt clogging the pipeline during online asphalt sampling and the emission of asphalt fume generated by online sampling.
发明内容Summary of the invention
本发明提供了一种液体沥青取样系统及方法,彻底解决了液体沥青在线取样时沥青堵塞管道和阀门的问题,同时解决了取样过程和清洗过程中沥青烟气排放污染环境的问题。The present invention provides a liquid asphalt sampling system and method, which completely solves the problem of asphalt blocking pipelines and valves during online sampling of liquid asphalt, and also solves the problem of asphalt fume emission polluting the environment during the sampling and cleaning processes.
为了达到上述目的,本发明采用以下技术方案实现:In order to achieve the above object, the present invention adopts the following technical solutions:
一种液体沥青取样系统,包括取样管道、冷却单元、取样单元及清洗单元;所述取样管道的一端连接△P装置上游的液体沥青管道,另一端连接△P装置下游的液体沥青管道;所述冷却单元包括冷却器;所述取样单元包括取样器;所述清洗单元包括高位罐和低位罐;所述取样管道上沿沥青流动方向依次设有清洗介质入口、冷却器、取样器、排气口、清洗介质出口;所述排气口通过排气管道连接高位罐,清洗介质出口通过清洗介质出口管道连接高位罐;所述高位罐的底部设底部出口通过底部管道连接低位罐的上部入口,低位罐的顶部设顶部出口通过顶部管道连接高位罐上部的上部入口;所述低位罐中设加热器,低位罐的底部设清洗介质出口通过清洗介质管道连接冷却器上游的取样管道。A liquid asphalt sampling system comprises a sampling pipeline, a cooling unit, a sampling unit and a cleaning unit; one end of the sampling pipeline is connected to the liquid asphalt pipeline upstream of a △P device, and the other end is connected to the liquid asphalt pipeline downstream of the △P device; the cooling unit comprises a cooler; the sampling unit comprises a sampler; the cleaning unit comprises a high-level tank and a low-level tank; the sampling pipeline is provided with a cleaning medium inlet, a cooler, a sampler, an exhaust port, and a cleaning medium outlet in sequence along the asphalt flow direction; the exhaust port is connected to the high-level tank through an exhaust pipe, and the cleaning medium outlet is connected to the high-level tank through a cleaning medium outlet pipe; a bottom outlet is provided at the bottom of the high-level tank, which is connected to an upper inlet of a low-level tank through a bottom pipe, and a top outlet is provided at the top of the low-level tank, which is connected to an upper inlet of the upper part of the high-level tank through a top pipe; a heater is provided in the low-level tank, and a cleaning medium outlet is provided at the bottom of the low-level tank, which is connected to the sampling pipeline upstream of the cooler through a cleaning medium pipe.
所述△P装置为阀门或减压装置。The ΔP device is a valve or a pressure reducing device.
所述冷却单元还包括压力表及温度表;压力表设于冷却器上游的取样管道上,温度表设于冷却器下游的取样管道上;冷却单元上游的取样管道上设阀门一。The cooling unit also includes a pressure gauge and a temperature gauge; the pressure gauge is arranged on the sampling pipeline upstream of the cooler, and the temperature gauge is arranged on the sampling pipeline downstream of the cooler; a valve is arranged on the sampling pipeline upstream of the cooling unit.
所述取样单元还包括软管一和软管二;所述取样器是由快速接头一、针型阀一、取样瓶、针型阀二、快速接头二依次连接组成的一体取样装置,快速接头一、快速接头二分别通过对应端的软管一、软管二与取样管道相连接。The sampling unit also includes a hose 1 and a hose 2; the sampler is an integrated sampling device composed of a quick connector 1, a needle valve 1, a sampling bottle, a needle valve 2, and a quick connector 2 connected in sequence, and the quick connector 1 and the quick connector 2 are respectively connected to the sampling pipeline through the hose 1 and the hose 2 at the corresponding ends.
