CN112167702A - Preparation method and application of ginger-flavored plant cigarette material - Google Patents
Preparation method and application of ginger-flavored plant cigarette material Download PDFInfo
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- CN112167702A CN112167702A CN202011178683.1A CN202011178683A CN112167702A CN 112167702 A CN112167702 A CN 112167702A CN 202011178683 A CN202011178683 A CN 202011178683A CN 112167702 A CN112167702 A CN 112167702A
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- OJYLAHXKWMRDGS-UHFFFAOYSA-N zingerone Chemical compound COC1=CC(CCC(C)=O)=CC=C1O OJYLAHXKWMRDGS-UHFFFAOYSA-N 0.000 description 2
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- NLDDIKRKFXEWBK-AWEZNQCLSA-N gingerol Chemical compound CCCCC[C@H](O)CC(=O)CCC1=CC=C(O)C(OC)=C1 NLDDIKRKFXEWBK-AWEZNQCLSA-N 0.000 description 1
- JZLXEKNVCWMYHI-UHFFFAOYSA-N gingerol Natural products CCCCC(O)CC(=O)CCC1=CC=C(O)C(OC)=C1 JZLXEKNVCWMYHI-UHFFFAOYSA-N 0.000 description 1
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Classifications
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B3/00—Preparing tobacco in the factory
- A24B3/08—Blending tobacco
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- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Cigarettes, Filters, And Manufacturing Of Filters (AREA)
Abstract
The invention discloses a preparation method and application of ginger-flavor plant cigarette material, wherein rhizomes of underground parts and stems and leaves of overground parts of ginger are respectively extracted, solid residues are respectively pulped, or the extracted rhizomes are dried and ground into ginger particles; mixing rhizome pulp, stem and leaf pulp, wood pulp fiber, filler and ginger particles according to the weight ratio of 0-40: 30-80: 10-30: 5-15: 5-20 pulp preparation, and making into a sheet base according to a papermaking process; respectively vacuum-concentrating the extracting solutions of ginger rhizome (underground part) and ginger stem leaf (overground part) into extracts, and mixing the extract of rhizome and stem leaf according to the weight ratio of 0-30: 30-100, coating the mixture on the substrate, drying to obtain the ginger-flavor plant cigarette material, shredding the ginger-flavor plant cigarette material, and blending the shredded tobacco into cigarette tobacco shreds in the form of plant slices, so that the special smell and taste of the cigarette can be increased, the ginger-flavor characteristic of the cigarette is highlighted, the oral stimulation of the cigarette during smoking can be improved, and a consumer has different smoking feeling.
Description
Technical Field
The invention belongs to the technical field of cigarette material preparation, and particularly relates to a preparation method and application of a ginger-flavored plant cigarette material.
Background
In the tobacco processing process, besides tobacco shreds, some cigarette materials are also required to be added for processing cigarettes or various materials used in the cigarette packaging process. Tobacco sheets, cigarette paper, cigarette tows, cigarette filter sticks, cigarette adhesives and the like belong to cigarette materials. In recent years, the tobacco industry is mainly dedicated to research, development and application of tar and harm reducing technology of cigarettes. The tobacco sheet is a cigarette material prepared by taking tobacco waste materials such as tobacco stems, tobacco scraps, cigarette ash rods and the like generated in the tobacco leaf threshing and redrying and cigarette production processing processes as main raw materials through the processes of extracting, pulping, concentrating, papermaking, coating and the like. The tobacco sheets are added in the cigarette production process, so that the cost can be reduced, and the purposes of reducing tar and reducing harm can be achieved. However, the tobacco sheet has the disadvantages of strong sense of stimulation, heavy wood smell, poor aroma amount and the like, and has no other special functions or taste. Therefore, besides the tobacco raw materials, other plant raw materials can be made into plant sheets to be added into cigarettes, different plant aromas are provided, and the special psychological needs of the consumers for the plant aromas are met: for example, Chinese patent CN 104223346A discloses a method for preparing functional reconstituted tobacco from orange grass, and prepares reconstituted tobacco with orange fragrance; chinese patent CN 103783650A applies stevia rebaudiana to prepare reconstituted tobacco, and endows the reconstituted tobacco with special fragrance; chinese patent CN 105077557B discloses a preparation method of lotus-flavor plant cigarette material, which is characterized in that lotus flowers, lotus leaves and lotus seeds are used as raw materials to prepare the plant cigarette material and the plant cigarette material is added into cigarettes, so that the faint scent and sweet fragrance of the cigarettes are increased, and the softness and fine feeling of smoke are improved. Although the above non-tobacco plants have been used to some extent in reconstituted tobacco, the characteristic notes are not readily apparent.