取样单元两端的取样管道上分别设阀门三和阀门四;阀门三上游的取样管道与阀门四下游的取样管道之间通过交通管连通,交通管上设阀门二。The sampling pipelines at both ends of the sampling unit are respectively provided with valve three and valve four; the sampling pipeline upstream of valve three is connected with the sampling pipeline downstream of valve four through a traffic pipe, and valve two is provided on the traffic pipe.
所述排气管道上设阀门五,所述清洗介质出口管道上设阀门六,所述底部管道上设阀门七,所述顶部管道上设阀门八;清洗介质入口下游的取样管道上设阀门九;清洗介质管道上设阀门十。The exhaust pipe is provided with valve five, the cleaning medium outlet pipe is provided with valve six, the bottom pipe is provided with valve seven, the top pipe is provided with valve eight; the sampling pipe downstream of the cleaning medium inlet is provided with valve nine; the cleaning medium pipe is provided with valve ten.
所述高位罐的顶部设放散气管及蒽油入口管。The top of the high-position tank is provided with a venting air pipe and an anthracene oil inlet pipe.
所述低位罐的顶部设安全阀,上部设加压氮气入口管;低位罐内还设有液位计及温度计。A safety valve is arranged on the top of the low-level tank, and a pressurized nitrogen inlet pipe is arranged on the upper part; a liquid level gauge and a thermometer are also arranged in the low-level tank.
一种液体沥青取样方法,包括:A liquid asphalt sampling method, comprising:
1)液体沥青管道中的来料沥青温度为130~400℃,取样开始时,△P装置上游的沥青依次经阀门一、冷却单元、交通管及阀门九后,返回到△P装置下游的液体沥青管道;1) The temperature of the incoming asphalt in the liquid asphalt pipeline is 130-400℃. When sampling begins, the asphalt upstream of the △P device passes through valve 1, cooling unit, traffic pipe and valve 9 in sequence, and then returns to the liquid asphalt pipeline downstream of the △P device;
2)如果沥青温度在130~150℃之间,冷却器不开启;如果沥青温度在150℃以上,开启冷却器,待温度表测得的沥青温度在130~150℃之间时,关闭阀门二,使沥青进入取样单元;2) If the asphalt temperature is between 130 and 150°C, the cooler is not turned on; if the asphalt temperature is above 150°C, the cooler is turned on, and when the asphalt temperature measured by the thermometer is between 130 and 150°C, valve 2 is closed to allow the asphalt to enter the sampling unit;
3)取样单元接收从冷却单元来的沥青,在逐渐关闭阀门二的同时,依次打开取样管道上的阀门三、针型阀一、针型阀二和排气管道上的阀门五,阀门四待上游取样管道中的气排空后打开,阀门四打开的同时关闭排气管道上的阀门五;液体沥青经过取样管道闭路循环后回到液体沥青管道中;3) The sampling unit receives the asphalt from the cooling unit, and while gradually closing valve 2, opens valve 3, needle valve 1, needle valve 2 and valve 5 on the sampling pipeline in sequence. Valve 4 is opened after the gas in the upstream sampling pipeline is emptied, and valve 5 on the exhaust pipeline is closed while valve 4 is opened; the liquid asphalt returns to the liquid asphalt pipeline after a closed-loop circulation through the sampling pipeline;
4)进行现流样截取,截取完样品后打开阀门二,关闭阀门三、阀门四、针型阀一、针型阀二,取下装有样品的取样器,同时换上清洁的取样器;4) Take the current sample, open valve 2 after taking the sample, close valve 3, valve 4, needle valve 1, needle valve 2, remove the sampler containing the sample, and replace it with a clean sampler;
5)对取样管道进行清洗;清洗过程中的沥青烟气及空气经排气管道排到高位罐中,最后经放散气管接入原有沥青放散气系统中,取样过程及清洗过程均无沥青烟气及空气外排。5) Clean the sampling pipeline; the asphalt fume and air in the cleaning process are discharged into the high-level tank through the exhaust pipe, and finally connected to the original asphalt venting system through the venting pipe. No asphalt fume and air are discharged during the sampling and cleaning processes.