Ginger (Zingier of fiscinale Rosc.) is a perennial herb of Zingiberaceae, and has yellow-green flower and pungent flavor. Ginger rhizome is thick, has multiple branches, has aromatic and spicy flavor, is an economic crop with development and utilization value, contains physiological active substances such as zingerone and gingerol, also contains protein, polysaccharide, vitamins and a plurality of trace elements, integrates nutrition, seasoning and health care, is regarded as a health care product with homology of medicine and food by medical scientists, and has a plurality of health care functions of dispelling cold, eliminating dampness, warming stomach, accelerating blood circulation and the like. The articles, namely extraction of chemical components of dried ginger and application of the chemical components in cigarettes and application of supercritical extraction of dried ginger and extracts of the dried ginger in cigarettes, apply the dried ginger extracts (volatile oil) to the cigarettes in the form of spices, and the results show that the cigarettes added with the dried ginger extracts (volatile oil) have unique smell and smoking taste, the quality and quantity of the smell are increased, and the harmony with the fragrance of the herbs of the cigarettes is better. The chemical components of the ginger extract are detected by gas chromatography-mass spectrometry to contain the chemical activity of moistening lung to arrest cough, and a new idea is provided for flavor compensation of low-tar cigarettes. Although there are reports on the research of perfuming cigarette with ginger extract, there are no reports on the research of preparing cigarette material with ginger as raw material and adding the cigarette material into cigarette in the form of plant slice.
Therefore, aiming at the defects of the prior art, the inventor provides a method for preparing a cigarette material with ginger flavor by taking ginger as a raw material, and the ginger flavor is added into cigarettes in the form of plant slices so as to endow the cigarettes with special smell and smoking taste and increase the comfort and safety of the cigarettes.
Disclosure of Invention
The purpose of the invention is realized by the following technical scheme.
A preparation method of a ginger-flavored plant cigarette material comprises the following steps:
(1) respectively extracting ginger rhizome (underground part) and ginger stem leaf (overground part) by an extraction process, and then carrying out solid-liquid separation to respectively obtain a ginger rhizome extracting solution, a ginger rhizome solid residue, a ginger stem leaf extracting solution and a ginger stem leaf solid residue;
(2) grinding the obtained ginger rhizome solid residue to obtain ginger rhizome slurry, and/or drying and grinding the ginger rhizome solid residue to obtain ginger particles;
(3) grinding the obtained solid residues of the stem and leaf of the ginger into thick liquid to obtain thick liquid of the stem and leaf of the ginger;
(4) mixing ginger rhizome slurry, ginger stem leaf slurry, wood pulp fiber, filler and ginger particles according to a mass ratio of 0-40: 30-80: 10-30: 5-15: 0-20, preparing pulp, and making into a sheet base according to a papermaking method;
(5) respectively vacuum-concentrating the ginger rhizome extracting solution and the ginger stem leaf extracting solution obtained in the step (1) to a density of 1.0-1.2 g/cm3 to obtain a rhizome extract and a stem leaf extract;
(6) and (3) mixing the rhizome extract and the stem leaf extract obtained in the step (5) according to a mass ratio of 30-100: 1-30, uniformly mixing, coating the mixture on the base sheet obtained in the step (4), and drying to obtain the ginger-flavor plant cigarette material.
The ginger is a perennial herb plant of the genus zingiberaceae, and mainly comprises one or a mixture of more than two of ginger varieties such as shannong ginger, Laiwu ginger, Shiwo pork ginger, Tongling white ginger, Laifeng ginger, Sichuan bamboo root ginger, Xilin Huo ginger, Anjiang No. 2 (yellow ginger), Taiwan fat ginger, south alpinia japonica, Roping yellow ginger and the like.
The extraction process used in the step (1) of the invention is a water extraction process or an organic solvent extraction process, wherein the water extraction process adopts extraction or reflux extraction, and the organic solvent extraction adopts reflux extraction; the ratio of the water extract to the feed liquid is 1: 5-1: 12, the extraction temperature is 60-90 ℃, and the extraction time is 30-120 min; the organic solvent extraction material-liquid ratio is 1: 5-1: 12, the extraction temperature is 60-90 ℃, the extraction time is 30-120 min, and the organic solvent is 30-80% of ethanol.
The beating degree of the ginger rhizome slurry and the ginger stem leaf slurry obtained in the steps (2) and (3) is 30-90 ︒ SR, and the particle size of ginger particles obtained by drying and grinding ginger rhizome in the step (2) is 40-100 meshes.
The concentration of the ginger rhizome slurry, the ginger stem and leaf slurry, the wood pulp fiber, the filler and the ginger particle prepared slurry in the step (4) is 3%.
The wood pulp fiber in the step (4) is one or a mixture of more of softwood pulp, hardwood pulp and gramineous pulp in any proportion; the filler is calcium carbonate.
The coating mode in the step (6) of the invention adopts dip coating or spray coating, and the coating rate is 20-50%.
Furthermore, the water content of the finished product of the ginger-flavored plant cigarette material prepared by the method is 10-12%.
The invention also provides application of the prepared ginger-flavor plant cigarette material, which is characterized in that the prepared ginger-flavor plant cigarette material is shredded and blended into cigarette tobacco shreds in a plant slice mode.
All percentages used in the present invention are mass percentages unless otherwise indicated.
Compared with the prior art, the invention has the following characteristics:
1. the invention selects the herbal plant ginger with the same function of medicine and food, all parts (underground rhizome and overground stem leaf) of the ginger are used for preparing the plant cigarette material, and the plant cigarette material is added into the cigarette as the plant slice, so that the characteristic aroma of the cigarette can be highlighted, the safety of the ginger is improved due to the medicine and food property of the ginger, and the health-care factors generated in the burning process of the cigarette can achieve the effects of reducing tar and reducing harm.
2. The ginger-flavor plant cigarette material is completely prepared from root, stem and leaf of ginger without adding tobacco raw materials, the sheet base mainly uses ginger root, stem and leaf pulp or prepared ginger particles, the coating liquid uses ginger root, stem and leaf extract concentrated solution, active ingredients and special flavor substances of a ginger extract are fully utilized, ginger flavor components can be guaranteed to be remained on the sheet, loss of the flavor substances is reduced, flavor style characteristics of the ginger material can be better highlighted, and cigarette flavor is coordinated.
3. The ginger-flavored plant cigarette material is blended in cigarette tobacco shreds for use, so that the cigarette has typical ginger flavor characteristics, the pungent and sweet flavor is increased, the irritation and the wood gas are reduced, the comprehensive sensory perception of the cigarette is improved, the special plant flavor psychological needs of consumers are met, and the characteristic needs of the cigarette can be better met.
4. The invention can increase the economic utilization value of the ginger raw material, has feasible production process, can realize industrial production and has good development and utilization prospect.
Detailed Description
The subject matter of the present invention is described in further detail below with reference to specific examples for better explaining the invention, but the invention is not limited to the specific examples described below.