所述清洗单元是利用沥青中的组分蒽油作为冲洗介质对取样管道进行清洗;具体过程如下:The cleaning unit uses anthracene oil, a component of asphalt, as a flushing medium to clean the sampling pipeline; the specific process is as follows:
1)将蒽油加入到高位罐中,打开底部管道上的阀门七和顶部管道上的阀门八,蒽油自流到低位罐中;关闭阀门七和阀门八,通过加热器对低位罐中的蒽油进行加热,加热温度用温度计监测,加热到设定温度后开始清洗;1) adding anthracene oil to the high-level tank, opening valve seven on the bottom pipeline and valve eight on the top pipeline, and allowing the anthracene oil to flow into the low-level tank by gravity; closing valve seven and valve eight, heating the anthracene oil in the low-level tank by a heater, monitoring the heating temperature with a thermometer, and starting cleaning after heating to a set temperature;
2)清洗前阀门开关确认:阀门一、阀门九在清洗过程中始终处于关闭状态,安全阀处于工作状态,冷却水上水处于未通入冷却器的状态;2) Confirm the valve switch before cleaning: valve 1 and valve 9 are always in the closed state during the cleaning process, the safety valve is in the working state, and the cooling water supply is not in the state of flowing into the cooler;
3)对取样管道进行清洗;清洁的取样器安装好后,阀门七、阀门八、阀门二、阀门四、阀门六均处于关闭状态,阀门十、阀门三、针型阀一、针型阀二、阀门五均处于开启状态;加热后的蒽油通过加压氮气入口管进入低位罐,在压力的作用下,蒽油从低位罐底部清洗介质出口依次经阀门十、冷却器、阀门三、软管一、快速接头一、针型阀一、取样瓶、针型阀二、快速接头二、软管二、阀门五后回到高位罐中;然后打开底部管道上的阀门七及顶部管道上的阀门八,将蒽油再次放入到低位罐中;重复上述过程对取样管道进行反复冲洗,直到冲洗干净为止;3) Clean the sampling pipeline; after the clean sampler is installed, valve seven, valve eight, valve two, valve four, and valve six are all in a closed state, and valve ten, valve three, needle valve one, needle valve two, and valve five are all in an open state; the heated anthracene oil enters the low-level tank through the pressurized nitrogen inlet pipe, and under the action of pressure, the anthracene oil returns to the high-level tank from the cleaning medium outlet at the bottom of the low-level tank through valve ten, cooler, valve three, hose one, quick connector one, needle valve one, sampling bottle, needle valve two, quick connector two, hose two, and valve five; then open valve seven on the bottom pipeline and valve eight on the top pipeline, and put the anthracene oil into the low-level tank again; repeat the above process to repeatedly rinse the sampling pipeline until it is clean;
4)冲洗交通管;关闭阀门三、阀门四及阀门五,打开阀门六、阀门二,加热后的蒽油从低位罐底部的清洗介质出口依次经阀门十、冷却器、阀门二、阀门六后,回到高位罐中,然后打开底部管道的阀门七及顶部管道上的阀门八,蒽油再次放回到低位罐中,重复上述过程对交通管进行反复冲洗,直到冲洗干净为止。4) Flush the traffic pipe; close valve three, valve four and valve five, open valve six and valve two, and the heated anthracene oil returns to the high-level tank from the cleaning medium outlet at the bottom of the low-level tank through valve ten, cooler, valve two, valve six in sequence, and then open valve seven on the bottom pipe and valve eight on the top pipe, and put the anthracene oil back into the low-level tank again, and repeat the above process to repeatedly flush the traffic pipe until it is clean.
与现有技术相比,本发明的有益效果是:Compared with the prior art, the present invention has the following beneficial effects:
1)本发明能够彻底清洗取样后残留在取样管道内的沥青,而且是无死角清洗,从而保持取样管道始终为清洁状态,彻底解决了取样管道及其上阀门的堵塞问题;并且随时取得的沥青样本都是现流样,不存在管道的残留沥青成分,保证了沥青样品的准确性。1) The present invention can thoroughly clean the asphalt remaining in the sampling pipeline after sampling, and clean without dead angles, thereby keeping the sampling pipeline always in a clean state, and completely solving the problem of blockage of the sampling pipeline and the valve thereon; and the asphalt samples obtained at any time are live flow samples, and there is no residual asphalt component in the pipeline, thereby ensuring the accuracy of the asphalt sample.