Example 1
A preparation method of ginger-flavor plant cigarette material comprises the following steps:
(1) weighing 500g of roots and stems of luoping Xiaohuangjiang, adding 6 times of water, leaching for 60min at the temperature of 80 ℃, and performing solid-liquid separation to obtain ginger root and stem extracting solution and ginger root and stem solid residues; weighing 1000g of roxburgh turmeric stem leaves, adding 8 times of water, leaching for 60min at the temperature of 80 ℃, and performing solid-liquid separation to obtain ginger stem leaf extract and ginger stem leaf solid residues;
(2) grinding (pulping) the ginger rhizome solid residue obtained in the step (1) to obtain ginger rhizome pulp, wherein the pulping degree is 40 ︒ SR;
(3) grinding (pulping) the solid residues of the stem and leaf of the ginger obtained in the step (1) to obtain a pulp with the pulping degree of 50 ︒ SR, so as to obtain a pulp of the stem and leaf of the ginger;
(4) taking 200g of ginger rhizome slurry, 600g of ginger stem leaf slurry, 100g of needle leaf wood pulp fiber and 100g of calcium carbonate, mixing the slurry, wherein the concentration of the mixed slurry is 3%, and making into a film base by a papermaking method;
(5) respectively vacuum concentrating the ginger rhizome extract and the ginger stem leaf extract obtained in the step (1) to the density of 1.2g/cm3Obtaining rhizome extract and stem leaf extract;
(6) and (3) uniformly mixing 70g of the rhizome extract and 30g of the stem leaf extract obtained in the step (5) to obtain a coating liquid, coating the coating liquid on the film base obtained in the step (4), controlling the coating rate to be 30%, and drying until the water content is 12% to obtain the 1# ginger-flavored plant cigarette material.
Example 2
A preparation method of ginger-flavor plant cigarette material comprises the following steps:
(1) weighing 1000g of roots and stems of luoping Xiaohuangjiang, adding 6 times of water, leaching for 60min at the temperature of 80 ℃, and performing solid-liquid separation to obtain ginger root and stem extracting solution and ginger root and stem solid residues;
weighing 1000g of roxburgh turmeric stem leaves, adding 8 times of water, leaching for 60min at the temperature of 80 ℃, and performing solid-liquid separation to obtain ginger stem leaf extract and ginger stem leaf solid residues;
(2) grinding (beating) 1/2 of the solid ginger rhizome residue obtained in the step (1) to obtain ginger rhizome slurry, wherein the beating degree is 40 ︒ SR, the rest ginger rhizome slurry is dried until the water content is about 12%, then ground, and sieved by a 40-mesh sieve to obtain ginger rhizome particles;
(3) grinding (pulping) the solid residues of the stem leaves of the ginger in the step (1) to obtain a pulp of the stem leaves of the ginger, wherein the pulping degree is 50 ︒ SR;
(4) 150g of ginger rhizome slurry, 600g of ginger stem leaf slurry, 100g of needle leaf wood pulp fiber, 50g of calcium carbonate and 100g of ginger rhizome particles are taken. Preparing pulp, wherein the concentration of the prepared pulp is 3%, and making into a film base by a papermaking method;
(5) vacuum concentrating the ginger rhizome extractive solution and the ginger stem leaf extractive solution obtained in step (1) to density of 1.1g/cm3Obtaining rhizome extract and stem leaf extract;
(6) and (3) uniformly mixing 50g of the rhizome extract and 50g of the stem leaf extract obtained in the step (5) to obtain a coating liquid, coating the coating liquid on the film base obtained in the step (4), controlling the coating rate to be 30%, and drying until the water content is 12% to obtain the 2# ginger-flavored plant cigarette material.
Example 3
A preparation method of ginger-flavor plant cigarette material comprises the following steps:
(1) weighing 500g of roots and stems of luoping Xiaohuangjiang, adding 6 times of 75% ethanol, performing reflux extraction at 80 ℃ for 60min, and performing solid-liquid separation to obtain ginger root and stem extracting solution and ginger root and stem solid residues;
weighing 1000g of roxburgh turmeric stem leaves, adding 8 times of 75% ethanol, leaching for 30min at 80 ℃, and performing solid-liquid separation to obtain ginger stem leaf extract and ginger stem leaf solid residues;
(2) grinding (pulping) the rhizome solid residue obtained in the step (1) to obtain ginger rhizome pulp, wherein the pulping degree is 30 ︒ SR;
(3) grinding (pulping) the solid residues of the stem leaves of the ginger in the step (1) to obtain a pulp of the stem leaves of the ginger, wherein the pulping degree is 30 ︒ SR;
(4) taking 100g of ginger rhizome slurry, 700g of ginger stem leaf slurry, 100g of needle leaf wood pulp fiber and 100g of calcium carbonate, mixing the slurry, wherein the concentration of the mixed slurry is 3%, and making into a film base by a papermaking method;
(5) vacuum concentrating the ginger rhizome extractive solution and the ginger stem leaf extractive solution obtained in step (1) to density of 1.2g/cm3Obtaining rhizome extract and stem leaf extract;
(6) and (3) uniformly mixing 60g of the rhizome extract and 40g of the stem leaf extract obtained in the step (5) to obtain a coating liquid, coating the coating liquid on the film base obtained in the step (4), controlling the coating rate to be 30%, and drying until the water content is 12% to obtain the 3# ginger-flavored plant cigarette material.
Example 4
A preparation method of ginger-flavor plant cigarette material comprises the following steps:
(1) weighing 800g of shannong ginger rhizome, adding 8 times of water, leaching for 60min at the temperature of 90 ℃, and performing solid-liquid separation to obtain ginger rhizome extracting solution and ginger rhizome solid residue;
weighing 1000g of shannong ginger stem leaves, adding 10 times of water, leaching for 60min at 90 ℃, and performing solid-liquid separation to obtain ginger stem leaf extract and ginger stem leaf solid residues;
(2) grinding (pulping) the ginger rhizome solid residue obtained in the step (1) to obtain ginger rhizome pulp, wherein the pulping degree is 50 ︒ SR;
(3) grinding (pulping) the solid residues of the stem leaves of the ginger in the step (1) to obtain a pulp of the stem leaves of the ginger, wherein the pulping degree is 40 ︒ SR;
(4) taking 300g of shannong ginger rhizome slurry, 500g of ginger stem leaf slurry, 150g of softwood pulp fiber and 50g of calcium carbonate, mixing the slurry, wherein the concentration of the mixed slurry is 3%, and making into a film base by a papermaking method;
(5) respectively vacuum concentrating the ginger rhizome extract and the ginger stem leaf extract obtained in the step (1) to the density of 1.1g/cm3Obtaining rhizome extract and stem leaf extract;
(6) and (3) uniformly mixing 80g of the rhizome extract and 20g of the stem leaf extract obtained in the step (5) to obtain a coating liquid, coating the coating liquid on the film base obtained in the step (4), controlling the coating rate to be 30%, and drying until the water content is 12% to obtain the 4# ginger-flavored plant cigarette material.
Comparative example 1
A preparation method of ginger-flavor plant cigarette material comprises the following steps:
(1) weighing 500g of roots and stems of luoping Xiaohuangjiang, adding 6 times of water, leaching for 60min at the temperature of 80 ℃, and performing solid-liquid separation to obtain ginger root and stem extracting solution; weighing 1000g of luoping yellow ginger stem leaves, adding 8 times of water, leaching for 60min at the temperature of 80 ℃, and performing solid-liquid separation to obtain ginger stem leaf extracting solution;
(2) adding 4 times of water into 1000g of tobacco stems, leaching for 60min at the temperature of 70 ℃, performing solid-liquid separation to obtain tobacco stem residues, and grinding the residues to obtain tobacco pulp;
(3) taking 800g of tobacco pulp, 100g of softwood pulp fiber and 100g of calcium carbonate, blending pulp with the concentration of 3%, and making into a sheet base by a papermaking method;
(5) respectively vacuum concentrating the ginger rhizome extract and the ginger stem leaf extract obtained in the step (1) to the density of 1.2g/cm3Obtaining rhizome extract and stem leaf extract;
(6) and (3) uniformly mixing 70g of the rhizome extract and 30g of the stem leaf extract obtained in the step (5) to obtain a coating liquid, coating the coating liquid on the film base obtained in the step (3), controlling the coating rate to be 30%, and drying until the water content is 12% to obtain the 5# ginger-flavored plant cigarette material.