2)保证了取样过程中及取样前后均没有沥青烟外排,同时也避免了高温沥青本身产生的危险,彻底解决刺激性气味的沥青烟气对周边环境的影响,对改善沥青生产作业环境起到了很好的作用。2) It ensures that no asphalt smoke is discharged during the sampling process and before and after sampling, while also avoiding the danger of high-temperature asphalt itself, completely solving the impact of asphalt smoke with pungent odor on the surrounding environment, and playing a good role in improving the asphalt production working environment.
附图说明BRIEF DESCRIPTION OF THE DRAWINGS
图1是本发明所述一种液体沥青取样系统的结构示意图。FIG1 is a schematic structural diagram of a liquid asphalt sampling system according to the present invention.
图中:1.阀门一 2.冷却器 3.阀门二 4.阀门九 5.阀门三 6.软管一 7.快速接头一 8.针型阀一 9.取样瓶 10.针型阀二 11.快速接头二 12.软管二 13.阀门四 14.阀门五 15.高位罐 16.低位罐 17.阀门七 18.阀门八 19.安全阀 20.阀门十 21.阀门六 22.压力表 23.温度表 24.液位计 25.加热器 26.放散气管 27.蒽油入口管 28.加压氮气入口管 29.排气管道 30.温度计 31.液体沥青管道 32.△P装置 33.原有沥青放散系统In the figure: 1. Valve 1 2. Cooler 3. Valve 2 4. Valve 9 5. Valve 3 6. Hose 1 7. Quick connector 1 8. Needle valve 1 9. Sampling bottle 10. Needle valve 2 11. Quick connector 2 12. Hose 2 13. Valve 4 14. Valve 5 15. High-level tank 16. Low-level tank 17. Valve 7 18. Valve 8 19. Safety valve 20. Valve 10 21. Valve 6 22. Pressure gauge 23. Thermometer 24. Liquid level gauge 25. Heater 26. Venting pipe 27. Anthracene oil inlet pipe 28. Pressurized nitrogen inlet pipe 29. Exhaust pipe 30. Thermometer 31. Liquid asphalt pipeline 32. △P device 33. Original asphalt venting system
具体实施方式DETAILED DESCRIPTION
下面结合附图对本发明的具体实施方式作进一步说明:The specific implementation of the present invention will be further described below in conjunction with the accompanying drawings:
如图1所示,本发明所述一种液体沥青取样系统,包括取样管道、冷却单元、取样单元及清洗单元;所述取样管道的一端连接△P装置32上游的液体沥青管道31,另一端连接△P装置32下游的液体沥青管道31;所述冷却单元包括冷却器2;所述取样单元包括取样器;所述清洗单元包括高位罐15和低位罐16;所述取样管道上沿沥青流动方向依次设有清洗介质入口、冷却器2、取样器、排气口、清洗介质出口;所述排气口通过排气管道29连接高位罐15,清洗介质出口通过清洗介质出口管道连接高位罐15;所述高位罐15的底部设底部出口(蒽油出口)通过底部管道连接低位罐16的上部入口(蒽油入口),低位罐16的顶部设顶部出口(气体出口)通过顶部管道连接高位罐15上部的上部入口(气体入口);所述低位罐16中设加热器25,低位罐16的底部设清洗介质出口通过清洗介质管道连接冷却器2上游的取样管道。As shown in FIG1 , a liquid asphalt sampling system of the present invention comprises a sampling pipeline, a cooling unit, a sampling unit and a cleaning unit; one end of the sampling pipeline is connected to a liquid asphalt pipeline 31 upstream of a △P device 32, and the other end is connected to a liquid asphalt pipeline 31 downstream of the △P device 32; the cooling unit comprises a cooler 2; the sampling unit comprises a sampler; the cleaning unit comprises a high-level tank 15 and a low-level tank 16; a cleaning medium inlet, a cooler 2, a sampler, an exhaust port, and a cleaning medium outlet are sequentially arranged on the sampling pipeline along the asphalt flow direction; The exhaust port is connected to the high-level tank 15 through the exhaust pipe 29, and the cleaning medium outlet is connected to the high-level tank 15 through the cleaning medium outlet pipe; the bottom of the high-level tank 15 is provided with a bottom outlet (anthracene oil outlet) connected to the upper inlet (anthracene oil inlet) of the low-level tank 16 through the bottom pipe, and the top of the low-level tank 16 is provided with a top outlet (gas outlet) connected to the upper inlet (gas inlet) of the high-level tank 15 through the top pipe; the low-level tank 16 is provided with a heater 25, and the bottom of the low-level tank 16 is provided with a cleaning medium outlet connected to the sampling pipe upstream of the cooler 2 through the cleaning medium pipe.