Comparative example 2
A preparation method of ginger-flavor plant cigarette material comprises the following steps:
(1) weighing 500g of roots and stems of luoping Xiaohuangjiang, adding 6 times of water, leaching for 60min at the temperature of 80 ℃, and performing solid-liquid separation to obtain solid residues of the roots and stems of the ginger; weighing 1000g of roxburgh turmeric stem leaves, adding 8 times of water, leaching for 60min at the temperature of 80 ℃, and performing solid-liquid separation to obtain solid residues of the stem leaves of the ginger; adding 4 times of water into 1000g of tobacco stems, leaching for 60min at 70 ℃, and performing solid-liquid separation to obtain tobacco stem extracting solution;
(2) grinding (pulping) the ginger rhizome solid residue obtained in the step (1) to obtain ginger rhizome pulp, wherein the pulping degree is 40 ︒ SR;
(3) grinding (pulping) the solid residues of the stem and leaf of the ginger obtained in the step (1) to obtain a pulp with the pulping degree of 50 ︒ SR, so as to obtain a pulp of the stem and leaf of the ginger;
(4) taking 200g of ginger rhizome slurry, 600g of ginger stem leaf slurry, 100g of needle leaf wood pulp fiber and 100g of calcium carbonate, mixing the slurry, wherein the concentration of the mixed slurry is 3%, and making into a film base by a papermaking method;
(5) vacuum concentrating the tobacco stalk extract obtained in step (1) to density of 1.2g/cm3Obtaining tobacco extract;
(6) and (4) coating 100g of the tobacco extract obtained in the step (5) on the sheet base obtained in the step (4), controlling the coating rate to be 30%, and drying until the water content is 12% to obtain the 6# ginger-flavored plant cigarette material.
Comparative example 3
A preparation method of ginger-flavor plant cigarette material comprises the following steps:
(1) weighing 1200g of roots and stems of luoping Xiaohuangjiang, adding 6 times of water, leaching for 60min at the temperature of 80 ℃, and performing solid-liquid separation to obtain ginger root and stem extracting solution and ginger root and stem solid residues;
(2) grinding (pulping) the ginger rhizome solid residue obtained in the step (1) to obtain ginger rhizome pulp, wherein the pulping degree is 40 ︒ SR;
(3) taking 800g of ginger rhizome slurry, 100g of softwood pulp fiber and 100g of calcium carbonate, blending the slurry, wherein the concentration of the blended slurry is 3%, and making into a film base by a papermaking method;
(4) concentrating the ginger rhizome extract obtained in step (1) to a density of 1.2g/cm3Obtaining rhizome extract;
(5) and (3) uniformly mixing 100g of the rhizome extract obtained in the step (4) to obtain a coating liquid, coating the coating liquid on the film base obtained in the step (3), controlling the coating rate to be 30%, and drying until the water content is 12% to obtain the 7# ginger-flavored plant cigarette material.
Comparative example 4
A preparation method of ginger-flavor plant cigarette material comprises the following steps:
(1) weighing 1200g of luoping Xiaohuang ginger stem leaves, adding 8 times of water, leaching for 60min at the temperature of 80 ℃, and performing solid-liquid separation to obtain ginger stem leaf extracting solution and ginger stem leaf solid residues;
(2) grinding (pulping) the solid residues of the stem and leaf of the ginger obtained in the step (1) to obtain a pulp with the pulping degree of 50 ︒ SR, so as to obtain a pulp of the stem and leaf of the ginger;
(3) taking 800g of ginger stem leaf slurry, 100g of softwood pulp fiber and 100g of calcium carbonate, blending the slurry, wherein the concentration of the blended slurry is 3%, and making into a film base by a papermaking method;
(4) vacuum concentrating the stem and leaf extract of ginger obtained in step (1) to density of 1.2g/cm3Obtaining stem leaf extract;
(5) and (3) uniformly mixing 100g of the stem leaf extract obtained in the step (4) to obtain a coating liquid, coating the coating liquid on the film base obtained in the step (4), controlling the coating rate to be 30%, and drying until the water content is 12% to obtain the 8# ginger-flavored plant cigarette material.
Comparative example 5
A preparation method of ginger-flavor plant cigarette material comprises the following steps:
(1) weighing 1200g of roots and stems of luoping Xiaohuangjiang, adding 6 times of water, leaching for 60min at the temperature of 80 ℃, and performing solid-liquid separation to obtain solid residues of the roots and stems of the ginger; weighing 1000g of stems, leaves and stems of luoping Xiaohuangjiang, adding 8 times of water, leaching for 60min at the temperature of 80 ℃, and performing solid-liquid separation to obtain ginger stem-leaf extracting solution;
(2) grinding (pulping) the ginger rhizome solid residue obtained in the step (1) to obtain ginger rhizome pulp, wherein the pulping degree is 40 ︒ SR;
(3) taking 800g of ginger rhizome slurry, 100g of softwood pulp fiber and 100g of calcium carbonate, blending the slurry, wherein the concentration of the blended slurry is 3%, and making into a film base by a papermaking method;
(4) vacuum concentrating the stem and leaf extract of ginger obtained in step (1) to density of 1.2g/cm3Obtaining stem leaf extract;
(5) and (3) uniformly mixing 100g of the stem leaf extract obtained in the step (4) to obtain a coating liquid, coating the coating liquid on the film base obtained in the step (3), controlling the coating rate to be 30%, and drying until the water content is 12% to obtain the 9# ginger-flavored plant cigarette material.
Comparative example 6
A preparation method of ginger-flavor plant cigarette material comprises the following steps:
(1) weighing 1000g of roots and stems of luoping Xiaohuangjiang, adding 6 times of water, leaching for 60min at the temperature of 80 ℃, and performing solid-liquid separation to obtain ginger root and stem extracting solution; weighing 1000g of stems, leaves and stems of luoping Xiaohuangjiang, adding 8 times of water, leaching for 60min at the temperature of 80 ℃, and performing solid-liquid separation to obtain solid residues of the stems, leaves and stems of the ginger;
(2) grinding (pulping) the solid residues of the stem and leaf of the ginger obtained in the step (1) to obtain a pulp with the pulping degree of 50 ︒ SR, so as to obtain a pulp of the stem and leaf of the ginger;
(3) taking 800g of ginger stem leaf slurry, 100g of softwood pulp fiber and 100g of calcium carbonate, blending the slurry, wherein the concentration of the blended slurry is 3%, and making into a film base by a papermaking method;
(4) respectively vacuum concentrating the ginger rhizome extract obtained in step (1) to density of 1.2g/cm3Obtaining rhizome extract;
(5) and (3) uniformly mixing 100g of the rhizome extract obtained in the step (4) to obtain a coating liquid, coating the coating liquid on the film base obtained in the step (3), controlling the coating rate to be 30%, and drying until the water content is 12% to obtain the 10# ginger-flavored plant cigarette material.
Shredding the prepared 1# -10# ginger-flavor plant cigarette material, blending the shredded tobacco into cigarette shreds according to a fixed design proportion of cigarettes according to a plant slice blending mode to prepare finished cigarettes, and specifically: the ginger-flavored plant cigarette material is adopted to replace 8 percent of cut tobacco by weight.
Test for smoking: the method comprises the steps of taking a cigarette without the ginger-flavored plant cigarette material as a control sample, taking a cigarette blended with the 1# -10# ginger-flavored plant cigarette material as an experimental sample, placing the sample into a constant-temperature and constant-humidity box for balancing for 24 hours, then randomly numbering, and forming a smoking panel by experts with smoking quality evaluation to perform sensory smoking evaluation. The results are shown in Table 1.
Table 11 # -10# ginger-flavor plant cigarette material blended cigarette sensory evaluation effect
The results of the smoke panel test show that: compared with a control sample, the experimental sample has typical ginger aroma characteristics, obvious sweet aroma, less irritation and wood gas and better tobacco aroma harmony. Compared with the control sample, the comparative sample has no obvious improvement effect, and the comprehensive score is not obviously improved compared with the control sample.
The foregoing is a further detailed description of the invention with reference to specific embodiments. Obvious modifications, variations or similar uses, which would occur to those skilled in the art to which the invention pertains without departing from the spirit of the invention, are to be considered as being within the scope of the invention.