所述△P装置32为阀门或减压装置。The ΔP device 32 is a valve or a pressure reducing device.
所述冷却单元还包括压力表22及温度表23;压力表22设于冷却器2上游的取样管道上,温度表23设于冷却器2下游的取样管道上;冷却单元上游的取样管道上设阀门一1。The cooling unit also includes a pressure gauge 22 and a temperature gauge 23; the pressure gauge 22 is arranged on the sampling pipeline upstream of the cooler 2, and the temperature gauge 23 is arranged on the sampling pipeline downstream of the cooler 2; a valve 1 is arranged on the sampling pipeline upstream of the cooling unit.
所述取样单元还包括软管一6和软管二12;所述取样器是由快速接头一7、针型阀一8、取样瓶9、针型阀二10、快速接头二11依次连接组成的一体取样装置,快速接头一7、快速接头二11分别通过对应端的软管一6、软管二12与取样管道相连接。The sampling unit also includes a hose 1 6 and a hose 2 12; the sampler is an integrated sampling device composed of a quick connector 1 7, a needle valve 1 8, a sampling bottle 9, a needle valve 2 10, and a quick connector 2 11 connected in sequence, and the quick connector 1 7 and the quick connector 2 11 are respectively connected to the sampling pipeline through the hose 1 6 and the hose 2 12 at the corresponding ends.
所述取样单元两端的取样管道上分别设阀门三5和阀门四13;阀门三5上游的取样管道与阀门四13下游的取样管道之间通过交通管连通,交通管上设阀门二3。The sampling pipelines at both ends of the sampling unit are respectively provided with valve three 5 and valve four 13; the sampling pipeline upstream of valve three 5 is connected with the sampling pipeline downstream of valve four 13 through a traffic pipe, and valve two 3 is provided on the traffic pipe.
所述排气管道19上设阀门五14,所述清洗介质出口管道上设阀门六21,所述底部管道上设阀门七17,所述顶部管道上设阀门八18;清洗介质入口下游的取样管道上设阀门九4;清洗介质管道上设阀门十20。A valve five 14 is provided on the exhaust pipe 19, a valve six 21 is provided on the cleaning medium outlet pipe, a valve seven 17 is provided on the bottom pipe, and a valve eight 18 is provided on the top pipe; a valve nine 4 is provided on the sampling pipe downstream of the cleaning medium inlet; and a valve ten 20 is provided on the cleaning medium pipe.
所述高位罐15的顶部设放散气管26及蒽油入口管27。The top of the high-position tank 15 is provided with a gas emission pipe 26 and an anthracene oil inlet pipe 27 .
所述低位罐16的顶部设安全阀19,上部设加压氮气入口管28;低位罐16内还设有液位计24及温度计30。A safety valve 19 is disposed at the top of the low-level tank 16 , and a pressurized nitrogen inlet pipe 28 is disposed at the upper portion; a liquid level gauge 24 and a thermometer 30 are also disposed in the low-level tank 16 .
一种液体沥青取样方法,包括:A liquid asphalt sampling method, comprising:
1)液体沥青管道31中的来料沥青温度为130~400℃,取样开始时,△P装置32上游的沥青依次经阀门一1、冷却单元2、交通管及阀门九4后,返回到△P装置32下游的液体沥青管道31;1) The temperature of the incoming asphalt in the liquid asphalt pipeline 31 is 130-400°C. When sampling begins, the asphalt upstream of the ΔP device 32 passes through valve 1, cooling unit 2, traffic pipe and valve 9 4 in sequence, and then returns to the liquid asphalt pipeline 31 downstream of the ΔP device 32;
2)如果沥青温度在130~150℃之间,冷却器2不开启;如果沥青温度在150℃以上,开启冷却器2,待温度表23测得的沥青温度在130~150℃之间时,关闭阀门二3,使沥青进入取样单元;2) If the asphalt temperature is between 130 and 150°C, cooler 2 is not turned on; if the asphalt temperature is above 150°C, cooler 2 is turned on, and when the asphalt temperature measured by the thermometer 23 is between 130 and 150°C, valve 2 3 is closed to allow the asphalt to enter the sampling unit;
3)取样单元接收从冷却单元来的沥青,在逐渐关闭阀门二3的同时,依次打开取样管道上的阀门三5、针型阀一8、针型阀二10和排气管道29上的阀门五14,阀门四13待上游取样管道中的气排空后打开,阀门四13打开的同时关闭排气管道29上的阀门五14;液体沥青经过取样管道闭路循环后回到液体沥青管道31中;3) The sampling unit receives the asphalt from the cooling unit, and while gradually closing the valve 2 3, opens the valve 3 5, the needle valve 1 8, the needle valve 2 10 and the valve 5 14 on the exhaust pipe 29 in sequence on the sampling pipe. The valve 4 13 is opened after the gas in the upstream sampling pipe is emptied. The valve 5 14 on the exhaust pipe 29 is closed while the valve 4 13 is opened; the liquid asphalt returns to the liquid asphalt pipe 31 after a closed-loop circulation through the sampling pipe;
4)进行现流样截取,截取完样品后打开阀门二3,关闭阀门三5、阀门四13、针型阀一8、针型阀二10,取下装有样品的取样器,同时换上清洁的取样器;4) Take the current sample, open valve 2 3 after taking the sample, close valve 3 5, valve 4 13, needle valve 1 8, needle valve 2 10, remove the sampler containing the sample, and replace it with a clean sampler;
5)对取样管道进行清洗;清洗过程中的沥青烟气及空气经排气管道29排到高位罐15中,最后经放散气管26接入原有沥青放散气系统33中,取样过程及清洗过程均无沥青烟气及空气外排。5) Clean the sampling pipeline; the asphalt fume and air during the cleaning process are discharged to the high-level tank 15 through the exhaust pipe 29, and finally connected to the original asphalt venting system 33 through the venting pipe 26. No asphalt fume and air are discharged during the sampling process and the cleaning process.