Claims (9)
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Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN112586795A (en) * | 2021-01-08 | 2021-04-02 | 中烟施伟策（云南）再造烟叶有限公司 | Plant scented chip for cigarette leaf group and preparation method thereof |
| CN112999173A (en) * | 2021-04-13 | 2021-06-22 | 云南氪莱铂科技有限公司 | Preparation method of functional heating smoke body and heating non-combustible cigarette |
| CN115336781A (en) * | 2022-09-19 | 2022-11-15 | 江苏中烟工业有限责任公司 | A kind of reconstituted tobacco leaf and its preparation method and application |
| CN117044983A (en) * | 2023-08-18 | 2023-11-14 | 云南中烟工业有限责任公司 | Reconstituted tobacco with elegant spicy fragrance and preparation method thereof |
| CN117044984A (en) * | 2023-08-18 | 2023-11-14 | 云南中烟工业有限责任公司 | Alcoholization method based on aroma enhancement and quality improvement of reconstituted tobacco |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US20090065013A1 (en) * | 2006-04-28 | 2009-03-12 | Swedish Match North Europe Ab | moist snuff non-tobacco composition and a method for producing thereof |
| CN105077557A (en) * | 2015-07-15 | 2015-11-25 | 河北中烟工业有限责任公司 | Preparation method and application for cigarette plant materials with violet scent |
| CN108936790A (en) * | 2018-06-01 | 2018-12-07 | 云南中烟工业有限责任公司 | The preparation method and the purposes in tobacco product of a kind of solid spice |
| CN110279163A (en) * | 2019-08-06 | 2019-09-27 | 四川三联新材料有限公司 | Fragrance dose for heating cigarette smoke section of not burning and its preparation method and application and heating are not burnt cigarette |
-
2020
- 2020-10-29 CN CN202011178683.1A patent/CN112167702A/en active Pending
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US20090065013A1 (en) * | 2006-04-28 | 2009-03-12 | Swedish Match North Europe Ab | moist snuff non-tobacco composition and a method for producing thereof |
| CN105077557A (en) * | 2015-07-15 | 2015-11-25 | 河北中烟工业有限责任公司 | Preparation method and application for cigarette plant materials with violet scent |
| CN108936790A (en) * | 2018-06-01 | 2018-12-07 | 云南中烟工业有限责任公司 | The preparation method and the purposes in tobacco product of a kind of solid spice |
| CN110279163A (en) * | 2019-08-06 | 2019-09-27 | 四川三联新材料有限公司 | Fragrance dose for heating cigarette smoke section of not burning and its preparation method and application and heating are not burnt cigarette |
Non-Patent Citations (1)
| Title |
|---|
| 广西中烟工业有限责任公司、广西烟草学会: "《天然烟用精油》", 28 February 2019, 广西科学技术出版社 * |
Cited By (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN112586795A (en) * | 2021-01-08 | 2021-04-02 | 中烟施伟策（云南）再造烟叶有限公司 | Plant scented chip for cigarette leaf group and preparation method thereof |
| CN112999173A (en) * | 2021-04-13 | 2021-06-22 | 云南氪莱铂科技有限公司 | Preparation method of functional heating smoke body and heating non-combustible cigarette |
| CN112999173B (en) * | 2021-04-13 | 2022-06-14 | 云南氪莱铂科技有限公司 | Preparation method of functional heating smoking body, heat not burning cigarette |
| CN115336781A (en) * | 2022-09-19 | 2022-11-15 | 江苏中烟工业有限责任公司 | A kind of reconstituted tobacco leaf and its preparation method and application |
| CN115336781B (en) * | 2022-09-19 | 2023-04-18 | 江苏中烟工业有限责任公司 | Reconstituted tobacco and preparation method and application thereof |
| CN117044983A (en) * | 2023-08-18 | 2023-11-14 | 云南中烟工业有限责任公司 | Reconstituted tobacco with elegant spicy fragrance and preparation method thereof |
| CN117044984A (en) * | 2023-08-18 | 2023-11-14 | 云南中烟工业有限责任公司 | Alcoholization method based on aroma enhancement and quality improvement of reconstituted tobacco |
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