所述清洗单元是利用沥青中的组分蒽油作为冲洗介质对取样管道进行清洗;具体过程如下:The cleaning unit uses anthracene oil, a component of asphalt, as a flushing medium to clean the sampling pipeline; the specific process is as follows:
1)将蒽油加入到高位罐15中,打开底部管道上的阀门七17和顶部管道上的阀门八18,蒽油自流到低位罐16中;关闭阀门七17和阀门八18,通过加热器25对低位罐16中的蒽油进行加热,加热温度用温度计30监测,加热到设定温度后开始清洗;1) Add anthracene oil to the high-level tank 15, open the valve 7 17 on the bottom pipeline and the valve 8 18 on the top pipeline, and the anthracene oil flows into the low-level tank 16 by gravity; close the valve 7 17 and the valve 8 18, heat the anthracene oil in the low-level tank 16 by the heater 25, monitor the heating temperature with a thermometer 30, and start cleaning after heating to the set temperature;
2)清洗前阀门开关确认:阀门一1、阀门九4在清洗过程中始终处于关闭状态,安全阀19处于工作状态,冷却水上水处于未通入冷却器2的状态;2) Confirm the valve switch before cleaning: valve 1 and valve 9 4 are always in the closed state during the cleaning process, the safety valve 19 is in the working state, and the cooling water supply is not in the state of being passed into the cooler 2;
3)对取样管道进行清洗;清洁的取样器安装好后,阀门七17、阀门八18、阀门二3、阀门四13、阀门六21均处于关闭状态,阀门十20、阀门三5、针型阀一8、针型阀二10、阀门五14均处于开启状态;加热后的蒽油通过加压氮气入口管28进入低位罐16,在压力的作用下,蒽油从低位罐16底部清洗介质出口依次经阀门十20、冷却器2、阀门三5、软管一6、快速接头一7、针型阀一8、取样瓶9、针型阀二10、快速接头二11、软管二12、阀门五14后回到高位罐15中;然后打开底部管道上的阀门七17及顶部管道上的阀门八18,将蒽油再次放入到低位罐16中;重复上述过程对取样管道进行反复冲洗,直到冲洗干净为止;3) Clean the sampling pipeline; after the clean sampler is installed, valve seven 17, valve eight 18, valve two 3, valve four 13, valve six 21 are all in a closed state, and valve ten 20, valve three 5, needle valve one 8, needle valve two 10, valve five 14 are all in an open state; the heated anthracene oil enters the low-level tank 16 through the pressurized nitrogen inlet pipe 28, and under the action of pressure, the anthracene oil returns to the high-level tank 15 from the cleaning medium outlet at the bottom of the low-level tank 16 through valve ten 20, cooler 2, valve three 5, hose one 6, quick connector one 7, needle valve one 8, sampling bottle 9, needle valve two 10, quick connector two 11, hose two 12, valve five 14; then open the valve seven 17 on the bottom pipeline and the valve eight 18 on the top pipeline, and put the anthracene oil into the low-level tank 16 again; repeat the above process to repeatedly rinse the sampling pipeline until it is rinsed clean;
4)冲洗交通管;关闭阀门三5、阀门四13及阀门五14,打开阀门六21、阀门二3,加热后的蒽油从低位罐16底部的清洗介质出口依次经阀门十20、冷却器2、阀门二3、阀门六21后,回到高位罐15中,然后打开底部管道的阀门七17及顶部管道上的阀门八18,蒽油再次放回到低位罐16中,重复上述过程对交通管进行反复冲洗,直到冲洗干净为止。4) Flush the traffic pipe; close valve three 5, valve four 13 and valve five 14, open valve six 21 and valve two 3, and the heated anthracene oil returns to the high-level tank 15 from the cleaning medium outlet at the bottom of the low-level tank 16 through valve ten 20, cooler 2, valve two 3, valve six 21, and then open valve seven 17 on the bottom pipeline and valve eight 18 on the top pipeline, and put the anthracene oil back into the low-level tank 16 again, and repeat the above process to repeatedly flush the traffic pipe until it is flushed clean.
本发明所述一种液体沥青取样系统中,设置冷却单元用于解决150℃以上高温沥青的冷却问题,把沥青温度降到130~150℃,便于取样和检测。取样单元中的取样器更容易拆卸及更换,便于取样操作。清洗单元主要解决取样过程中以及取样前后的取样管道及阀门的清洗及沥青烟气的排放问题,保证整个取样系统始终处于洁净状态,无残留沥青,而且做到了沥青烟气无外排,全部进入原有的沥青放散系统中。In the liquid asphalt sampling system described in the present invention, a cooling unit is provided to solve the problem of cooling high-temperature asphalt above 150°C, and the asphalt temperature is reduced to 130-150°C, which is convenient for sampling and testing. The sampler in the sampling unit is easier to disassemble and replace, which is convenient for sampling operation. The cleaning unit mainly solves the problem of cleaning the sampling pipeline and valves and the emission of asphalt fume during the sampling process and before and after sampling, ensuring that the entire sampling system is always in a clean state without residual asphalt, and that the asphalt fume is not discharged externally and all enters the original asphalt emission system.
本发明所述一种液体沥青取样系统的工作原理是:取样单元接收从冷却单元来的沥青,打开取样管道上的对应阀门和排气管道上的阀门,待取样管道的气排空后,关闭排气管道上的阀门,进行现流样截取,截取完样品后打开交通管上的阀门,关闭取样管道上的对应阀门和取样瓶前后的针型阀,通过快速接头取下取样器,将沥青送化验室化验。在取样管道上阀门的前后端均留有残余的沥青,如果不及时进行清洗,很容易堵塞取样管道,影响下次样品的采集。而截取完样品取下取样器后,软管处的沥青暴露在大气中,沥青烟气还会影响周边环境,所以需要及时安装上清洁的取样器,进行取样管道的清洗。The working principle of the liquid asphalt sampling system described in the present invention is: the sampling unit receives asphalt from the cooling unit, opens the corresponding valve on the sampling pipeline and the valve on the exhaust pipeline, and after the gas in the sampling pipeline is emptied, closes the valve on the exhaust pipeline to intercept the current flow sample, opens the valve on the traffic pipe after intercepting the sample, closes the corresponding valve on the sampling pipeline and the needle valves before and after the sampling bottle, removes the sampler through the quick connector, and sends the asphalt to the laboratory for testing. There is residual asphalt left at the front and rear ends of the valve on the sampling pipeline. If it is not cleaned in time, it is easy to block the sampling pipeline and affect the collection of the next sample. After the sample is intercepted and the sampler is removed, the asphalt at the hose is exposed to the atmosphere, and the asphalt smoke will also affect the surrounding environment, so it is necessary to install a clean sampler in time to clean the sampling pipeline.
清洗单元利用沥青中的组分——蒽油作为冲洗介质对取样管道进行清洗,蒽油加入高位罐中,然后自流到低位罐中,通过加热器将蒽油加热后即可开始清洗。首先关闭取样管道两端的阀门,然后通过加压氮气入口管向低位罐中引入加压氮气,把热蒽油打入取样管道对残余沥青进行清洗。清洗后的蒽油通过取样器化验,看是否还能用于清洗沥青,如果能则蒽油打回高位罐,如果不能则蒽油打入液体沥青管道。由于沥青本身组分就含有蒽油,并且打入的蒽油量相对于整个沥青的量很小,可以忽略不计,因此对沥青的质量不会产生影响。The cleaning unit uses anthracene oil, a component in asphalt, as a flushing medium to clean the sampling pipeline. The anthracene oil is added to the high-level tank and then flows to the low-level tank by gravity. The cleaning can begin after the anthracene oil is heated by the heater. First, close the valves at both ends of the sampling pipeline, and then introduce pressurized nitrogen into the low-level tank through the pressurized nitrogen inlet pipe, and inject the hot anthracene oil into the sampling pipeline to clean the residual asphalt. The cleaned anthracene oil is tested by the sampler to see if it can still be used to clean asphalt. If it can, the anthracene oil is injected back to the high-level tank. If not, the anthracene oil is injected into the liquid asphalt pipeline. Since the asphalt itself contains anthracene oil, and the amount of anthracene oil injected is very small relative to the amount of the entire asphalt and can be ignored, it will not affect the quality of the asphalt.
以上所述,仅为本发明较佳的具体实施方式,但本发明的保护范围并不局限于此,任何熟悉本技术领域的技术人员在本发明揭露的技术范围内,根据本发明的技术方案及其发明构思加以等同替换或改变,都应涵盖在本发明的保护范围之内。The above description is only a preferred specific implementation manner of the present invention, but the protection scope of the present invention is not limited thereto. Any technician familiar with the technical field can make equivalent replacements or changes according to the technical scheme and inventive concept of the present invention within the technical scope disclosed by the present invention, which should be covered by the protection scope of the present invention.
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